Classifications

• • G—PHYSICS
  • G01—MEASURING; TESTING
  • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
  • G01N1/00—Sampling; Preparing specimens for investigation
  • G01N1/02—Devices for withdrawing samples
  • G01N1/10—Devices for withdrawing samples in the liquid or fluent state
  • G01N1/20—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
• • G—PHYSICS
  • G01—MEASURING; TESTING
  • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
  • G01N1/00—Sampling; Preparing specimens for investigation
  • G01N1/02—Devices for withdrawing samples
  • G01N1/10—Devices for withdrawing samples in the liquid or fluent state
  • G01N1/18—Devices for withdrawing samples in the liquid or fluent state with provision for splitting samples into portions
• • G—PHYSICS
  • G01—MEASURING; TESTING
  • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
  • G01N1/00—Sampling; Preparing specimens for investigation
  • G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
  • G01N1/38—Diluting, dispersing or mixing samples
• • G—PHYSICS
  • G01—MEASURING; TESTING
  • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
  • G01N1/00—Sampling; Preparing specimens for investigation
  • G01N1/02—Devices for withdrawing samples
  • G01N1/10—Devices for withdrawing samples in the liquid or fluent state
  • G01N2001/1006—Dispersed solids
  • G01N2001/1012—Suspensions
  • G01N2001/1025—Liquid suspensions; Slurries; Mud; Sludge

Definitions

• the present invention relates to a method and apparatus for taking slurry samples containing solids from a large process flow, into which process flow a sampling device is at least partly immersed.
• a combined sample often composed of several small single samples for further laboratory measurements.
• a combined sample represents the operation carried out in the plant in question within one shift or within 24 hours.
• the representability of the sample is affected by the fact that the sampler is prevented from being blocked by impurities possibly contained in the process flow or in the slurry.
• samplers For freely flowing slurries in atmospheric pressure, there are generally used vertical sample cutters that cut a small slice of the process flow. The moving samplers move back and forth transversally against the flowing direction and extract a representative sample even if the process flow is not homogeneous. Fixed cutter samplers extract a representative sample, if the process flow is homogeneous in the horizontal direction. Fixed cutter samplers also allow a certain degree of non-homogeneousness in the vertical direction of the flow.
• the input flow orifice of a cutter used for sampling must be sufficiently large in order to prevent occasional large particles or impurities from blocking the orifice too easily.
• the minimum width of the orifice is 8 mm, but often there is needed an orifice with a width that is larger than 20 mm.
• a sample obtained from large process flows that is extracted by letting the slurry flow freely into the sample cutter is too large for analysis.
• the constriction of the sample flow lowers the flow speed at the input orifice of the cutter, which leads to separation, and the obtained sample is therefore not representative.
• the right solution is to extract the sample from the process flow in two steps, as is described for example in the FI patent application 20002348.
• the process flow and the sample flow are at least partly nested, in which case the samplers must be specially designed in order to create speed differences therebetween.
• the object of the present invention is to eliminate some of the drawbacks of the prior art and to realize an improved and simple method and apparatus for taking a representative slurry sample containing solids at least in two steps from a large, proceeding process flow in atmospheric pressure.
• the essential novel features of the invention are enlisted in the appended claims.
• the first-step sampler advantageously comprises at least three sampling units that are arranged adjacently and at least partly immersed in a solids-bearing slurry flow proceeding in the horizontal direction, in such a position that in the slurry flow direction, at the same spot where part of the slurry flow enters the sample units, the slurry flow left outside the sample units is conducted to a lower level.
• those elements of the slurry flow channel that are located on different sides of the sampling spot are installed at different heights with respect to the horizontal level.
• the sample flow is advantageously conducted through the input orifice to a space that is provided in the sampler after the sampler unit.
• the sample flows are combined and mixed together before the second-step sampling is carried out by methods known as such.
• the combined sample flow is according to the invention subjected to another sampling of the first step by at least two new sampling units, and the obtained new sample flows are combined and mixed prior to the sampling of the third step.
• the sampling units in between the sampling units and the space provided after the sampling units, there can, according to the invention, be installed a moving sampling device that cuts part of the flow obtained from the sampling units and conducts the cut section to the space provided after the sampling units. That part of the flow obtained from the sampling units that is left outside the cutter is returned to the main process flow proceeding in the flow channel.
• the extracting of the slurry to be analyzed from the slurry flow containing solids by first creating by at least a one-step sampling system a sample flow, from which sample flow there is obtained the sample flow to be fed to the analyzer or to the combination sampler.
• the slurry flow containing solids and the sample flow obtained from said slurry flow are advantageously separated by conducting the slurry flow that is left outside the sample flow to a lower level. In that case for instance pumping or separation based on pressure difference is not needed for conducting the slurry flow and the sample flow in different directions.
• the elements constituting the flow channel that contains the slurry flow bearing solids are mutually installed so that that element of the flow channel that is located in the flowing direction after the point of orientation is placed lower with respect to the horizontal level than the element of the flow channel that is located in the flowing direction before the point of orientation.
• the element of the flow channel that is located before and the element that is located after are mutually aligned, so that the elements are interconnected by means of a connecting element placed in an essentially inclined position, said connecting element being advantageously similar in cross-section as the flow channel.
• Said connecting element can also be arranged in an essentially vertical position.
• a sampler comprising at least three adjacent sampling units, said sampler being at least partly immersed in the slurry flow.
• a mixing step that transforms the sample proceeding in the flow channel to a chute flow.
• the sampling units are designed so that the slurry flow entering the sampling units continues to proceed into the space provided in the sampler after the sampling units.
• the slurry flow that is left outside the sampler is conducted, via a conduit piece arranged between the flow channel elements, to a horizontally lower level, but continues flowing, advantageously in the same direction as the flow channel element that was located prior to the sampler.
• the walls of the sampling units are mutually installed so that the walls are drawn apart in the direction of the slurry flow, when proceeding away from the input orifices of the slurry flow contained in the sampler unit.
• the space available for the slurry flow entering the sampling unit is increased, the flowing speed of the slurry flow is reduced and the surface of the slurry flow with respect to the wall of the sampling unit is lowered, so that the suction created by the lowering of the surface compensates some of the friction caused by the sampler unit.
• the slurry flows entering through the sampling units and a possible moving sampling device are combined, and the slurry flows are subjected to mixing in the space provided after the sampling units prior to further treatment in the sampling step that alternatively comprises either a repetition of the first sampling step or the extraction of a sample to be analyzed.
• the mixing can be carried out by example by installing an agitator in the slurry flow.
• the mixing can also be carried out so that the direction of the combined slurry flow on the horizontal level is altered, so that the slurry flow forms an angle of at least 60 degrees, advantageously at least 90 degrees, with the original flowing direction.
• the change in the flowing direction also reduces the space needed for the sampling equipment.
• the slurry flow that forms an angle with respect to the original flowing direction can be conducted, depending on the size of the slurry flow, directly to the second-step sampling, where from the slurry flow there is extracted a sample that advantageously has a suitable size and is representative, to be further conducted to the analyzer in order to be analyzed or for extracting a combined sample.
• the slurry flow that forms an angle in the original flowing direction is again conducted to a sampler comprising at least two sampling units but being located separately with respect to the sampler that was placed prior to the change of the flowing direction.
• the sampler that is arranged separately with respect to the sampler that was placed prior to the change of the flowing direction is installed in a similar position with respect to the slurry flow as the sampler that was placed prior to the change of the flowing direction, in which case the slurry flow entering the sampling units proceeds flowing into the space provided after the sampling units.
• the slurry flows are combined, and they are subjected to mixing, advantageously by changing the flowing direction on the horizontal level.
• the combined and mixed slurry flow generally has, after two steps of sampling, an advantageous size for extracting a combined sample or for creating a representative sample flow that can be analyzed in an analyzer.
• the slurry flow that is left outside the sampling units it is again conducted, via a conduit piece of the elements of the slurry flow channel that are horizontally arranged at different levels, to flow onto a horizontally lower level than the slurry flow that proceeded in the flow channel prior to the sampling units.
• the slurry flow left outside the sampling units is at the sampling spot directed downwardly.
• the direction of the slurry flow that has proceeded through the sampling units is on the horizontal level altered in the space provided after the sampling units.
• the slurry flow is subjected to one or several first-step samplings according to the invention by directing the slurry flow left outside the sampling units downwardly at the sampling spot.
• at least one moving sampler which as such has an advantageous effect when defining required first-step samplings according to the invention.
• figurel is a schematical illustration of a preferred embodiment of the invention, seen from the side
• figure2 is a more detailed illustration of the sampler according to figure 1
• figure 3 is a schematical illustration of another preferred embodiment of the invention, seen from the side
• figure 4 is a schematical illustration of the first-step sampling of the embodiment of figure 3, seen from the top.
• the sampler 2 comprising several sampling units 1 is installed in an element 5 of a solids-containing slurry flow 3, the direction of said flow being indicated by means of the arrows 4, said element 5 being arranged on a level that is horizontally higher than the element 6 of the flowing channel.
• Said elements 5 and 6 of the flowing channel are mutually connected by means of a conduit piece 7 that is arranged in an essentially inclined position.
• the sampler 2 is installed in the element 5 of the flowing channel so that the sampler 2 is in mechanical contact with the flowing channel element 5 only at the first end thereof, when seen in the flowing direction 4.
• the sampler 2 can also be installed so that there is no mechanical contact with the flowing channel element 5, but the sampler 2 is completely supported from outside the element 5.
• the sampler 2 is installed essentially near to the angle created by the flowing channel element 5 and the conduit piece 7, so that in the flowing direction 4, the slurry flow coming from the flowing channel element 5 is partly conducted into the sampler 2 and partly to the flowing channel element 6 via the conduit piece 7 and the orientation elements 9 connected to the sampler 2.
• the slurry flows entering the sampler 2 via the sampling units 1 are conducted into a space 10 arranged in succession to the sampling units 1.
• the walls 11 and 12 of the sampling units are mutually installed so that said walls 11 and 12 are drawn apart with respect to the flowing direction 4 of the slurry flow.
• the slurry flows obtained from separate sampling units 1 are combined, and the direction of the created combined slurry flow is changed, essentially on the same horizontal level as the space 10, so that the angle of change of the flowing direction is 90 degrees.
• the slurry flows obtained from separate sampling units 1 are advantageously mixed together.
• the combined slurry flow is returned to sampling in a new sampler 13, provided with several adjacent sampling units 14.
• the slurry flow left outside the sampling units 14 is conducted, via an aperture 15 provided between the sampling units 14, to a lower level.
• the sampler 13 essentially corresponds to the sampler 2, but there is one difference: the number of the sampling units 14 is at least two; thus the slurry flow that has entered the sampling units 14 is further conducted to a space 16 arranged after the sampling units 14, where the slurry flows obtained from separate sampling units 14 are combined.
• the combined slurry flow leaving the space 16 provided after the sampling units 14 is subjected, in order to achieve a good mixing, to a change of the flowing direction, so that the angle of change is 90 degrees, essentially on the same horizontal level as the space 16.
• the slurry flow that proceeds into analysis is discharged from the sampling arrangement through an outlet orifice 17.
• the slurry flow discharged through the outlet orifice 17 can, depending on the size of the flow, be conducted either to be directly analyzed, or the slurry flow can be subjected to one more sampling 18, for instance by means of a regular sample cutting.
• the slurry flow 3 that proceeds to the sampling units 1 from the flowing channel 5, the flowing direction of said slurry flow 3 being indicated by means of the arrow 4, is after the sampling units 1 subjected to another sampling step by a moving sampling device 21.
• the moving sampling device 21 moves in an essentially horizontal direction and cuts a slice of the flow of the sampling conduits 19, after which said slice is conducted into a space 20 provided after the sampling units, where the entering sample flow is subjected to mixing in a way described above. That part of the slurry flow that is not directed into the sampling units 1 and via the moving sampling conduits 19 to the space 20 is conducted, via the conduit 7, to the part 6 of the flowing channel and further to the next process step.

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• Life Sciences & Earth Sciences (AREA)
• Hydrology & Water Resources (AREA)
• Physics & Mathematics (AREA)
• Health & Medical Sciences (AREA)
• Chemical & Material Sciences (AREA)
• Analytical Chemistry (AREA)
• Biochemistry (AREA)
• General Health & Medical Sciences (AREA)
• General Physics & Mathematics (AREA)
• Immunology (AREA)
• Pathology (AREA)
• Sampling And Sample Adjustment (AREA)

Priority Applications (6)

Applications Claiming Priority (2)

Publications (1)

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Family Applications (1)

Country Status (11)

Cited By (4)

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Citations (9)

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• 2002
  • 2002-02-14 FI FI20020295A patent/FI117522B/fi not_active IP Right Cessation
• 2003
  • 2003-01-29 AR ARP030100260A patent/AR038338A1/es unknown
  • 2003-02-03 CA CA2472749A patent/CA2472749C/en not_active Expired - Lifetime
  • 2003-02-03 BR BR0307602-4A patent/BR0307602A/pt active Search and Examination
  • 2003-02-03 AU AU2003201985A patent/AU2003201985B2/en not_active Expired
  • 2003-02-03 WO PCT/FI2003/000083 patent/WO2003069313A1/en not_active Application Discontinuation
  • 2003-02-03 CN CNB038025027A patent/CN100437075C/zh not_active Expired - Lifetime
  • 2003-02-03 EP EP03700833A patent/EP1474673A1/en not_active Withdrawn
  • 2003-02-03 EA EA200400771A patent/EA006491B1/ru not_active IP Right Cessation
  • 2003-02-07 PE PE2003000140A patent/PE20030996A1/es not_active Application Discontinuation
• 2004
  • 2004-06-25 ZA ZA2004/05061A patent/ZA200405061B/en unknown

Patent Citations (9)

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