WO1996013680B1 - Multi-layer fuel and vapor tube - Google Patents
Multi-layer fuel and vapor tubeInfo
- Publication number
- WO1996013680B1 WO1996013680B1 PCT/US1995/013570 US9513570W WO9613680B1 WO 1996013680 B1 WO1996013680 B1 WO 1996013680B1 US 9513570 W US9513570 W US 9513570W WO 9613680 B1 WO9613680 B1 WO 9613680B1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- layer
- fluoride
- thermoplastic
- tubing
- vinylidine
- Prior art date
Links
- 239000000446 fuel Substances 0.000 title 1
- 229920001169 thermoplastic Polymers 0.000 claims abstract 25
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract 25
- 229920002725 Thermoplastic elastomer Polymers 0.000 claims abstract 7
- 229920002313 fluoropolymer Polymers 0.000 claims abstract 6
- 230000003993 interaction Effects 0.000 claims abstract 3
- 239000000463 material Substances 0.000 claims 21
- 229920001577 copolymer Polymers 0.000 claims 18
- KRHYYFGTRYWZRS-UHFFFAOYSA-M fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims 13
- 239000000203 mixture Substances 0.000 claims 12
- 229920001971 elastomer Polymers 0.000 claims 9
- 229920002620 polyvinyl fluoride Polymers 0.000 claims 9
- CYXIKYKBLDZZNW-UHFFFAOYSA-N 2-Chloro-1,1,1-trifluoroethane Chemical compound FC(F)(F)CCl CYXIKYKBLDZZNW-UHFFFAOYSA-N 0.000 claims 8
- 239000000956 alloy Substances 0.000 claims 8
- 229910045601 alloy Inorganic materials 0.000 claims 8
- 239000005060 rubber Substances 0.000 claims 8
- 239000004020 conductor Substances 0.000 claims 5
- 229920000098 polyolefin Polymers 0.000 claims 4
- 229920000915 polyvinyl chloride Polymers 0.000 claims 4
- 239000004800 polyvinyl chloride Substances 0.000 claims 4
- XUCNUKMRBVNAPB-UHFFFAOYSA-N Vinyl fluoride Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 claims 3
- 229920002635 polyurethane Polymers 0.000 claims 3
- 239000004814 polyurethane Substances 0.000 claims 3
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims 2
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 239000004811 fluoropolymer Substances 0.000 claims 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- LCJRHAPPMIUHLH-UHFFFAOYSA-N 1-$l^{1}-azanylhexan-1-one Chemical compound [CH]CCCCC([N])=O LCJRHAPPMIUHLH-UHFFFAOYSA-N 0.000 claims 1
- GUOSQNAUYHMCRU-UHFFFAOYSA-N 11-Aminoundecanoic acid Chemical compound NCCCCCCCCCCC(O)=O GUOSQNAUYHMCRU-UHFFFAOYSA-N 0.000 claims 1
- UUAGAQFQZIEFAH-UHFFFAOYSA-N Chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 claims 1
- 229920000840 ETFE Polymers 0.000 claims 1
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 claims 1
- 229920000571 Nylon 11 Polymers 0.000 claims 1
- 229920000299 Nylon 12 Polymers 0.000 claims 1
- 229920002292 Nylon 6 Polymers 0.000 claims 1
- 239000004743 Polypropylene Substances 0.000 claims 1
- JIAARYAFYJHUJI-UHFFFAOYSA-L Zinc chloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- 239000000806 elastomer Substances 0.000 claims 1
- QHSJIZLJUFMIFP-UHFFFAOYSA-N ethene;1,1,2,2-tetrafluoroethene Chemical group C=C.FC(F)=C(F)F QHSJIZLJUFMIFP-UHFFFAOYSA-N 0.000 claims 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 1
- 229910052737 gold Inorganic materials 0.000 claims 1
- 239000010931 gold Substances 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- -1 polypropylene Polymers 0.000 claims 1
- 229920001155 polypropylene Polymers 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- 229910052709 silver Inorganic materials 0.000 claims 1
- 239000004332 silver Substances 0.000 claims 1
- BQCADISMDOOEFD-UHFFFAOYSA-N silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 1
- 235000005074 zinc chloride Nutrition 0.000 claims 1
- 239000011592 zinc chloride Substances 0.000 claims 1
- 150000007824 aliphatic compounds Chemical class 0.000 abstract 1
- 150000001491 aromatic compounds Chemical class 0.000 abstract 1
Abstract
A layered tubing (10) for use in a motor vehicle composed of a thick outer layer (12) having an inner and an outer face, the outer layer (12) made of an extrudable thermoplastic elastomer; a thin intermediate bonding layer (14) bonded to the inner face of the thick outer layer (12), the bonding layer (14) composed of an extrudable melt-processible thermoplastic capable of sufficiently permanent laminar adhesion with the thick outer layer (12); an interior layer (16) bonded to the intermediate bonding layer (14), the interior layer (16) composed of a fluoroplastic which is resistant to permeation by and interaction with short-chain aliphatic and aromatic compounds; and an innermost electrostatic dissipation layer (18).
Claims
AMENDED CLAIMS
[received by the International Bureau on 5 June 1996 (05.06.96); original claim 16 cancelled; original claims 1,14,17 and 19 amended; remaining claims unchanged (7 pages)] 1. A layered tubing for use in a motor vehicle, the tubing comprising: a thick flexible outer layer having a given thickness and an inner and an outer face, the outer layer consisting essentially of an extrudable thermoplastic; an intermediate bonding layer bonded to the inner face of the thick outer layer, the bonding layer consisting essentially of an extrudable melt processible thermoplastic material capable of sufficiently permanent laminar adhesion to the inner face of the outer layer, wherein the thermoplastic material employed in the bonding layer consists essentially of: a thermoplastic elastomeric compound selected from the group consisting of alloys of rubber and polyvinyl chloride, alloys of rubber and polyolefin and mixtures thereof; and a fluoropolymer selected from the group consisting of polyvinylidine fluoride, polyvinyl fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinylidine fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinyl fluoride, and mixtures thereof; an interior layer bonded to the intermediate bonding layer, the interior layer consisting essentially of an extrudable, melt-processible thermoplastic material capable of sufficiently permanent laminar adhesion with the intermediate bonding layer, the melt-processible thermoplastic which is chemically dissimilar to the thermoplastic employed in the outer layer, the chemically dissimilar thermoplastic being resistant to permeation by the interaction with short-chain aliphatic and aromatic hydrocarbon compounds; and an innermost electrostatic dissipation layer integrally bonded to the interior layer, the electrostatic dissipation layer consisting of an extrudable, melt-processible thermoplastic material the intermediate bonding layer and of dissipating electrostatic energy, the electrostatic dissipation capacity being in a range between about 104 to 109 ohm/cm2.
2. The layered tubing of claim 1 wherein the thick flexible outer layer consists essentially of a thermoplastic elastomer selected from the group consisting of alloys, rubber and polyvinyl chloride, alloys of rubber and polyolefins and mixtures thereof.
ED SHEET ARTICLE 1fl - 26 - 3. The layered tubing of claim 3 wherein the thermoplastic elastomer has an ability to withstand impacts of at least 2 foot pounds at temperatures below about -20°C.
4. The layered tubing of claim 4 wherein the thermoplastic elastomer has an elongation value of 150% at 23°C.
5. The layered tubing of claim 2 wherein the interior layer is a composed of thermoplastic material consisting essentially of a fluoroplastic material selected from the group consisting of polyvinylidine fluoride, polyvinyl fluoride, and mixtures thereof.
6. The layered tubing of claim 5 wherein the fluoroplastic material further consists of copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinylidine fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinyl fluoride, and mixtures thereof.
7. The layered tubing of claim 5 wherein the interior layer has a thickness between about 10% and about 20% of the thick outer layer.
8. The layered tubing of claim 2 wherein the innermost electrostatic dissipation layer consists of a thermoplastic material which is chemically dissimilar to the thick outer layer.
9. The layered tubing of claim 8 wherein the innermost electrostatic dissipation layer is composed of a thermoplastic material consisting essentially of: a copolymer of a vinyl fluoride and chlorotrifluoroethylene, the vinyl fluoride material - 27 - selected from the group consisting of polyvinylidine fluoride, polyvinyl fluoride, and mixtures thereof; a copolymer of a vinyl fluoride material and ethylene tetrafluoroethylene; and a non-fluorinated elastomer comprising polyurethane.
10. The layered tubing of claim 9 wherein the electrostatic dissipation layer consists essentially of: between about 10% and about 18% by weight of a vinylidine fluoride-chlorotrifluoroethylene copolymer, the copolymer having between about 40% and 60% by weight vinylidine fluoride; between about 50% and about 70% by weight of a vinylidine fluoride-tetrafluoroethylene copolymer, the copolymer having between about 40% and about 60% by weight vinylidine fluoride; and between about 10% and about 25% by weight polyurethane.
11. The layered tubing of claim 8 wherein the innermost electrostatic dissipation has a thickness between about 10% and about 20% of the thick outer layer.
12. The layered tubing of claim 11 wherein the innermost electrostatic dissipation layer further contains quantities of a conductive material sufficient to provide electrostatic dissipation capability in a range between about 104 and about 109 of ohm/cm2.
13. The layered tubing of claim 9 wherein the conductive material is selected from a group consisting of elemental carbon, copper, silver, gold, nickel, silicon, and mixtures thereof.
14. The layered tubing of claim 9 wherein the conductive material is present in an amount less than - 28 - about 5% by volume of the electrostatic dissipation layer thermoplastic material.
15. The layered tubing of claim 9 wherein the conductive material is interstitially integrated into the electrostatic dissipation layer thermoplastic material.
Claim 16 is cancelled.
17. The layered tubing of claim 17 wherein the thermoplastic elastomeric compound employed in the bonding layer is a thermoplastic vulcanate present in an amount between about 30% and 70% by volume of the total thermoplastic material, the balance being the fluoropolymer.
18. The tubing of claim 1 further comprising an exterior jacket overlying the thick outer tubing, the exterior jacket composed of a material consisting essentially of a thermoplastic material selected from the group consisting of Nylon 11, Nylon 12, zinc chloride resistant Nylon 6, polypropylene, thermoplastic elastomers and mixtures thereof.
19. A layered tubing for use in a motor vehicle, the tubing comprising:
- 29 - a thick flexible outer tubing having a given thickness and an inner and an outer face, the outer tubing consisting essentially of an extrudable thermoplastic elastomer selected from the group consisting of alloys of rubber and polyolefin, alloys of rubber and polyvinyl chloride, and mixtures thereof; an intermediate bonding layer having a thickness between about 0.05 mm and about 0.1 mm bonded to the inner face of the thick outer layer, the bonding layer consisting essentially of an extrudable thermoplastic capable of sufficiently permanent laminar adhesion to the thick flexible outer tubing; an interior layer bonded to the intermediate bonding layer, the interior layer having a thickness between about 0.05 mm and about 0.15 mm and consisting essentially of an extrudable, melt-processible thermoplastic material capable of sufficiently permanent laminar adhesion with the intermediate bonding layer, the melt-processible thermoplastic resistant to permeation by and interaction with short-chain aliphatic and aromatic hydrocarbon compounds selected from the group consisting of polyvinylidine fluoride, polyvinyl fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinylidine fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinyl fluoride, and mixtures thereof; and an innermost electrostatic dissipation layer integrally bonded to the interior layer, the electrostatic discharge layer having a thickness between about 0.1 mm and about 0.2 mm and consisting essentially of an extrudable, melt-processible thermoplastic material capable of sufficiently permanent laminar adhesion with the intermediate bonding layer and of dissipating electrostatic energy, the electrostatic dissipation capacity being in a range between about 104 and about - 30 - 109 ohm/cm2, the melt-processible thermoplastic employed in the innermost electrostatic dissipation layer consisting essentially of: between about 10% and about 18% by weight of a vinylidine fluoride-chlorotrifluoroethylene copolymer, the copolymer having between about 40% and 60% by weight vinylidine fluoride; between about 50% and about 70% by weight of a vinylidine fluoride-tetrafluoroethylene copolymer, the copolymer having between about 40% and about 60% by weight vinylidine fluoride; and between about 10% and about 25% by weight polyurethane.
20. The layered tubing of claim 19 wherein the intermediate bonding layer consists essentially of: a thermoplastic elastomer selected from the group consisting of alloys of rubber and polyvinyl chloride, alloys of rubber and polyolefins, and mixtures thereof; and a fluoroplastic selected from the group consisting of polyvinylidine fluoride, polyvinyl fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinylidine fluoride, copolymers of vinylidine difluoride and chlorotrifluoroethane copolymerized with polyvinyl fluoride, and mixtures thereof.
- 31 -
STATEMENT UNDER ARTICLE 19
Claims l and 12 have been amended to clarify the electrostatic dissipation capacity defined therein. This electrostatic dissipation capacity as now expressed conforms with the disclosure in the specification of the amount of conductive material which can be employed in the thermoplastic material. Analogous, correction of the specification will be presented in due course during prosecution.
Claim 1 has been further amended to more particularly define the material employed in the intermediate bonding layer; defining this material away from that disclosed in the cited references.
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP51465596A JP3356288B2 (en) | 1994-10-27 | 1995-10-11 | Multilayer fuel and steam tubes |
EP95939555A EP0788589B1 (en) | 1994-10-27 | 1995-10-11 | Multi-layer fuel and vapor tube |
DE69526741T DE69526741T2 (en) | 1994-10-27 | 1995-10-11 | MULTILAYER FUEL AND STEAM PIPE |
AT95939555T ATE217692T1 (en) | 1994-10-27 | 1995-10-11 | MULTI-LAYER FUEL AND STEAM PIPE |
BR9509437A BR9509437A (en) | 1994-10-27 | 1995-10-11 | Multi-layered steam and fuel pipe |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/329,900 US5743304A (en) | 1992-04-14 | 1994-10-27 | Multi-layer fuel and vapor tube |
US08/329,900 | 1994-10-27 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO1996013680A1 WO1996013680A1 (en) | 1996-05-09 |
WO1996013680B1 true WO1996013680B1 (en) | 1996-07-18 |
Family
ID=23287504
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US1995/013570 WO1996013680A1 (en) | 1994-10-27 | 1995-10-11 | Multi-layer fuel and vapor tube |
Country Status (7)
Country | Link |
---|---|
US (1) | US5743304A (en) |
EP (3) | EP1120240B2 (en) |
JP (1) | JP3356288B2 (en) |
AT (3) | ATE285539T1 (en) |
BR (1) | BR9509437A (en) |
DE (3) | DE69533880T9 (en) |
WO (1) | WO1996013680A1 (en) |
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DE3901928C1 (en) * | 1989-01-24 | 1990-03-08 | Technoform Caprano + Brunnhofer Kg, 3501 Fuldabrueck, De | |
US5142782A (en) * | 1989-02-02 | 1992-09-01 | Teleflex Incorporated | Coated braided hose method and assembly |
DE4001125C1 (en) * | 1989-11-20 | 1990-12-13 | Technoform Caprano + Brunnhofer Kg, 3501 Fuldabrueck, De | |
DE9007303U1 (en) * | 1989-11-20 | 1990-12-20 | Technoform Caprano + Brunnhofer KG, 3501 Fuldabrück | Plastic automotive piping manufactured by coextrusion |
DE3942353A1 (en) * | 1989-12-21 | 1991-06-27 | Tecalemit Gmbh Deutsche | Strong, flexible laminar thermoplastic pipe - has innermost impervious lining bonded to mechanically strong layer, then braiding for reinforcement, and outermost thermoplastic sleeve |
DE4006870C2 (en) | 1990-03-05 | 1998-04-23 | Inventa Ag | Fuel line |
US5143122A (en) * | 1990-09-11 | 1992-09-01 | Bundy Corporation | Composite flexible conduit assembly |
US5441782A (en) * | 1991-07-16 | 1995-08-15 | Central Glass Company, Limited | Plastic laminate having polyamide resin surface layer and fluororesin surface layer |
JPH085167B2 (en) * | 1992-01-06 | 1996-01-24 | パイロット インダストリーズ、インコーポレイテッド | Fluoropolymer composite tube and method of manufacturing the same |
US5524673A (en) * | 1992-04-14 | 1996-06-11 | Itt Corporation | Multi-layer tubing having electrostatic dissipation for handling hydrocarbon fluids |
DE69331071T2 (en) * | 1992-04-14 | 2002-03-21 | Itt Mfg Enterprises Inc | Multi-layer fuel and steam hose |
DE69326766T2 (en) * | 1992-06-11 | 2000-03-02 | Itt Mfg Enterprises Inc | MULTILAYER FUEL AND STEAM PIPE |
WO1996000657A1 (en) * | 1994-06-30 | 1996-01-11 | Cadillac Rubber & Plastics, Inc. | Composite fuel and vapor barrier tube and process for making same |
-
1994
- 1994-10-27 US US08/329,900 patent/US5743304A/en not_active Expired - Lifetime
-
1995
- 1995-10-11 AT AT00116767T patent/ATE285539T1/en not_active IP Right Cessation
- 1995-10-11 BR BR9509437A patent/BR9509437A/en not_active IP Right Cessation
- 1995-10-11 JP JP51465596A patent/JP3356288B2/en not_active Expired - Fee Related
- 1995-10-11 DE DE69533880T patent/DE69533880T9/en not_active Revoked
- 1995-10-11 EP EP01109314A patent/EP1120240B2/en not_active Expired - Lifetime
- 1995-10-11 WO PCT/US1995/013570 patent/WO1996013680A1/en active IP Right Grant
- 1995-10-11 DE DE69526741T patent/DE69526741T2/en not_active Expired - Fee Related
- 1995-10-11 AT AT01109314T patent/ATE262136T1/en not_active IP Right Cessation
- 1995-10-11 EP EP00116767A patent/EP1059478B1/en not_active Revoked
- 1995-10-11 AT AT95939555T patent/ATE217692T1/en active
- 1995-10-11 EP EP95939555A patent/EP0788589B1/en not_active Expired - Lifetime
- 1995-10-11 DE DE69532731T patent/DE69532731T3/en not_active Expired - Fee Related
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