WO1996040618A3 - Concentrated aqueous lysine propionate solution and method of preparation thereof - Google Patents

Concentrated aqueous lysine propionate solution and method of preparation thereof Download PDF

Info

Publication number
WO1996040618A3
WO1996040618A3 PCT/US1996/008554 US9608554W WO9640618A3 WO 1996040618 A3 WO1996040618 A3 WO 1996040618A3 US 9608554 W US9608554 W US 9608554W WO 9640618 A3 WO9640618 A3 WO 9640618A3
Authority
WO
WIPO (PCT)
Prior art keywords
lysine
propionic acid
weight
concentrated aqueous
preparation
Prior art date
Application number
PCT/US1996/008554
Other languages
French (fr)
Other versions
WO1996040618A2 (en
Inventor
Frank J Ivey
William D Shermer
Melvin L Briggs
Original Assignee
Novus Int Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Novus Int Inc filed Critical Novus Int Inc
Priority to AU61491/96A priority Critical patent/AU6149196A/en
Publication of WO1996040618A2 publication Critical patent/WO1996040618A2/en
Publication of WO1996040618A3 publication Critical patent/WO1996040618A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/122—Propionic acid
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/105—Aliphatic or alicyclic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/142—Amino acids; Derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/26—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one amino group bound to the carbon skeleton, e.g. lysine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Animal Husbandry (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Fodder In General (AREA)
  • Feed For Specific Animals (AREA)

Abstract

A concentrated aqueous solution comprising lysine and propionic acid, and containing at least about 45 % by weight lysine solute. The solution is prepared by loading protonated lysine onto a cation exchange resin and eluting with propionic acid. The concentrate is advantageously used to prepare an animal feed composition comprising solid nutrients and containing between about 0.05 % and about 0.4 % by weight lysine, and between about 0.02 % and about 1 % by weight propionic acid, in a weight proportion of propionic acid to lysine of between about 0.5 and about 10. Also provided are concentrated aqueous solutions of lysine propionate containing lysine solute in the range from about 45 % to about 66 % by weight useful for preparing animal feed compositions. A bulk station for delivery of lysine propionate concentrate and propionic acid in any desired ratio is also disclosed.
PCT/US1996/008554 1995-06-07 1996-06-04 Concentrated aqueous lysine propionate solution and method of preparation thereof WO1996040618A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU61491/96A AU6149196A (en) 1995-06-07 1996-06-04 Concentrated aqueous lysine propionate solution and method o f preparation thereof

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US48329695A 1995-06-07 1995-06-07
US08/483,296 1995-06-07
US64270196A 1996-05-17 1996-05-17
US08/642,701 1996-05-17

Publications (2)

Publication Number Publication Date
WO1996040618A2 WO1996040618A2 (en) 1996-12-19
WO1996040618A3 true WO1996040618A3 (en) 1997-04-24

Family

ID=27047591

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1996/008554 WO1996040618A2 (en) 1995-06-07 1996-06-04 Concentrated aqueous lysine propionate solution and method of preparation thereof

Country Status (3)

Country Link
AU (1) AU6149196A (en)
IL (1) IL118435A0 (en)
WO (1) WO1996040618A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19753321A1 (en) * 1997-12-02 1999-06-10 Basf Ag Process for the production and use of lysine formate
JP2000256290A (en) * 1999-03-11 2000-09-19 Ajinomoto Co Inc Stabilized aqueous solution of lysine

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3024272A (en) * 1958-04-22 1962-03-06 Du Pont Organic acid salts of basic amino acids and their use
DE2357119A1 (en) * 1972-11-15 1974-05-22 Spofa Vereinigte Pharma Werke PROCESS FOR PRODUCING A STABLE CONCENTRATE WITH A HIGH CONTENT OF ESSENTIAL BIOFACTORS
US4919945A (en) * 1982-11-18 1990-04-24 Degussa Aktiengesellschaft Use of Aqueous L-lysine solutions for supplementing feeds and indistrially produced mixed feeds with L-lysine

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3024272A (en) * 1958-04-22 1962-03-06 Du Pont Organic acid salts of basic amino acids and their use
DE2357119A1 (en) * 1972-11-15 1974-05-22 Spofa Vereinigte Pharma Werke PROCESS FOR PRODUCING A STABLE CONCENTRATE WITH A HIGH CONTENT OF ESSENTIAL BIOFACTORS
US4919945A (en) * 1982-11-18 1990-04-24 Degussa Aktiengesellschaft Use of Aqueous L-lysine solutions for supplementing feeds and indistrially produced mixed feeds with L-lysine

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
B. OBERBARNSCHEIDT ET AL.: "Konservieren von feuchtem Futtergetreide in Flachsilos", LANDTECHNIK, vol. 47, no. 6, 1992, pages 260,285 - 288, XP000645212 *

Also Published As

Publication number Publication date
WO1996040618A2 (en) 1996-12-19
AU6149196A (en) 1996-12-30
IL118435A0 (en) 1996-09-12

Similar Documents

Publication Publication Date Title
AU586286B2 (en) Pharmaceutical and dietary composition
IL71849A0 (en) Cyclohexanedionecarboxylic acid derivatives,their preparation and their use as herbicides and plant growth regulators
CA2128617A1 (en) Ruminant feed supplement
EP0930339A4 (en) Resin composition, process for preparing the same, and laminate containing layer of said resin composition
IL57452A0 (en) Method and compositions containing cyclo-alkanecarboxylic acid derivatives for regulating plant growth,certain such novel compounds and their preparation
AU5994190A (en) Ensiling composition
AU6619794A (en) Process for delivering a selected effective amount of a dry granular antimicrobial composition to an aqueous system
IE821911L (en) Preparing insulin derivatives
HUT47793A (en) Herbicide compositions containing 2,6-substituted-pyridine-carboxylic acid derivatives as active components and process for producing the active components
CA2221298A1 (en) Preparation of ammonium glyphosate using aqueous ammonium hydroxide in a solid reaction system
WO1996040618A3 (en) Concentrated aqueous lysine propionate solution and method of preparation thereof
HUT39960A (en) Plant growth regulating composition containing 1-phenyl-imidazole-5-carboxylic acid as active ingredient and process for preparing the active ingredient
IL62228A0 (en) Plant growth regulating compositions comprising phenylacetic acid derivatives,certain such novel compounds and their preparation
AU564530B2 (en) Process for the preparation of a composition suitable for pormoting the utilization/ digestibility/ of fodder by the animals
CA2016768A1 (en) Method of weaning piglets
CA2099351A1 (en) Preparation of Shaped Zirconia Particles
DE3367595D1 (en) Functional derivatives of acetic acid containing phosphorus, process for preparing them and herbicidal and growth regulating compositions containing them
HUT43937A (en) Herbicidal and plant growth regulator compositions comprising 1,6-anhydro-beta- hexopyranose derivatives as active substance and process for preparing such compounds
IE821450L (en) Tetrahydropyran derivatives as growth promoters
EP0508901A3 (en) Alpha-methylene-4-((phenoxy)methyl))5-thiazolacetic acid derivatives, process for their preparation, intermediates in this process, their use as fungicides and compositions containing them
CA2040521A1 (en) Aqueous solutions or dispersions of oligoruethanes containing (meth)acryloyl groups, a process for their production and coated substrates prepared therefrom
AU4095589A (en) Preparation of the trisodium salt of isoserine-n, n-diacetic acid
GR3036840T3 (en) Amorphous monospheric forms of insulin derivatives.
DE3166825D1 (en) Process for manufacture of a coated acetylsalicylic-acid formulation
AU700834B2 (en) Method for applying metal-amino acid complexes as supplements to feed

Legal Events

Date Code Title Description
AK Designated states

Kind code of ref document: A2

Designated state(s): AL AM AT AU AZ BB BG BR BY CA CH CN CZ DE DK EE ES FI GB GE HU IS JP KE KG KP KR KZ LK LR LS LT LU LV MD MG MK MN MW MX NO NZ PL PT RO RU SD SE SG SI SK TJ TM TR TT UA UG UZ VN AM AZ BY KG KZ MD RU TJ TM

AL Designated countries for regional patents

Kind code of ref document: A2

Designated state(s): KE LS MW SD SZ UG AT BE CH DE DK ES FI FR GB GR IE IT LU MC NL PT SE BF BJ CF CG CI CM GA GN ML

DFPE Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101)
121 Ep: the epo has been informed by wipo that ep was designated in this application
REG Reference to national code

Ref country code: DE

Ref legal event code: 8642

122 Ep: pct application non-entry in european phase
NENP Non-entry into the national phase

Ref country code: CA