US901009A - Process of making chloracetic ether. - Google Patents
Process of making chloracetic ether. Download PDFInfo
- Publication number
- US901009A US901009A US37123707A US1907371237A US901009A US 901009 A US901009 A US 901009A US 37123707 A US37123707 A US 37123707A US 1907371237 A US1907371237 A US 1907371237A US 901009 A US901009 A US 901009A
- Authority
- US
- United States
- Prior art keywords
- ether
- making
- chloracetic
- chlor
- imbert
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 title description 6
- 238000000034 method Methods 0.000 title description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- GIAJLXBOALRQTE-UHFFFAOYSA-N 1,1-dichloro-2-ethenoxyethane Chemical group ClC(Cl)COC=C GIAJLXBOALRQTE-UHFFFAOYSA-N 0.000 description 1
- YAKWKNULMWMIJR-UHFFFAOYSA-N 1,1-dichloro-2-ethoxyethene Chemical group CCOC=C(Cl)Cl YAKWKNULMWMIJR-UHFFFAOYSA-N 0.000 description 1
- 241000920033 Eugenes Species 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/62—Halogen-containing esters
- C07C69/63—Halogen-containing esters of saturated acids
Definitions
- I claim as my invention A process for producing chlor-acetic ether from (li-chlor-ethoxy-ethylene, which consists in subjecting the latter to the action of Waiter in the proportion of 1:1 grammolecu e.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
Description
UNITED STATES GEORGES IMBERT, OF NUREMBERG, GERMANY.
PROCESS OF MAKING GHLORACETIC ETHER.
Specification of Letters Patent.
Patented Oct. 13, 1908.
Application filed May 1, 1907. V Serial No. 371,237.
To all whom it may concern:
Be it known that I, GEORGES IMBERT, a subject of the German Empire, and residing at N o. 54 Guaelstrasse, Nurcnrbe'rg, Bavaria, Germany, have invented a new and. useful Frocess of Producing Chloracctic Ether,-of which the following is a description.
In the British Patent No. 678 of 1906 the production of chlor-acetic ether from dichlorethoxy-ethylene and alcohol is described, the processbeing represented by the following 'equation: 7
C Cl H.OO H +C H OH= My experiments have shown, that the alcohol present in the reaction may be replaced by an equivalent quantity of water, the process being thus rendered considerably 20 cheaper. The process is then represented by the following equation ogol nloo n +HOII= n01 +oH,c1.oooc,u,.
Example: 141 kilos of di-chlor-ethoxyethylene are heated to the boiling point and 18 kilos of water are allowed to slowly flow in. Hydrochloric acid escapes in streams and chlor-acetic ether remains. The output is approximately quantitative.
I claim as my invention A process for producing chlor-acetic ether from (li-chlor-ethoxy-ethylene, which consists in subjecting the latter to the action of Waiter in the proportion of 1:1 grammolecu e.
In testimony whereof I affix my signature in the presence of two witnesses.
' GEORGES IMBERT.
Witnesses: I
EUGEN SALIGENSTEIN, JOHANN FAMMERTHAL.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US37123707A US901009A (en) | 1907-05-01 | 1907-05-01 | Process of making chloracetic ether. |
| US418898A US935606A (en) | 1907-05-01 | 1908-03-02 | Process of obtaining chlor-acetic acid. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US37123707A US901009A (en) | 1907-05-01 | 1907-05-01 | Process of making chloracetic ether. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US901009A true US901009A (en) | 1908-10-13 |
Family
ID=2969432
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US37123707A Expired - Lifetime US901009A (en) | 1907-05-01 | 1907-05-01 | Process of making chloracetic ether. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US901009A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2874074A (en) * | 1956-05-08 | 1959-02-17 | Nat Aluminate Corp | 1, 2-substituted imidazolinium salt and treatment of cellulosic fibrous materials therewith |
-
1907
- 1907-05-01 US US37123707A patent/US901009A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2874074A (en) * | 1956-05-08 | 1959-02-17 | Nat Aluminate Corp | 1, 2-substituted imidazolinium salt and treatment of cellulosic fibrous materials therewith |
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