WO1998035933A1 - New polydynamic chemical composition of multiple applications and method of preparation thereof - Google Patents

New polydynamic chemical composition of multiple applications and method of preparation thereof Download PDF

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Publication number
WO1998035933A1
WO1998035933A1 PCT/GR1998/000004 GR9800004W WO9835933A1 WO 1998035933 A1 WO1998035933 A1 WO 1998035933A1 GR 9800004 W GR9800004 W GR 9800004W WO 9835933 A1 WO9835933 A1 WO 9835933A1
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WO
WIPO (PCT)
Prior art keywords
chemical composition
weight
content
composition according
mixture
Prior art date
Application number
PCT/GR1998/000004
Other languages
French (fr)
Inventor
Timoleon Venetsianos
Original Assignee
Timoleon Venetsianos
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Timoleon Venetsianos filed Critical Timoleon Venetsianos
Priority to AU57748/98A priority Critical patent/AU5774898A/en
Priority to CA002278276A priority patent/CA2278276A1/en
Priority to EP98901419A priority patent/EP0954518A1/en
Publication of WO1998035933A1 publication Critical patent/WO1998035933A1/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/12—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/62—Quaternary ammonium compounds
    • C07C211/63—Quaternary ammonium compounds having quaternised nitrogen atoms bound to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00—Materials not provided for elsewhere
    • C09K3/16—Anti-static materials
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/655—Compounds containing ammonium groups
    • D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups

Definitions

  • the present invention refers to a novel polydynamic chemical composition and to the method of preparation thereof, composed by benzyl - dimethyl - dodecyl (lauryl) ammonium chloride and benzyl - dimethyl tetradecyl (myristyl) ammonium chloride and other chemical substances or compounds, which composition is used in a wide field of applications, such as disinfectant and cleansing means of general use, as a means of water purification, as an augmentative of plant growth, as a synergistic material in fubric dying methods and procedures, as a synergistic material in insecticidal means , as a synergistic material in the biological purification of water and of the atmospheric air ,as an antifrictional material, as an antistatic means , as an infiltration means because of its penetration ability as well as in various other applications.
  • the proposed composition and its method of use which consists of compounds such as quaternary salts , as above, converts the conventional production methods into methods of high technology , because of the composition, which, thanks to its mechanical, chemical and electrostatic properties has excellent results to all the fields of its application in an easy, complete and not all expensive way.
  • the new composition of the present invention presents the following advantages with regard to the prior art compounds of similar applications :
  • the content of the active substance in the new polydynamic composition amounts to 5% by weight of the salts in the water of 91% ontent by weight and 4% by weight of the materials, which include alcohols of 2% by weight, aromatizators and complex compounds of non-ionic character of a total content 2% by weight.
  • Quaternary salts are received , i.e benzyl - dimethyl - dodecyl (lauryl) ammonium chloride and benzyl - dimethyl (myristyl) ammonium chloride in a quantity of 5% by weight and they are heated in a high and stable temperature, i.e. 70 oC for 6 hours in a water- bath. Following this, the mixture is put into dionized water of 91% content by weight of the total mixture which is enriched with metals, substantially with iron, in stable temperature of 55 oC . A light stirring follows for 1 hour in stable temperature , while afterwards a mixing with double recycling by swirl is caused tothe mixture , i.e.
  • the alcohols are poured into the working tub in a content of 2% by weight .which have a stable content temperature of 40 oC.
  • the temperature is gradually reduced until it is stabilized at 40°C, so that the temperature of the mixture and the alcohols is equated.
  • a stirring occurs, at the same time increasing the temperature until it reaches a temperature of 55°C and then, the essential oils (aromatizators) and the complex substances (oil, water, alcohol) are put which have a total content of 2% by weight.
  • the stirring of the mixture is continued until it obtains an homogenous form while the pH is adjusted to 7 by adding reagents (acids or caustic soda) in the suitable quantity.
  • reagents ascids or caustic soda
  • the mixture is allowed to cool down by transusing it into a polyesteric or glass tank. Quality control of the final product follows.
  • the new composition that is produced according to the present invention has various applications and usages in a wide field of the production of disinfectant and cleansing products a swell as in the procedure of cleansing water of sewage, in agriculture, in the filed of sanitation of public places, the disinfection of medical machines, the industry of fabric dying and several others, which all fall under the scope object and claims of the present invention.
  • the mixture is allowed to cool down by transfusing it into a polyesteric or glass tank and a quality control of the final product follows.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Textile Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Materials Engineering (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Method of a chemical composition, which consists of quaternary ammonium salts benzyl - dimethyl - dodecyl (lauryl) ammonium chloride and benzyl - dimethyl tetradecyl (myristyl) ammonium chloride in a content of 5 % by weight totally, as well as on alcohols in a content of 2 % by weight totally, aromatizators in a content of 2 % by weight totally and deionized water in a content of 91 % by weight, which is used in a wide field of applications, such as disinfectant and cleansing means and as a synergistic material in industrial processings and in the agriculture.

Description

NEW POLYDYNAMIC CHEMICAL COMPOSITION OF MULTIPLE APPLICATIONS AND METHOD OF PREPARATION THEREOF
The present invention refers to a novel polydynamic chemical composition and to the method of preparation thereof, composed by benzyl - dimethyl - dodecyl (lauryl) ammonium chloride and benzyl - dimethyl tetradecyl (myristyl) ammonium chloride and other chemical substances or compounds, which composition is used in a wide field of applications, such as disinfectant and cleansing means of general use, as a means of water purification, as an augmentative of plant growth, as a synergistic material in fubric dying methods and procedures, as a synergistic material in insecticidal means , as a synergistic material in the biological purification of water and of the atmospheric air ,as an antifrictional material, as an antistatic means , as an infiltration means because of its penetration ability as well as in various other applications.
As it is known until today, similar chemical compounds are commercially available for various use of cleansing, disinfection, plant growth e.t.c, which, on the other hand present several problems and disadvantages, such as, that, either a large amount of active substance is necessary, resulting in certain side effects and harmful influences that finally make the product ineffective , or a long duration is needed for it to act or due to its incompatibility with other compositions the product and its method of use become expensive and non-profitable.
The proposed composition and its method of use, which consists of compounds such as quaternary salts , as above, converts the conventional production methods into methods of high technology , because of the composition, which, thanks to its mechanical, chemical and electrostatic properties has excellent results to all the fields of its application in an easy, complete and not all expensive way. The new composition of the present invention presents the following advantages with regard to the prior art compounds of similar applications :
- A wide range of applications both in the field of industrial production and in the level of its use as a final product in a pluralityof fields.
- Excellent and quick efficiency. - Relatively low content of the active substance, a fact that reduces substantially the cost of production and eliminates the disadvantages and the side effects that are usually du to the high content of the active substance. - A composition of cationic character , that, on the other hand, presents tolerance (is compatible) to non-ionic or anionic compositions , resulting in the improved efficiency and the elimination , substancially, of the incompatibility with other materials and compounds of anionic character, which it comes in contact with. - Increased bonding (linking) ability of the used matrials and improved activation of thematerial to be elaborated.
- Improved and suitable surfactant possibility of the used materials.
- Low toxicity with excellent possible efficiency.
- Increased strength resulting to the increase ofthe duration of the active time of the product.
The content of the active substance in the new polydynamic composition amounts to 5% by weight of the salts in the water of 91% ontent by weight and 4% by weight of the materials, which include alcohols of 2% by weight, aromatizators and complex compounds of non-ionic character of a total content 2% by weight.
Method of preparation : Quaternary salts are received , i.e benzyl - dimethyl - dodecyl (lauryl) ammonium chloride and benzyl - dimethyl (myristyl) ammonium chloride in a quantity of 5% by weight and they are heated in a high and stable temperature, i.e. 70 oC for 6 hours in a water- bath. Following this, the mixture is put into dionized water of 91% content by weight of the total mixture which is enriched with metals, substantially with iron, in stable temperature of 55 oC . A light stirring follows for 1 hour in stable temperature , while afterwards a mixing with double recycling by swirl is caused tothe mixture , i.e. by pumping it and reflowing it into the working tub. After the one- hour stirring, the alcohols are poured into the working tub in a content of 2% by weight .which have a stable content temperature of 40 oC. During the flowing of the alcohols into the working tub , the temperature is gradually reduced until it is stabilized at 40°C, so that the temperature of the mixture and the alcohols is equated. Afterwards, a stirring occurs, at the same time increasing the temperature until it reaches a temperature of 55°C and then, the essential oils (aromatizators) and the complex substances (oil, water, alcohol) are put which have a total content of 2% by weight. The stirring of the mixture is continued until it obtains an homogenous form while the pH is adjusted to 7 by adding reagents (acids or caustic soda) in the suitable quantity. The mixture is allowed to cool down by transusing it into a polyesteric or glass tank. Quality control of the final product follows.
The new composition that is produced according to the present invention, has various applications and usages in a wide field of the production of disinfectant and cleansing products a swell as in the procedure of cleansing water of sewage, in agriculture, in the filed of sanitation of public places, the disinfection of medical machines, the industry of fabric dying and several others, which all fall under the scope object and claims of the present invention.
1. The mixture is allowed to cool down by transfusing it into a polyesteric or glass tank and a quality control of the final product follows.
2. A chemical composition which is produced with the method of the claim (1), which includes
- benzyl-dimethyl-dodecyl (lauryl) ammonium chloride and benzyl- dimethyl tetradecyl (myristyl) ammonium chloride in a content of 5% by weight.
- water in a content of 91% by weight on the total of the mixture, enriched with metals and especially with iron
- alcohols in a content of 2% by weight
- aromatizators and compound materials in a content of 2% per weight. 3. A chemical composition according to the claims (1) and (2), which is used as a synergistic material in fabric dying procedures.
4. A chemical composition according to the claims (1) and (2), which is used as a synergistic material in the biological cleansing of water and sewage.
5. A chemical composition according to the claims (1) and (2), which is used as an augmentation means for the growth of plants and agricultures.
6. A chemical substance, according to the claims (1) and (2), which is sued as a synergistic material in the cleansing of the atmospheric air.
7. A chemical substance according to the claims (1) and (2), which is used as an antifrictional material. 8. A chemical substance according to the claims (1) and (2), which is used as an antistatic means.
9. A chemical substance according to the claims (1) and (2), which is used as a means of infiltration 10. A chemical substance according to the claims (1) and (2), which is used as a disinfectant and cleansing means as well as in insecticidal formulations.

Claims

1. Method of preparation of a chemical composition, which consists of quaternary ammonium salts benzyl-dimethyl (lauryl) ammonium chloride and benzyl-dimethyl tetradecyl (myristyl) ammonium chloride in a content of 5% by weight in total and which is characterized by the following stages:
- quaternary salts are received, i.e. benzyl-dimethyl-dodecyl (lauryl) ammonium chloride and benzyl-dimethyl (ministryl) ammonium chloride in a quantity of 5% by weight in total and they are heated in a high and stable temperature, i.e. 70 ┬░C for 6 hours in a water-bath.
- they are put into deionized water of 91% content by weight of the total mixture, which is enriched with metals, substantially with iron, in stable temperature of 55┬░C.
- a light stirring follows for 1 hour in stable temperature, while afterwards a mixing with double recycling by swirl is caused to the mixture, i.e. by pumping it and reflowing it into the working tub,
- the alcohols are thrown into the working tub in a content of 2% per weight, which have a stable temperature of 40┬░C.
- while the temperature of the mixture is gradually reduced until it is stabilized at 40┬░C, so that the temperature of the mixture and the alcohols is equated,
- a stirring occurs with an increase of the temperature until it reaches at 55┬░C and then, the essential oils (aromatizators) and the complex substances (oil, water, alcohol) are put which have a total content of 2% by weight.
- the stirring of the mixture is continued until it obtains an homogeneous form while the pH is adjusted to 7 by adding reagents (acids or caustic soda) in the suitable quantity,
- the mixture is allowed to cool down by transfusing it into a polyesteric or glass tank and a quality control of the final product follows.
2. A chemical composition which is produced with the method of the claim (1) which includes
- benzyl-dimetyl-doecyl (lauryl) ammonium chloride and benzyl-dimethyl tetradecyl (ministyl) ammonium chloride in a content of 5% by weight - water in a content of 91% by weight on the total of the mixture, enriched with metals and especially with iron
- alcohols in a content of 2% by weight
- aromatizators and compound materials in a content of 2% by weight.
3. A chemical composition according to the claims (1) and (2), which is used as a synergistic material in fabric dying procedures
4. A chemical composition according to the claims (1) and (2), which is used as a synergistic material in the biological cleansing of water and sewage.
5. A chemical composition according to the claims (1) and (2), which is used as an augmentation means for the growth of plants and agricultures.
6. A chemical composition according to the claims (1) and (2), which is used as a synergistic material in the cleansing of the atmospheric air.
7. A chemical composition according to the claims (1) and (2), which is used as an antifrictional material.
8. A chemical composition according to the claims (1) and (2), which is used as an antistatic means.
9. A chemical composition according to the claims (1) and (2), which is used as means of infiltration.
10. A chemical composition according to the claims (1) and (2), which is used as a disinfectant and cleansing means as well as in insecticidal formulations .
PCT/GR1998/000004 1997-02-14 1998-02-10 New polydynamic chemical composition of multiple applications and method of preparation thereof WO1998035933A1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
AU57748/98A AU5774898A (en) 1997-02-14 1998-02-10 New polydynamic chemical composition of multiple applications and method of preparation thereof
CA002278276A CA2278276A1 (en) 1997-02-14 1998-02-10 New polydynamic chemical composition of multiple applications and method of preparation thereof
EP98901419A EP0954518A1 (en) 1997-02-14 1998-02-10 New polydynamic chemical composition of multiple applications and method of preparation thereof

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GR970100054 1997-02-14
GR97100054 1997-02-14

Publications (1)

Publication Number Publication Date
WO1998035933A1 true WO1998035933A1 (en) 1998-08-20

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PCT/GR1998/000004 WO1998035933A1 (en) 1997-02-14 1998-02-10 New polydynamic chemical composition of multiple applications and method of preparation thereof

Country Status (5)

Country Link
EP (1) EP0954518A1 (en)
AU (1) AU5774898A (en)
CA (2) CA2207267A1 (en)
GR (1) GR1002937B (en)
WO (1) WO1998035933A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002062142A1 (en) * 2001-01-04 2002-08-15 Byotrol Llc Anti-microbial composition
US8003593B2 (en) 2007-09-17 2011-08-23 Byotrol Plc Formulations comprising an anti-microbial composition
US8178484B2 (en) 2007-07-17 2012-05-15 Byotrol Plc Anti-microbial composition comprising a siloxane and anti-microbial compound mixture

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1068378A (en) * 1963-10-29 1967-05-10 Michigan Tool Co Aqueous disinfectant composition
DE3534102A1 (en) * 1984-10-05 1986-04-10 Sandoz-Patent-GmbH, 7850 Lörrach Process for dyeing leather
US4952398A (en) * 1988-03-17 1990-08-28 Jean Tapin Biocidal composition with copper algicide
US5215676A (en) * 1992-09-14 1993-06-01 Stone John A Rust and stain removal composition
WO1993021766A1 (en) * 1992-04-27 1993-11-11 Ethyl Corporation Quaternary ammonium composition and process

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1068378A (en) * 1963-10-29 1967-05-10 Michigan Tool Co Aqueous disinfectant composition
DE3534102A1 (en) * 1984-10-05 1986-04-10 Sandoz-Patent-GmbH, 7850 Lörrach Process for dyeing leather
US4952398A (en) * 1988-03-17 1990-08-28 Jean Tapin Biocidal composition with copper algicide
WO1993021766A1 (en) * 1992-04-27 1993-11-11 Ethyl Corporation Quaternary ammonium composition and process
US5215676A (en) * 1992-09-14 1993-06-01 Stone John A Rust and stain removal composition

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
"The Merck Index", 1996, MERCK RESEARCH LABORATORIES, WHITEHOUSE STATION, NJ (USA), XP002040849 *
"The Sigma Catatogue. Part B. Alphabetical List of Compounds", January 1997, SIGMA CHEMICAL COMPANY, XP002040850 *
DATABASE WPI Section Ch Derwent World Patents Index; Class C01, AN 72-64239T, XP002040851 *
RICHARDS, R. M. E. ET AL: "Differences in antibacterial activity of benzalkonium chloride", J. PHARM. SCI. (1978), 67(3), 380-3 CODEN: JPMSAE;ISSN: 0022-3549, 1978, XP002071748 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2002062142A1 (en) * 2001-01-04 2002-08-15 Byotrol Llc Anti-microbial composition
AU2002216292B2 (en) * 2001-01-04 2007-08-30 Byotrol Plc Anti-microbial composition
US7674473B2 (en) 2001-01-04 2010-03-09 Byotrol Plc Anti-microbial composition
US8178484B2 (en) 2007-07-17 2012-05-15 Byotrol Plc Anti-microbial composition comprising a siloxane and anti-microbial compound mixture
US8575085B2 (en) 2007-07-17 2013-11-05 Byotrol Plc Anti-microbial composition comprising a quaternary ammonium biocide and organopolysiloxane mixture
US8003593B2 (en) 2007-09-17 2011-08-23 Byotrol Plc Formulations comprising an anti-microbial composition
US8598106B2 (en) 2007-09-17 2013-12-03 Byotrol Plc Anti-microbial composition exhibiting residual anti-microbial properties on a surface

Also Published As

Publication number Publication date
CA2207267A1 (en) 1998-08-14
GR1002937B (en) 1998-07-13
AU5774898A (en) 1998-09-08
CA2278276A1 (en) 1998-08-20
EP0954518A1 (en) 1999-11-10

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