US986645A - Metallic body. - Google Patents

Metallic body. Download PDF

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Publication number
US986645A
US986645A US561933A US1910561933A US986645A US 986645 A US986645 A US 986645A US 561933 A US561933 A US 561933A US 1910561933 A US1910561933 A US 1910561933A US 986645 A US986645 A US 986645A
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United States
Prior art keywords
titanium
metallic body
disk
metallic
treated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US561933A
Inventor
Auguste J Rossi
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Tam Ceramics LLC
Original Assignee
Titanium Alloy Manufacturing Co
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Filing date
Publication date
Priority claimed from US42586408A external-priority patent/US986504A/en
Application filed by Titanium Alloy Manufacturing Co filed Critical Titanium Alloy Manufacturing Co
Priority to US561933A priority Critical patent/US986645A/en
Application granted granted Critical
Publication of US986645A publication Critical patent/US986645A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C28/00Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S148/00Metal treatment
    • Y10S148/902Metal treatment having portions of differing metallurgical properties or characteristics
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S428/00Stock material or miscellaneous articles
    • Y10S428/922Static electricity metal bleed-off metallic stock
    • Y10S428/9335Product by special process
    • Y10S428/938Vapor deposition or gas diffusion
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12458All metal or with adjacent metals having composition, density, or hardness gradient

Definitions

  • the object of my present invention is to I have treated, by my said process, a ferrie incorporate into a given metallic body, o1' body', z'. e. a steel disk, said disk being oneinto portions thereof as required, aldesired half inch in thickness and five inches in 65 addition of titanium, and to accomplish thisl diameter as follows, viz: In an ordinary without fusion or mechanical treatment.
  • I graphite receptacle I packed the said disk in attain this object by my vnovel process as powdered ferro-titanium (the alloy of iron follows, viz: I pack the metallic body, or and titanium) pulverized to pass through a those portions thereof to be permeated by inch mesh, or finer.
  • Said ferro-titanium 70 titanium in a powder composed of, or concontained about 20% of titanium and 80% taining in powdered state an alloy of titaof iron. I closely packed said powdered nium with, preferably, the same metal as ferro-titanium on all sides of said disk.
  • the titanium appearsto be abcopper and 10% of titanium, and in this in- 90 sorbed, or to have ermeated, as aforesaid, stance, the copper disk, -at the conclusion of in minute subdivisions or particles, which the operation, was found to contain, near are found Conglomerated Wit-h the mtl its surface 2.72% of titanium, with corre- 40-constitutin the said metallic body, or is, as Sponding similar increase of toughness and it were, a oyed with said metal with howhardness, I have further disccvered that; ever the notable characteristic that, other the amount 0f such other metal absorbed or things being equal, the respective number of incorporated into the metallic body treated said particles so to speak, indifferent planes by my process as aforesaid, and the degree 45 projectedthrough said metallic body in arof the penetration of such other metal into allelism with that surface thereof whic is such metallic body, may, within limits, be proximate to said plane is inversely proporregulated as desired
  • the absorption, or impregnation may chanical means, as drilling or the like, and be extended from the surface inwardly, even also without resort to fusion, an actual conto the center of the metallic body treated,
  • -steel armor plate for instance, can thereby be hardened and toughened t or near 'its vsurface by incorporation there of titanium, and thus new and desirable qualities, suchas hardness, imparted to the plate near its surface Without affecting other normal desired qualities of the steel through- I 4out the remainder of said plate.
  • the temperature required, as aforesaid, for the ractice of isaid process may be produce and applieclI to the materials employed, in any convenient manner, depending u on the character, size, etc., -of the metallic body treated, as for instance in a gas furnace, in an open hearth coke fire, or electrically as by a resistance or otherwise.
  • the annexed drawing indicates symbolically the supposed arrangement and relaoseis metal, in fragment of a steel plate A shown 1n section without hatchings, the dots suggesting the relative location and extent of the particles of incorporated met-al extendin from each surface of the plate inwardly.
  • pregnations of titanium the extent of such impregnations being, in any plane parallel with that of the proximate surface of said body, substantially in inverse ratio to the distance of said plane from said surface.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Footwear And Its Accessory, Manufacturing Method And Apparatuses (AREA)
  • Pressure Welding/Diffusion-Bonding (AREA)
  • Arc Welding In General (AREA)

Description

A. I. BSSI.
nume sont. Y LRPLIUTIOI 'II- ID HAY l.. IIN.
9861645 Patented MaJ-'..liisufjx raeaf Zr: Y*
', magg.:
UNITED STATES PATENT OFFICE.
A'UGUSTE J. ROSSI, OF FALLS, NEW YORK, ASSIGNOR TO .THE TITANIUM ALLOY MANUFACTURING COMBANY, OF NEW YORK, N. Y., A CORPORATION '0F MAINE.
METALLIC BODY.
986,645. l Spccication of Letters Patent. Patented B131', 14, 1911,
Original application led Aprl'l, 1908, Serial No. 425,864. Divided and this application vled Hay 18, 1910. Serial No. 561,933.
tent of titanium conglomerated therewith,
and' its final content of the added metal.
To all it may concern: -and this without distorting or substantially 55 A -Be it known that I, AUGUSTE J. ROSSI, a changing the form of the metallic body, or citizen of the United States, and aresident article treated, thereby imparting thereto of the city of Niagara Falls, county of inew and desired characteristics, properties,
agara, and State of New York, have 1ncapacities and behavior. Y
vented certain new and useful Improve- That those skilled in the art may better 60 ments in Metallic Bodies, of which the folunderstand my procedure, I. will mention, lowing is a specification. for illustration, the following examples, viz:
The object of my present invention is to I have treated, by my said process, a ferrie incorporate into a given metallic body, o1' body', z'. e. a steel disk, said disk being oneinto portions thereof as required, aldesired half inch in thickness and five inches in 65 addition of titanium, and to accomplish thisl diameter as follows, viz: In an ordinary without fusion or mechanical treatment. I graphite receptacle I packed the said disk in attain this object by my vnovel process as powdered ferro-titanium (the alloy of iron follows, viz: I pack the metallic body, or and titanium) pulverized to pass through a those portions thereof to be permeated by inch mesh, or finer. Said ferro-titanium 70 titanium, in a powder composed of, or concontained about 20% of titanium and 80% taining in powdered state an alloy of titaof iron. I closely packed said powdered nium with, preferably, the same metal as ferro-titanium on all sides of said disk. The
2O that constitutin or preponderating in said graphite receptacle, and its said contents,
body. I then su ject the mass to a high temwere then, in a Crucible, raised to a temperaperature approximating, but, in all cases, ture indicated by a bright yellow heat and lower than the fusing point of said met-als, maintained in this temperature during about or either of them, and maintain said temper-v four hours. The said disk on cooling, and
25 ature until the desired amount of incorpora, removal from the remaining powder, was
tion and permeation has been effected. On found to contain, near its suirfacefifrom coolinfr and withdrawing the metallic body 0.65%. to 0.72% of titanium, said titanium treate it will be found to have absorbed having been apparently as aforesaid aband to contain, in permeations from its sursorbed by the steel, and imparting thereto,
80 face, inwardly more or less of the titanium where present, greatly increased toughness contained in said powder, the extent ofsaid and hardness. On another occasion a simi- 85 incorporation, permeation and absorption Of lar disk 0f copper was treated in all respects said titanium being inversely, proportional `as before, except that it was packed in to its distance from that surface of the mepowdered cupro-titanium. (the alloy of ooptallic body through which tho-.titanium has per and titanium) containing about 90% of entered it. The titanium appearsto be abcopper and 10% of titanium, and in this in- 90 sorbed, or to have ermeated, as aforesaid, stance, the copper disk, -at the conclusion of in minute subdivisions or particles, which the operation, was found to contain, near are found Conglomerated Wit-h the mtl its surface 2.72% of titanium, with corre- 40-constitutin the said metallic body, or is, as Sponding similar increase of toughness and it were, a oyed with said metal with howhardness, I have further disccvered that; ever the notable characteristic that, other the amount 0f such other metal absorbed or things being equal, the respective number of incorporated into the metallic body treated said particles so to speak, indifferent planes by my process as aforesaid, and the degree 45 projectedthrough said metallic body in arof the penetration of such other metal into allelism with that surface thereof whic is such metallic body, may, within limits, be proximate to said plane is inversely proporregulated as desired. by varying the protional to `the, distance of such planerom portion of such other metal inthe powder suchV surface. There is thus imparted to the m which the metallic body is packed, or by 50 metallic body treated, where and to the exvarying the duration of the said treatment.
tent required, and without resort to me- Thus the absorption, or impregnation, may chanical means, as drilling or the like, and be extended from the surface inwardly, even also without resort to fusion, an actual conto the center of the metallic body treated,
found to have absorbed, in addition to the tive location of the absorbed, or permeating titanium, some carbon.
The manifold utilities of my present invention will be obvious to those skilled in the art,-steel armor plate, for instance, can thereby be hardened and toughened t or near 'its vsurface by incorporation there of titanium, and thus new and desirable qualities, suchas hardness, imparted to the plate near its surface Without affecting other normal desired qualities of the steel through- I 4out the remainder of said plate.
The temperature required, as aforesaid, for the ractice of isaid processmay be produce and applieclI to the materials employed, in any convenient manner, depending u on the character, size, etc., -of the metallic body treated, as for instance in a gas furnace, in an open hearth coke fire, or electrically as by a resistance or otherwise.
The annexed drawing indicates symbolically the supposed arrangement and relaoseis metal, in fragment of a steel plate A shown 1n section without hatchings, the dots suggesting the relative location and extent of the particles of incorporated met-al extendin from each surface of the plate inwardly.
y present application for patent is a division of my pending application, Serial No. 425,864, filed April 8th 1908.
HavingI thus described my invention,
what I claim as new and desire to secure by Letters Patent is the following, viz
1. A metallic body conglomerated with impregnations of titanium, the extent of such impregnations being, in any plane parallel with that of the proximate surface of said body, substantially in inverse ratio o the distance of said plane from said surace.
pregnations of titanium, the extent of such impregnations being, in any plane parallel with that of the proximate surface of said body, substantially in inverse ratio to the distance of said plane from said surface.
3. A steel body conglomerated with irnpregnations of titanium, the extent of such impregnations being, in any plane parallel with that of the proximate surface of said body, substantially in inverse ratio to the distance of said plane from said surface.
AUGUSTE J. ROSSI.
Witnesses:
WALTER D. EDMONDS, PHILIP C. Pncx. 4
2. A ferric body conglomerated with imi
US561933A 1908-04-08 1910-05-18 Metallic body. Expired - Lifetime US986645A (en)

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Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US42586408A US986504A (en) 1908-04-08 1908-04-08 Process of treating metallic bodies.
US561933A US986645A (en) 1908-04-08 1910-05-18 Metallic body.

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3125805A (en) * 1964-03-24 Cladding ferrous-base alloys with titanium
US3502493A (en) * 1966-01-24 1970-03-24 Forestek Plating & Mfg Co Deposition of micron-sized particles into porous surfaces

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3125805A (en) * 1964-03-24 Cladding ferrous-base alloys with titanium
US3502493A (en) * 1966-01-24 1970-03-24 Forestek Plating & Mfg Co Deposition of micron-sized particles into porous surfaces

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