USRE13462E - John wexebx qp kkw txbk - Google Patents
John wexebx qp kkw txbk Download PDFInfo
- Publication number
- USRE13462E USRE13462E US RE13462 E USRE13462 E US RE13462E
- Authority
- US
- United States
- Prior art keywords
- iodin
- solution
- john
- wexebx
- txbk
- Prior art date
Links
- VXMKYRQZQXVKGB-CWWHNZPOSA-N Tannin Chemical compound O([C@H]1[C@H]([C@@H]2OC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)O[C@H]([C@H]2O)O1)O)C(=O)C1=CC(O)=C(O)C(O)=C1 VXMKYRQZQXVKGB-CWWHNZPOSA-N 0.000 description 12
- 229920001864 tannin Polymers 0.000 description 12
- 235000018553 tannin Nutrition 0.000 description 12
- 239000001648 tannin Substances 0.000 description 12
- 239000000843 powder Substances 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 239000006188 syrup Substances 0.000 description 10
- 235000020357 syrup Nutrition 0.000 description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- 235000011187 glycerol Nutrition 0.000 description 8
- 230000002335 preservative Effects 0.000 description 8
- 239000003755 preservative agent Substances 0.000 description 8
- 239000002253 acid Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- CZMRCDWAGMRECN-UGDNZRGBSA-N D-sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 239000001263 FEMA 3042 Substances 0.000 description 4
- 210000004940 Nucleus Anatomy 0.000 description 4
- 229940033123 Tannic Acid Drugs 0.000 description 4
- LRBQNJMCXXYXIU-NRMVVENXSA-N Tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 235000015523 tannic acid Nutrition 0.000 description 4
- 229920002258 tannic acid Polymers 0.000 description 4
- 240000003670 Sesamum indicum Species 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 229910000175 cerite Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000266 injurious Effects 0.000 description 2
- 230000003522 irritant Effects 0.000 description 2
- 239000002085 irritant Substances 0.000 description 2
- 231100000021 irritant Toxicity 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
Definitions
- My invention relates to a novel method for producin iodin in solution in a chemically availab e and functionally active form, and to the combination of chemicals having free "iodin therein in solution obtained by this method as a' new article of manufacture,
- crystalline iodin may be dissolved in a solution of tannin and glycerin without changing its chemical rties.
- 03st e iodin is first re- .duced mechanic y to a fine wder.
- One part of this powder is then p aced in asoution of four parts of tannin to sixteen parts of 'glycerm in a closed vessel and I slowly agitated.
- the iodin willbecome entire] dissolved thereby without changing or a ecting its chemical, properties.
- a perfect solution is thus obtained which is staso'ble, has no sediments, and will not i i;
- the syrup acts as. a'preservative main in its free state but is changed into I the art that tannin made of white rock candy and does not reof the iodin solution and as it has no wass or elements which attack the the latter remains With many solvents the iodin salts or other chemical compounds, or is accompanied by acids which prevent its being used in many cases where the efiects of the iodin or the functions which it is capable of performing are desirable but can not be obtained safely. By my novel method this want is supplied.
- the solution, or the solution with its preservative syru is free from salts, contains no free. acid, ans is not irritant nor injurious.
- the 'herem solution containing free iodin comprising four parts of tannin, sixteen parts of glycerin with one part of iodin.
- the herein described solution containfree iodin, comprising four parts of so "tannin,.sixteen parts of glycerin with one part of iodin, and a preservative syrup of sugar and water.
- free iodin in solution which comprises :ducing crystalline iodin to a powder, placing one part of said powder in a closed vesso] .with four arts of tannin and sixteen parts of glycerin, agitating said vessel un til the powder is dissolved, and adding to this iodin solution a preservative syrup of sugar and water.
Description
2 characteristics or pro P TENT OFFICE.
some wmnm, or? m 1031:, N. Y.
ronm sonu'nom 13 ,46 1 1mm. Original Io. 1,Q18,91 8,
- Specification of aeiu ea Letters Patent. -Reisued a z'i', 1912. dated Ianuaril, 1912, Serial No. 557,110. 3 Application for reissue fled 14, 1913, Serial 16.. 888,870.
To all whom it may concern Be'it known that I, J 0111: Warren, a citi-,
\ zen of the United States, and a resident of' the city, county, and State of New Yor 5 United States of America, have inven certain new anduseful Improvements in V Iodin Solutions, of which the followingis a specification.
My invention relates to a novel method for producin iodin in solution in a chemically availab e and functionally active form, and to the combination of chemicals having free "iodin therein in solution obtained by this method as a' new article of manufacture,
orja substance not heretofore known in the a I have discovered that crystalline iodin may be dissolved in a solution of tannin and glycerin without changing its chemical rties. According to my invention 03st e iodin is first re- .duced mechanic y to a fine wder. One part of this powder is then p aced in asoution of four parts of tannin to sixteen parts of 'glycerm in a closed vessel and I slowly agitated. The iodin willbecome entire] dissolved thereby without changing or a ecting its chemical, properties. A perfect solution is thus obtained which is staso'ble, has no sediments, and will not i i;
pure v v a ter, referably of such r0 rtions that there be seven and one pounds 85. of the rock candy to each gallon of the syrup. This is then mixed with iodin solution which .I have already described; I
have used this in the proportions of ten I parts of the syrup to one part of the iodin 40 solution. The syrup acts as. a'preservative main in its free state but is changed into I the art that tannin made of white rock candy and does not reof the iodin solution and as it has no dients or elements which attack the the latter remains With many solvents the iodin salts or other chemical compounds, or is accompanied by acids which prevent its being used in many cases where the efiects of the iodin or the functions which it is capable of performing are desirable but can not be obtained safely. By my novel method this want is supplied. The solution, or the solution with its preservative syru is free from salts, contains no free. acid, ans is not irritant nor injurious.
It will be understood by those skilled in contains the nucleus coon What I claim and desire to secure by Letters Patent of the United States is 1. The herein described solution of iodin comprising. g1 cerite of tannic acid with free iodin belt; in solution therein.
2. The herein described solution of iodin comprising glycerite of tannic "acid with free iodin held in splution thelrein, and a reservative'syru 0 so r an water.
The 'herem solution containing free iodin, comprising four parts of tannin, sixteen parts of glycerin with one part of iodin.
a. The herein described solution containfree iodin, comprising four parts of so "tannin,.sixteen parts of glycerin with one part of iodin, and a preservative syrup of sugar and water.
" 5 5. The herein described method of obtaining free iodin in solution which comprises reducing crystalline iodln to a powder, placing it in a closed vessel wlth glycerite of tannic acid and causing it to'be moved through said liquid.
free iodin in solution "which comprises :ducing crystalline iodin to a powder, placing one part of said powder in a closed vesso] .with four arts of tannin and sixteen parts of glycerin, agitating said vessel un til the powder is dissolved, and adding to this iodin solution a preservative syrup of sugar and water.
7. The herein described solution of iodin 6. The herein described method of obtainmprising glycerite of a substance contain- 20 mg a nucleus as follows:
coon J 25 oH-\,/ on s" with free iodin held in solution therein.
In testimony whereof have hereunto signed my name in the presence of two sub scribing Witnesses.
JOHN WEMER. Witnesses C. G. HEYLMUN, M. E. MoNlnon.
Family
ID=
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