US912245A - Solder for incandescent-lamp filaments. - Google Patents
Solder for incandescent-lamp filaments. Download PDFInfo
- Publication number
- US912245A US912245A US29688406A US1906296884A US912245A US 912245 A US912245 A US 912245A US 29688406 A US29688406 A US 29688406A US 1906296884 A US1906296884 A US 1906296884A US 912245 A US912245 A US 912245A
- Authority
- US
- United States
- Prior art keywords
- carbon
- solder
- carbid
- incandescent
- lamp filaments
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229910000679 solder Inorganic materials 0.000 title description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 25
- 229910052799 carbon Inorganic materials 0.000 description 24
- 229910052751 metal Inorganic materials 0.000 description 21
- 239000002184 metal Substances 0.000 description 21
- 150000002739 metals Chemical class 0.000 description 11
- 238000002844 melting Methods 0.000 description 6
- 230000008018 melting Effects 0.000 description 6
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 6
- 229910052721 tungsten Inorganic materials 0.000 description 6
- 239000010937 tungsten Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000006104 solid solution Substances 0.000 description 4
- 235000011837 pasties Nutrition 0.000 description 3
- 238000005476 soldering Methods 0.000 description 3
- 229910052720 vanadium Inorganic materials 0.000 description 3
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 229920000084 Gum arabic Polymers 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 241000978776 Senegalia senegal Species 0.000 description 2
- 235000010489 acacia gum Nutrition 0.000 description 2
- 239000000205 acacia gum Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 150000001722 carbon compounds Chemical class 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- 239000010955 niobium Substances 0.000 description 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/90—Carbides
- C01B32/914—Carbides of single elements
- C01B32/949—Tungsten or molybdenum carbides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/36—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest
- B23K35/3601—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest with inorganic compounds as principal constituents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Definitions
- HANS KUZEL OF BADEN, NEAR VIENNA, AUSTRIA-HUNGARY.
- My invention relates to the means for electrically connecting the carbon filaments of electric glow lamps with the supply wires, and the object of the invention is to obtain a good connection of a metallic character, which conducts the current better than the usual carbon cements and carbon coatin s, and for this urpose I make use of a metal ic material me ting at a high temperature and which adheres equallv well to the filament and to the metal supply wires.
- metal earbids melting at high temperatures and their solid solutions in an excess of metal constitute the desired metallic connecting material. It has been found that the carbon compounds of the metals melting at extremely high temperatures such as manganese, chromium, molybdenum, tungsten, uranium, vanadium, tantalum, niobium, titanium, zirconium, nickel, cobalt, iron are particularlysuitable for the above pur iose. 'lhe earbids of all of these metals and the solid solutions of such carbids in an excess of metal have a certain affinity for carbon owing to the fact that they con tain carbon themselves and very firmly adhereto carbon if applied thereto in a molten state.
- the ends of a carbon filament are dipped into molten carbid of tungsten pre ared by the method of Moissan the pores 0 the carbon filament ends are soaked or filled with the carbid and after withdrawing tho ends of the filament from the molten carbid it will be found that these ends are covered with a metallic coating.
- the thickness of this coating may be increased at will by repeatedly dip in the filament ends into the molten carbi an this coating so firmly-adheres to the carbon that in most cases it cannot be removed from the same without destro ing the carbon.
- a metal wire-is dipped into the molten carbid it becomes also coated with the latter. If therefore the molten carbid is a plied in an suitable mannew to the ends 0 acarbon ament and its metallic (say nickel)" supply wires while they;
- T e carbid of tungsten or any other carbid used need not be employed in their pure state for the purposes of the present invention.
- the raw product obtained for instance by the methods of Moissan, in the above case for instance by reducing tungstic acidby carbon, and containing from 0.67 to 6.33% of carbon may be directly used, but those products which approximately correspond to the formula CW, are more suitable than the solid solutions of the carbid in the metal which are poorer in carbon and also more suitable than products richer in carbon because on the one hand the adhesion between the carbon and the molten metals depends upon the proportion of carbon contained in the metals as has been already recognized by Moissan while on the other hand the products richer in carbon are liable to give off carbon in the form of scaly graphite whereby the connection between the filament and the supply wire might be loosened.
- Another form of carrying into practice the soldering together of filaments and their su ply wires by means of carbids and their so id solutions consists in mixing such finely powdered substances with just a suilicient quantity of an agglomerant such as gum arabic solution of sugar or the like or with a 100 colloidal metal or metals or with a colloidal oxid or oxids of a metal or metals so-thata pasty mass is obtained and a plying .isuch mass to the point at which t e two parts have to be connected.
- the mass is grad- 10:3
- This modification is particularly suitable for metals capable of lorming carbids very rich in carbon for instance for vanadium.
- a solder very suitable for the process described is obtained by mixing 90 parts of finely 0wdered vanadium, 5 parts of finely pow cred gra bite and 5 parts gum arabic with a itt 0 water so as to form a pasty mass which is used in the manner described.
- colloidal metals or- 055 advantageouslycolloidaloxids may be employed as agglomerants.
- Claims 1 As a new means of connecting inca11 descent lamp filaments to their supply wires, a solder containing a carbid of a n'iet-al melting at a very high temperature, substantially as described.
Description
UNITED STATES PATENT OFFICE.
HANS KUZEL, OF BADEN, NEAR VIENNA, AUSTRIA-HUNGARY.
SOLDER FOR INCANDESCENT-LAMP FILAMENTS.
To all whom it may concern:
Be it known that l, llans Knish, a subfict of the Emperor of Germany, residim at aden, near Vienna, Empire of Austriadiimar), have invented certain new and'useful Improvements in Solders for Incandescent- Lamp Filaments, of which the following is a specification.
My invention relates to the means for electrically connecting the carbon filaments of electric glow lamps with the supply wires, and the object of the invention is to obtain a good connection of a metallic character, which conducts the current better than the usual carbon cements and carbon coatin s, and for this urpose I make use of a metal ic material me ting at a high temperature and which adheres equallv well to the filament and to the metal supply wires.
1 have found that metal earbids melting at high temperatures and their solid solutions in an excess of metal constitute the desired metallic connecting material. It has been found that the carbon compounds of the metals melting at extremely high temperatures such as manganese, chromium, molybdenum, tungsten, uranium, vanadium, tantalum, niobium, titanium, zirconium, nickel, cobalt, iron are particularlysuitable for the above pur iose. 'lhe earbids of all of these metals and the solid solutions of such carbids in an excess of metal have a certain affinity for carbon owing to the fact that they con tain carbon themselves and very firmly adhereto carbon if applied thereto in a molten state. if for Instance, the ends of a carbon filament are dipped into molten carbid of tungsten pre ared by the method of Moissan the pores 0 the carbon filament ends are soaked or filled with the carbid and after withdrawing tho ends of the filament from the molten carbid it will be found that these ends are covered with a metallic coating. The thickness of this coatingmay be increased at will by repeatedly dip in the filament ends into the molten carbi an this coating so firmly-adheres to the carbon that in most cases it cannot be removed from the same without destro ing the carbon. If instead of a carbon fi ament a metal wire-is dipped into the molten carbid it becomes also coated with the latter. If therefore the molten carbid is a plied in an suitable mannew to the ends 0 acarbon ament and its metallic (say nickel)" supply wires while they;
Specification of Letters Patent.
Application filed January 19, 1806.
Patented Feb. 9, 1909.
Serial No. 296,884.
are held in juxtaposition or in contact with each other or temporarily secured to each other by any mechanical means such carbid will solder firmly together the two parts although they consist of heterogeneous materials and as the soldering knot may be made as large as may be desired a connection is established thereby, the electric resistance of which is the minimum of what may be practically obtained. The same. result may be obtained if instead of a carbon filament a filament of some other material such as metal, boron or silicon, or instead of the carbid of tungsten another carbid melting at a very high tem erature is used.
T e carbid of tungsten or any other carbid used need not be employed in their pure state for the purposes of the present invention. The raw product obtained for instance by the methods of Moissan, in the above case for instance by reducing tungstic acidby carbon, and containing from 0.67 to 6.33% of carbon may be directly used, but those products which approximately correspond to the formula CW, are more suitable than the solid solutions of the carbid in the metal which are poorer in carbon and also more suitable than products richer in carbon because on the one hand the adhesion between the carbon and the molten metals depends upon the proportion of carbon contained in the metals as has been already recognized by Moissan while on the other hand the products richer in carbon are liable to give off carbon in the form of scaly graphite whereby the connection between the filament and the supply wire might be loosened.
Another form of carrying into practice the soldering together of filaments and their su ply wires by means of carbids and their so id solutions consists in mixing such finely powdered substances with just a suilicient quantity of an agglomerant such as gum arabic solution of sugar or the like or with a 100 colloidal metal or metals or with a colloidal oxid or oxids of a metal or metals so-thata pasty mass is obtained and a plying .isuch mass to the point at which t e two parts have to be connected. The mass is grad- 10:3
u ally heated to a white heat either inthe ordinary wa or by means of the electric current or o the voltaic arc and if required in the absence of air; either in vacuum or in gases",- or vapors such as dlummatmgI-gas, 11c
hydro en, nitrogen, benzin, vapors etc. whereby it is molten or sintered. A modification of this form of carrying into practice my invention consists in that the carbids or their solid solutions are not used when already formed but are formed in the course of the soldering process, that is to say, metals melting at a very high temperature and in a finely powdered state are mixed with carbon or an organic substance giving oil carbon on being heated and with just sullicient quantity of an agglomerant so as to form a pasty mass. This mass is applied to the parts at the point where they are to be connected and heated as above described. The carbon present or given oil combines with the metals used whereby carbids of the latter are formed. This modification is particularly suitable for metals capable of lorming carbids very rich in carbon for instance for vanadium. From this a solder very suitable for the process described is obtained by mixing 90 parts of finely 0wdered vanadium, 5 parts of finely pow cred gra bite and 5 parts gum arabic with a itt 0 water so as to form a pasty mass which is used in the manner described. Instead of or anic agglomerants also colloidal metals or- 055 advantageouslycolloidaloxidsmay be employed as agglomerants.
I do not claim in this case the process of p a solder containing carbid of tungsten,
electrically connecting the filaments to the leadin -in wires, as that forms the subject of a divisional application for patent filed by me March 26, 1907, Pat. No. 898,979, Sept. 15, 1908.
Claims 1. As a new means of connecting inca11 descent lamp filaments to their supply wires, a solder containing a carbid of a n'iet-al melting at a very high temperature, substantially as described.
2. As a new means of connecting incandescent lamp filaments to their sup )ly wires, a solder containing carbids of metals melting at very high temperatures, substantially as described.
3. As a new means of connecting incandescent lamp filaments to their supply wires,
substantially as described.
4. As a new means of connecting incandescent lamp filaments to their supply wires, a solder consisting of carbid of tungsten, substantially as described.
In testimony whereof I have signed my name to this specification, in the presence of two subscribing witnesses. v
HANS KUZEL.
Witnesses:
'l. GEORGE HARDY, ALVESTO S. HooUE.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29688406A US912245A (en) | 1906-01-19 | 1906-01-19 | Solder for incandescent-lamp filaments. |
| US364732A US898979A (en) | 1906-01-19 | 1907-03-26 | Process of electrically connecting filaments to supply-wires in electric glow-lamps. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29688406A US912245A (en) | 1906-01-19 | 1906-01-19 | Solder for incandescent-lamp filaments. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US912245A true US912245A (en) | 1909-02-09 |
Family
ID=2980681
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US29688406A Expired - Lifetime US912245A (en) | 1906-01-19 | 1906-01-19 | Solder for incandescent-lamp filaments. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US912245A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2614322A (en) * | 1946-01-09 | 1952-10-21 | Walter A Pendleton | Spring cutter |
| US2991192A (en) * | 1958-10-30 | 1961-07-04 | Frank A Halden | Process of coating graphite with niobium-titanium carbide |
| US3017286A (en) * | 1958-09-08 | 1962-01-16 | James S Kane | Method for coating graphite with niobium carbide |
| US3208872A (en) * | 1956-12-31 | 1965-09-28 | Filmore F Criss | Carbide coatings on graphite |
| US3208870A (en) * | 1956-12-31 | 1965-09-28 | Filmore F Criss | Carbide coatings for graphite |
-
1906
- 1906-01-19 US US29688406A patent/US912245A/en not_active Expired - Lifetime
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2614322A (en) * | 1946-01-09 | 1952-10-21 | Walter A Pendleton | Spring cutter |
| US3208872A (en) * | 1956-12-31 | 1965-09-28 | Filmore F Criss | Carbide coatings on graphite |
| US3208870A (en) * | 1956-12-31 | 1965-09-28 | Filmore F Criss | Carbide coatings for graphite |
| US3017286A (en) * | 1958-09-08 | 1962-01-16 | James S Kane | Method for coating graphite with niobium carbide |
| US2991192A (en) * | 1958-10-30 | 1961-07-04 | Frank A Halden | Process of coating graphite with niobium-titanium carbide |
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