USRE1686E - Improvement in the manufacture and refining of iron - Google Patents
Improvement in the manufacture and refining of iron Download PDFInfo
- Publication number
- USRE1686E USRE1686E US RE1686 E USRE1686 E US RE1686E
- Authority
- US
- United States
- Prior art keywords
- iron
- refining
- metal
- manufacture
- air
- Prior art date
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title description 62
- 229910052742 iron Inorganic materials 0.000 title description 32
- 238000007670 refining Methods 0.000 title description 26
- 238000004519 manufacturing process Methods 0.000 title description 12
- 229910052751 metal Inorganic materials 0.000 description 40
- 239000002184 metal Substances 0.000 description 40
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 20
- 229910052799 carbon Inorganic materials 0.000 description 18
- 229910000831 Steel Inorganic materials 0.000 description 12
- 239000010959 steel Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 10
- 239000011780 sodium chloride Substances 0.000 description 8
- 235000002639 sodium chloride Nutrition 0.000 description 8
- 229910000805 Pig iron Inorganic materials 0.000 description 4
- 239000005864 Sulphur Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910000499 pig iron Inorganic materials 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 4
- 229910001018 Cast iron Inorganic materials 0.000 description 2
- 210000003800 Pharynx Anatomy 0.000 description 2
- 241001201614 Prays Species 0.000 description 2
- PPTYJKAXVCCBDU-UHFFFAOYSA-N Rohypnol Chemical compound N=1CC(=O)N(C)C2=CC=C([N+]([O-])=O)C=C2C=1C1=CC=CC=C1F PPTYJKAXVCCBDU-UHFFFAOYSA-N 0.000 description 2
- 238000003723 Smelting Methods 0.000 description 2
- 241000282898 Sus scrofa Species 0.000 description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 2
- 229910052785 arsenic Inorganic materials 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000011449 brick Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000005262 decarbonization Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 238000005242 forging Methods 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910001338 liquidmetal Inorganic materials 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
Definitions
- my invention or discovery consists in the improvement of the manufacture of crude molten iron or pig-iron from ore in smelting-furnaces, and refining and converting the same, or of the remelted pig-iron intosuperior metal and grades of refined iron or steel through the employment and introduction of a current or currents of atmospheric air under pressure for removing from the crude metal a certain portion of carbon, combining the same with the oxygen of the air.
- the decarbonization thus produced has for effect a brisk ebnllition of the molten metal, attended with great heat and increased fluidity.
- the flux may be applied at or near 7 the hearth of the blast-furnace by efl'ecting the introduction through the tuyere-pipe by the pressure and force of the blast, or the salt can be applied to the metal in the refiningfire or crucible when the converting process is commenced.
- the refining and steel-producing blast for the conversion of crude met-alinto ingots can be applied at the smelting furnace after a sufficient deposit has accrued; but itwere preferable to transfer the molten iron to an outside 'from eight to ten or aperture fordischarging the May 31, 1864. 1
- the crucible so to be employed I make of plate-iron, lined inside with best quality of fire-brick, or with any inconsumable material, in order to resist the action of the metal, and
- the refined metal may either be tapped ofi' near the bottom of the refining apparatus or made to pour out into the ingotmolds.
- the metal can be discharged into the refini'ngfire or crucible by a conduct'or leading from the furnace-hearth.
- the process of refining consists in starting an air-blast under high pressure into the liquid metal, which-at once kindlesa blaze and extending through the whole mass, filling the upper part and throat of the vessel vwith flame occasioned by the oxygen of the air,
- V I Refined iron or steel contain three-fourths of one per cent.- to one and a half per cent.
- the metal from the smelting-furnace and place it in a converting fire or vessel for refining and I converting into ingots for forging purposes. .In this converting process I use one-half of one per cent. to one per cent. of manganese.
- My refining t-uyere-pipes I make of any inconsumable material. Before the refined metal is tapped from the crucible it must stand a few minutes to allow the dross to rise to the filled in the ingot-molds.
- the air-blast can be introduced into the re-' surface before it is fi uin g-vessel in different ways to penetrate the -metal, to combine the air with the carbon of the crude 'iron to effect the refining and converting process. 4
- Blowing air into the refining or run-ont fire with the use of coal for fuel has been practiced before.
Description
" UNITED STATES.
PATENT OFFIC CHRISTIAN SHUNK, OF YOUNGSTOWN, QHI".
IMPROVEMENT lN l'HE MANUFACTURE AND BEFININGOF IRON.
Specification forming part of Letters Patent N0. 14,257, dated February 12, 1856; Reissue No.1 ,686,-dated To all whom it may concern;
Be it known that I, CHRISTIAN SHUNK,
formerly of Slate Lick, in the county of Arm-r strong-State of Pennsylvania,now of Youngstown, Mahoning county, Ohio, prays for the grant of a reissue of his patent granted to him on the twelfth (12th) day of February, eightecn hundred and fifty-six, (1856,) the same being grounded on his application and specificati n which was filed in the Patent Ofiice on the 'wenty-eighth (28th) day of August, eighteen hundred and fifty-four, (1854,) this his said application beingaccompanied with the required oath, according to the act of Congress in that case made'audprovided, together with the necessary petition and statement required.
The nature of my invention or discovery consists in the improvement of the manufacture of crude molten iron or pig-iron from ore in smelting-furnaces, and refining and converting the same, or of the remelted pig-iron intosuperior metal and grades of refined iron or steel through the employment and introduction of a current or currents of atmospheric air under pressure for removing from the crude metal a certain portion of carbon, combining the same with the oxygen of the air. The decarbonization thus produced has for effect a brisk ebnllition of the molten metal, attended with great heat and increased fluidity. To this I superadd the use of common salt (chloride of sodium) as aflux, solvent, and purifier, to gain further fluidity by divesting the metal of sulphur and other contamination. A gallon-measure of the dry salt is asufficient charge per ton of crude metal; and it should be remembered that, although the use of the article has been attempted insom'e'forms of the iron business, I am not aware of its having been used in the way and to the end used by me. The flux may be applied at or near 7 the hearth of the blast-furnace by efl'ecting the introduction through the tuyere-pipe by the pressure and force of the blast, or the salt can be applied to the metal in the refiningfire or crucible when the converting process is commenced. r
The refining and steel-producing blast for the conversion of crude met-alinto ingots can be applied at the smelting furnace after a sufficient deposit has accrued; but itwere preferable to transfer the molten iron to an outside 'from eight to ten or aperture fordischarging the May 31, 1864. 1
crucible or converting-fire appropriated to the operation of refiningz'. e., to constitute a refining apparatus.
' The crucible so to be employed I make of plate-iron, lined inside with best quality of fire-brick, or with any inconsumable material, in order to resist the action of the metal, and
the whole to be'established a convenient distance from the supply-furnace and to suit local circumstances. The refined metal may either be tapped ofi' near the bottom of the refining apparatus or made to pour out into the ingotmolds. The metal can be discharged into the refini'ngfire or crucible by a conduct'or leading from the furnace-hearth.
The converting fire or apparatus thus described, being duly charged with crude molten metal, the process of refining consists in starting an air-blast under high pressure into the liquid metal, which-at once kindlesa blaze and extending through the whole mass, filling the upper part and throat of the vessel vwith flame occasioned by the oxygen of the air,
consuming a portion of carbon from the iron. The workmen derive a clue to the progress of the combustionfrom the gradual decline in;
the am ount of flame developed. For instance, it is estimated that when an appreciable decline sets in the quality of the metal is that of refined, iron or hard steel, but when the flame is about to cease the product is low or semi steel of good" tensile strength to mold into in gots, fit to be hammered or rolled; or the carbon can be reduced still lower by continuing the blast of air a few seconds longer,
then by adding a given amount of highly carbonated pig metal, chipped or broken fine, the carbon will rise again in a state of combination of hardness, aecordin g to-the amount of carbon added. This new supply of carbon is introduced a few minutes after the blast is discontinued, to allow time for the metal to cease boiling. The carbon is then immediately imbibed through the fluid mass in a combined state for molding into ingots.
One thousand cubic feet of air per minute, under a pressure of seven pounds, will refine and convert one ton of crude molten metal in minutes. The aggregate pipe section stated amount of .blast at seven pounds pressare is three square inches.
I a V I Refined iron or steel contain three-fourths of one per cent.- to one and a half per cent.
' ot'carbon in a combined state, according to -intothe metal for the discharge of the air;
but, as already stated, it is preferable to take the metal from the smelting-furnace and place it in a converting fire or vessel for refining and I converting into ingots for forging purposes. .In this converting process I use one-half of one per cent. to one per cent. of manganese.
'This article is not new in the iron business.
My refining t-uyere-pipes I make of any inconsumable material. Before the refined metal is tapped from the crucible it must stand a few minutes to allow the dross to rise to the filled in the ingot-molds.
The air-blast can be introduced into the re-' surface before it is fi uin g-vessel in different ways to penetrate the -metal, to combine the air with the carbon of the crude 'iron to effect the refining and converting process. 4
In the manufacture of 'metal in the blastfurnaces I find it-desirable to subject the ore to slow roasting at the entrance of the stack or tunnel-head of the blastfurnace by making that part the widest, or funnel-shaped outward, causing the descent there to be as slow as convenient, thereby afi'ordingtime for ac cumnlation of heat, and with the large surface of ore exposed, gradual expulsion from the mineral of volatile impurities, such as sulphur, arsenic and phosphorus, and a superior carbonated and pure molten metal is produced 'for refining and converting purposes.
This completes the description of my improvements in the manufacture of iron and refined iron or steel; and I wish to be understood that the details presented are not to be regarded as limiting me in respect to the use of operation. V
Blowing air into the refining or run-ont fire with the use of coal for fuel has been practiced before.
What I claim as my invention, and for which I ask Letters Patent, is-+ 1. The manufacture and refining of crude of what is otherwise new-in my mode or modes iron by the several processes herein set forth and described.
2. Refining cast-iron through compressed air by diflfusing the same, so. as permeate the liquid mass of the iron.
3. The employment and application of common salt, as stated.
These claims I make jointly and separately in the manner and for the tially as specified.
CHRISTIAN sHUnK.
Witnesses:
Guns. DU Bors, '1. ScnEsrLm.
purposes substan-
Family
ID=
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