WO1997038786A1 - Filter membranes with controlled product flow and systems using same - Google Patents

Filter membranes with controlled product flow and systems using same Download PDF

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Publication number
WO1997038786A1
WO1997038786A1 PCT/US1997/006418 US9706418W WO9738786A1 WO 1997038786 A1 WO1997038786 A1 WO 1997038786A1 US 9706418 W US9706418 W US 9706418W WO 9738786 A1 WO9738786 A1 WO 9738786A1
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WIPO (PCT)
Prior art keywords
filter
ofthe
filter vessel
vessel
membrane
Prior art date
Application number
PCT/US1997/006418
Other languages
French (fr)
Inventor
Robert L. Bradley
David R. Anderson
Original Assignee
United States Filter Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by United States Filter Corporation filed Critical United States Filter Corporation
Publication of WO1997038786A1 publication Critical patent/WO1997038786A1/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/145Ultrafiltration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025Reverse osmosis; Hyperfiltration
    • B01D61/026Reverse osmosis; Hyperfiltration comprising multiple reverse osmosis steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/10Accessories; Auxiliary operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/12Controlling or regulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/145Ultrafiltration
    • B01D61/146Ultrafiltration comprising multiple ultrafiltration steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/20Accessories; Auxiliary operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/22Controlling or regulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/16Rotary, reciprocated or vibrated modules

Definitions

  • the present invention relates generally to filter membranes with controlled product
  • Filter membranes are commonly used to purify water and other fluids.
  • Fluid flowing in a feed stream enters the filter membrane and is separated into a
  • filter membranes are often arranged in series
  • the waste stream from a first filter vessel serves as the feed stream into the next filter vessel.
  • This series arrangement of filter vessels is commonly referred to as staging.
  • the pressure of the waste stream leaving the filter vessel is less than the pressure of
  • the pressure of the waste stream is reduced to a pressure too low to serve as the
  • the filter vessel may be any number of filter vessels used in a filtration system.
  • the number of filter vessels used in a filtration system may be
  • unpurified fluid can pass through only a relatively small number of ultrafilter membranes
  • filter vessels do not typically contain more than about four ultrafilter
  • any filter membrane is not too low to serve as the feed stream for the next filter membrane.
  • the transmembrane pressure across each filter membrane is approximately the same such that
  • the product flow rate is approximately the same for each membrane such that overfluxing of
  • upstream membranes is substantially reduced.
  • staged filter vessels with a comparatively high number of filter membranes are arranged in
  • the present invention provides an improved filter
  • upstream membrane can be increased to a relatively high value without overfluxing and
  • the present invention provides a filter for purifying a
  • the filter comprises a filter membrane and a flow control device.
  • the filter membrane is a filter membrane and a flow control device.
  • the flow control device has an inlet, a product outlet and a waste outlet.
  • the flow control device is in fluid
  • the product outlet to control flow rate of fluid through the product outlet.
  • the present invention provides a filter vessel for
  • At least two filter membranes are arranged in series within the filter vessel.
  • the inlet ofthe first filter membrane is in fluid communication with the inlet ofthe filter
  • flow control device is in fluid communication with the product outlet ofthe filter vessel, first
  • the present invention provides a filter vessel
  • the present invention provides a filter vessel that
  • the present invention provides a method for filtering a fluid with a filtration system.
  • the method comprises the steps of: providing a first
  • filter vessel having a plurality of filter membranes arranged in series; introducing a feed
  • the present invention provides a filtration
  • first filter vessel is in fluid communication with the inlet ofthe second filter vessel.
  • filter vessel includes a plurality of filter membranes.
  • Fig. 1 is a schematic view of one embodiment of a filter according to the present
  • Fig. 2 is a schematic view of one embodiment of a filter vessel according to the
  • Fig. 3 is a schematic view of one embodiment of a filtration system according to the
  • Fig. 4 is a schematic view of one embodiment of a filtration system according to the related art.
  • the present invention relates to an improved filter 10 (Fig. 1) which is designed so
  • Filter 10 includes a filter membrane 12, an inlet 14, a feed path that
  • a portion of a feed fluid may pass through membrane 12 along the
  • waste path without being purified and exit through waste outlet 16.
  • the flow rate of purified fluid that exits filter 10 through product outlet 18 depends on
  • Flow control device 20 is designed to
  • transmembrane pressure can be controlled while the pressure of the feed fluid at inlet 14 is
  • the feed fluid is varied. For example, by varying the back pressure supplied by flow control
  • feed fluid at inlet 14 may be increased without increasing the product flow rate and without
  • a "flow control" device may be any device that can be placed in fluid communication with the product outlet of a filter membrane so that the device is capable of supplying a back
  • a flow control device is a
  • control devices supply a back pressure to the product outlet independent ofthe flow rate of
  • Static flow control devices include fixed orifice
  • An example of a fixed orifice device is a flat plate
  • d is the diameter ofthe orifice in a direction normal to the path ofthe product
  • a capillary device may be
  • coiled tube formed from a coiled tube.
  • the length and diameter of the coiled tube should be chosen such
  • a flow control device may be formed from a plurality of ball valves.
  • the ball valves should be selected manually to obtain the desired amount of purified fluid.
  • Dynamically responsive flow control devices supply a back pressure to the product
  • Dynamically responsive flow control devices may be variable orifice flow control devices.
  • Such devices may include a flat plate having an orifice disposed therein and a rubber grommet located within the fixed orifice.
  • grommet increases the back pressure to outlet 18, reducing the flow rate of purified fluid
  • a flow control device is a Dole valve.
  • Filter membranes appropriate for use in the present invention include, but are not
  • a filter membrane is an ultrafiltration membrane.
  • membrane may be configured as a spiral wound membrane, a hollow fiber membrane or a
  • a filter membrane is a spiral wound membrane.
  • a filter membrane is a spiral wound ultrafiltration
  • Fig. 2 depicts an embodiment of a filter vessel 30 which includes a plurality of filter
  • each filter membrane can be controlled to allow the feed pressure of vessel 30 to be increased
  • Filter vessel 30 includes
  • Filters 40, 50, 60 and 70 have membranes 42, 52, 62 and 72 as well as inlets 44, 54, 64
  • filters 40, 50, 60 and 70 have waste outlets 46, 56, 66 and
  • Waste outlets 46, 56 and 66 are in
  • Filters 40, 50 and 60 furthermore,
  • flow control device 49 includes flow control device 49, 59 and 69, respectively.
  • Flow control devices 49, 59 and 69 include flow control device 49, 59 and 69, respectively.
  • outlets 48, 58 and 68 supply a back pressure to outlets 48, 58 and 68, respectively.
  • Filters 40, 50, 60 and 70 are arranged within filter vessel 30 such that a purified fluid flowing through outlet 48, 58, 68 or 78 exits vessel 30 through outlet 36. Therefore, the flow
  • passing through outlet 78 may be controlled without the use of an additional flow control
  • product outlet 36 can be controlled independent of the pressure ofthe fluid at inlet 32 of
  • the pressure ofthe feed stream at inlet 32 may be increased to increase the pressure of
  • these flow rates vary by less than approximately 20%, more preferably less than approximately 10% and most preferably less than approximately 5%.
  • transmembrane pressure across each filter should be approximately equal notwithstanding the
  • the decrease in feed stream pressure of a filter membrane may be
  • control device in fluid communication with a filter membrane changes in response to the
  • transmembrane pressure of each membrane is less than approximately 20%, more preferably
  • the arrangement of flow control devices within a filter vessel is
  • the filter vessel should have at least one flow control device. Therefore, a
  • filter vessel may have a flow control device in fluid communication with the product outlet of
  • a filter vessel may be used to filter each filter as well as the product outlet ofthe filter vessel.
  • a filter vessel may be any filter vessel.
  • a dynamically responsive flow control device is in fluid communication with the product outlet ofthe filter vessel and all but the most downstream
  • filter membrane have a flow control device in fluid communication with their respective
  • a filter vessel typically has from two to four filters.
  • the filter membranes are typically, however, a filter vessel has from two to four filters.
  • disposed within the filters of a filter vessel may be the same or different types.
  • the filter membranes disposed are all the same type and have approximately the
  • a filter configured to filter the same pore size and active membrane area.
  • a filter is particularly preferred.
  • vessel has from two to four spiral wound ultrafiltration membranes, each membrane having
  • control devices may be incorporated into filter vessels such that the
  • vessel inlet may be increased without changing the amount of purified fluid flowing through
  • Fig. 3 depicts an embodiment of a staged filtration system 80 including filter vessels
  • Filtration system 80 includes a first filter vessel bank 82 and a second filter
  • First filter vessel bank 82 includes filter vessels 100, 102, 104 and
  • second filter vessel bank 84 includes filter vessels 108, 110 and 1 12.
  • Feed stream 81 and recirculation stream 83 are combined and flow
  • stream 85 passes through system 80, it may be filtered by a filter within filter vessel 100, 102,
  • first product stream 120 the fluid may flow through first
  • the fluid may be
  • vessel bank 84 may flow through vessel bank 84 without being filtered and enter system waste stream 126.
  • a fluid that is filtered by system 80 enters stream 120 or 124 which combine to form
  • a fluid flowing in stream 128 passes through flow control device
  • a flow control device may be disposed along
  • a flow control device may be disposed along stream 124 to control the flow rate ofthe
  • vessels and filter membranes may have flow control devices as described herein.
  • a fluid that passes through system 80 without being filtered enters system waste
  • stream 126 The flow of stream 126 is controlled by valves 130 and 132 such that a fluid in
  • stream 126 may flow to drain 92 or enter recirculation loop 88.
  • the filter vessels within a filter vessel bank are in a parallel arrangement such that the
  • inlets of the filter vessels are each in fluid communication with a common feed stream
  • the outlets ofthe filter vessels are each in fluid communication with a common product
  • FIG. 2 Although shown in Fig. 2 as including three or four
  • a filter vessel bank is not limited by this number of filter
  • a filter vessel bank may have any number of filter vessels equal to or greater
  • filter vessels in a filter vessel bank need not all be arranged in
  • a filter vessel bank may include portions in which filter vessels are
  • a filter vessel bank may include more than one portion in which filter vessels are arranged in
  • a filter vessel bank may have multiple parallel filter vessel portions as
  • a typical ultrafilter membrane that can be used in the present invention is an OSMO ®
  • the ultrafilter vessel has an operating
  • the pressure ofthe feed stream at the inlet ofthe filter vessel is 30
  • membrane 3 is the most downstream ultrafiltration membrane.
  • Reject corresponds to the flow rate of the waste stream from each ultrafiltration membrane, and avg. press is the average pressure within an ultrafiltration membrane.
  • product is the flow rate of the filtered product that flows from each ultrafiltration membrane, and total represents the total flow rate of filtered product from the ultrafilter vessel.
  • dP is the pressure drop across each membrane.
  • FIG. 4 shows a non-staged ultrafiltration system 200 designed to provide 160 GPM of filtered fluid.
  • the system includes a feed stream 201, a pump 202, a filter vessel bank 204 having a valved inlet 206. a product stream outlet 208 and a waste stream outlet 210.
  • the waste stream may flow to a waste drain 212 along flow path 21 1 or pass through a recirculation loop 214 to feed stream 200 along flow path 213.
  • the flow rate along paths 21 1 and 213 is regulated by valves 215 and 217. With this arrangement, the total flow rate into system 200 is the sum of the flow rates of stream 201 and 213.
  • Filter vessel bank 204 includes filter vessels 216-234 arranged in parallel such that the inlet each filter vessel is in fluid communication with the inlet 206, the waste outlet of each
  • filter vessel is in fluid communication with waste outlet 210, and the product outlet of each
  • Each filter vessel is in fluid communication with product outlet 208.
  • Each filter vessel includes three
  • vessel bank 204 is 510 GPM, and the flow rate of streams 201 and 213 are 176 GPM and 334
  • Pump 202 operates at 50 horsepower (HP) to supply filter vessel bank
  • filtration system 200 has a 90% recovery rate.
  • feed stream for the system had a flow rate of 176 GPM and the flow rate ofthe fluid in the
  • waste stream flowing to the drain had a flow rate of 16 GPM.
  • Feed corresponds to the flow rate ofthe feed
  • brine corresponds to the flow rate of the waste stream from each membrane.
  • product is the flow rate of fluid from each membrane, and delta
  • p is the difference between the inlet pressure and the outlet pressure of each membrane.
  • Pressure feed, net driv, trans P, pressure brine, orifice and drill represent the pressure ofthe
  • Table 2 indicates that utilizing flow control devices in accordance with the present

Abstract

Filter membranes with controlled product flow as well as filter vessels (100-112) and filtration systems (80) which use the same. In one embodiment, the present invention provides a filter for purifying a fluid. The filter comprises a filter membrane and a flow control device (96). The flow control device (96) is in fluid communication with the product outlet (128) of the filter membrane such that the flow control device (96) supplies a backpressure to the product outlet (128) to control the flow rate of a fluid through the product outlet. Filter vessels (100-112) having a plurality of such filter membranes arranged in series are also described. Furthermore, the present invention provides filtration systems which include a plurality of such filter vessels arranged in series and/or parallel. The present invention also provides methods of using such filter membranes, filter vessels and filtration systems.

Description

FILTER MEMBRANES WITH CONTROLLED PRODUCT FLOW AND SYSTEMS
USING SAME
BACKGROUND OF THE INVENTION
JL Field of the Invention
The present invention relates generally to filter membranes with controlled product
flow and filtration systems using the same.
2. Description of the Related Art
Filter membranes are commonly used to purify water and other fluids. Various
membrane configurations have been proposed, including spiral wound, hollow fiber and plate
and frame. Fluid flowing in a feed stream enters the filter membrane and is separated into a
filtered product stream and an unfiltered or brine waste stream. To increase efficiency and
reduce cost associated with fluid purification, it is desirable to dispose filter membranes in a
series configuration such that the waste stream from one filter membrane becomes the feed
stream of the next filter membrane. Therefore, filter membranes are often arranged in series
within a filter vessel, and the filter vessels, themselves, are also disposed in series such that
the waste stream from a first filter vessel serves as the feed stream into the next filter vessel.
This series arrangement of filter vessels is commonly referred to as staging.
While an ideal filtration system would include a large number of staged filter vessels,
such a system is not normally practical because, as a feed stream flows through a filter vessel,
friction between the stream and each filter membrane reduces the pressure of the stream. As
a result, the pressure of the waste stream leaving the filter vessel is less than the pressure of
the feed stream entering the same filter vessel. Ultimately, after passing through a number of filter vessels, the pressure of the waste stream is reduced to a pressure too low to serve as the
feed stream ofthe next filter vessel.
To alleviate this problem, the pressure ofthe feed stream into the first filter vessel
may be increased, causing the waste stream pressure to increase as well. However, this can
cause overfluxing ofthe upstream filter membranes, premature fouling of these membranes,
increased maintenance and time associated with the filter vessel, and a reduced duty cycle for
the filter vessel. Alternatively, the number of filter vessels used in a filtration system may be
decreased, but this decreases the level of filtration achieved by the system. Another option is
to provide a pump between stages of filter vessels, but this increases the power necessary to
utilize the filtration system, resulting in relatively high costs.
Filtration systems that include ultrafilter membranes are particularly susceptible to the
problem of decreased waste stream pressure because the pressure drop between the feed
stream and waste stream of an ultrafilter membrane is comparatively high. As a result, an
unpurified fluid can pass through only a relatively small number of ultrafilter membranes
before the waste stream pressure becomes too low to act as the feed stream for another filter
membrane. Therefore, filter vessels do not typically contain more than about four ultrafilter
membranes, and filter vessels having ultrafilters are not normally staged.
SUMMARY OF THE INVENTION
Therefore, it is an object ofthe present invention to provide a filtration system having
a number of filter membranes arranged in series such that the pressure of the waste stream of
any filter membrane is not too low to serve as the feed stream for the next filter membrane.
It is another object ofthe present invention to provide a filter vessel having a plurality of filter membranes arranged in series such that the product flow rate from each filter
membrane is approximately the same such that overfluxing of upstream membranes is
substantially reduced.
It is yet another object ofthe present invention to provide such a filter vessel such that
the transmembrane pressure across each filter membrane is approximately the same such that
the product flow rate is approximately the same for each membrane such that overfluxing of
upstream membranes is substantially reduced.
It is a further object ofthe present invention to provide a filtration system having
staged filter vessels with a comparatively high number of filter membranes are arranged in
series such that cost and increase the efficiency associated with purifying fluids.
To achieve these and other objects, the present invention provides an improved filter
membrane designed such that a plurality ofthe filter membranes can be arranged in series
without having the waste stream pressure drop too low to serve as the feed stream for the next
filter membrane. This is attained by controlling the pressure differential between the feed
stream and the product stream of each membrane such that a predetermined value for this
pressure differential may be obtained independent ofthe feed stream pressure. Since the
product flow rate of each membrane depends on this pressure differential, the product flow
rate of each membrane is also be controlled independent ofthe feed stream pressure. By
controlling the product flow rate of each membrane, the feed stream pressure ofthe most
upstream membrane can be increased to a relatively high value without overfluxing and
premature fouling of this membrane. At the same time, the increased feed stream pressure
allows a comparatively large number of filter membranes to be arranged in series without the
waste stream pressure becoming too low for the waste stream to act as the feed stream for another filter vessel.
In one illustrative embodiment, the present invention provides a filter for purifying a
fluid. The filter comprises a filter membrane and a flow control device. The filter membrane
has an inlet, a product outlet and a waste outlet. The flow control device is in fluid
communication with the product outlet ofthe filter membrane and supplies a backpressure to
the product outlet to control flow rate of fluid through the product outlet.
In another illustrative embodiment, the present invention provides a filter vessel for
purifying a fluid. At least two filter membranes are arranged in series within the filter vessel.
The inlet ofthe first filter membrane is in fluid communication with the inlet ofthe filter
vessel to allow a fluid to flow therebetween, and the waste outlet ofthe first filter membrane
is in fluid communication with the inlet ofthe second filter membrane so that the waste
stream ofthe first filter membrane serves as the feed stream ofthe second filter membrane. A
flow control device is in fluid communication with the product outlet ofthe filter vessel, first
filter membrane or the second filter membrane such that the flow control device supplies a
back pressure to the product outlet with which it is in fluid communication to control the flow
rate ofthe fluid through the product outlet.
In yet another illustrative embodiment, the present invention provides a filter vessel
that has the at least two filter membranes arranged in series such that the product flow rate is
approximately the same for both filter membranes.
In a further illustrative embodiment, the present invention provides a filter vessel that
has the at least two filter membranes arranged in series such that the transmembrane pressure
is approximately the same for both filter membranes.
In still a further illustrative embodiment, the present invention provides a method for filtering a fluid with a filtration system. The method comprises the steps of: providing a first
filter vessel having a plurality of filter membranes arranged in series; introducing a feed
stream at a first pressure into the first filter vessel; and maintaining a relatively constant
product flow rate through each ofthe filter membranes.
In yet a further illustrative embodiment, the present invention provides a filtration
system which includes first and second filter vessels arranged such that the waste outlet of the
first filter vessel is in fluid communication with the inlet ofthe second filter vessel. Each
filter vessel includes a plurality of filter membranes.
BRIEF DESCRIPTION OF THE DRAWINGS
The objects, advantages and features ofthe present invention will be more clearly
appreciated from the following detailed description when taken in conjunction with the
accompanying drawings, in which:
Fig. 1 is a schematic view of one embodiment of a filter according to the present
invention;
Fig. 2 is a schematic view of one embodiment of a filter vessel according to the
present invention;
Fig. 3 is a schematic view of one embodiment of a filtration system according to the
present invention; and
Fig. 4 is a schematic view of one embodiment of a filtration system according to the related art. DETAILED DESCRIPTION
The present invention relates to an improved filter 10 (Fig. 1) which is designed so
that a plurality of such filters can be arranged in series while maintaining a relatively high
waste stream pressure. Filter 10 includes a filter membrane 12, an inlet 14, a feed path that
terminates at a waste outlet 16, a product path that terminates at a product outlet 18 and a
flow control device 20. A portion of a feed fluid may pass through membrane 12 along the
waste path without being purified and exit through waste outlet 16. Alternatively, the fluid
may be purified by filter membrane 12 and leave through product outlet 18. After flowing
through product outlet 18, the purified fluid passes through flow control device 20.
The flow rate of purified fluid that exits filter 10 through product outlet 18 depends
approximately linearly on the transmembrane pressure of filter 10 which is the pressure
differential between the fluid entering filter 10 at inlet 14 and the purified fluid leaving filter
10 at outlet 18. Therefore, as the transmembrane pressure of membrane 10 increases, the
flow rate of fluid through product outlet 18 increases. Flow control device 20 is designed to
supply a back pressure to the purified fluid flowing through product outlet 18 such that the
transmembrane pressure can be controlled while the pressure of the feed fluid at inlet 14 is
varied. Since the flow rate of fluid through product outlet 18 depends on the transmembrane
pressure of membrane 10, device 20 also controls the product flow rate while the pressure of
the feed fluid is varied. For example, by varying the back pressure supplied by flow control
device 20 to maintain a constant transmembrane pressure across filter 10, the pressure of the
feed fluid at inlet 14 may be increased without increasing the product flow rate and without
causing overfluxing of filter membrane 12.
A "flow control" device may be any device that can be placed in fluid communication with the product outlet of a filter membrane so that the device is capable of supplying a back
pressure to the product outlet ofthe filter membrane. Preferably, a flow control device is a
static flow control device or a dynamically responsive flow control device. Static flow
control devices supply a back pressure to the product outlet independent ofthe flow rate of
purified fluid through the product outlet. Static flow control devices include fixed orifice
devices, capillary devices and valves. An example of a fixed orifice device is a flat plate
having an orifice disposed therethrough such that the fluid flowing through the product outlet
passes through the orifice and is partially blocked by the flat plate. The size ofthe orifice
should be selected to achieve the desired flow of purified fluid using the equation:
Figure imgf000009_0001
where hf is the pressure ofthe product stream in feet of water, Q is the flow rate ofthe
product stream, d is the diameter ofthe orifice in a direction normal to the path ofthe product
stream through the orifice, and k is a constant value of 0.0044. A capillary device may be
formed from a coiled tube. The length and diameter of the coiled tube should be chosen such
that a predetermined amount of purified fluid passes through the coiled tube. A valve
appropriate for use as a flow control device may be formed from a plurality of ball valves.
The ball valves should be selected manually to obtain the desired amount of purified fluid.
Dynamically responsive flow control devices supply a back pressure to the product
outlet that depends upon the flow rate of purified fluid through the product outlet.
Dynamically responsive flow control devices may be variable orifice flow control devices.
Such devices may include a flat plate having an orifice disposed therein and a rubber grommet located within the fixed orifice. As the pressure ofthe fluid leaving product outlet
18 increases, the diameter ofthe rubber grommet decreases. The reduced diameter ofthe
grommet increases the back pressure to outlet 18, reducing the flow rate of purified fluid
through outlet 18. One example of such a flow control device is a Dole valve.
Filter membranes appropriate for use in the present invention include, but are not
limited to, ultrafiltration membranes, microfiltration membranes and reverse osmosis
filtration membranes. Preferably, a filter membrane is an ultrafiltration membrane. The filter
membrane may be configured as a spiral wound membrane, a hollow fiber membrane or a
plate and frame membrane. Preferably, a filter membrane is a spiral wound membrane. In a
particularly preferred embodiment, a filter membrane is a spiral wound ultrafiltration
membrane.
Fig. 2 depicts an embodiment of a filter vessel 30 which includes a plurality of filter
membranes arranged in series such that the transmembrane pressure and product flow rate of
each filter membrane can be controlled to allow the feed pressure of vessel 30 to be increased
without resulting in overfluxing ofthe upstream filter membranes. Filter vessel 30 includes
inlet 32, waste outlet 34, product outlet 36, flow control device 38 and filters 40, 50, 60 and
70. Filters 40, 50, 60 and 70 have membranes 42, 52, 62 and 72 as well as inlets 44, 54, 64
and 74, respectively. In addition, filters 40, 50, 60 and 70 have waste outlets 46, 56, 66 and
76 and product outlets 48, 58, 68 and 78, respectively. Waste outlets 46, 56 and 66 are in
fluid communication with inlets 52, 62 and 72, respectively. Filters 40, 50 and 60 further
include flow control device 49, 59 and 69, respectively. Flow control devices 49, 59 and 69
supply a back pressure to outlets 48, 58 and 68, respectively.
Filters 40, 50, 60 and 70 are arranged within filter vessel 30 such that a purified fluid flowing through outlet 48, 58, 68 or 78 exits vessel 30 through outlet 36. Therefore, the flow
rate of purified fluid through outlet 36 is the sum ofthe flow rates through outlets 48. 58, 68
and 78. After passing through outlet 36, the purified fluid then passes through flow control
device 38 which is designed to supply a back pressure through outlets 48, 58, 68 and 78 to
achieve a predetermined flow rate of purified fluid leaving filter vessel 30 through outlet 36.
It is to be noted that with this arrangement of filter vessel 30, since the flow rates of purified
fluid flowing through outlets 36, 48, 58 and 68 are controlled, the flow rate of purified fluid
passing through outlet 78 may be controlled without the use of an additional flow control
device. Furthermore, the total flow rate of purified fluid exiting filter vessel 30 through
product outlet 36 can be controlled independent ofthe pressure ofthe fluid at inlet 32 of
vessel 30.
As discussed above, the pressure of an unpurified stream decreases as it flows through
each filter membrane in a filter vessel, so the pressure of a feed fluid at a filter vessel inlet is
higher than the pressure of the waste stream leaving the same filter vessel. This leads to
overfluxing ofthe upstream membranes and premature fouling of these membranes.
However, with the configuration of filter membranes and flow control devices depicted in
Fig. 2, the pressure ofthe feed stream at inlet 32 may be increased to increase the pressure of
the stream flowing through waste outlet 34 without causing overfluxing of filter membranes
40, 50 or 60.
For embodiments in which it is desirable to reduce the amount of overfluxing of
upstream filter membranes in a filter vessel to avoid premature fouling of these membranes,
the flow rates of purified fluid through the product outlets of each filter should be
approximately equal. Preferably, these flow rates vary by less than approximately 20%, more preferably less than approximately 10% and most preferably less than approximately 5%. To
achieve an approximately uniform flow rate of purified fluid through each product outlet,
back pressure supplied by each flow control device is predetermined such that the
transmembrane pressure across each filter should be approximately equal notwithstanding the
decrease in the pressure ofthe feed stream for each successive filter membrane. For static
flow control devices, the decrease in feed stream pressure of a filter membrane may be
compensated for by increasing the orifice ofthe flow control device in fluid communication
with that filter membrane. For dynamic flow control devices, the size ofthe orifice of a flow
control device in fluid communication with a filter membrane changes in response to the
decrease in feed stream pressure for that filter membrane to maintain a substantially constant
product flow rate for each filter membrane. Preferably, the variation between the
transmembrane pressure of each membrane is less than approximately 20%, more preferably
less than approximately 10% and most preferably less than approximately 5%.
Although an arrangement of flow control devices for a filter vessel is shown in Fig. 2,
it is to be appreciated that the present invention is not limited by this arrangement. According
to the present invention, the arrangement of flow control devices within a filter vessel is
limited only in that the filter vessel should have at least one flow control device. Therefore, a
filter vessel may have a flow control device in fluid communication with the product outlet of
each filter as well as the product outlet ofthe filter vessel. Alternatively, a filter vessel may
only have a flow control device in fluid communication with the filter vessel, without having
a flow control device for any ofthe filters. Other arrangements of flow control devices are
contemplated to be within the scope of the present invention. Preferably, however, a filter
vessel is arranged such that a dynamically responsive flow control device is in fluid communication with the product outlet ofthe filter vessel and all but the most downstream
filter membrane have a flow control device in fluid communication with their respective
product outlets.
Although depicted in Fig. 2 as having four filters, a filter vessel many any number of
filters. Typically, however, a filter vessel has from two to four filters. The filter membranes
disposed within the filters of a filter vessel may be the same or different types. Preferably,
however, the filter membranes disposed are all the same type and have approximately the
same pore size and active membrane area. In a particularly preferred embodiment, a filter
vessel has from two to four spiral wound ultrafiltration membranes, each membrane having
approximately the same pore size and active membrane area.
As noted above, control devices may be incorporated into filter vessels such that the
amount of purified fluid passing therethrough may be controlled independently ofthe
pressure ofthe fluid at the inlet ofthe filter vessel. Thus, the pressure ofthe fluid at the
vessel inlet may be increased without changing the amount of purified fluid flowing through
the filter vessel and without causing overfluxing ofthe upstream filter membranes. As a
result, the pressure ofthe unfiltered fluid exiting the filter vessel through the waste outlet can
be increased to allow this unfiltered fluid to serve as the feed stream of another filter vessel,
allowing filter vessels to be staged within a filtration system.
Fig. 3 depicts an embodiment of a staged filtration system 80 including filter vessels
arranged in series such that a high level purification of a fluid can be achieved without
excessive overfluxing or premature fouling ofthe upstream filter membranes housed within
the filter vessels. Filtration system 80 includes a first filter vessel bank 82 and a second filter
vessel bank 84 as well as a pump 86, a recirculation loop 88, a drain 92, a system inlet 94 and flow control device 96. First filter vessel bank 82 includes filter vessels 100, 102, 104 and
106, and second filter vessel bank 84 includes filter vessels 108, 110 and 1 12.
Feed stream 81 and recirculation stream 83 (described below) are combined and flow
through pump 86 to form inlet stream 85 which is input to system inlet 94. As a fluid in
stream 85 passes through system 80, it may be filtered by a filter within filter vessel 100, 102,
104 or 106 and enter first product stream 120. Alternatively, the fluid may flow through first
filter vessel bank 82 without being filtered and enter first waste stream 122. A fluid in stream
122 flows into second filter vessel bank 84. After entering vessel bank 84, the fluid may be
filtered by filter vessels 108, 1 10 or 112 and enter second product stream 124, or the fluid
may flow through vessel bank 84 without being filtered and enter system waste stream 126.
A fluid that is filtered by system 80 enters stream 120 or 124 which combine to form
system product stream 128. A fluid flowing in stream 128 passes through flow control device
96 which is designed to supply a back pressure such that the flow rate of stream 128 is
controlled. Although not shown in Fig. 3, a flow control device may be disposed along
stream 120 to control the flow rate ofthe purified fluid flowing from first vessel bank 82,
and/or a flow control device may be disposed along stream 124 to control the flow rate ofthe
purified fluid flowing from second filter vessel bank 84. In addition, any or all ofthe filter
vessels and filter membranes may have flow control devices as described herein.
A fluid that passes through system 80 without being filtered enters system waste
stream 126. The flow of stream 126 is controlled by valves 130 and 132 such that a fluid in
stream 126 may flow to drain 92 or enter recirculation loop 88. A fluid flowing through loop
88 is combined with the feed stream 81, passes through pump 86 and re-enters filtration
system 80. The filter vessels within a filter vessel bank are in a parallel arrangement such that the
inlets of the filter vessels are each in fluid communication with a common feed stream, and
the outlets ofthe filter vessels are each in fluid communication with a common product
and/or waste stream for the filter vessels. Although shown in Fig. 2 as including three or four
filter vessel arranged in parallel, a filter vessel bank is not limited by this number of filter
vessels. Instead, a filter vessel bank may have any number of filter vessels equal to or greater
than one. In addition, the filter vessels in a filter vessel bank need not all be arranged in
parallel. For example, a filter vessel bank may include portions in which filter vessels are
arranged in series and portions in which filter vessels are arranged in parallel. Alternatively,
a filter vessel bank may include more than one portion in which filter vessels are arranged in
parallel. In addition, a filter vessel bank may have multiple parallel filter vessel portions as
well as portions in which filter vessels are arranged in series.
The following examples are intended to demonstrate certain aspects ofthe present
invention and are in no way intended to be construed as limiting.
EXAMPLE 1
A typical ultrafilter membrane that can be used in the present invention is an OSMO®
ultrafiltration membrane (Model 815PT3PS, available from Osmonics, located in
Minnetonka, MN). Table 1 demonstrates various parameters for an ultrafilter vessel having
three such ultrafiltration membranes arranged in series. The ultrafilter vessel has an operating
temperature of 25 °C. The pressure ofthe feed stream at the inlet ofthe filter vessel is 30
pounds per square inch (PSI), and the flow rate ofthe fluid at the filter vessel inlet is 51
gallons per minute (GPM). Relative to feed stream ofthe filter vessel, membrane 1 is the
most upstream ultrafiltration membrane, and membrane 3 is the most downstream ultrafiltration membrane. Reject corresponds to the flow rate of the waste stream from each ultrafiltration membrane, and avg. press is the average pressure within an ultrafiltration membrane. In addition, product is the flow rate of the filtered product that flows from each ultrafiltration membrane, and total represents the total flow rate of filtered product from the ultrafilter vessel. Furthermore, dP is the pressure drop across each membrane. As can be seen from Table 1 , without the use of a flow control device to provide product side throttling, the product flow rate from each ultrafiltration membrane in the ultrafilter vessel is different. As a result, membrane 1 is exposed to a higher flux of fluid than membranes 2 or 3.
Table 1
Figure imgf000016_0001
EXAMPLE 2 Fig. 4 shows a non-staged ultrafiltration system 200 designed to provide 160 GPM of filtered fluid. The system includes a feed stream 201, a pump 202, a filter vessel bank 204 having a valved inlet 206. a product stream outlet 208 and a waste stream outlet 210. The waste stream may flow to a waste drain 212 along flow path 21 1 or pass through a recirculation loop 214 to feed stream 200 along flow path 213. The flow rate along paths 21 1 and 213 is regulated by valves 215 and 217. With this arrangement, the total flow rate into system 200 is the sum of the flow rates of stream 201 and 213.
Filter vessel bank 204 includes filter vessels 216-234 arranged in parallel such that the inlet each filter vessel is in fluid communication with the inlet 206, the waste outlet of each
filter vessel is in fluid communication with waste outlet 210, and the product outlet of each
vessel is in fluid communication with product outlet 208. Each filter vessel includes three
Model 815PT3PS OSMO® ultrafiltration membranes arranged in series.
To provide the desired product flow rate of 160 GPM, the total flow rate into filter
vessel bank 204 is 510 GPM, and the flow rate of streams 201 and 213 are 176 GPM and 334
GPM, respectively. Pump 202 operates at 50 horsepower (HP) to supply filter vessel bank
204 with the 510 GPM at a backing pressure of 50 PSI. Since only 16 GPM of the fluid
flows to drain 212, filtration system 200 has a 90% recovery rate.
EXAMPLE 3
An ultrafiltration system designed to provide a product flow rate of 160 GPM was
arranged similar to the system depicted in Fig. 3. Fixed orifice flow control devices were
used for the filters and Dole valves as the flow control device for the filter vessels. Each filter
vessel included four OSMO® 815PT3PS ultrafiltration membranes arranged in series. The
feed stream for the system had a flow rate of 176 GPM and the flow rate ofthe fluid in the
recirculation loop was 90 GPM. The pump operated at 25 HP such that the fluid at the inlet
ofthe filtration system had a flow rate of 266 GPM and a backing pressure of 90 PSI. The
waste stream flowing to the drain had a flow rate of 16 GPM.
Table 2 demonstrates various parameters for this filtration system. Stages 1 and 2
relate to the filters in the first filter and second vessel banks, respectively, from the most
upstream filter to the most downstream filter. Feed corresponds to the flow rate ofthe feed
stream for each membrane, and brine corresponds to the flow rate of the waste stream from each membrane. In addition, product is the flow rate of fluid from each membrane, and delta
p is the difference between the inlet pressure and the outlet pressure of each membrane.
Pressure feed, net driv, trans P, pressure brine, orifice and drill represent the pressure ofthe
fluid at the filter inlet, the back pressure against the outlet ofthe filter, the transmembrane
pressure, the pressure ofthe waste stream, the diameter ofthe orifice in the flow control
device and the size ofthe drill bit used to form the orifice, respectively.
Table 2 indicates that utilizing flow control devices in accordance with the present
invention can result in a constant product flow rate for each membrane in a filtration system.
Because the flow rate of purified fluid from each product outlet is approximately the same,
overfluxing ofthe upstream filters ofthe filtration is reduced.
Table 2
Figure imgf000018_0001
Having thus described certain embodiments ofthe present invention, various
alterations, modifications and improvements will readily occur to those skilled in the art.
Such alterations, modifications, and improvements are intended to be part of this disclosure, and are intended to be within the spirit and scope of the invention.
What is claimed is:

Claims

1. A filter vessel for purifying a fluid, the filter vessel having an inlet, a waste outlet and
a product outlet, the filter vessel comprising:
a housing;
a first filter disposed within the housing, the first filter comprising:
a filter membrane having an inlet in fluid communication with the inlet ofthe
filter vessel, a waste outlet and a product outlet;
a second filter disposed within the housing, the second filter comprising:
a filter membrane having an inlet in fluid communication with the waste outlet
ofthe filter membrane ofthe first filter, a waste outlet in fluid communication with the waste
outlet ofthe filter vessel and a product outlet in fluid communication with the product outlet
ofthe filter vessel; and
a first flow control device in fluid communication with an outlet selected from the
group consisting of the product outlet ofthe filter vessel, the product outlet ofthe first filter
and the product outlet ofthe second filter, the first flow control device being capable of
supplying a backpressure to the outlet to control a flow rate of a fluid through the outlet.
2. The filter vessel according to claim 1, wherein the first flow control device is in fluid
communication with the product outlet ofthe filter vessel for supplying a backpressure to the product outlet ofthe filter vessel to control a flow rate of a fluid through the product outlet of
the filter vessel.
3. The filter vessel according to claim 2, further comprising a second flow control device in fluid communication with the product outlet ofthe first filter membrane for supplying a
backpressure to the product outlet ofthe first filter membrane to control a flow rate of a fluid
through the product outlet ofthe first filter membrane.
4. The filter vessel according to claim 3, further comprising a third flow control device is
in fluid communication with the product outlet ofthe second filter membrane for supplying a
backpressure to the product outlet ofthe second filter membrane to control a flow rate of a
fluid through the product outlet ofthe second filter membrane.
5. The filter vessel according to claim 2, further comprising a second flow control device
in fluid communication with the product outlet of the second filter membrane for supplying a
back pressure to the product outlet ofthe second membrane to control a flow rate of a fluid
through the product outlet of the second membrane.
6. The filter vessel according to claim 1 , wherein the first flow control device is in fluid
communication with the product outlet ofthe first filter membrane for supplying a
backpressure to the product outlet ofthe first filter membrane to control a flow rate of a fluid
through the product outlet ofthe first filter membrane.
7. The filter vessel according to claim 6, further comprising a second flow control device
in fluid communication with the product outlet ofthe second filter membrane for supplying a
backpressure to the product outlet ofthe second filter membrane to control a flow rate of a
fluid through the product outlet ofthe second filter membrane.
8. The filter vessel according to claim 7, wherein the first flow control device supplies a
back pressure to the product outlet ofthe first filter membrane such that the first filter
membrane has a first transmembrane pressure, and wherein the second flow control device
supplies a back pressure to the product outlet ofthe second filter membrane such that the
second filter membrane has a second transmembrane pressure approximately equal to the first
transmembrane pressure.
9. The filter vessel according to claim 7, wherein the first flow control device supplies a
back pressure to the product outlet ofthe first filter membrane such that the filter membrane
has a first product flow rate, and wherein the second flow control device supplies a back
pressure to the product outlet ofthe second filter membrane such that the second filter
membrane has a second product flow rate approximately equal to the first product flow rate.
10. The filter vessel according to claim 1 , wherein the first flow control device is in fluid
communication with the product outlet ofthe second filter membrane for supplying a
backpressure to the product outlet ofthe second filter membrane to control a flow rate of a
fluid through the product outlet of the second filter membrane.
11. The filter vessel according to claim 1 , wherein the flow control device is a stationary
flow control device.
12. The filter vessel according to claim 1, wherein the flow control device is a fixed orifice device.
13. The filter vessel according to claim 1, wherein the flow control device is a capillary
device.
14. The filter vessel according to claim 1 , wherein the flow control device is valve device.
15. The filter vessel according to claim 1 , wherein the flow control device is a
dynamically responsive flow control device.
16. The filter vessel according to claim 1 , wherein the flow control device is a Dole valve.
17. The filter vessel according to claim 1 , wherein the first filter membrane is an
ultrafilter membrane.
18. The filter vessel according to claim 17, wherein the second filter membrane is an
ultrafilter membrane.
19. The filter vessel according to claim 1 , wherein the second filter membrane is an
ultrafilter membrane.
20. A filter vessel for purifying a fluid, the filter vessel having an inlet, a waste outlet and
a product outlet, the filter vessel comprising: a first filter disposed within the filter vessel, the first filter comprising:
a filter membrane having an inlet in fluid communication with the inlet of the
filter vessel, a waste outlet, a product outlet and a first product flow rate; and
a second filter disposed within the filter vessel, the second filter comprising:
a filter membrane having an inlet in fluid communication with the waste outlet
ofthe filter membrane ofthe first filter, a waste outlet in fluid communication with the waste
outlet ofthe filter vessel, a product outlet in fluid communication with the product outlet of
the filter vessel and a second product flow rate approximately equal to the first product flow
rate.
21. The filter vessel according to claim 20, wherein the first filter membrane is an
ultrafilter membrane.
22. The filter vessel according to claim 21, wherein the second filter membrane is an
ultrafilter membrane .
23. The filter vessel according to claim 20, wherein the second filter membrane is an
ultrafilter membrane.
24. A filter vessel for purifying a fluid, the filter vessel having an inlet, a waste outlet and
a product outlet, the filter vessel comprising:
a first filter disposed within the filter vessel, the first filter comprising:
a filter membrane having a an inlet in fluid communication with the inlet of the filter vessel, a waste outlet, a product outlet and a first transmembrane pressure; and
a second filter disposed within the filter vessel, the second filter comprising:
a filter membrane having an inlet fluid communication with the waste outlet of
the filter membrane ofthe first filter, a waste outlet in fluid communication with the waste
outlet ofthe filter vessel, a product outlet in fluid commumcation with the product outlet of
the filter vessel and a second transmembrane pressure approximately equal to the first
transmembrane pressure.
25. The filter vessel according to claim 24, wherein the first filter membrane is an
ultrafilter membrane.
26. The filter vessel according to claim 25, wherein the second filter membrane is an
ultrafilter membrane.
27. The filter vessel according to claim 24, wherein the second filter membrane is an
ultrafilter membrane.
28. A method of purifying a fluid with a filtration system, the method comprising the steps of:
providing a first filter vessel having a plurality of filter membranes arranged in series;
introducing a feed stream at a first pressure into the first filter vessel; and
maintaining a relatively constant product flow rate through each of the filter
membranes.
29. The method according to claim 28, wherein the step of maintaining a relatively
constant product flow rate includes the step of:
filtering a portion ofthe feed stream with at least one ofthe plurality of filter
membranes to form a purified stream; and
passing the purified stream through a flow control device in fluid communication with
a product outlet of the at least one of the plurality of filter membranes.
30. The method according to claim 29, wherein the step of filtering a portion ofthe feed
stream with at least one ofthe plurality of filter membranes to form a purified stream includes
the step of: filtering a portion ofthe feed stream with each ofthe plurality of filter membranes to
form a purified stream.
31. The method according to claim 30, wherein the step of passing the purified stream
through a flow control device in fluid communication with a product outlet ofthe at least one
ofthe plurality of filter membranes includes the step of:
passing the purified stream through a plurality of flow control devices, each ofthe
plurality of flow control devices being in fluid communication with one of the plurality of
filter membranes.
32. The method according to claim 28, further comprising the steps of:
providing a second filter vessel having a plurality of filter membranes arranged in series; transferring a waste stream from the first filter vessel to the second filter vessel;
introducing the waste stream into the second filter vessel; and
maintaining a relatively constant product flow rate through each of the filter
membranes in the second filter vessel.
33. The method according to claim 32, wherein the step of maintaining a relatively
constant product flow rate includes the step of:
filtering a portion of the feed stream with at least one ofthe plurality of filter
membranes to form a purified stream; and
passing the purified stream through a flow control device in fluid communication with
a product outlet of the at least one ofthe plurality of filter membranes.
34. The method according to claim 33, wherein the step of passing the purified stream
through a flow control device in fluid communication with a product outlet ofthe at least one
ofthe plurality of filter membranes includes the step of:
passing the purified stream through a plurality of flow control devices, each ofthe
plurality of flow control devices being in fluid communication with one ofthe plurality of
filter membranes.
35. A filtration system for purifying a fluid, the filtration system having an inlet, a waste
outlet and a product outlet, the filtration system comprising:
a first filter vessel bank having an inlet in fluid communication with the inlet ofthe filtration system, a product outlet, a waste outlet and at least one filter vessel, the at least one
filter vessel having a product outlet in fluid communication with the product outlet ofthe first
filter vessel bank, a waste outlet in fluid communication with the waste outlet of the first filter
vessel bank, an inlet in fluid communication with the inlet ofthe first filter vessel bank, and
at least one filter, the at least one filter including a filter membrane having an inlet in fluid
communication with the inlet ofthe at least one filter vessel, a product outlet in fluid
communication with the product outlet ofthe at least one filter vessel and a waste outlet in
fluid communication with the waste outlet ofthe at least one filter vessel; and
a second filter vessel bank having an inlet in fluid communication with the waste
outlet ofthe first filter vessel bank, a waste outlet in fluid communication with the waste
outlet ofthe filtration system, a product outlet in fluid communication with the product outlet
ofthe filtration system, and at least one filter vessel, the at least one filter vessel having a
product outlet in fluid communication with the product outlet of the second filter vessel bank,
a waste outlet in fluid communication with the waste outlet of the second filter vessel bank,
an inlet in fluid communication with the inlet ofthe second filter vessel bank, and a filter, the
filter having an inlet in fluid communication with the inlet ofthe at least one filter vessel of
the second filter vessel bank, a product outlet in fluid communication with the product outlet
ofthe at least one filter vessel ofthe second filter vessel bank, and a waste outlet in fluid
communication with the waste outlet of the at least one filter vessel ofthe second filter vessel
bank,
wherein the at least one first filter vessel ofthe first filter vessel bank further includes
a flow control device in fluid communication with the product outlet ofthe at least one filter
ofthe at least one filter vessel ofthe first filter vessel bank.
36. The filtration system according to claim 35, wherein the at least one filter vessel ofthe
first filter vessel bank includes a first plurality of filter vessels, each of the first plurality of
filter vessels having an inlet in fluid communication with the inlet ofthe first filter vessel
bank, a product outlet in fluid communication with the product outlet of the first filter vessel
bank, and a waste outlet in fluid communication with the waste outlet ofthe first filter vessel
bank, wherein the at least one first filter vessel ofthe first filter vessel bank further includes a
flow control device in fluid communication with the product outlet ofthe at least one filter of
the at least one filter vessel of the first filter vessel bank.
37. The filtration system according to claim 36, wherein the at least one filter vessel ofthe
second filter vessel bank includes a second plurality of filter vessels, each ofthe first plurality
of filter vessels having an inlet in fluid communication with the inlet ofthe second filter
vessel bank, a product outlet in fluid communication with the product outlet ofthe second
filter vessel bank, and a waste outlet in fluid communication with the waste outlet ofthe
second filter vessel bank.
38. The filtration system according to claim 35, wherein the at least one filter vessel ofthe
second filter vessel bank includes a second plurality of filter vessels, each of the first plurality
of filter vessels having an inlet in fluid communication with the inlet ofthe second filter
vessel bank, a product outlet in fluid communication with the product outlet of the second
filter vessel bank, and a waste outlet in fluid communication with the waste outlet of the
second filter vessel bank.
39. The filtration system according to claim 35, wherein the at least one first filter vessel
ofthe second filter vessel bank further includes a flow control device in fluid communication
with the product outlet of the at least one filter ofthe at least one filter vessel ofthe second
filter vessel bank.
40. The filtration system according to claim 35, wherein the at least one first filter vessel
of the second filter vessel bank further includes a flow control device in fluid communication
with the product outlet of the at least one filter ofthe at least one filter vessel ofthe second
filter vessel bank.
41. The filtration system according to claim 35, wherein the filter membrane ofthe at
least one filter ofthe at least one filter vessel ofthe first filter vessel bank is an ultrafilter
membrane.
42. The filtration system according to claim 41 , wherein the filter membrane of the at
least one filter ofthe at least one filter vessel ofthe second filter vessel bank is an ultrafilter
membrane.
43. The filtration system according to claim 35, wherein the filter membrane of the at
least one filter of the at least one filter vessel ofthe second filter vessel bank is an ultrafilter
membrane.
PCT/US1997/006418 1996-04-12 1997-04-11 Filter membranes with controlled product flow and systems using same WO1997038786A1 (en)

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Cited By (2)

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WO2001044124A1 (en) * 1999-12-17 2001-06-21 Warner Lambert Research And Development Ireland Limited Production of pyrogen controlled water
WO2008096108A3 (en) * 2007-02-06 2009-05-22 H2Oil & Gas Ltd Filtration system

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WO1993012864A1 (en) * 1990-02-23 1993-07-08 Nature's Sunshine Products, Inc. Reverse osmosis system for home use

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EP0272632A2 (en) * 1986-12-23 1988-06-29 Osmonics, Inc. Flow control manifold for cross-flow membrane apparatus
WO1993012864A1 (en) * 1990-02-23 1993-07-08 Nature's Sunshine Products, Inc. Reverse osmosis system for home use

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Publication number Priority date Publication date Assignee Title
WO2001044124A1 (en) * 1999-12-17 2001-06-21 Warner Lambert Research And Development Ireland Limited Production of pyrogen controlled water
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WO2008096108A3 (en) * 2007-02-06 2009-05-22 H2Oil & Gas Ltd Filtration system
US8795527B2 (en) 2007-02-06 2014-08-05 H2Oil & Gas Ltd Filtration system

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