WO1987006800A1 - Treatment of soybeans - Google Patents

Treatment of soybeans Download PDF

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Publication number
WO1987006800A1
WO1987006800A1 PCT/AU1987/000135 AU8700135W WO8706800A1 WO 1987006800 A1 WO1987006800 A1 WO 1987006800A1 AU 8700135 W AU8700135 W AU 8700135W WO 8706800 A1 WO8706800 A1 WO 8706800A1
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WO
WIPO (PCT)
Prior art keywords
sbm
temperature
treatment
moisture content
soybean
Prior art date
Application number
PCT/AU1987/000135
Other languages
French (fr)
Inventor
Thomas John Rowland
Original Assignee
Thomas John Rowland
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Thomas John Rowland filed Critical Thomas John Rowland
Priority to KR1019880700013A priority Critical patent/KR880701077A/en
Publication of WO1987006800A1 publication Critical patent/WO1987006800A1/en

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L11/00Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L11/00Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
    • A23L11/30Removing undesirable substances, e.g. bitter substances
    • A23L11/31Removing undesirable substances, e.g. bitter substances by heating without chemical treatment, e.g. steam treatment, cooking
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L11/00Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
    • A23L11/05Mashed or comminuted pulses or legumes; Products made therefrom
    • A23L11/07Soya beans, e.g. oil-extracted soya bean flakes

Definitions

  • the present invention relates to a process and plant for the treatment of soybean meal (SBM) to reduce the levels of trypsin inhibitor and urease present in raw SBM while substantially preserving the nutritionally available lysine content of the SBM, and to the product produced by this process.
  • SBM soybean meal
  • Soybean meal is of particular use in animal feeds as a protein source, however, raw soybeans contain proteolytic-inhibiting substances and urease.
  • the most important proteolytic inhibiting substance in animal nutrition is trypsin inhibitor. Trypsin is an enzyme produced in the pancreas and is required for protein digestion. It is known that raw soybeans, due to their trypsin inhibitor content, cause an enlargement of the pancreas and have a growth retarding effect on the growth of chicks.
  • US Patents 3,220,851 and 3,845,229 are directed toward processes for the treatment of soybean involving adjusting the pH of the soybeans to 8-9 by adding an alkali and then cooking the soybeans with steam at a temperature of 100-110°C.
  • the process exemplified in US 3,220,851 also involves the use of a proteolytic enzyme in the treatment process, whilst US 3,845,229 exemplifies the use of urea to raise the pH of treatment mixture and the use of solvent to extract oil from the soybean.
  • British Patent Specification 1,459,422 also relates to adjusting the pH of the soybeans prior to heating, however, in contrast to the US patents discussed above, this specification relates to a method of treatment in which the pH is adjusted to less than 5.5 prior to heating.
  • the combined teaching of this prior art is that if soybeans are to be treated to destroy trypsin inhibitor whilst preserving other nutritionally important protein content of the soybean, it is essential that the pH be controlled. Contrary to the teaching of this prior art the present inventor has discovered that no pH control is required providing a strict treatment regimen is followed.
  • the present inventor has discovered a soybean treatment process involving 6 steps with no alteration of the natural pH of the soybean. From various trials using this process the present inventor has found that each step is crucial - if one step is omitted a product is obtained in which trypsin inhibitor is still present.
  • the process of the present invention results in a product in which the trypsin inhibitor has been inactivated whilst the lysine present has not been rendered nutrionally unavailable.
  • the present invention consists in a process for the treatment of soybean meal (SBM) , the process comprising the following steps: 1. passing the SBM through a grinding means to grind the SBM;
  • step 3 adding steam to the moistened ground SBM to achieve a moisture content of between 20 and 30% w/w and a temperature of between 100 and 110°C; 4. maintaining the SBM from step 3 at a temperature of between 95° and 105°C for 10 to 30 minutes;
  • step 4 is carried out at a temperature between 100 and 105°C.
  • the moisture content achieved in step 3 is 25% w/w and the duration of step 4 10 is 20 minutes.
  • the grinding means is provided by a ripple mill.
  • the ground SBM is put over a sieve to remove larger particles which are returned to 15 the grinding means.
  • the moisture content and temperature of the pelletized SBM is decreased in a cooler/dryer .to obtain SBM pellets of ambient temperature having a moisture content of 10-12% 20 w/w.
  • the SBM during steps 2 to 5 is agitated to ensure uniform treatment.
  • the pelletized treated SBM is ground in a ripple mill, passed over a sieve to remove large particles, which are returned to the ripple mill, and the finely ground treated SBM stored as a powder.
  • Figure 1 is a flow chart illustrating the process of the present invention.
  • the process for the treatment of SBM can be seen to comprise a number of steps the first being the grinding of raw soybeans in a first ripple mill.
  • the ground SBM is then screened to remove large particles which are returned to the first ripple mill.
  • Moisture is then added to the ground SBM.
  • the moistened SBM is then passed through a first feeder following which the moistened SBM is conditioned by the addition of steam in a first conditioner.
  • the SBM from the first conditioner is then retained in a ripener to allow ripening to occur.
  • the ripened SBM is then passed through a second feeder following which a further addition of steam to the ripened SBM takes place in a second conditioner.
  • the SBM is then pelleted in a pellet mill and the SBM pellets cooled and dried in a cooler/dryer. These SBM pellets are then ground in a second ripple mill and the ground SBM passed through a screener to remove large particles which are returned to the second ripple mill. The finely ground treated SBM is then stored until required. As mentioned previously the contents of the feeders, conditioners and ripener are agitated to ensure thorough mixing.

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Beans For Foods Or Fodder (AREA)
  • Fodder In General (AREA)

Abstract

A method of treating soybean meal (SBM), by application of steam, to remove trypsin inhibitor/urease without destroying nutritionally valuable protein. The process, conducted at the natural pH of the soybean, involves the steps of grinding the soybean, adding moisture, raising the temperature to between 100 and 110°C and the moisture content to between 20 and 30 % (W/W) by the addition of steam, maintaining the SBM at between 95 and 105°C for 10 to 30 minutes, reheating the SBM to between 100 and 110°C with steam, and pelletizing the treated SBM.

Description

TREATMENT OF SOYBEANS
The present invention relates to a process and plant for the treatment of soybean meal (SBM) to reduce the levels of trypsin inhibitor and urease present in raw SBM while substantially preserving the nutritionally available lysine content of the SBM, and to the product produced by this process.
Soybean meal is of particular use in animal feeds as a protein source, however, raw soybeans contain proteolytic-inhibiting substances and urease. The most important proteolytic inhibiting substance in animal nutrition is trypsin inhibitor. Trypsin is an enzyme produced in the pancreas and is required for protein digestion. It is known that raw soybeans, due to their trypsin inhibitor content, cause an enlargement of the pancreas and have a growth retarding effect on the growth of chicks.
It is therefore common practice to heat raw soybeans to destroy the trypsin inhibitor, however, too much heat can destroy the protein contained in the SBM while not enough will result in the SBM containing active trypsin inhibitor. Steam heat will destroy proteolytic-inhibiting substances, however overheating will destroy or render unavailable several essential amino acids particularly lysine and arginine. In order to overcome this problem of heating to destroy trypsin inhibitor resulting in an accompanying destruction of nutritionally valuable protein in the soybean it has been proposed to conduct the treatment at certain pHs. In this regard US Patents 3,220,851 and 3,845,229 are directed toward processes for the treatment of soybean involving adjusting the pH of the soybeans to 8-9 by adding an alkali and then cooking the soybeans with steam at a temperature of 100-110°C. The process exemplified in US 3,220,851 also involves the use of a proteolytic enzyme in the treatment process, whilst US 3,845,229 exemplifies the use of urea to raise the pH of treatment mixture and the use of solvent to extract oil from the soybean.
British Patent Specification 1,459,422 also relates to adjusting the pH of the soybeans prior to heating, however, in contrast to the US patents discussed above, this specification relates to a method of treatment in which the pH is adjusted to less than 5.5 prior to heating. The combined teaching of this prior art is that if soybeans are to be treated to destroy trypsin inhibitor whilst preserving other nutritionally important protein content of the soybean, it is essential that the pH be controlled. Contrary to the teaching of this prior art the present inventor has discovered that no pH control is required providing a strict treatment regimen is followed. The present inventor has discovered a soybean treatment process involving 6 steps with no alteration of the natural pH of the soybean. From various trials using this process the present inventor has found that each step is crucial - if one step is omitted a product is obtained in which trypsin inhibitor is still present.
The process of the present invention results in a product in which the trypsin inhibitor has been inactivated whilst the lysine present has not been rendered nutrionally unavailable.
The present invention consists in a process for the treatment of soybean meal (SBM) , the process comprising the following steps: 1. passing the SBM through a grinding means to grind the SBM;
2. adding moisture to the ground SBM;
3. adding steam to the moistened ground SBM to achieve a moisture content of between 20 and 30% w/w and a temperature of between 100 and 110°C; 4. maintaining the SBM from step 3 at a temperature of between 95° and 105°C for 10 to 30 minutes;
5. adding steam to the SBM from step 4 to raise the temperature of the SBM to between 100 and 110°C; and
5 6. pelletizing the SBM by means of a pelleting mill. In a preferred embodiment of the present invention step 4 is carried out at a temperature between 100 and 105°C. In a further embodiment the moisture content achieved in step 3 is 25% w/w and the duration of step 4 10 is 20 minutes.
In a further preferred embodiment of the present invention the grinding means is provided by a ripple mill. In a further embodiment the ground SBM is put over a sieve to remove larger particles which are returned to 15 the grinding means.
In another embodiment of the present invention the moisture content and temperature of the pelletized SBM is decreased in a cooler/dryer .to obtain SBM pellets of ambient temperature having a moisture content of 10-12% 20 w/w.
In a further embodiment of the present invention the SBM during steps 2 to 5 is agitated to ensure uniform treatment.
In yet another preferred embodiment of the present 25 invention the pelletized treated SBM is ground in a ripple mill, passed over a sieve to remove large particles, which are returned to the ripple mill, and the finely ground treated SBM stored as a powder.
The invention will now be described by means of an 30 example. , It has been shown that destruction of urease in SBM by heat treatment, approximately parallels the destruction ^ of trypsin inhibitor. As urease activity is readily measured this criteria is used as an index of the adequacy 35 of soybean treatment. Table 1 shows the results of different treatment regimes. Sample 1, untreated ground soybean; Sample 2, 10 minute heat soak then pelleted; Sample 3, 15 minute heat soak then pelleted; Sample 4, 20 minute heat soak then pelleted; Sample 5, 5% moisture precondition, 10 minute heat soak then pelleted; Sample 6, 5% moisture precondition, 15 minute heat soak then pelleted; Sample 7, 5% moisture precondition, 20 minute heat soak then pelleted. The soybean in each case was ground as fine as possible and the heat soak was carried out in sealed plastic drums.
TABLE 1
SAMPLE UREASE ACTIVITY AVAILABLE LYSINE
( pH) (%)
1 2.17 1.60/1.72 2 0.20 3 0.13 4 0.18 1.82/1.86 5 0.08 6 0.01 7 0.00 1.73/1.72
Hereinafter, given by way of example only, are preferred embodiments of the present invention described with reference to the accompanying drawing in which:
Figure 1 is a flow chart illustrating the process of the present invention.
With reference to Fig. 1 the process for the treatment of SBM according to a preferred embodiment of the present invention can be seen to comprise a number of steps the first being the grinding of raw soybeans in a first ripple mill. The ground SBM is then screened to remove large particles which are returned to the first ripple mill. Moisture is then added to the ground SBM. The moistened SBM is then passed through a first feeder following which the moistened SBM is conditioned by the addition of steam in a first conditioner. The SBM from the first conditioner is then retained in a ripener to allow ripening to occur. The ripened SBM is then passed through a second feeder following which a further addition of steam to the ripened SBM takes place in a second conditioner. The SBM is then pelleted in a pellet mill and the SBM pellets cooled and dried in a cooler/dryer. These SBM pellets are then ground in a second ripple mill and the ground SBM passed through a screener to remove large particles which are returned to the second ripple mill. The finely ground treated SBM is then stored until required. As mentioned previously the contents of the feeders, conditioners and ripener are agitated to ensure thorough mixing.

Claims

CLAIMS :
1. A process for the treatment of soybean meal (SBM), the process comprising the following steps:
1. passing the SBM through a grinding means to grind the SBM;
2. adding moisture to the ground SBM;
3. adding steam to the moistened ground SBM to achieve a moisture content of between 20 and 30% w/w and a temperature of between 100 and 110°C;
4. maintaining the SBM from step 3 at a temperature of between 95° and 105°C for 10 to 30 minutes;
5. adding steam to the SBM from step 4 to raise the temperature of the SBM to between 100 and 110°C; and
6. pelletizing the SBM by means of a pelleting mill.
2. A process as claimed in claim 1 in which at step 4 the SBM is maintained at temperature of between 100 and 105°C.
3. A process as claimed in either claim 1 or 2 in which the moisture content achieved in step 3 is 25% w/w and the duration of step 4 is 20 minutes.
4. A process as claimed in any one of claims 1 to 3 further comprising the step of decreasing the moisture content and temperature of the pelletized SBM in a cooler/dryer to obtain treated SBM pellets of ambient temperature having a moisture content of 10 to 12% w/w.
5. A process as claimed in any one of claims 1 to 4 in which the grinding means is a ripple mill.
6. A process as claimed in any one of claims 1 to 5 further comprising the steps of assaying the SBM following grinding to remove large particles and returning the large particles to the ripple mill.
7. A process as claimed in any one of claims 1 to 6 in which the SBM during steps 2 to 5 is agitated to ensure uniform treatment.
Figure imgf000009_0001
8. Pelletized soybean meal obtained according to process as claimed in any one of claims 1 to 7.
9. A process for the treatment of soybean meal substantially as hereinbefore described with reference to the accompanying drawing.
f.
PCT/AU1987/000135 1986-05-12 1987-05-12 Treatment of soybeans WO1987006800A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1019880700013A KR880701077A (en) 1986-05-12 1987-05-12 Soybean Treatment

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AUPH5855 1986-05-12
AUPH585586 1986-05-12

Publications (1)

Publication Number Publication Date
WO1987006800A1 true WO1987006800A1 (en) 1987-11-19

Family

ID=3771611

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/AU1987/000135 WO1987006800A1 (en) 1986-05-12 1987-05-12 Treatment of soybeans

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JP (1) JPH01502316A (en)
KR (1) KR880701077A (en)
AU (1) AU596423B2 (en)
WO (1) WO1987006800A1 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8993036B2 (en) * 2010-03-12 2015-03-31 Otsuka Pharmaceutical Co., Ltd. Method for producing soybeans having reduced urease content
CN111671050A (en) * 2020-07-30 2020-09-18 广东华大生物实业股份有限公司 Process for removing urease from whole soybeans

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU280733A1 (en) *
GB1400470A (en) * 1972-07-28 1975-07-16 Kwee Seong Lo Process for preparing a soybean beverage
AU1099076A (en) * 1975-03-03 1977-08-18 Archer Daniels Midland Company Process for preparing soy protein concentrate
US4194018A (en) * 1976-10-08 1980-03-18 Societe D'assistance Technique Pour Produits Nestle S.A. Method of producing an aqueous soya suspension
US4359480A (en) * 1977-05-17 1982-11-16 Akzo N.V. Production of a soybean meal
WO1984000476A1 (en) * 1982-08-05 1984-02-16 Victor Markus Lewis Soybean products
SU1118334A1 (en) * 1982-11-29 1984-10-15 Одесский технологический институт пищевой промышленности им.М.В.Ломоносова Method of reducing the content of trypsin inhibitor in soybean seeds
WO1985000728A1 (en) * 1981-03-13 1985-02-28 The Edlong Corporation Soymilk process

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2407088A (en) * 1987-10-23 1989-04-27 Keith Waldon Gray Soybean+legume processing apparatus

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU280733A1 (en) *
AU2017956A (en) * 1956-07-25 1957-01-31 Duchange Guillaume Process of obtaining non-bitter stabilizedsoya bean flour, product thus obtained and applications thereof and plant for carrying out said process
AU5565865A (en) * 1964-03-06 1966-08-25 Nago Nabrmittel Ag A method forthe production of soymilk extract
AU2047870A (en) * 1970-04-06 1972-03-30 Triple `f', Inc. Method and machine for treating soybeans
GB1400470A (en) * 1972-07-28 1975-07-16 Kwee Seong Lo Process for preparing a soybean beverage
AU1099076A (en) * 1975-03-03 1977-08-18 Archer Daniels Midland Company Process for preparing soy protein concentrate
US4194018A (en) * 1976-10-08 1980-03-18 Societe D'assistance Technique Pour Produits Nestle S.A. Method of producing an aqueous soya suspension
US4359480A (en) * 1977-05-17 1982-11-16 Akzo N.V. Production of a soybean meal
WO1985000728A1 (en) * 1981-03-13 1985-02-28 The Edlong Corporation Soymilk process
WO1984000476A1 (en) * 1982-08-05 1984-02-16 Victor Markus Lewis Soybean products
SU1118334A1 (en) * 1982-11-29 1984-10-15 Одесский технологический институт пищевой промышленности им.М.В.Ломоносова Method of reducing the content of trypsin inhibitor in soybean seeds

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
CHEMICAL ABSTRACTS, Volume 102, No. 3, issued 1985, January 21 (Columbus, Ohio, USA), B.V. EGOROV et al.: "Decreasing the Content of a Trypsin Inhibitor in Soybeans", see page 574, column 1, Abstract No. 232335; & SU,A,1118334. *
DERWENT ABSTRACT, Accession No. 71-49843S/30, Class D13; & SU,A,280733 (RZHEKHIN V.P. et al.), 24 November 1970 (24.11.70). *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8993036B2 (en) * 2010-03-12 2015-03-31 Otsuka Pharmaceutical Co., Ltd. Method for producing soybeans having reduced urease content
CN111671050A (en) * 2020-07-30 2020-09-18 广东华大生物实业股份有限公司 Process for removing urease from whole soybeans
CN111671050B (en) * 2020-07-30 2021-11-16 广州同康生物科技有限公司 Process for removing urease from whole soybeans

Also Published As

Publication number Publication date
JPH01502316A (en) 1989-08-17
KR880701077A (en) 1988-07-25
AU596423B2 (en) 1990-05-03
AU7398587A (en) 1987-12-01

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