WO2004110869A1 - Method and device for electron beam irradiation - Google Patents
Method and device for electron beam irradiation Download PDFInfo
- Publication number
- WO2004110869A1 WO2004110869A1 PCT/SE2004/000894 SE2004000894W WO2004110869A1 WO 2004110869 A1 WO2004110869 A1 WO 2004110869A1 SE 2004000894 W SE2004000894 W SE 2004000894W WO 2004110869 A1 WO2004110869 A1 WO 2004110869A1
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- WO
- WIPO (PCT)
- Prior art keywords
- chamber
- web
- outlet opening
- outlet
- opening
- Prior art date
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/02—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using physical phenomena
- A61L2/08—Radiation
- A61L2/087—Particle radiation, e.g. electron-beam, alpha or beta radiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
- B65B55/04—Sterilising wrappers or receptacles prior to, or during, packaging
- B65B55/08—Sterilising wrappers or receptacles prior to, or during, packaging by irradiation
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- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21K—TECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR; IRRADIATION DEVICES; GAMMA RAY OR X-RAY MICROSCOPES
- G21K5/00—Irradiation devices
- G21K5/02—Irradiation devices having no beam-forming means
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21K—TECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR; IRRADIATION DEVICES; GAMMA RAY OR X-RAY MICROSCOPES
- G21K5/00—Irradiation devices
- G21K5/04—Irradiation devices with beam-forming means
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2202/00—Aspects relating to methods or apparatus for disinfecting or sterilising materials or objects
- A61L2202/20—Targets to be treated
- A61L2202/23—Containers, e.g. vials, bottles, syringes, mail
Definitions
- the present invention refers to a device for electron beam irradiation of at least one side of a web and a method of ventilating said device.
- packages formed from a web of packaging material comprising different layers of paper or board, liquid barriers of for example polymers and gas barriers of for example thin films of aluminium.
- the web is formed into a tube by overlappingly sealing the longitudinal edges of the web.
- the tube is continuously filled with a product and then transversally sealed and formed into cushions.
- the cushions are separated and formed into for example parallelepipedic containers.
- a device for web sterilization is formed with openings for the entrance and exit of the web.
- bacteria and dirt particles may enter through the openings and also through interconnections between different portions of the device and the surrounding equipment. If these bacteria and dirt particles are left in the device they may recontaminate the web after it has been sterilised.
- the second consideration is how to safely discharge ozone (O 3 ) from the device thereby minimising the risk of ozone leakage to the outside of the device. It is common knowledge that the presence of oxygen molecules (O 2 ) in an electron irradiation device give rise to the formation of ozone during electron irradiation because of radical reactions.
- an object of the invention has been to provide a device for electron beam irradiation in which both of the above mentioned considerations have been taken into account and solved.
- the present invention relates to a method of ventilating a device for electron beam irradiation of at least one side of a web.
- the method comprises the steps of: providing a first chamber comprising a web inlet opening and a web outlet opening, providing a second chamber extending inside the first chamber, the second chamber comprising a web inlet opening, a web outlet opening, and an electron exit surface through which electrons are adapted to be emitted into the second chamber, passing the web through the second chamber, and creating a flow of a gaseous fluid through both the first and second chambers in a direction opposite the direction of travel of the web by supplying said fluid into the web outlet opening of the first chamber and providing at least one outlet.
- a desired level of sterilization can be maintained inside the device. Any bacteria or dirt particles entering the device at any point will be transported by the flow to that end of the device where the unsterilised web enters, and there it will be discharged from the device through the outlet. The risk of recontamination of the sterilised web before filling and sealing operations is thereby minimised. Further, ozone (O 3 ) that is formed during irradiation with electrons can be effectively and reliably discharged from both the first and second chambers by the same flow of gaseous fluid. The risk of leakage of ozone to the outside of the device is thereby minimised.
- An additional advantage is that the flow of gaseous fluid is suitable for use during pre-sterilization of the device.
- Hydrogen peroxide can for example be supplied to the gaseous fluid and thereby the surfaces of both the first and second chambers are sterilised.
- the method comprises the steps of: providing a first chamber comprising a web inlet opening and a web outlet opening, providing a second chamber extending inside the first chamber, the second chamber comprising a web inlet opening, a web outlet opening, and an electron exit surface through which electrons are adapted to be emitted into the second chamber, passing the web through the second chamber, providing fluid connection between the web outlet opening of the second chamber and the web outlet opening of the first chamber, preventing fluid connection between the first chamber and the web outlet opening of the first chamber, and creating a flow of a gaseous fluid through both the first and second chambers in a direction opposite the direction of travel of the web by supplying said fluid into the first chamber and into the web outlet opening of the first chamber and providing at least one outlet.
- the method comprises the step of providing fluid connection between the web inlet opening of the first chamber and both the first chamber and the web inlet opening of the second chamber.
- the gaseous fluid from the first chamber can be discharged from the second chamber, which makes it possible to provide only one outlet.
- the method comprises the step of providing fluid connection between the web outlet opening of the first chamber and both the first chamber and the web outlet opening of the second chamber. In this way both chambers may be easily supplied by the same gaseous fluid supply.
- the web outlet opening of the second chamber is located at a distance from and preferably substantially in line with the web outlet opening of the first chamber. In this way it is not necessary to arrange web guides between the two chambers, and the gaseous fluid that enters through the outlet opening of the first chamber is easily supplied to both chambers.
- the outlet is provided in vicinity of the web inlet opening of the second chamber.
- the outlet is provided inside the second chamber in the vicinity of the web inlet opening.
- the ozone is not likely to reach the first chamber, which further minimises the risk of leakage to the outside of the device.
- the outlet is provided in the vicinity of the web inlet opening of the first chamber. In this way the discharge can be made in a reliable way with minimised risk of recontamination of the sterilised web.
- the method comprises the step of controlling the flow of gaseous fluid so that a first overpressure is created inside the first closed chamber, and a second overpressure is created inside the second chamber.
- the overpressures are chosen so that the first overpressure and the second overpressure are the same. In this way undesired transport of for example ozone or dirt particles between the two chambers is prevented.
- the overpressures are chosen so that the first overpressure and the second overpressure are different.
- the first overpressure can be higher than the second overpressure.
- One reason for choosing such is to keep the ozone within the second chamber where it can be immediately discharged.
- One reason for choosing the second overpressure so that it is higher than the first overpressure could be to obtain a fast evacuation of ozone and eventual other volatile substances, that for example cause off-flavour, from the second chamber.
- the invention also comprises a device for electron beam irradiation of at least one side of a web.
- the device comprises a first chamber comprising a web inlet opening and a web outlet opening, a second chamber extending inside the first chamber, the second chamber comprising a web inlet opening, a web outlet opening, and being adapted to receive an electron beam emitter provided with an electron exit window through which electrons are adapted to be emitted into the second chamber, the web being adapted to pass the second chamber, and the web outlet opening of the first chamber being adapted to be in communication with a gaseous fluid supply and both chambers being in communication with an outlet, the supply and the outlet are adapted to create a flow of the gaseous fluid through both the first and second chambers in a direction opposite the direction of travel of the web.
- a desired level of sterilization can be maintained inside the device.
- ozone that is formed during irradiation with electrons can be effectively and reliably discharged from both the first and second chambers. The risk of leakage of ozone to the outside of the device is thereby minimised.
- the invention also comprises a device for electron beam irradiation of at least one side of a web, the device comprising a first chamber comprising a web inlet opening and a web outlet opening, a second chamber extending inside the first chamber, the second chamber comprising a web inlet opening, a web outlet opening, and being adapted to receive an electron beam emitter provided with an electron exit window through which electrons are adapted to be emitted into the second chamber, the web being adapted to pass the second chamber, a fluid connection is adapted to be provided between the web outlet opening of the second chamber and the web outlet opening of the first chamber, a fluid connection is adapted to be prevented between the first chamber and the web outlet opening of the first chamber, the web outlet opening of the first chamber being adapted to be in communication with a first gaseous fluid supply, the first chamber being adapted to be in communication with a second gaseous fluid supply, both chambers being in communication with an outlet, and the first and second supplies and the outlet are adapted to create a flow of the gaseous fluid through
- the invention further comprises a device for electron beam irradiation of at least one side of a web, the device comprising a first chamber comprising a web inlet opening and a web outlet opening, a second chamber extending inside the first chamber, the second chamber comprising a web inlet opening, a web outlet opening, and an electron beam emitter provided with an electron exit window through which electrons are to be emitted into the second chamber, the web being adapted to pass the second chamber, and the web outlet opening of the first chamber is in communication with a gaseous fluid supply and both chambers are in communication with an outlet, the supply and the outlet are adapted to create a flow of the gaseous fluid through both the first and second chambers in a direction opposite the direction of travel of the web.
- the invention also comprises a device for electron beam irradiation of at least one side of a web, the device comprising: a first chamber comprising a web inlet opening and a web outlet opening, a second chamber extending inside the first chamber, the second chamber comprising a web inlet opening, a web outlet opening, and an electron beam emitter provided with an electron exit window through which electrons are emitted into the second chamber, the web being adapted to pass the second chamber, a fluid connection is provided between the web outlet opening of the second chamber and the web outlet opening of the first chamber, the first chamber is prevented from being in fluid connection with the web outlet opening of the first chamber, the web outlet opening of the first chamber being in communication with a first gaseous fluid supply, the first chamber is in communication with a second gaseous fluid supply, both chambers being in communication with an outlet, and the first and second supplies and the outlet are adapted to create a flow of the gaseous fluid through both the first and second chambers in a direction opposite the direction of travei of the web
- Fig. 1 shows a schematic cross section of the embodiment of the device
- Fig. 2 shows a schematic view illustrating the segments of the tunnel, the angles and the inner housing with the emitters
- Fig. 3 shows a schematic first illustration on the relation between the tunnel widths, the angles and the lengths of the segments
- Fig. 4 shows a schematic second illustration on the relation between the tunnel widths, the angles and the lengths of the segments
- Fig. 5 shows a schematic cross section of an emitter enclosed in the device
- Fig. 6 shows a schematic view of the air system according to the invention.
- Fig. 7 shows a schematic view like Fig. 1 , but shown from the other side and which shows an alternative embodiment.
- the device shown in Fig. 1 , comprises an inner housing 1 in which one or two emitters 2,3 are mounted. A central portion of the inner housing is adapted to receive the emitters.
- the inner housing 1 forms a tunnel and a packaging material web W is fed through the tunnel past the emitters 2,3. Further, the inner housing 1 is provided with an inlet portion 5 and an outlet portion 6 for the entrance and the exit of the web.
- the web inlet portion 5 is designed such that the inlet direction of the web W into the inlet portion 5 is angled in relation to the outlet direction of the web W out of the inlet portion 5.
- the outlet direction of the web W out of the inlet portion 5 is equal to the direction in which the web W passes the emitters 2,3.
- the angle between the inlet and the outlet direction of the web W in the inlet portion 5 is at least 90°.
- the inlet portion 5 is formed such that it is angled at at least two locations.
- Fig. 2 is shown that the inlet portion 5 comprises three successive segments, an entrance segment 5a, a central segment 5b and an exit segment 5c.
- the central segment 5b forming a first angle ⁇ to the entrance segment 5a and the exit segment 5c forming a second angle ⁇ to the central segment 5b.
- the relation between the tunnel widths, said angles ⁇ , ⁇ and the lengths of the segments 5a-c is such that an imagined straight line hitting the tunnel wall in the entrance segment 5a also hits the tunnel wall of at least the exit segment 5c, before exiting the exit segment 5c, and that an imagined straight line passing through the entrance segment 5a hits the tunnel wall of the central segment 5b such that it also hits the tunnel wall of at least the exit segment 5c, before exiting the exit segment 5c.
- Fig. 3 and 4 are illustrated how the design can be obtained with help of paper, a ruler and a pen.
- Fig. 3 a first worst case scenario is disclosed.
- a straight line is drawn beginning outside the entrace segment 5a and pointing substantially towards the outer comer between the entrance segment 5a and the central segment 5b.
- the line hits the tunnel wall in the entrance segment 5a and is drawn pointing substantially towards the inner corner between the central segment 5b and the exit segment 5c. If the relation between tunnel widths, angles ⁇ , ⁇ and segment lengths is to be considered good enough, the straight line will be forced to hit the tunnel wall of the exit segment 5c before exiting the exit segment 5c.
- Fig. 4 a second worst case scenario is disclosed.
- a straight line is now drawn beginning outside the entrace segment 5a and pointing substantially towards the inner corner close to the exit of the entrance segment 5a, but is hitting the tunnel wall in the central segment 5b.
- the line is then drawn substantially towards the inner corner between the central segment 5b and the exit segment 5c. If the relation between tunnel widths, angles ⁇ , ⁇ and segment lengths is to be considered good enough, the straight line will be forced to hit the tunnel wall of the exit segment 5c before exiting the exit segment 5c. Thus, it is realised that if a certain angle is used, the parameters that can be modified are either the tunnel width or the length of the segment. A wide tunnel necessitates a long segment. If there is a need for a short segment, the tunnel width must be decreased. Another possibility is of course to change one or both of the angles.
- the change in the running direction of the web W is accomplished by providing the inlet portion 5 with at least one web guide.
- the web guide is a first and a second roller 9, 10 mounted inside the inlet portion 5.
- the web W runs substantially horizontal into the inlet portion 5 and substantially vertically upwards when it leaves the inlet portion 5 and enters the inner housing 1.
- the rollers 9, 10 being formed and mutually located in such a way that the first roller 9 angles the web W the second angle ⁇ and that the second roller 10 angles the web W the first angle ⁇ .
- the rollers 9, 10 are journalled in support members.
- the support members can for example be bearings provided with an outer shielding or with a bearing housing designed following the same design criteria as the tunnel.
- the outlet portion 6 is similarly designed with an entrance segment 6a, a central segment 6b and an exit segment 6c.
- the outlet portion 6 comprises one or more rollers 11 , 12.
- the inlet portion 5 and the outlet portion 6 are mounted and designed such that the web W runs in the same direction as it leaves the outlet portion 6 as it does as it enters the inlet portion 5.
- the inlet portion 5 and the outlet portion 6 are identical and mounted to two opposite faces 1a, 1b of the inner housing 1 using the same flange on respective portion 5, 6 but turned 180° about an axis A extending along the centre line of the web W running through the inner housing 1.
- the respective entrance segment 5a, 6a of the inlet portion 5 and the outlet portion 6 are adjacent the central portion of the tunnel and that the respective exit segment 5c, 6c of the inlet portion 5 and the outlet portion 6 are directed away from each other.
- An outer housing 4 surrounds the inner housing 1 and the outer housing 4 is provided with openings forming an inlet 7 and an outlet 8 for the entrance and the exit of the web W.
- the emitters 2, 3 transmit an electron beam out through the exit windows 21 , 31.
- One side of the web W is irradiated by the first emitter 2 and the other side is irradiated by the second emitter 3.
- the second electron beam emitter 3 is positioned substantially opposite the first emitter 2 and the electron exit window 31 of the second emitter 3 is positioned substantially opposite the first electron exit window 21.
- the emitter 2 generally comprises a vacuum chamber 22 in which a filament 23 and a cage 24 is provided.
- the filament 23 is made of tungsten.
- the electrical resistance of the filament 23 causes the filament 23 to be heated to a temperature in the order of 2000 0 C. This heating causes the filament 23 to emit a cloud of electrons.
- a cage 24 provided with a number of openings surrounds the filament 23. The cage 24 serves as a Faraday cage and help to distribute the electrons in a controlled manner.
- the electrons are accelerated by a voltage between the cage 24 and the exit window 21.
- the emitters used are generally denoted low voltage electron beam emitters, which emitters normally have a voltage below 300 kV. In the disclosed design the accelerating voltage is in the order of 70-85 kV. This voltage results in a kinetic (motive) energy of 70-85 keV in respect of each electron.
- the electron exit window is substantially planar and provided substantially in parallell with the web. Further, the exit window 21 is made of a metallic foil and has a thickness in the order of 6 ⁇ m. A supporting net formed of aluminium supports the exit window 21.
- An emitter of this kind is described in more detail in US-B1 - 6,407,492.
- US-A-5,637,953 is another emitter disclosed. This emitter generally comprises a vacuum chamber with an exit window, wherein a filament and two focusing plates are provided within the vacuum chamber.
- US-A-4, 910,435 is yet another emitter disclosed, wherein the electrons are emitted by secondary emittance from a material bombarded by ions.
- the X-ray When such an X-ray hits the inner wall of the housing, the X-ray enters a certain distance into the material and causes emittance of new X-rays in all directions from the point of entrance of the first X- ray. Every time an X-ray hits the wall of the housing and gives rise to a secondary X-ray, the energy is about 700-1000 times less, dependent upon the choice of material for the housing.
- Stainless steel has a reduction ratio of about 800, i.e. the energy of a secondary X-ray is reduced about 800 times in relation to the primary X-ray.
- Lead is a material often being considered when radiation is involved. Lead has a lower reduction ratio, but has on the other hand a higher resistance against transmission of the X-rays through the material.
- the inner housing 1 is made of stainless steal having a thickness of 22 mm. This thickness is calculated for X-rays travelling perpendicular to the wall. An X-ray travelling inclined in relation to the wall will experience a longer distance in the wall to reach the same depth, i.e. the wall will appear thicker. The wall thickness is determined by the governmental regulations concerning amount of radiation outside the housing.
- the limiting value that the radiation must be less than is 0,1 ⁇ Sv/h measured at a distance of 0,1 m form any accessible surface, i.e outside shielding. It should be noted that the choice of material and the dimensions are influenced by the regulations presently applicable and that new regulations might alter the choice of material or the dimensions.
- the energy of each electron (80keV) and the number of electrons determine the total energy of the electron cloud. This total energy results in a total energy transfer to the surface to be sterilized. This radiation energy is measured in the unit Gray (Gy). In case of the electron emitter briefly described above (with a filament and Faraday cage) it is presently considered suitable to use a current of about 17mA through the filament.
- the fluid is air, but it can of course be any gaseous fluid suitable for the field of application in which the device is used.
- the air system 100 of the machine comprises a compressor 101 and a water separator 102 from which pressurised air is obtained.
- This air is supplied to a heat exhanger 103 in which the air is pre- heated to about 100 0 C.
- the air is fed to a superheater 104 in which the air is heated to a temperature within the range 330- 450 0 C.
- any bacteria in the air is killed. The killing rate is dependent upon the temperature and the time the bacteria are subjected to said temperature.
- the air from the superheater 104 is returned to the heat exhanger 103 for achieving the above-described pre-heating of the incoming air.
- the air After the second passage through the heat exchanger 103, the air has a temperature of about 9O 0 C.
- the air is then fed to a change-over valve 106 having a first branch in fluid connection with the tower 105 of the filling machine and a second branch in fluid connection with a first chamber 107 formed by the outer housing 4.
- a small amount of the air supplied to the tower 105 will follow the web W out of the tower 105 through an outlet opening 108.
- the web W In the tower 105 the web W is formed into a tube by overlappingly sealing the longitudinal edges of the web.
- the tube is continuously filled with a product via a product pipe 109 extending into the tube from the end where the web W has not yet been transformed into a tube.
- the outlet opening 108 is provided with a sealing ring (not shown) in order to have a controlled flow of air out of the outlet opening 108. This can also be achieved by forming the outlet opening 108 with a given clearance in respect of the tube being fed out through the opening 108.
- the tube is transversally sealed and formed into cushions, which are separated and formed into parallelepipedic containers. Again, this technology is well known per se and will not be described in detail.
- a significant portion of the air supplied to the tower 105 flows in the tower 105 in a direction opposite the direction of travel of the web W.
- the tower 105 is provided with a web inlet opening 110 acting as an air outlet opening 110.
- the air from the tower 105 is fed to a second chamber 111 formed of the inner housing 1.
- dashed lines represent two alternative embodiments of the air flow into the first and second chambers.
- the lines are continuous and represents a closed communication directly between a web outlet opening 112 of the second chamber 111 and a web outlet opening 121 , also denoted outlet 8, of the first chamber 107.
- the lines are not present and represents an open communication between both the first and second chambers 107, 111 and the web outlet opening 121 of the first chamber 107.
- the fluid connection can for example comprise a pipe that connects the web outlet opening 112 of the second chamber 111 with the web outlet opening 121 of the first chamber 107.
- the web outlet opening 112 of the second chamber 111 extends to the web outlet opening 121 of the first chamber 107.
- a fluid connection between the first chamber 107 and the web outlet opening 121 of the first chamber 107 is thereby prevented.
- the change-over valve 106 is acting as air supply 106 for the first chamber 107.
- both the first chamber 107 and the second chamber 111 are in fluid connection with the web outlet opening 121 of the first chamber 107, thus both chambers 107, 111 being in connection with the air supply in the tower 105.
- the first chamber 107 is being in contact with valve 106 for additional supply of air.
- both embodiments the air in the second chamber 11 1 flows in a direction opposite the direction of travel of the web W through the second chamber 111. After passage almost completely through the second chamber 111 the air is fed via a discharge outlet 113 for ultimate disposal of the air.
- the air provided to the first chamber 107 flows in a direction opposite the direction of travel of the web W.
- the air from the first chamber 107 and the second chamber 111 is discharged via the outlet 113.
- both chambers 107, 111 being in contact with the outlet.
- a small amount of the air supplied to the first chamber 107 escapes via a web inlet opening 115, also denoted inlet 7. The amount escaping is dependent of the shape of the gap and the sealing used. This in turn depend amongst others upon if the web is supplied with pre-applied opening devices or not.
- the discharge outlet 113 is located close to the web inlet opening 114 of the second chamber 111.
- the outlet 113 is located inside the second chamber 111.
- the outlet 1 13 can be located in the vicinity of the web inlet opening 114 of the second chamber 111.
- the outlet 113 is discharging almost all the air from the second chamber 111 and most of the air from the first chamber 107.
- the outlet 113 comprises two branches 113a, 113b in fluid connection with the second chamber 111.
- the first outlet branch 113a is located in the top of the chamber wall in the vicinity of the web inlet opening 114 of the second chamber 111
- the second outlet branch 113b is located in the bottom wall opposite the first.
- the flow of air in the system is controlled so that a first overpressure is created inside the first chamber 107.
- the pressure is in the order of 30 mm H 2 O.
- a second overpressure is created inside the second chamber 111.
- the overpressures can for example be choosen so that the first overpressure and the second overpressure are the same. Alternatively, the overpressures are choosen so that the first overpressure and the second overpressure are different.
- the first pressure can be higher than the second pressure and vice versa.
- One reason for choosing the first overpressure so that it is higher than the second overpressure is to keep ozone (O 3 ), formed during irradiation, within the second chamber 111 where it can be immediately discharged through the outlet 113.
- a lower second overpressure helps during pre-sterilization of the device at for example start-up of the machine.
- a sufficient amount of the hydrogen peroxide used during the sterilization is forced inside the second chamber.
- the pre-sterilization will be explained in more detail below.
- One reason for choosing the second overpressure so that it is higher than the first overpressure could be to obtain a fast evacuation of ozone and eventual other volatile substances, that for example cause off-flavour, from the second chamber.
- Inside the inner housing 1 i.e. around the emitters 2,3, is provided a pressure that is preferably lower than the pressure inside the second chamber 111.
- the pressure in the inner housing 1 can be atmospheric pressure. However, it should be understood that the inner housing 1 may be pressurised if necessitated by the emitters used.
- the air system 100 is provided with a so- called zero point 116.
- the zero point 116 is a device making sure that if something fails in the system, any air needed to avoid a pressure below the atmospheric pressure will be fed into the system via the zero point 116. This way it is secured that the pressure inside the tower 105, the first chamber 107 and the second chamber 111 at least not will drop below the atmospheric pressure.
- the zero point 116 generally comprises a housing with an inlet 117 and an outlet 118 and an opening 119 being closed by a valve 120. Any pressure above the atmospheric pressure pushes the valve outwards sealingly closing of the opening 119. If the pressure inside the zero point 116 drops below the atmospheric pressure the valve 120 will not be pushed against the opening 119 (on the contrary it will be pushed inwards into the zero point 116 and air can be introduced into the system via the opening 119).
- the air system 100 can be used for sterilizing the surfaces inside of tower 105 and the chambers 107,111 prior to entering the web W.
- the sterilization is made with hydrogen peroxide (H2O2).
- Sterilization using hydrogen peroxide is known per se, but will be briefly described in the following with regard to the air system 100.
- the tower 105 is in connection with a hydrogen peroxide supply, which is provided with aerosol nozzles. The nozzles feed hydrogen peroxide into the air as spray and the air supplied in the tower is heated to a temperature at which the hydrogen peroxide vapourises, normally a temperature in the order of 40-50 0 C.
- the hydrogen peroxide contained air flows through the tower and the chambers 107,111 in the earlier described direction and is discharged at the discharge outlet 113. Along the way the hydrogen peroxide condenses on the surfaces.
- the hydrogen peroxide is then removed from the surfaces by supplying air of a temperature at or above the hydrogen peroxide vapourisation temperature. In this embodiment a temperature in the order of 70-90 0 C is used. By providing a temperture well above the vaporisation temperature the hydrogen peroxide is effectively and quickly removed from the surfaces.
- the web W is provided to pass through the tunnel.
- the tunnel is being provided with a web inlet portion 5, a web outlet portion 6 and a central portion adapted to receive an electron beam emitter 2, 3 provided with an electron exit window 21 , 31. Electrons are emitted into the tunnel from the emitter 2,3 through the electron exit window 21 , 31 , and any X-ray being formed by the electrons during irradiation of the web W is forced to hit the tunnel wall twice before exiting the tunnel.
- the tunnel is being formed angled at at least two locations in each of the inlet and outlet portions 5, 6.
- the method comprises forming the inlet portion 5 so that it comprises a line of three sucsessive segments, an entrance segment 5a, a central segment 5b and an exit segment 5c.
- the central segment 5b is made so that it forms a first angle ⁇ to the entrance segment 5a.
- the exit segment 5c forms a second angle ⁇ to the central segment 5b.
- the outlet portion 6 is similarily designed.
- a relation between the tunnel widths, said angles ⁇ , ⁇ and the lengths of the segments 5a-c is formed so that an imagined straight line hitting the tunnel wall in the entrance segment 5a is also hitting the tunnel wall of at least the exit segment 5c, before exiting the exit segment 5c, and that an imagined straight line passing through the entrance segment 5a is hitting the tunnel wall of the central segment 5b such that it is also hitting the tunnel wall of at least the exit segment 5c, before exiting the exit segment 5c.
- the invention also comprises a method of ventilating the device.
- the method comprises the step of providing a first chamber 107 comprising a web inlet opening 115 and a web outlet opening 121.
- the first chamber 107 being the outer housing 4.
- a second chamber 111 being the tunnel, is also provided and extends inside the first chamber 107.
- the second chamber 111 is formed comprising a web inlet opening 114 and a web outlet opening 112. Further, an electron exit window 21 , 31 is provided through which electrons are adapted to be emitted into the second chamber 111.
- the web W is passing through the second chamber 111 , and a flow of air through both the first and second chambers 107, 111 is created.
- the air flow flows in a direction opposite the direction of travel of the web W.
- the air is supplied into the web outlet opening 121 of the first chamber 107 and there is provided at least one outlet 113.
- fluid connection is being provided between the web outlet opening 121 of the second chamber 111 and the web outlet opening 112 of the first chamber 107.
- fluid connection between the first chamber 107 and the web outlet opening 121 of the first chamber 107 is prevented.
- a flow of air through both the first and second chambers 107, 111 in a direction opposite the direction of travel of the web W can then be created by supplying said air into the first chamber 107 and into the web outlet opening 121 of the first chamber 107 and providing at least one outlet 113.
- Air is supplied to the first chamber 107 through a valve 106 being in fluid connection with the first chamber 107.
- the web W is thus entering the device through the web inlet opening 115 of the first chamber 107 and enters the second chamber 111 at its web inlet opening 114. Both openings 115, 114 are located such that the web W is kept straight, substantially horizontal when passing them. Inside the inlet portion 5 the web W is angled the second angle ⁇ at the first roller 9 and angled the first angle ⁇ at the second roller 10. During travelling, the web W meets an airflow flowing in a direction opposite the web W. When the web W passes the central portion of the tunnel, now travelling in a vertical direction, it passes electron exit windows 21 , 31 through which the web W is irradiated by emitters 2, 3.
- the electron exit windows 21 , 31 are located on opposite sides of the tunnel thereby irradiating both sides of the web W. After the irradiation the web W enters into the outlet portion 6 in which it is angled twice like in the inlet portion 5. Finally, it is exiting the device through the web outlet opening 112 of the second chamber 111 , and then through the web outlet opening 121 of the first chamber 107, thereby entering the tower 105.
- the described embodiment comprises two emitters 2,3, one for electron irradiation of one side of the web W and the other for electron irradiation of the other side of the web W.
- the device does not need to comprise two emitters 2,3, but can comprise only one emitter.
- the two emitters 2,3 are located opposite each other. Alternatively they can be located at a distance from each other in the web direction.
- the number of emitters can be more than two. It is for example possible to have several emitters side by side to handle wide webs. It is also possible to have two or more emitters located after each other along the direction of the web to form either subsequent sterilizing zones which together provide the decided radiation level, or as measure of selective radiation of a certain point, for example a closure device, that may need a higher radiation level.
- the location of the outlet 113 can be modified. In the above-described emodiment the outlet 113 is located inside the second chamber 111. Alternatively the outlet 113 can for example be located in vicinity of the web inlet opening 114 of the second chamber 111 or in the vicinity of the web inlet opening 115 of the first chamber 107. It is also possible to locate the outlet 113 outside, near the inlet opening 115, of the first chamber 107.
- the outlet 113 is located inside the second chamber 111 and the first chamber 107 is in fluid connection with the second chamber 111.
- the web inlet opening 114 of the second chamber 111 is in fluid connection with the web inlet opening 115 of the first chamber 107, while fluid connection between the first chamber 107, its web inlet opening 115 and the web inlet opening 114 of the second chamber 111 is prevented.
- the two chambers 107,111 will then be in communication with separate outlets. At least one outlet can be located in the first chamber 107 and at least one outlet can be located in the second chamber 111 or in fluid connection with the second chamber 111.
- the air system described using hydrogen peroxide is preferably used in aseptic fields of application.
- the air flows are similar, although the machine sterilization is usually made by using filtered air.
- the system can then comprise a filter and a fan.
- the system can be provided with a catalytic converter.
- the web inlet opening 114 of the second chamber 111 is located at a distance from and preferably in line with the web inlet opening 115 of the first chamber 107.
- the second chamber 111 can extend all the way up to the web inlet opening 115 of the first chamber thereby preventing fluid connection between the first chamber 107 and the web inlet opening 115.
- the wall of the second chamber 111 is then instead provided with throughgoing openings, preferably slits, at a distance from the web inlet opening, but before the outlet 113. Fluid connection between the two chambers is thereby provided and the arrangement give rise to a so called injector effect making air flow from the first chamber through the slits into the second chamber where it can be evacuated through the outlet 113. A small amount of air is also sucked from outside the housings through the web inlet opening 115.
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- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- High Energy & Nuclear Physics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Epidemiology (AREA)
- Toxicology (AREA)
- Mechanical Engineering (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
- Recrystallisation Techniques (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Heating, Cooling, Or Curing Plastics Or The Like In General (AREA)
Abstract
Description
Claims
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP04736366A EP1638846B1 (en) | 2003-06-19 | 2004-06-08 | Method and device for electron beam irradiation |
AU2004247607A AU2004247607B2 (en) | 2003-06-19 | 2004-06-08 | Method and device for electron beam irradiation |
BRPI0409943A BRPI0409943B1 (en) | 2003-06-19 | 2004-06-08 | method of venting an electron beam irradiation device and, electron beam irradiation device |
US10/561,230 US7417239B2 (en) | 2003-06-19 | 2004-06-08 | Method and device for electron beam irradiation |
MXPA05013235A MXPA05013235A (en) | 2003-06-19 | 2004-06-08 | Method and device for electron beam irradiation. |
DE602004011056T DE602004011056T2 (en) | 2003-06-19 | 2004-06-08 | METHOD AND DEVICE FOR IRRADIATION BY ELECTRON BEAMS |
JP2006508580A JP4563380B2 (en) | 2003-06-19 | 2004-06-08 | Method and apparatus for electron beam irradiation |
HK07100500.6A HK1093717A1 (en) | 2003-06-19 | 2007-01-15 | Method and device for electron beam irradiation |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SE0301781-1 | 2003-06-19 | ||
SE0301781A SE525347C2 (en) | 2003-06-19 | 2003-06-19 | Electron irradiation method and apparatus |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2004110869A1 true WO2004110869A1 (en) | 2004-12-23 |
Family
ID=27607347
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/SE2004/000894 WO2004110869A1 (en) | 2003-06-19 | 2004-06-08 | Method and device for electron beam irradiation |
Country Status (14)
Country | Link |
---|---|
US (1) | US7417239B2 (en) |
EP (1) | EP1638846B1 (en) |
JP (1) | JP4563380B2 (en) |
CN (1) | CN100413762C (en) |
AT (1) | ATE382548T1 (en) |
AU (1) | AU2004247607B2 (en) |
BR (1) | BRPI0409943B1 (en) |
DE (1) | DE602004011056T2 (en) |
ES (1) | ES2295872T3 (en) |
HK (1) | HK1093717A1 (en) |
MX (1) | MXPA05013235A (en) |
RU (1) | RU2333140C2 (en) |
SE (1) | SE525347C2 (en) |
WO (1) | WO2004110869A1 (en) |
Cited By (4)
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WO2007099120A1 (en) | 2006-02-28 | 2007-09-07 | Novo Nordisk A/S | A method and an apparatus for sterilizing packaging material |
EP1849746A1 (en) * | 2006-04-26 | 2007-10-31 | Shibuya Kogyo Co., Ltd | Apparatus and method for sterilization of vessels |
US7560714B2 (en) | 2005-10-26 | 2009-07-14 | Tetra Laval Holdings & Finance S.A. | Sensor and system for sensing an electron beam |
US7592613B2 (en) | 2006-06-14 | 2009-09-22 | Tetra Laval Holdings & Finance S.A. | Sensor and system for sensing an electron beam |
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SE526700C2 (en) * | 2003-06-19 | 2005-10-25 | Tetra Laval Holdings & Finance | Apparatus and method for sterilizing an electron beam material web |
US20130097302A9 (en) * | 2003-10-01 | 2013-04-18 | Robert Khedouri | Audio visual player apparatus and system and method of content distribution using the same |
US7291854B2 (en) * | 2005-07-18 | 2007-11-06 | Trinity Health Corporation | Radiation attenuation corridor |
SE530589C2 (en) * | 2006-12-11 | 2008-07-15 | Tetra Laval Holdings & Finance | Method of irradiating objects |
DE102007003334A1 (en) | 2007-01-17 | 2008-08-07 | Khs Ag | Method and device for the continuous sterilization of pouches |
WO2011005307A2 (en) | 2009-07-07 | 2011-01-13 | Advanced Electron Beams | Method and apparatus for ebeam treatment of webs and products made therefrom |
DE102011015344A1 (en) | 2011-03-28 | 2012-10-04 | Krones Aktiengesellschaft | Method and device for sterilizing packaging materials |
EP3170756B1 (en) * | 2015-11-23 | 2018-09-19 | Tetra Laval Holdings & Finance S.A. | Device and method for sterilization of a sheet of packaging material and filling machine |
MY195270A (en) * | 2016-08-20 | 2023-01-11 | Buehler Ag Geb | Apparatuses and methods for pasteurizing and/or sterilizing par-ticulate material and cassette |
EP3575227B1 (en) * | 2018-06-01 | 2021-04-07 | Tetra Laval Holdings & Finance S.A. | Packaging machine and method for producing sealed packages |
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JP2002171949A (en) * | 2000-12-07 | 2002-06-18 | Ishikawajima Harima Heavy Ind Co Ltd | Electron beam sterilization method and electron beam sterilizer |
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2003
- 2003-06-19 SE SE0301781A patent/SE525347C2/en not_active IP Right Cessation
-
2004
- 2004-06-08 JP JP2006508580A patent/JP4563380B2/en not_active Expired - Fee Related
- 2004-06-08 ES ES04736366T patent/ES2295872T3/en not_active Expired - Lifetime
- 2004-06-08 AT AT04736366T patent/ATE382548T1/en active
- 2004-06-08 EP EP04736366A patent/EP1638846B1/en not_active Expired - Lifetime
- 2004-06-08 US US10/561,230 patent/US7417239B2/en active Active
- 2004-06-08 CN CNB2004800171086A patent/CN100413762C/en not_active Expired - Fee Related
- 2004-06-08 RU RU2006101398/11A patent/RU2333140C2/en active
- 2004-06-08 BR BRPI0409943A patent/BRPI0409943B1/en not_active IP Right Cessation
- 2004-06-08 DE DE602004011056T patent/DE602004011056T2/en not_active Expired - Lifetime
- 2004-06-08 AU AU2004247607A patent/AU2004247607B2/en not_active Ceased
- 2004-06-08 MX MXPA05013235A patent/MXPA05013235A/en active IP Right Grant
- 2004-06-08 WO PCT/SE2004/000894 patent/WO2004110869A1/en active IP Right Grant
-
2007
- 2007-01-15 HK HK07100500.6A patent/HK1093717A1/en not_active IP Right Cessation
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US4035981A (en) * | 1974-12-11 | 1977-07-19 | Alcan Research And Development Limited | Aseptic packaging |
US4252413A (en) * | 1978-10-05 | 1981-02-24 | Energy Sciences Inc. | Method of and apparatus for shielding inert-zone electron irradiation of moving web materials |
JP2002171949A (en) * | 2000-12-07 | 2002-06-18 | Ishikawajima Harima Heavy Ind Co Ltd | Electron beam sterilization method and electron beam sterilizer |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7560714B2 (en) | 2005-10-26 | 2009-07-14 | Tetra Laval Holdings & Finance S.A. | Sensor and system for sensing an electron beam |
WO2007099120A1 (en) | 2006-02-28 | 2007-09-07 | Novo Nordisk A/S | A method and an apparatus for sterilizing packaging material |
US7972558B2 (en) | 2006-02-28 | 2011-07-05 | Novo Nordisk A/S | Method and an apparatus for sterilizing packaging material |
EP1849746A1 (en) * | 2006-04-26 | 2007-10-31 | Shibuya Kogyo Co., Ltd | Apparatus and method for sterilization of vessels |
US7592613B2 (en) | 2006-06-14 | 2009-09-22 | Tetra Laval Holdings & Finance S.A. | Sensor and system for sensing an electron beam |
Also Published As
Publication number | Publication date |
---|---|
JP4563380B2 (en) | 2010-10-13 |
BRPI0409943B1 (en) | 2018-05-08 |
SE0301781L (en) | 2004-12-20 |
SE0301781D0 (en) | 2003-06-19 |
DE602004011056D1 (en) | 2008-02-14 |
RU2333140C2 (en) | 2008-09-10 |
MXPA05013235A (en) | 2006-03-09 |
CN1809495A (en) | 2006-07-26 |
DE602004011056T2 (en) | 2008-04-10 |
HK1093717A1 (en) | 2007-03-09 |
EP1638846A1 (en) | 2006-03-29 |
US7417239B2 (en) | 2008-08-26 |
EP1638846B1 (en) | 2008-01-02 |
AU2004247607A1 (en) | 2004-12-23 |
BRPI0409943A (en) | 2006-04-25 |
US20060145093A1 (en) | 2006-07-06 |
CN100413762C (en) | 2008-08-27 |
ES2295872T3 (en) | 2008-04-16 |
ATE382548T1 (en) | 2008-01-15 |
SE525347C2 (en) | 2005-02-08 |
AU2004247607B2 (en) | 2008-11-20 |
JP2006526549A (en) | 2006-11-24 |
RU2006101398A (en) | 2006-06-27 |
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