WO2006086873A8 - Method for determining native wood constituents using visible-light raman spectrometry - Google Patents

Method for determining native wood constituents using visible-light raman spectrometry

Info

Publication number
WO2006086873A8
WO2006086873A8 PCT/CA2006/000200 CA2006000200W WO2006086873A8 WO 2006086873 A8 WO2006086873 A8 WO 2006086873A8 CA 2006000200 W CA2006000200 W CA 2006000200W WO 2006086873 A8 WO2006086873 A8 WO 2006086873A8
Authority
WO
WIPO (PCT)
Prior art keywords
native wood
sample
visible
solid native
peak
Prior art date
Application number
PCT/CA2006/000200
Other languages
French (fr)
Other versions
WO2006086873A1 (en
Inventor
Thanh P Trung
Paul A Watson
Paul A F Bicho
Denys F Leclerc
Shanon Kelly Huntley
Original Assignee
Pulp Paper Res Inst
Thanh P Trung
Paul A Watson
Paul A F Bicho
Denys F Leclerc
Shanon Kelly Huntley
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pulp Paper Res Inst, Thanh P Trung, Paul A Watson, Paul A F Bicho, Denys F Leclerc, Shanon Kelly Huntley filed Critical Pulp Paper Res Inst
Publication of WO2006086873A1 publication Critical patent/WO2006086873A1/en
Publication of WO2006086873A8 publication Critical patent/WO2006086873A8/en

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/65Raman scattering
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/46Wood
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/65Raman scattering
    • G01N2021/653Coherent methods [CARS]
    • G01N2021/656Raman microprobe

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)

Abstract

A method for the determination of solid native wood chemical constituents, such as total lignin content, Klason lignin, cellulose, hemicelluloses, and other carbohydrates, in native wood samples such as cores, strips, boards, logs, and in boreholes made in standing trees, with the aid of Raman spectrometry. The method typically comprises the steps of subjecting the sample to a monochromatic visible-light source, collecting the scattered light from the sample at either 180° back-scattering mode or 90° scattering mode for a set integration time over a predetermined range of wave numbers so as to produce Raman shift spectra, acquiring the spectral data over a pre-determined length of time, determining the peak scattering intensity, correlating by univariate or multivariate calibration between peak-intensity and/or spectral data with known values of solid native wood chemical composition and quantifying said spectra to previously determined calibration so as to determine solid native chemical compositions of unknown samples.
PCT/CA2006/000200 2005-02-16 2006-02-10 Method for determining native wood constituents using visible-light raman spectrometry WO2006086873A1 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US65312205P 2005-02-16 2005-02-16
US60/653,122 2005-02-16
US66234705P 2005-03-17 2005-03-17
US60/662,347 2005-03-17

Publications (2)

Publication Number Publication Date
WO2006086873A1 WO2006086873A1 (en) 2006-08-24
WO2006086873A8 true WO2006086873A8 (en) 2006-10-12

Family

ID=36916134

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CA2006/000200 WO2006086873A1 (en) 2005-02-16 2006-02-10 Method for determining native wood constituents using visible-light raman spectrometry

Country Status (1)

Country Link
WO (1) WO2006086873A1 (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102435594B (en) * 2011-09-19 2014-10-22 北京林业大学 Method for testing lignification degrees of plant cell walls
SE540910C2 (en) * 2017-05-02 2018-12-18 Gorzsas Andras Spectroscopic method and device for determining the characteristics of a tree
FI128736B (en) * 2018-03-09 2020-11-13 Valmet Automation Oy Method and measurement apparatus for measuring suspension
CN114002203B (en) * 2020-12-31 2024-08-09 安徽农业大学 Method and device for analyzing content of wood components based on Raman spectrum
CN114166819A (en) * 2021-11-26 2022-03-11 中南林业科技大学 Method for measuring water content of wood cell wall based on Raman spectrum technology
CN115266676B (en) * 2022-07-11 2024-09-13 中国农业大学 In-situ synchronous quantification method for crop rhizome wood fiber components
CN115219702B (en) * 2022-07-15 2024-06-21 安徽农业大学 Prediction method and prediction model for hemicellulose content of wood after heat treatment

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11258161A (en) * 1998-03-14 1999-09-24 Oji Paper Co Ltd Method and apparatus for determining components of tree and program recording medium for determination method
US6525319B2 (en) * 2000-12-15 2003-02-25 Midwest Research Institute Use of a region of the visible and near infrared spectrum to predict mechanical properties of wet wood and standing trees
SE519246C2 (en) * 2001-06-20 2003-02-04 Allan Holmgren Wood analysis method, uses Raman spectroscopy to determine type of wood and presence of rot

Also Published As

Publication number Publication date
WO2006086873A1 (en) 2006-08-24

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