USRE36660E - Fluidized bed reactor and distribution system - Google Patents
Fluidized bed reactor and distribution system Download PDFInfo
- Publication number
- USRE36660E USRE36660E US08/690,217 US69021796A USRE36660E US RE36660 E USRE36660 E US RE36660E US 69021796 A US69021796 A US 69021796A US RE36660 E USRE36660 E US RE36660E
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- US
- United States
- Prior art keywords
- fluid
- riser
- reactor
- level
- network
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/02—Aerobic processes
- C02F3/08—Aerobic processes using moving contact bodies
- C02F3/085—Fluidized beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1818—Feeding of the fluidising gas
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/28—Anaerobic digestion processes
- C02F3/2806—Anaerobic processes using solid supports for microorganisms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/10—Biological treatment of water, waste water, or sewage
Definitions
- This invention relates to fluidized bed reactors and more particularly to an improved fluid distribution system for such reactors.
- Fluidized beds of sand, activated carbon, or other media have been used for a wide variety of aerobic and anaerobic waste treatment processes. Because of their extremely high surface areas for biological growth and high hydraulic loading rates, fluidized beds have demonstrated significant cost and performance advantages for biological treatment of industrial, process, and municipal waste water. Nevertheless, a significant number of these systems which were built over the last twenty years have become inoperable or have been subject to excessive maintenance. These operational problems can be traced to the chronic clogging of the inlet distribution system which distributes the influent at the bottom of the filter bed.
- the inlet distribution system of these biological fluidized beds can become clogged for two principal reasons.
- the problem occurs because the media has a greater density than the fluid and therefore tends to displace the fluid in, for example, the lateral elements of the distribution plumbing.
- Conventional check valves which attempt to prevent this require some degree of backflow in order to activate them. They are thus ineffective in preventing clogging of the inlet system.
- conventional check valves are subject to sticking when even small amounts of media become caught in them.
- the second, principal cause of clogging occurs when foreign materials become lodged in the laterals or openings in the distribution system and impedes normal operation.
- a third factor may play a role in clogging the laterals.
- the flow in the laterals is turbulent. Pressure fluctuations associated with such flow conditions appear to draw media into the laterals even under normal operating conditions.
- this invention provides a fluidized bed reactor for filtering fluids and a method for inhibiting the clogging of a fluid distribution network of such a reactor.
- the reactor has a tank containing a media bed.
- the reactor also has fluid inlet to the tank, a fluid outlet from the tank and a distribution network connected to receive fluid from the inlet and having outlet ports or nozzles for the substantially even distribution of fluid through the media bed.
- the outlet maintains a selected fluid level in the tank, which level is above the level for the media.
- a means is also provided for temporarily maintaining a fluid flow through at least a portion of the distribution network after a termination in fluid flow to the distribution network from the fluid inlet.
- the technique for temporarily maintaining fluid flow generally involves providing at least one fluid reserve or column, with each such reserve column being positioned over a selected portion of the distribution network.
- the reserve/column fluid is permitted to flow into and through at least the corresponding selected portion of the network when there is a termination in fluid flow from the inlet.
- the distribution network includes a plurality of spaced lateral tubes which extend from opposite sides of a conduit connected to receive fluid from the fluid inlet.
- Each lateral tube has a plurality of spaced ports or nozzles for delivering fluid to the media and has at least one riser extending therefrom, the riser preferably extending from a point near the end of the lateral tube.
- a valve controlled opening is preferably provided near the top of each riser.
- the distribution network in general, and the lateral tube connected to the riser in particular, may be purged of media material which has migrated into the tube by opening the valve, permitting fluid in the riser and in the lateral tube to gush from the resulting opening, carrying with it any media material from the lateral tube.
- the opening also permits access to the lateral tube and its nozzles without requiring removal of media from the tank.
- a small orifice may also be provided near the top of each riser.
- This orifice serves a number of functions, including serving as an escape hole for trapped air so that fluid may rise in the risers, and serving as a vacuum break to permit fluid from the riser to flow back into a lateral tube. Finally, a small quantity of fluid may spray from the orifice, providing a visual indication that the riser is full.
- the second way in which the flow maintaining function may be performed is for the fluid inlet to enter the tank at a level above the fluid level in the tank and to be connected to the distribution network through a substantially vertical pipe.
- a vacuum breaker for example a large float valve, is provided near the fluid inlet so that, when there is an interruption in fluid flow to the inlet, the fluid in the pipe may flow into the distribution network to temporarily maintain fluid flow to the network.
- FIG. 1 is a simplified cross-sectional view of a fluidized bed reactor in accordance with a preferred embodiment of the invention.
- FIG. 2 is a cross-sectional view of the reactor taken generally along the line 2--2 in FIG. 1.
- FIG. 3 is a plan cross-sectional view of the reactor taken generally along the line 3--3 in FIG. 1.
- the fluidized bed apparatus or reactor of the invention is applicable to the removal of contaminants and other compounds or matter from a fluid such as water.
- a fluid such as water.
- Liquids from wastewater treatment plants, activated slude processes, aquaculture tanks, and fish farming ponds, are examples of waters that might be treated with the apparatus.
- the fluid to be treated can contain a variety of compounds, including ammonia, amines, nitrites and nitrates. Fluids high in ammonia may be subjected to oxidation and the action of aerobic bacteria that live on the media.
- the reactor can also be used with denitrifying bacteria to convert oxidized nitrogen compounds, i.e., nitrates and/or nitrites) to nitrogen gas.
- the "fluidized bed” refers to the flow of fluid (and the materials to be removed from it) through a bed of fine particles.
- the velocity of the water or other fluid is chosen to slightly expand the bed of particles (by, for example, 30%) and to impart to them a gentle movement.
- the media When in this state, the media may be referred to as being "fluidized”.
- the microorganisms to cause the desired change in the water may come from a natural contamination or they may be deliberately added.
- a fluidized bed reactor 10 which includes a reactor vessel of tank 12 having sidewalls 14 and a base 16 connecting the sidewalls.
- a fluid inlet pipe 15 is provided for delivering fluid to the reactor.
- Inlet pipe 15 preferably extends over wall 14 and into the reactor where it is jointed to a fluid delivery pipe 11 in fluid communication with a distribution network 13.
- a vacuum breaker/air relief valve 17 is located at the top of inlet pipe 15, at, for example, the junction of this pipe with pipe 11.
- Valve 17 may, for example, be a float valve which is closed when there is fluid pressure applied to inlet 15 and which opens when such fluid pressure is removed.
- Distribution network 13 is positioned near the bottom of tank 12 and includes a horizontal main conduit 42 extending along a diameter of the tank (FIG. 3) which is connected to receive fluid from delivery pipe 11 and a plurality of horizontal or lateral tubes 44 extending at right angles from both sides of conduit 42.
- Each lateral tube 44 (sometimes hereinafter referred to as a lateral) has a plurality of downward-facing ports or nozzles The nozzles provide a sufficient pressure drop for uniform flow distribution through media bed 18. Since nozzles 46 are directed downward, the fluid flows down out of the nozzles. However, since the fluid cannot flow through the solid floor 16 of the tank, it reverses direction and flows up through the media bed. The desired microorganisms are normally innoculated into the system and subsequently grow on the media.
- the velocity of the fluid is such that it expands the media bed, the expanded media bed being, for example, at the level 20.
- the media bed settles back to an unexpanded condition over a period of time which is generally a few seconds.
- Outlet 24 controls the fluid level 22 in the reactor, although, depending on the actual flow conditions, the steady state reactor fluid level maintained within the reactor may be at a height above that of fluid outlet 24.
- Fluid is exhausted from the reactor 10 by way of outlet 24 after passage through the media bed 18. Selected portions of the exhausted fluid may be recycled through conduit 26 as required for complete filtering or to promote further growth of the biocatalyst on the media bed.
- An additional conduit 28 can be connected to the fluid inlet 15 to provide additional oxygen sources and/or carbon, nitrogen or other nutrients for the biocatalyst in sufficient amounts to satisfy growth and metabolism requirements of the biocatalyst. The metering of sufficient amounts of these additional sources may be conducted automatically by providing conventional nutrient and/or gas analyzers which may be adapted to periodically sample the influent fluid and determine its nutrient and/or gas content.
- a plurality of tubes 30 are in fluid communication with the distribution network 13. These riser tubes can be located outside tank 12, although they preferably are located within the tank. Each riser tube has one end connected to the distribution system 13 and another end 34 that is located above both the fluidized media bed level 20 and the reactor fluid level 22. Upper end 34 of each riser tube is normally closed by a valve 52 and a small opening or orifice 36 is provided in the riser some distance below the closed end and above reactor fluid level 22. For a preferred embodiment, opening 36 is approximately 1/4. A small quantity of fluid 38 may spray from orifice 36, indicating that the riser is full. Valve 52 may be a knife-gate valve. Upper end 34 of each riser extends over tank 12 so that when valve 52 is in an open position, fluid flows through the corresponding lateral tube 44 and riser 30 and out valve 52 into the tank.
- Tank 12 can be made of a variety of materials, the material utilized preferably being inert (i.e., not chemically or physically altered) to the to the biocatalyst and inert to the particular fluid flowing through the reactor.
- Exemplary materials for constructing the tank and other components of the reactor include noncorrosive metals such as stainless steel, polymers such as polyvinylidene chloride, polyethylene, polytetrafluorethylene, polypropylene, fiberglass-reinforced plastic, and other materials such as concrete.
- Particularly preferred materials for the tank are fiberglass-reinforced plastic.
- Suitable materials for the media bed include natural or artificial substances such as coal, volcanic cinders, glass or plastic beads, sand, activated carbon particles, and alumina.
- the size of the individual particles of the media bed are a function of both their specific gravity and surface area. For the most part, it is preferred to employ media particles of between about 0.1 to 10 mm in diameter. Most preferably, the particles are of a uniform size. While the above media bed materials are illustrative of the preferred materials which are useful, other materials inert to the biocatalyst, either natural or synthetic, can be employed.
- Fluid flow through the media bed is preferably kept within a narrow range of flow rates; the range being primarily a function of the type, size and specific gravity of the media bed, type of fluid and reactor vessel size.
- Exemplary flow rates in the preferred embodiments should be sufficient to produce an approximately 30% expansion in volume of the media above the media bed volume at no flow.
- biocatalyst is a prokaryotic and/or eukaryotic organism, preferably a microorganism, that can convert organic and inorganic materials in the fluid to other products.
- biocatalysts can include nitrifying bacteria (e.g., Nitrosomonas, Nitrobacter) that can convert ammonia or amines to nitrates or nitrites.
- nitrifying bacteria e.g., Nitrosomonas, Nitrobacter
- Protozoans and/or fungi are other examples of biocatalysts that can be used to perform a particular transformation.
- biocatalyst is also meant to include recombinantly derived microorganisms, fragments of these microorganisms, and enzymes isolated from these microorganisms. It will be understood that the exact kind and quantity of biocatalyst is not intended to limit the scope of the present invention.
- the biocatalyst can be introduced by the operator into the media bed as a substantially pure or mixed culture of micro-organisms.
- the biocatalyst can also be introduced into the media bed, and can colonize the media bed, by way of the fluid itself.
- valves 52 are normally closed and fluid under pressure is applied to fluid inlet 15.
- the fluid in inlet pipe 15 causes valve 17 to be closed.
- This fluid flows through pipe 11 and conduit 42 to the laterals 44.
- the fluid pressure is sufficient so that the fluid entering laterals 44 is passed through nozzles 46 into media bed 18 to fluidize the bed.
- the fluid pressure in laterals 44 also causes fluid to rise in risers 30 to the level of valves 34. While some fluid sprays from orifices 36, the orifices are small enough, being for example 1/4 inch in diameter for a 4 inch diameter riser, that the orifices do not have a significant adverse affect either on the height or pressure of fluid in the risers.
- a mechanism has been provided for providing a temporary continuance of fluid flow and pressure at the nozzles during the defluidization period of the media to minimize the likelihood of media entering the nozzles and laterals during this period.
- this objective is achieved both by inlet feed tube 11 and by risers 30. More specifically, when fluid flow at inlet 15 terminates, there is a volume of fluid in pipe 11 which, depending on the length of the pipe and its diameter, may be 10 to 20 gallons. The absence of fluid in inlet pipe 15 permits vacuum break valve 17 to open, allowing air to enter pipe 11 and permitting the fluid in this pipe to flow into conduit 42 and through laterals 44 to the nozzles.
- the opening at vacuum release 17 and the flow resistance in distribution network 13 as a result, for example, of nozzle size will determine the rate at which fluid flows from pipe 11. These factors may be controlled so that the time period required for pipe 11 to completely empty is roughly equal to the settling time of media 18 so that fluid pressure is maintained at the nozzles during substantially the entire fluid settling time, minimizing the migration of media into the nozzles and laterals.
- a technique has thus been provided for maintaining a sufficient fluid flow in the distribution network of a fluidized bed reactor during defluidization of the reactor to minimize migration of media into the nozzles and laterals of the distribution network during this period.
- the apparatus of this invention also may be utilized to purge media which has migrated into the distribution network and to provide access to the network without requiting the nightmarish process of removing the media bed.
- the valves 54 may be periodically opened, for example once a week or once every two weeks, while fluid pressure is being applied to the system from inlet 15.
- opening of the valve permits fluid in the risers and at least in the lateral to which a riser is attached to gush from the opening 34, which may for a preferred embodiment be a relatively large opening, for example four inches, carrying any media which has migrated into the lateral with it.
- the fluid and media exiting end 34 of each riser are returned to tank 12.
- this purge operation will remove a sufficient quantity of media which may have accumulated in a lateral 44 behind any nozzle 46 so that when valve 52 is closed, causing the lateral and nozzles to be repressurized, any remaining media at the nozzles will be forced out by the fluid pressure, completely freeing the nozzles.
- valve 52 is closed, causing the lateral and nozzles to be repressurized, any remaining media at the nozzles will be forced out by the fluid pressure, completely freeing the nozzles.
- a blockage in a lateral or the clogging of a nozzle may be such that the purge and repressurization operation described above is not adequate to fully unclog the system.
- valve 52 for the riser connected to the lateral which is clogged or the lateral containing clogged nozzles may be fully opened and either a flexible reaming device or brush may be passed through the riser into the lateral to loosen the caked media so that it may be removed during a subsequent purge.
- a hose may be snaked into the riser to an appropriate position to direct high pressure water or other fluid into the lateral to clear the clog or some other suitable implement may be manipulated through the open end 34 of the riser and the riser to the lateral to clear the clogs.
- an easily accessible access port is provided to the laterals and nozzles to permit clogs to be cleared without requiring removal of the media bed.
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Biodiversity & Conservation Biology (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Combustion & Propulsion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
Description
Claims (17)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/690,217 USRE36660E (en) | 1993-02-26 | 1996-07-12 | Fluidized bed reactor and distribution system |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/023,323 US5330652A (en) | 1993-02-26 | 1993-02-26 | Fluidized bed reactor and distribution system |
US08/690,217 USRE36660E (en) | 1993-02-26 | 1996-07-12 | Fluidized bed reactor and distribution system |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US08/023,323 Reissue US5330652A (en) | 1993-02-26 | 1993-02-26 | Fluidized bed reactor and distribution system |
Publications (1)
Publication Number | Publication Date |
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USRE36660E true USRE36660E (en) | 2000-04-18 |
Family
ID=21814421
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
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US08/023,323 Ceased US5330652A (en) | 1993-02-26 | 1993-02-26 | Fluidized bed reactor and distribution system |
US08/690,217 Expired - Lifetime USRE36660E (en) | 1993-02-26 | 1996-07-12 | Fluidized bed reactor and distribution system |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
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US08/023,323 Ceased US5330652A (en) | 1993-02-26 | 1993-02-26 | Fluidized bed reactor and distribution system |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7341660B1 (en) | 2004-10-07 | 2008-03-11 | Pentair Pump Group, Inc. | Unitary three stage wastewater treatment system |
Families Citing this family (13)
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---|---|---|---|---|
US5591273A (en) * | 1994-12-30 | 1997-01-07 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Process for distributing ultra high purity gases with minimized contamination and particulates |
US5733454A (en) * | 1996-04-26 | 1998-03-31 | Ehh Holding Co., Inc. | Process and apparatus for the treatment of flowable waste |
JP3350364B2 (en) * | 1996-09-06 | 2002-11-25 | シャープ株式会社 | Wastewater treatment method and wastewater treatment device |
US5714678A (en) * | 1996-11-26 | 1998-02-03 | American Air Liquide Inc. | Method for rapidly determining an impurity level in a gas source or a gas distribution system |
US6117313A (en) * | 1996-12-27 | 2000-09-12 | Goldman; Joshua | Method and apparatus for aquaculture and for water treatment related thereto |
EP1033348A4 (en) * | 1998-03-06 | 2002-02-06 | Nippon Kokan Kk | Method and apparatus for treating waste water |
US6436288B1 (en) | 1999-02-08 | 2002-08-20 | Mississippi State University | Bast medium biological reactor treatment system for remediation and odor suppression of organic waste streams |
US6048459A (en) * | 1999-04-09 | 2000-04-11 | Mockba Corporation | Method and apparatus for fluidization of particulate bed materials |
US6458276B1 (en) * | 2001-05-16 | 2002-10-01 | Shell Oil Company | Method and apparatus for biodegradation of alkyl ethers and tertiary butyl alcohol |
US6740232B1 (en) * | 2002-05-01 | 2004-05-25 | Aquascape Designs, Inc. | Constructed wetlands system, treatment apparatus and method |
US7058471B2 (en) | 2003-01-14 | 2006-06-06 | Watanabe John S | System and method for custom-made clothing |
US7754072B2 (en) | 2003-11-07 | 2010-07-13 | Aquascape Designs, Inc. | Water feature construction |
US20050211644A1 (en) * | 2004-03-24 | 2005-09-29 | Aquatic Advisors, Llc | Mixed bed trickling reactor using microbeads |
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- 1993-02-26 US US08/023,323 patent/US5330652A/en not_active Ceased
-
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- 1996-07-12 US US08/690,217 patent/USRE36660E/en not_active Expired - Lifetime
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Publication number | Priority date | Publication date | Assignee | Title |
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US7341660B1 (en) | 2004-10-07 | 2008-03-11 | Pentair Pump Group, Inc. | Unitary three stage wastewater treatment system |
Also Published As
Publication number | Publication date |
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US5330652A (en) | 1994-07-19 |
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