WO2002007870A3 - Utilisation de la chimie combinatoire pour optimiser une synthese multiphase - Google Patents

Utilisation de la chimie combinatoire pour optimiser une synthese multiphase Download PDF

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Publication number
WO2002007870A3
WO2002007870A3 PCT/US2001/022128 US0122128W WO0207870A3 WO 2002007870 A3 WO2002007870 A3 WO 2002007870A3 US 0122128 W US0122128 W US 0122128W WO 0207870 A3 WO0207870 A3 WO 0207870A3
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WO
WIPO (PCT)
Prior art keywords
reaction conditions
catalysts
reactions
conditions
optimum
Prior art date
Application number
PCT/US2001/022128
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English (en)
Other versions
WO2002007870A2 (fr
Inventor
Dennis J O'rear
Charles L Kibby
Georgieanna L Scheuerman
Original Assignee
Chevron Usa Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chevron Usa Inc filed Critical Chevron Usa Inc
Priority to EP01957146A priority Critical patent/EP1315562A2/fr
Priority to AU2001278915A priority patent/AU2001278915A1/en
Publication of WO2002007870A2 publication Critical patent/WO2002007870A2/fr
Publication of WO2002007870A3 publication Critical patent/WO2002007870A3/fr

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0033—Optimalisation processes, i.e. processes with adaptive control systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/0054—Means for coding or tagging the apparatus or the reagents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00585—Parallel processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00603—Making arrays on substantially continuous surfaces
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00686—Automatic
    • B01J2219/00689—Automatic using computers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00695—Synthesis control routines, e.g. using computer programs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00698—Measurement and control of process parameters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B01J2219/00707—Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/00747—Catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/0075—Metal based compounds
    • B01J2219/00754—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B30/00—Methods of screening libraries
    • C40B30/08—Methods of screening libraries by measuring catalytic activity
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B40/00—Libraries per se, e.g. arrays, mixtures
    • C40B40/18—Libraries containing only inorganic compounds or inorganic materials
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B70/00—Tags or labels specially adapted for combinatorial chemistry or libraries, e.g. fluorescent tags or bar codes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Automation & Control Theory (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention concerne des procédés permettant de découvrir des catalyseurs et/ou des conditions de réaction optimaux pour effectuer des réactions multiphases, en particulier des réactions catalytiques multiphases. Les catalyseurs et/ou les conditions de réaction optimaux pour effectuer lesdites réactions sont identifiés par approche combinatoire. Les réactions sont réalisées dans les cavités d'un réacteur adapté pouvant supporter des conditions de haute température et de haute pression et permettant en outre d'effectuer une pluralité de réactions simultanées ou sensiblement simultanées. Ces procédés peuvent avantageusement être utilisés pour créer une base de données regroupant des combinaisons de systèmes de catalyse et/ou de conditions de réaction permettant d'obtenir différents écoulements de produits. Ainsi, en cas de changement des conditions du marché et/ou des spécifications des produits, les conditions adaptées à la formation des produits désirés peuvent être identifiées avec peu ou pas de temps d'arrêt. Les catalyseurs peuvent être évalués à travers la mise en oeuvre de conditions de réaction variées, permettant d'obtenir a) une bibliothèque combinatoire des écoulements de produits et une base de données contenant la combinaison de catalyseurs et de conditions de réaction permettant d'obtenir chaque écoulement de produits et/ou b) la combinaison optimale de catalyseurs et de conditions de réaction permettant d'obtenir un écoulement de produits désiré.
PCT/US2001/022128 2000-07-24 2001-07-13 Utilisation de la chimie combinatoire pour optimiser une synthese multiphase WO2002007870A2 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP01957146A EP1315562A2 (fr) 2000-07-24 2001-07-13 Utilisation de la chimie combinatoire pour optimiser une synthese multiphase
AU2001278915A AU2001278915A1 (en) 2000-07-24 2001-07-13 Use of combinatorial chemistry to optimize multi-step synthesis

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US62521600A 2000-07-24 2000-07-24
US09/625,216 2000-07-24

Publications (2)

Publication Number Publication Date
WO2002007870A2 WO2002007870A2 (fr) 2002-01-31
WO2002007870A3 true WO2002007870A3 (fr) 2002-07-25

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2001/022128 WO2002007870A2 (fr) 2000-07-24 2001-07-13 Utilisation de la chimie combinatoire pour optimiser une synthese multiphase

Country Status (3)

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EP (1) EP1315562A2 (fr)
AU (1) AU2001278915A1 (fr)
WO (1) WO2002007870A2 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005016851A1 (fr) 2003-05-08 2005-02-24 Valent Technologies, Llc Molecules recombinees et leur preparation
US7150182B2 (en) 2003-10-31 2006-12-19 Chevron Oronite Company, Llc High throughput screening methods for lubricating oil compositions
US7462490B2 (en) * 2003-10-31 2008-12-09 Chevron Oronite Company Llc Combinatorial lubricating oil composition libraries
US20050095714A1 (en) * 2003-10-31 2005-05-05 Wollenberg Robert H. High throughput preparation of lubricating oil compositions for combinatorial libraries
US7579192B2 (en) * 2003-10-31 2009-08-25 Chevron Oronite Company Llc High throughput screening methods for lubricating oil compositions

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4099923A (en) * 1977-01-17 1978-07-11 The Standard Oil Company Automatic catalytic screening unit
WO1996011878A1 (fr) * 1994-10-18 1996-04-25 The Regents Of The University Of California Synthese combinatoire de materiaux nouveaux
US6030917A (en) * 1996-07-23 2000-02-29 Symyx Technologies, Inc. Combinatorial synthesis and analysis of organometallic compounds and catalysts
WO2000032308A2 (fr) * 1998-12-04 2000-06-08 Symyx Technologies, Inc. Reacteur a alimentation continue en parallele
US6214195B1 (en) * 1998-09-14 2001-04-10 Nanomaterials Research Corporation Method and device for transforming chemical compositions

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4099923A (en) * 1977-01-17 1978-07-11 The Standard Oil Company Automatic catalytic screening unit
WO1996011878A1 (fr) * 1994-10-18 1996-04-25 The Regents Of The University Of California Synthese combinatoire de materiaux nouveaux
US6030917A (en) * 1996-07-23 2000-02-29 Symyx Technologies, Inc. Combinatorial synthesis and analysis of organometallic compounds and catalysts
US6214195B1 (en) * 1998-09-14 2001-04-10 Nanomaterials Research Corporation Method and device for transforming chemical compositions
WO2000032308A2 (fr) * 1998-12-04 2000-06-08 Symyx Technologies, Inc. Reacteur a alimentation continue en parallele

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
AKPORIAYE ET AL.: "Combinatorial approach to the hydrothermal synthesis of zeolites", ANGEW. CHEM. INT. ED., vol. 37, no. 5, March 1998 (1998-03-01), pages 609 - 611, XP000982283 *
KLEIN ET AL.: "Combinatorial material libraries on the microgram scale with an example of hydrothermal synthesis", ANGEW. CHEM. INT. ED., vol. 37, no. 24, December 1998 (1998-12-01), pages 3369 - 3372, XP000982281 *
PITTMAN ET AL.: "Sequential multistep reactions catalyzed by polymer-anchored homogeneous catalysts", J. AM. CHEM. SOC., vol. 97, no. 7, April 1975 (1975-04-01), pages 1749 - 1754, XP002948880 *

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Publication number Publication date
WO2002007870A2 (fr) 2002-01-31
AU2001278915A1 (en) 2002-02-05
EP1315562A2 (fr) 2003-06-04

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