WO2000029704A1 - Method of forming evacuated glass panels - Google Patents
Method of forming evacuated glass panels Download PDFInfo
- Publication number
- WO2000029704A1 WO2000029704A1 PCT/AU1999/000965 AU9900965W WO0029704A1 WO 2000029704 A1 WO2000029704 A1 WO 2000029704A1 AU 9900965 W AU9900965 W AU 9900965W WO 0029704 A1 WO0029704 A1 WO 0029704A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- sheet
- pump
- out tube
- cavity
- edge portion
- Prior art date
Links
Classifications
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/6612—Evacuated glazing units
-
- E—FIXED CONSTRUCTIONS
- E06—DOORS, WINDOWS, SHUTTERS, OR ROLLER BLINDS IN GENERAL; LADDERS
- E06B—FIXED OR MOVABLE CLOSURES FOR OPENINGS IN BUILDINGS, VEHICLES, FENCES OR LIKE ENCLOSURES IN GENERAL, e.g. DOORS, WINDOWS, BLINDS, GATES
- E06B3/00—Window sashes, door leaves, or like elements for closing wall or like openings; Layout of fixed or moving closures, e.g. windows in wall or like openings; Features of rigidly-mounted outer frames relating to the mounting of wing frames
- E06B3/66—Units comprising two or more parallel glass or like panes permanently secured together
- E06B3/677—Evacuating or filling the gap between the panes ; Equilibration of inside and outside pressure; Preventing condensation in the gap between the panes; Cleaning the gap between the panes
- E06B3/6775—Evacuating or filling the gap during assembly
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
- Y02A30/249—Glazing, e.g. vacuum glazing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B80/00—Architectural or constructional elements improving the thermal performance of buildings
- Y02B80/22—Glazing, e.g. vaccum glazing
Definitions
- This invention relates to a method of forming an evacuated glass panel having a chamber that is defined (ie, enclosed) by a glass wall that includes a port through which evacuation is effected.
- the invention has been developed in the context of evacuated door and/or window glazing ("vacuum glazing") and the invention is herein after described in that context. However, it will be understood that the invention does have broader application, for example in forming evacuated solar collector panels and panel-form display devices.
- two plane spaced-apart sheets of glass are positioned in face-to-face confronting relationship and are hermetically sealed around their edges with a low melting point glass that commonly is referred to a solder glass.
- the space (ie, chamber) between the sheets is evacuated and the face-to-face separation of the sheets is maintained by a network of small support pillars.
- the glazing may comprise glass sheets that have a surface area in the order of 0.02 to 4.00 square metres, sheet thicknesses in the order of 2.0 to 5.0 millimetres and a face-to- face spacing in the order of 0.10 to 0.20 millimetres.
- the evacuation of glazing presents special problems (relative to the evacuation of many other glass objects), in that the region at which evacuation is effected should not be obtrusive in the final product and in that the evacuating procedure must be appropriate to panels having large surface areas or linear dimensions.
- the evacuating procedure involves heating the glazing to a high temperature in a so-called bake-out oven (whilst the chamber to be evacuated is connected to an evacuating system) in order to remove gases from surface regions of the sheets and the pillars.
- a small pump- out tube is connected (ie, sealed) to the external surface of one of the glass sheets in communication with an aperture that extends through the glass sheet.
- the connection between the tube and the glass sheet is made using solder glass, normally at the same time that the solder glass edge-seal is made between the sheets.
- the solder glass sealing is normally effected at a temperature around 450°C, that is at a temperature that is high enough to melt the solder glass and make a leak-free joint but below a temperature at which significant deformation might occur in the glass sheets.
- a metal evacuating head is positioned over the pump-out tube and is connected to a remote vacuum pump.
- the evacuating head includes a central cavity that is dimensioned to receive the pump-out tube and to which the vacuum pump is connected.
- the glazing structure and the evacuating head are loaded into the bake- out oven where evacuation is effected whilst the complete structure is subjected to an out-gassing temperature. Thereafter, the outer end of the pump-out tube is closed by heating the tube to its melting temperature.
- the present invention is directed to a method of forming an evacuated glass panel and which facilitates the location of a pump-out tube close to an edge of the finished panel.
- the invention provides a method of forming an evacuated glass panel and which comprises the steps of:
- the evacuating head may comprise one that has a first cavity that is arranged in use to communicate with the pump-out tube, and at least one further cavity that surrounds the first cavity and which is arranged in use to contact the wall portion of the first glass sheet that surrounds the pump-out tube.
- the chamber will be evacuated by way of the first cavity whilst a vacuum is maintained in the further cavity or, if more than one, in each of the further cavities.
- the evacuating head preferably comprises one having a first cavity that communicates with the pump-out tube and a second surrounding cavity that contains a polymer O-ring that contacts the wall portion of the first glass sheet that surrounds the pump-out tube.
- Figure 1 shows sequential steps A to E in a preferred method of fabricating glazing
- FIG. 2 shows sequential steps A to E in an alternative method of fabricating glazing
- Figure 3 shows a schematic representation of the glazing located within a bake-out oven and connected to one or more external vacuum pumps by way of an evacuating head.
- an evacuating head 10 is mounted to glazing 11 that is to be evacuated.
- the glazing comprises two plane glass sheets 12 and 13 that are maintained in spaced-apart face-to-face confronting relationship.
- the glass sheets would normally be composed of soda-lime glass and be interconnected along their edges by a bead 14 of edge-sealing solder glass.
- a chamber 15 is defined by the two glass sheets 12 and 13 and the sheets are maintained in spaced-apart relationship by a network or array of support pillars 16.
- the chamber 15 is evacuated to a level below 10 "3 Torr, this providing for gaseous heat conduction between the sheets that is negligible relative to other heat flow mechanisms.
- the glass sheet 12 is formed with an aperture 17, and a glass pump-out tube 18 is positioned to locate within and project outwardly from the aperture 17.
- the pump-out tube is sealed to the glass sheet by a bead 19 of solder glass.
- a metal filament 20 is shown to surround the pump-out tube 18 and this may be employed, following evacuation of the cavity 15, to melt and close the pump-out tube, although other techniques may be employed for this purpose.
- the evacuating head 10 as shown in Figure 1 comprises a metal body 21 which incorporates a central, first cavity 22.
- the first cavity is shaped and dimensioned to receive the pump-out tube 18 and to provide for unrestricted movement of gas during evacuation and out-gassing of the chamber 15.
- the first cavity 22 is connected by way of a port 23 and a conduit 24 to a vacuum pump 25 that is located outside a baking chamber 32, as shown schematically in Figure 3.
- a second, annular cavity 26 also is provided within the body 21 of the evacuating head.
- the second cavity 26 is positioned to surround the first cavity 22 and it contains a polymer O-ring 26A which contacts and, in use, seals against the surface of the glass sheet 12 that surrounds the pump-out tube 18.
- a first annular land is located between the first and second cavities 22 and 26, and a second annular land 28 surrounds the annular second cavity 26.
- Each of the two lands 27 and 28 makes contact with the surface of the glass sheet over a small area.
- the evacuating head 10 as shown in Figure 2 is in some respects similar to that shown in Figure 1 and like reference numerals are employed to identify like parts.
- the evacuating head 10 comprises a metal body 21 which incorporates a central, first cavity 22.
- the first cavity 22 is shaped and dimensioned to receive the pump-out tube 18 and to provide for unrestricted movement of gas during evacuation and out-gassing of the chamber 15.
- the first cavity 22 is connected by way of a port 23 and a conduit 24 to a vacuum pump 25 that is located outside of the baking chamber 32.
- a second, annular cavity 26 also is provided within the body 21 of the evacuating head.
- the second cavity 26 is positioned to surround the first cavity 22 and is arranged in use to be closed by the surface of the glass sheet 12 that surrounds the pump-out tube 18.
- a first annular land 27 is located between the first and second cavities 22 and 26, and a second annular land 28 surrounds the annular second cavity 26.
- Each of the two lands 27 and 28 makes contact with the surface of the glass sheet 12 over a small area and so limits gas flow into the second cavity 26 and between the two cavities 22-26.
- the second cavity 26 is connected by way of a port 29 and a conduit 30 to a further vacuum pump 31, as indicated in Figure 3.
- the evacuating heads 10 as shown in Figures 1 and 2 will typically have an outside diameter of 50 mm to 100 mm and the first, central cavity 22 will typically have a diameter in the order of 10 mm to 20 mm.
- the lands 27 and 28 will each have a radial width in the order of 1 mm but may be in the range 0.10 mm to 10 mm.
- the further fabrication steps may then be performed by way of a single heating procedure or two heating procedures depending upon the levels of heat to be employed and/or on the type of evacuating head to be used.
- the glazing unit 11 is heated to around 450°C within the oven 32 and, during this process, the solder glass melts to form seals around the edges of the glazing and around the pump out tube.
- the glazing is then cooled to a temperature (around 380°C) at which the solder glass solidifies, and evacuation of the chamber 15 between the two glass sheets 12 and 13 is then effected by connecting the vacuum system 25 to the central cavity 22 of the evacuating head 10. Evacuation of the chamber is maintained as the glazing and evacuating head are cooled.
- the specific temperature/time schedule that is used during this cooling period will depend upon the time necessary to achieve adequate out-gassing of the internal surfaces of the glazing.
- the pump-out tube 18 is melted and fused closed, using the filament element 20. Thereafter, the margin of sheet 12 is trimmed as described above with reference to Figures IE and 2E.
Landscapes
- Engineering & Computer Science (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Joining Of Glass To Other Materials (AREA)
Abstract
Description
Claims
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2000582671A JP2002530259A (en) | 1998-11-18 | 1999-11-04 | Method of forming vacuum glass panel |
EP99957703A EP1131529A4 (en) | 1998-11-18 | 1999-11-04 | Method of forming evacuated glass panels |
CA002351818A CA2351818A1 (en) | 1998-11-18 | 1999-11-04 | Method of forming evacuated glass panels |
AU15325/00A AU1532500A (en) | 1998-11-18 | 1999-11-04 | Method of forming evacuated glass panels |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AUPP7192 | 1998-11-18 | ||
AUPP7192A AUPP719298A0 (en) | 1998-11-18 | 1998-11-18 | Method of forming evacuated glass panels |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2000029704A1 true WO2000029704A1 (en) | 2000-05-25 |
Family
ID=3811401
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/AU1999/000965 WO2000029704A1 (en) | 1998-11-18 | 1999-11-04 | Method of forming evacuated glass panels |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP1131529A4 (en) |
JP (1) | JP2002530259A (en) |
AU (1) | AUPP719298A0 (en) |
CA (1) | CA2351818A1 (en) |
WO (1) | WO2000029704A1 (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003000613A1 (en) * | 2001-06-22 | 2003-01-03 | Nippon Sheet Glass Co., Ltd. | Method of manufacturing glass panel |
WO2003095388A1 (en) * | 2002-05-13 | 2003-11-20 | Nippon Sheet Glass Co., Ltd. | Depressurizing container for glass panel |
EP1529921A2 (en) | 2003-10-27 | 2005-05-11 | Werner Wüthrich | Heat transmission reducing closure element |
US10697231B2 (en) | 2015-08-20 | 2020-06-30 | Vkr Holding A/S | Small diameter evacuation head for VIG unit manufacture |
US10704320B2 (en) | 2015-08-20 | 2020-07-07 | Vkr Holding A/S | Method for producing a VIG unit having an improved temperature profile |
US11149487B2 (en) | 2017-06-29 | 2021-10-19 | Vkr Holding A/S | Gasket and sealing system for a VIG unit production |
EP3906351B1 (en) * | 2019-01-02 | 2024-07-10 | VKR Holding A/S | Sealant in a vacuum insulated glazing unit |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004220545A (en) * | 2003-03-03 | 2004-08-05 | Toshiaki Eto | Crime prevention system for multilayer window material and multilayer window material |
IT1391434B1 (en) * | 2008-09-26 | 2011-12-23 | Tvp Solar Sa | SOLAR THERMAL VACUUM PANEL WITH RADIATIVE SCREEN |
CN102079630A (en) * | 2010-11-25 | 2011-06-01 | 沈阳工业大学 | Vacuum insulating layer and manufacturing method thereof |
US8794033B2 (en) * | 2011-12-15 | 2014-08-05 | Guardian Industries Corp. | Apparatuses for vacuum insulating glass (VIG) unit tip-off, and/or associated methods |
CN108947279B (en) * | 2017-05-25 | 2021-06-04 | 张跃 | Vacuum glass |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4281488A (en) * | 1976-01-20 | 1981-08-04 | Para-Press S.A. | Multipane window with adjustable light admission |
DE3045060A1 (en) * | 1980-11-29 | 1982-07-01 | Bernd 6093 Flörsheim Delvo | Window double glazing pane sealing strip - is fitted on original pane by producing suction with subsequent sealant application around edges |
EP0691200A2 (en) * | 1994-07-08 | 1996-01-10 | Sintokogio, Ltd. | Apparatus for setting a gap for a glass panel |
US5643644A (en) * | 1993-09-27 | 1997-07-01 | Saint Gobain Vitrage | Insulating glazing |
WO1998004802A1 (en) * | 1996-07-31 | 1998-02-05 | Saint-Gobain Vitrage | Method for producing a vacuum between two glass sheets and insulating glazing |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL8401434A (en) * | 1984-05-04 | 1985-12-02 | Condensafe Bv | DRILLING DEVICE FOR DRILLING HOLES IN GLASS PLATES. |
ATE136093T1 (en) * | 1989-08-23 | 1996-04-15 | Univ Sydney | METHOD FOR PRODUCING A HEAT-DAMPED GLASS PANEL AND HEAT-DAMPED GLASS PANEL THEREFORE. |
-
1998
- 1998-11-18 AU AUPP7192A patent/AUPP719298A0/en not_active Abandoned
-
1999
- 1999-11-04 EP EP99957703A patent/EP1131529A4/en not_active Withdrawn
- 1999-11-04 JP JP2000582671A patent/JP2002530259A/en active Pending
- 1999-11-04 WO PCT/AU1999/000965 patent/WO2000029704A1/en not_active Application Discontinuation
- 1999-11-04 CA CA002351818A patent/CA2351818A1/en not_active Abandoned
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4281488A (en) * | 1976-01-20 | 1981-08-04 | Para-Press S.A. | Multipane window with adjustable light admission |
DE3045060A1 (en) * | 1980-11-29 | 1982-07-01 | Bernd 6093 Flörsheim Delvo | Window double glazing pane sealing strip - is fitted on original pane by producing suction with subsequent sealant application around edges |
US5643644A (en) * | 1993-09-27 | 1997-07-01 | Saint Gobain Vitrage | Insulating glazing |
EP0691200A2 (en) * | 1994-07-08 | 1996-01-10 | Sintokogio, Ltd. | Apparatus for setting a gap for a glass panel |
WO1998004802A1 (en) * | 1996-07-31 | 1998-02-05 | Saint-Gobain Vitrage | Method for producing a vacuum between two glass sheets and insulating glazing |
Non-Patent Citations (1)
Title |
---|
See also references of EP1131529A4 * |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003000613A1 (en) * | 2001-06-22 | 2003-01-03 | Nippon Sheet Glass Co., Ltd. | Method of manufacturing glass panel |
AU2002350220B2 (en) * | 2001-06-22 | 2007-02-15 | Nippon Sheet Glass Co., Ltd | Method of manufacturing glass panel |
WO2003095388A1 (en) * | 2002-05-13 | 2003-11-20 | Nippon Sheet Glass Co., Ltd. | Depressurizing container for glass panel |
EP1529921A2 (en) | 2003-10-27 | 2005-05-11 | Werner Wüthrich | Heat transmission reducing closure element |
US10697231B2 (en) | 2015-08-20 | 2020-06-30 | Vkr Holding A/S | Small diameter evacuation head for VIG unit manufacture |
US10704320B2 (en) | 2015-08-20 | 2020-07-07 | Vkr Holding A/S | Method for producing a VIG unit having an improved temperature profile |
US11149487B2 (en) | 2017-06-29 | 2021-10-19 | Vkr Holding A/S | Gasket and sealing system for a VIG unit production |
EP3906351B1 (en) * | 2019-01-02 | 2024-07-10 | VKR Holding A/S | Sealant in a vacuum insulated glazing unit |
Also Published As
Publication number | Publication date |
---|---|
JP2002530259A (en) | 2002-09-17 |
EP1131529A1 (en) | 2001-09-12 |
AUPP719298A0 (en) | 1998-12-17 |
CA2351818A1 (en) | 2000-05-25 |
EP1131529A4 (en) | 2003-06-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CA2351221C (en) | Method of and apparatus for evacuating a glass chamber | |
EP0953719B1 (en) | Methods of construction of evacuated glazing | |
US6054195A (en) | Method of construction of evacuated glazing | |
EP1171397B1 (en) | Method of sealing glass | |
US5009218A (en) | Heat-insulating building and/or light element | |
EP1185758B1 (en) | Glass panel | |
US9695628B2 (en) | Vacuum insulated glass (VIG) window unit including pump-out tube protection ring and/or cap and methods for making same | |
KR101533263B1 (en) | Vacuum solar thermal panel with a vacuum tight glass-metal sealing | |
WO1991002878A1 (en) | A thermally insulating glass panel and method of construction | |
WO2000029704A1 (en) | Method of forming evacuated glass panels | |
USH975H (en) | Thermal insulated glazing unit | |
US20190177219A1 (en) | Method and apparatus for vacuum insulated glazings | |
WO2001075260A1 (en) | Vacuum ig unit with seal for pump-out aperture | |
US6212852B1 (en) | Evacuated glazing containing a thermally insulating vacuum | |
KR20130022535A (en) | Vacuum glass panel and method of manufacturing thereof | |
WO1999045225A1 (en) | A window comprising an insulating pane and a frame, a method of producing such a window, and a valve for use in carrying out the method | |
US20080063839A1 (en) | Architectural glass block with a formed slot and method of making same | |
US11465938B2 (en) | Manufacturing method of glass panel unit, manufacturing method of glass window, and glass panel unit | |
JP6295005B1 (en) | Mass production type vacuum low-pressure double-layer glass and method for producing the same | |
AU641423B2 (en) | A thermally insulating glass panel and method of construction | |
AU759410B2 (en) | Glass panel | |
JP2019535623A (en) | Vacuum insulating glass having polymer spacer matrix and method for producing the same | |
Selkowitz et al. | Thermal insulated glazing unit | |
KR19980014107A (en) | Vacuum window manufacturing method using low melting point glass or torser |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
ENP | Entry into the national phase |
Ref document number: 2000 15325 Country of ref document: AU Kind code of ref document: A |
|
AK | Designated states |
Kind code of ref document: A1 Designated state(s): AE AL AM AT AU AZ BA BB BG BR BY CA CH CN CR CU CZ DE DK DM EE ES FI GB GD GE GH GM HR HU ID IL IN IS JP KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX NO NZ PL PT RO RU SD SE SG SI SK SL TJ TM TR TT TZ UA UG US UZ VN YU ZA ZW |
|
AL | Designated countries for regional patents |
Kind code of ref document: A1 Designated state(s): GH GM KE LS MW SD SL SZ TZ UG ZW AM AZ BY KG KZ MD RU TJ TM AT BE CH CY DE DK ES FI FR GB GR IE IT LU MC NL PT SE BF BJ CF CG CI CM GA GN GW ML MR NE SN TD TG |
|
121 | Ep: the epo has been informed by wipo that ep was designated in this application | ||
DFPE | Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101) | ||
ENP | Entry into the national phase |
Ref document number: 2000 582671 Country of ref document: JP Kind code of ref document: A |
|
ENP | Entry into the national phase |
Ref document number: 2351818 Country of ref document: CA Kind code of ref document: A Ref document number: 2351818 |
|
WWE | Wipo information: entry into national phase |
Ref document number: 1999957703 Country of ref document: EP |
|
WWP | Wipo information: published in national office |
Ref document number: 1999957703 Country of ref document: EP |
|
REG | Reference to national code |
Ref country code: DE Ref legal event code: 8642 |
|
WWE | Wipo information: entry into national phase |
Ref document number: 09856120 Country of ref document: US |
|
WWW | Wipo information: withdrawn in national office |
Ref document number: 1999957703 Country of ref document: EP |