WO1981001578A1 - Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series - Google Patents

Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series Download PDF

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Publication number
WO1981001578A1
WO1981001578A1 PCT/SU1979/000120 SU7900120W WO8101578A1 WO 1981001578 A1 WO1981001578 A1 WO 1981001578A1 SU 7900120 W SU7900120 W SU 7900120W WO 8101578 A1 WO8101578 A1 WO 8101578A1
Authority
WO
WIPO (PCT)
Prior art keywords
results
ugleροdnyχ
acid
concentration
ions
Prior art date
Application number
PCT/SU1979/000120
Other languages
English (en)
French (fr)
Russian (ru)
Inventor
D Ashurov
A Akhmedov
D Bairamov
N Babaev
G Tedoradze
Original Assignee
Inst Elektrokhimii
Inst Chlororgan Sint
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inst Elektrokhimii, Inst Chlororgan Sint filed Critical Inst Elektrokhimii
Priority to PCT/SU1979/000120 priority Critical patent/WO1981001578A1/ru
Priority to DE792953906T priority patent/DE2953906A1/de
Priority to JP50015879A priority patent/JPS56501613A/ja
Priority to GB8121898A priority patent/GB2075095A/en
Publication of WO1981001578A1 publication Critical patent/WO1981001578A1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C25B3/20—Processes
    • C25B3/27—Halogenation

Definitions

  • P ⁇ lucheyuschzyasya s ⁇ lyanaya ⁇ isl ⁇ a is ⁇ lzue ⁇ sya for further gene ⁇ atsii ⁇ l ⁇ a ⁇ ⁇ ea ⁇ tsii 2 ( ⁇ .e. ⁇ edla- gzemym s ⁇ s ⁇ b ⁇ y ⁇ eshae ⁇ sya ⁇ bleya u ⁇ ilizetsii ⁇ b ⁇ azuyu- scheysya abgazn ⁇ y s ⁇ lyan ⁇ y ⁇ isl ⁇ y) and ⁇ l ⁇ n ⁇ va ⁇ is ⁇ eya ⁇ isl ⁇ a vs ⁇ u ⁇ ze ⁇ in ⁇ ea ⁇ tsiyu ⁇ l ⁇ g ⁇ d ⁇ sili ⁇ veniya with ne ⁇ e- delnyy uglev ⁇ d ⁇ d ⁇ y, ne ⁇ ime ⁇ . Allyloles: ⁇ ns ⁇ ⁇ cn ⁇ cn nd
  • elec- toralysis is subject to the concentration of ions in the electorate of the 1–4th city, - in Lithuania,
  • CZESI is unprofitable, as it is also a waste of electronic power.
  • electrically discharged rising above 75 ° C, the sputtering of the original non-weekly carbohydrates deteriorates. Injection through dust and waste in
  • ⁇ edlagaey ⁇ m s ⁇ s ⁇ be y ⁇ zhn ⁇ is ⁇ lz ⁇ - va ⁇ , ne ⁇ iye ⁇ , ⁇ l ⁇ is ⁇ y allyl, divinyl (bu ⁇ adien- -1,3) iz ⁇ en (2-me ⁇ ilbu ⁇ edien- ⁇ , 3), pyrene (1,3- -pentzedien).
  • Electricity can be made from any source of energy, stable to the effect of eroded salty acid and hydrogen, and there is no harm to it.
  • the cooling system is switched on and the temperature is maintained at 60-65 ° C.
  • food and water are used.
  • Salted acid that is produced by this reaction can be used for further generation of chlorine, and acid that can be removed from the skin is in contact with elastomer
  • Condensed salted acid increases in elec- trulizere, a mixture of hydrogen and elastomeric acid, which is easily degradable
  • the last call is returned to the device, and the network is returned to the electric drive.
  • the appliance comes through a separate source of calcium, which is an indication of the lack of alcohol, after which it burns.
  • the resulting product is distinguished by a vacant divergent after the release of water.
  • ⁇ e ⁇ iy ⁇ b ⁇ ez ⁇ y increase ⁇ ntsen ⁇ etsii i ⁇ n ⁇ v ⁇ l ⁇ - ⁇ e in ele ⁇ li ⁇ e above 4 g-i ⁇ n ⁇ v in li ⁇ e ⁇ iv ⁇ di ⁇ ⁇ znzchi ⁇ eln ⁇ mu ⁇ vysheniyu vy ⁇ dz ⁇ b ⁇ chny ⁇ ⁇ du ⁇ v and s ⁇ - 30 ⁇ ve ⁇ s ⁇ venn ⁇ susches ⁇ venn ⁇ yu ⁇ edeniyu vy ⁇ de tselev ⁇ g ⁇ ⁇ du ⁇ e.
  • the process is subject to conditions of 2, but the most concentrated concentration of ions in the electricity makes 35 0.7 g-sources in Lithuania.
  • the process is carried out under conditions of 2, but at a temperature of 80 ° C.
  • Example 2 The process is carried out under the conditions of Example 2, but with the same density of 0.30 ⁇ / ⁇ .
  • P ⁇ iye ⁇ 12 P ⁇ tsess ⁇ v ⁇ dya ⁇ in usl ⁇ viya ⁇ ⁇ iy ⁇ e 2 ⁇ l ⁇ vyes ⁇ ⁇ l ⁇ is ⁇ g ⁇ ne ⁇ iya is ⁇ lzuyu ⁇ ⁇ l ⁇ is ⁇ y ⁇ ely with ⁇ z ⁇ iy ⁇ zsche ⁇ y, ch ⁇ by suyyz ⁇ naya ⁇ ntsen ⁇ ztsiya i ⁇ n ⁇ v ⁇ l ⁇ - ⁇ e in ele ⁇ li ⁇ e s ⁇ s ⁇ evlyale Sr-i ⁇ nz in li ⁇ e.
  • the process is subject to conditions of 2, but instead of taking advantage of it, it may result in the risk of being ill-treated.
  • P ⁇ tsess ⁇ v ⁇ dya ⁇ in usl ⁇ viya ⁇ ⁇ iye ⁇ a 2 ⁇ l ⁇ vyes- ⁇ ⁇ l ⁇ is ⁇ g ⁇ neg ⁇ iya is ⁇ lzuyug mixture ⁇ l ⁇ id ⁇ v s ⁇ ntsiya and bz ⁇ iya (ves ⁇ v ⁇ e s ⁇ n ⁇ shenie 1: 1) to ⁇ e ⁇ im ⁇ esche ⁇ m, ch ⁇ by summz ⁇ nzya ⁇ ntsen ⁇ ztsiya i ⁇ n ⁇ v ⁇ l ⁇ z in el ⁇ li ⁇ e s ⁇ s ⁇ zvlyale 3 gram i ⁇ nz in li ⁇ e.
  • the process is carried out under conditions of I, but the endurance of the load is 0, 20 / o.
  • Example 19 (average) ..
  • the process is simple, but in the case of I, but the end-to-end density is 0.50 k / o.
  • the process is subject to conditions of Example 2, only in the case of electricity, there are 15 acid and external products used.
  • the process is subject to the conditions of the highest level of concentration of ions in the electric power of I Mr. in - 13 - lit.
  • EXAMPLE 27 5 The process is carried out under conditions of an increased concentration of ions in the electric power of 1.5 g. In Lithuania.
  • the process is subject to the conditions of the highest concentration of ions in the power supply of the 2nd generation in Lithuania.
  • the process is subject to conditions of I, but the temperature is at 75 ° C,
  • the process is subject to conditions 2, but the temperature is maintained at a temperature of 40 ° C.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Exposure Of Semiconductors, Excluding Electron Or Ion Beam Exposure (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
PCT/SU1979/000120 1979-11-28 1979-11-28 Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series WO1981001578A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
PCT/SU1979/000120 WO1981001578A1 (en) 1979-11-28 1979-11-28 Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series
DE792953906T DE2953906A1 (de) 1979-11-28 1979-11-28 Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series
JP50015879A JPS56501613A (enrdf_load_stackoverflow) 1979-11-28 1979-11-28
GB8121898A GB2075095A (en) 1979-11-28 1979-11-28 Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
WOSU79/00120 1979-11-28
PCT/SU1979/000120 WO1981001578A1 (en) 1979-11-28 1979-11-28 Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series

Publications (1)

Publication Number Publication Date
WO1981001578A1 true WO1981001578A1 (en) 1981-06-11

Family

ID=21616569

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/SU1979/000120 WO1981001578A1 (en) 1979-11-28 1979-11-28 Method of obtaining monochlorohydrin or dichlorohydrin alcohols of saturated series

Country Status (4)

Country Link
JP (1) JPS56501613A (enrdf_load_stackoverflow)
DE (1) DE2953906A1 (enrdf_load_stackoverflow)
GB (1) GB2075095A (enrdf_load_stackoverflow)
WO (1) WO1981001578A1 (enrdf_load_stackoverflow)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3598874A (en) * 1969-05-09 1971-08-10 Procter & Gamble Preparation of chlorohydrins by reacting hypochlorous acid and long-chain olefins
GB1279586A (en) * 1970-02-20 1972-06-28 Hoechst Ag Process for the continuous preparation of dichloropropanols
US3845145A (en) * 1969-01-21 1974-10-29 Olin Corp Preparation of chlorohydrins
US3845144A (en) * 1970-05-11 1974-10-29 Basf Ag Continuous production of propylene chlorohydrin

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52113167A (en) * 1976-03-19 1977-09-22 Nippon Telegr & Teleph Corp <Ntt> X-ray exposing device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3845145A (en) * 1969-01-21 1974-10-29 Olin Corp Preparation of chlorohydrins
US3598874A (en) * 1969-05-09 1971-08-10 Procter & Gamble Preparation of chlorohydrins by reacting hypochlorous acid and long-chain olefins
GB1279586A (en) * 1970-02-20 1972-06-28 Hoechst Ag Process for the continuous preparation of dichloropropanols
US3845144A (en) * 1970-05-11 1974-10-29 Basf Ag Continuous production of propylene chlorohydrin

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Zhurnal obshchei khimii AN SSSR, volume 44, No. 8, published in 1974 by "Nauka" publishing house (Leningrad), D.A. Ashurov et al: "Elektrokhimicheskoe gipokhlorirovavie olefinov", page 1842 *

Also Published As

Publication number Publication date
DE2953906A1 (de) 1982-02-04
GB2075095A (en) 1981-11-11
JPS56501613A (enrdf_load_stackoverflow) 1981-11-05

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