US863949A - Vinegar apparatus. - Google Patents

Vinegar apparatus. Download PDF

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US863949A
US863949A US34831606A US1906348316A US863949A US 863949 A US863949 A US 863949A US 34831606 A US34831606 A US 34831606A US 1906348316 A US1906348316 A US 1906348316A US 863949 A US863949 A US 863949A
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generators
receptacle
valves
chargers
vinegar
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Eugene A Spink
James W Norton
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • C12J1/10Apparatus

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  • This invention relates to improvements in vinegar apparatus and automatic feeders or chargers therefor, the purpose ⁇ of our invention being to provide means for delivering a charge or predetermined quantity of alcoholic solution to the generators at intervals, the quantity of the charge and the time between the charges being under control of the operator, a second purpose of the invention is to provide'means whereby the charges will not be exposed to the external atmosphere after being drawn from the supply tank, and to generally improve the mechanism so that friction will be reduced and leakage will be avoided.
  • FIG. l is a sectional elevation showing the several floors of vinegar works, provided with the invention.
  • Figs. 2 and 3 are front and side elevations.
  • Fig. 4 is a view partly in section showing one of the chargers and the first and second generators.
  • Fig. 5 is a side elevation.
  • Fig. 6 is a sectional view of one form of the bucket that operates the supply and cut-off valves when lowered.
  • Figs. 7 and 8 are detail sections.
  • the supply tank 9 receives the alcoholic solution through a pipe I0 and during the process of making vinegar the liquefied aldehydic products are delivered to the supply tank through the pipe ll, and air under pressure is delivered to the lowerportion of the generators through branch pipes l2 that are coupled to the main air supply pipe I3,
  • the generators are preferably arranged in both vertical and horizontal series, and a charge container I4 is provided for each of the vertical series of generators, and in the present instance we have shown three generators, l5, IG and 17 arranged in vertical series on different horizontal planes.
  • the charge containers I4 are connected to the upper generators l5, and the lower end of the upper generator is connected to the second generator 16 such generator being connected to the lower generator that discharges into a receiving tank lS.
  • the connections shown in detail by Fig. 8 of'the drawings comprise sections of wooden pipe I9 and 2O that are connected by a larger section 2l, the lower pipe 2() has attached thereto a leather apvalve 22 which opens upward and when closed will rest upon the upper end of the pipe, such valves have attached thereto blocks as shown.
  • the tubes are apertu-red to provide bearings for spindles 23 that carry pins 24, the heads of the spindles project beyond the pipes 2l and carry an arm 25 to which the valve raising or opening mechanism is attached.
  • valves may be raised from their seats with very little effort, and there is no liability of leakage or the spindles jamming by the wood swelling or contracting.
  • the valves for the horizontal pipes are constructed in the same manner as the valves for the vertical pipes, see Fig. 7 of the drawings.
  • shafts or rock-bars 29, 30 and 3l they being of suilicient length to extend across one of the horizontal series of generators, and each of the shafts carry arms 32, such arms being connected to the arms 25 of the valves 2G, 27 and 28 by rods 33 so that when the shafts are turned the valves will be opened.
  • the shafts or rock-bars each carry a disk or wheel 34, about which passes a flexible connection 35, to one end of which a weight 3G is secured and to the other end is secured a receptacle 37, which when empty is over-balanced by the weight.
  • the receptacles 37 are provided with a valved outlet opening and below the receptacles there are pans 38 from which depend pipes or spouts, such pans having upward extending pins that are intended to engage the valves and raise the same when the receptacles are lowered so that any and all liquid contained in the receptacles will be discharged.
  • Each receptacle 37 has an outward projecting pin or stud 39 that is adapted to engage a pivoted catch-and-release-bar 40 that is so constructed and positioned that the same will hold the receptacle 37 when it has been filled and lowered to turn the shaft and operate the valves.
  • the shafts may be rocked or turned by any suitable mechanical means and they can be coupled so that they will be turned successively or one after the other, the periods intervening between the operating oi the valves being under the control oi time mechanism, an independent water supply, or an attendant, in practice we prefer to use the devices shown, as the pivoted catch and release bars 40 are simple and effective.
  • the closed charge containers I4 are connected together by pipes 4l located slightly below the upper ends of the kegs or chargers 14, the last of the series of chargers having an air outlet pipe 48, that extends upward above the normal level of the liquid in the supply tank.
  • the kegs or chargers are filled through a pipe 42, the pipe having a valve 43 that may be adjusted so that the chargers may be iilled within a certain period of time, and when the chargers have all been filled from the supply tank 9, the overflow will pass from the first charger through the pipe 44, that leaves the same at a higher level than the pipe 41, the
  • the shaft 47 may be connected to the outlet pipes of the lower generator, when the same have valves, but in practice such pipes are usually open as they lead directly into the storage tank.
  • the receptacles may be suitably guided and the pins 39 not only engage the hooks but also serve as a stop to limit the swing of the catch-and-release-bars in ⁇ one direction.
  • the overflow that is used to operate the automatic valve opening mechanism is usually discharged into a waste pipe or sewer but if desired it may be collected in a tank and returned to the supply tank 9,
  • the outlet openings for the receptacles 37 may be of such construction that the out-flow Inay be regulated to hold the receptacle down for the period of time desired, for instance the upper receptacle may have a comparatively small discharge opening so that the valves will be held open for quite a long period of time while the chargers are emptying themselves into the upper generators, and the counter weights on the second and third receptacles may be varied so that less liquid will be required to cause the receptacles to descend, and as to such details our invention may be modified or varied to meet such requirements as may arise. l
  • the generators which contain shavings are charged with an alcoholic solution to saturate the shavings, and vinegar' cultures are introduced, they propagating on the shavings, and as air is introduced into the generators the alcohol before becoming vinegar is converted into aldehyde, and it is upon the aldehyde that the bacteria feed.
  • the generators are closed in order to prevent the introduction of bacteria not essential in converting low wines into vinegar.
  • the alcoholic solution is pumped or fed from a still into the supply tank 9, and such solution contains not more than 25 of alcohol.
  • the tank 9 is supplied with an alcoholic liquidithrough the'pipe 10, and with aldehyde or condensed alcoholic vapors that arise from oxidation of the alcohol, the vapors being expelled from the generators by the air that is forced therein, the vapors being Condensed and then carried from the condenser to the supply tank.
  • the temperature in the upper generator will be about 90D F., and in the next generator below about 80 F., and in the last or lower generator about 7 6 F., the largest amount of aldehyde being recovered from the first generator, and by rising closed generators and saving the products that are usually lost by evaporation we are able to convert the alcoholic solution into very strong and pure vinegar.
  • the pipe 42 having a valve 43 enters the first of a series of charge containers, and as each of the containers are being filled the air therefrom escapes through a vent or air outlet pipe 48.
  • the generators are of the closed type, and filtered air is forced into each generator through pipes 12, such pipes being connected with an air supply pipe 13.
  • the vapors that are given ott by the oxidation o the alcohol and the air that is forced into the generators passout oi' the generators through pipes that lead to a condenser, and the condensed products are pumped into the supply tank.
  • the quantity lost by evaporation when open generators are used amounts to about 15%, and this waste is saved lby the use of the apparatus shown.
  • valves between the chargers and the generators are opened and closed successively or one after the other, and when the Supply valve to the chargers is properly adjusted the process is practically automatic.
  • l.. ln an apparatus of the character set forth, a supply tank, a plurality of-charge containers connected therewith, a plurality of generators connected to the charge containers, a valve or cut-oit in the connection between each ot' the charge containers and each of the generators, means tor connecting the valves or cutotfs to each other, and means for actuating the connection when a charge has been admitted to the containers.
  • L. ln a vinegar apparatus, a supply tank, a horizontal series of charge containers connected to the supply tank, a vertical series of generators connected with the charge containers. valves in the connections between the charge containers and the upper generators ot' a series, rockshafts connected to each of the valves, an overflow pipe from one of the charge containers and receiving means for the overflow operatively connected with the rock-shafts.
  • a vinegarI apparatus In a vinegarI apparatus, a supply tank, a plurality oi. charge containers connected with the supply tank and to each other so that the charge containers will be filled successively, a vertical series of generators, valved pipes for connecting the charge containers and thenpper generators, valved pipes between each of the generators constituting a vertical series, a series ot rock-shafts one for each horizontal series ol valves.r connections between the rockshafts and the valves. and automatic means for successively openingl the horizontal series of valves. substantially as shown and for the purpose set forth.
  • a vinegar apparatus a plurality of generators, closed chargers maintained above the generators, a supply tankfa pipe leading from the supply tank to "one of the chargers, pipes connecting the chargers so that they will be iilled successively, an overflow through which liquid passes irom the chargers when all have been filled, and means operated bysuch overflow for establishing communication between the chargers and the generators.
  • a vinegar apparatus the combination of a receptacle that is adapted to receive a predetermined quantity of liquid in a certain time, means for operatively connecting such receptacle with valve operatingl mechanism, means i'or holding the receptacle in its lowered position, and means for releasing the holding means when the contents of the receptacle have been discharged therefrom.
  • G. 'lhe combination with a supply tank, a series of chargers and generators that are supplied therefrom, means for connecting valves in the connections between the generators and the valves between the chargers and the upper series of generators, a rock shat't ior cach horizontal series ot' valves, receptacles connected with each oi the rock shafts, an overflow connected with one of the chargers and adapted to discharge into the upper receptacle, means for holding the receptacle lowered and other means for releasing the receptacle when the contents thereoi has been discharged.
  • a vinegar apparatus In a vinegar apparatus, a supply tank, a series of charge containers in communication with the supply tank, an air-outlet pipe attached to one of the charge containers, an overflow pipe from one of the charge containers, a ver tical series oi generators below each charge container, valved connections between the charge containers and the upper series of generators. valved connections between the generators constituting a vertical series, a series ot' rockshafts, connections between such rock-shafts and the 75 valves. and means t'or turning automatically the rock shai'ts to open the valves when the charge containers have been tilled, substantially as set forth.

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Description

No. 999,949.l Y A PATENTBD AUG. zo, 1907. E; A. SPINK'& J. w. NORTON.
VINEGAR APPARATUS.
APPLIOATION FILED 9110.17.1996.' s ysmuzTs-SHEET 1.
No. 963,949. l PATENTED AUG. 2o, 1907.v B. A., SPINK 9 J.vv W. NORTON. VINEGAR APPARATUS.
APPLICATION FILED DBO.17,1906.
mm-m l u@ A@ l TH: :vonnis PETERS cu., wAsmNomN, n. c.
No. 869,949; PUBMED-AUG. 2o, 190:7. E. A. SPINK 9 J. W. NORTON.
VINEGAR APPARATUS,
APPLICATION FILED DEO.17.1906. l
3 SHEETS-SHEET 3- warwom A /7 1HE Ivo/ems Pzrsks cu.. wlsumaron, D. c.
UNITED STATES PATENT OFFICE.
EUGENE A. SPINK, OF CHICAGO, ILLINOIS, AND JAMES W. NORTON, OF WASHINGTON,
DISTRICT OF COLUMBIA.
VINEGAR APPARATUS.
Specieation of Letters Patent.
Patented Aug. 20, 1907'.
Application iiled December 17,1906. Serial No. 348.316.
To all whom it may concern:
Bc it known that we, EUGENE A. SPINK, a citizen of the United States, residing at Chicago, in the county of Cook, State of Illinois, and JAMES W. NORTON, a citizen of the United States, residing at Washington, in the District of Columbia, have jointly invented certain new and useful Improvements in Vinegar Apparatus and Automatic Feeders Therefor, of which the following is a specication.
This invention relates to improvements in vinegar apparatus and automatic feeders or chargers therefor, the purpose `of our invention being to provide means for delivering a charge or predetermined quantity of alcoholic solution to the generators at intervals, the quantity of the charge and the time between the charges being under control of the operator, a second purpose of the invention is to provide'means whereby the charges will not be exposed to the external atmosphere after being drawn from the supply tank, and to generally improve the mechanism so that friction will be reduced and leakage will be avoided.
Our invention in a preferred form is illustrated in the accompanying drawings, in which- Figure l is a sectional elevation showing the several floors of vinegar works, provided with the invention. Figs. 2 and 3 are front and side elevations. Fig. 4 is a view partly in section showing one of the chargers and the first and second generators. Fig. 5 is a side elevation. Fig. 6 is a sectional view of one form of the bucket that operates the supply and cut-off valves when lowered. Figs. 7 and 8 are detail sections.
The supply tank 9, receives the alcoholic solution through a pipe I0 and during the process of making vinegar the liquefied aldehydic products are delivered to the supply tank through the pipe ll, and air under pressure is delivered to the lowerportion of the generators through branch pipes l2 that are coupled to the main air supply pipe I3, The generators are preferably arranged in both vertical and horizontal series, and a charge container I4 is provided for each of the vertical series of generators, and in the present instance we have shown three generators, l5, IG and 17 arranged in vertical series on different horizontal planes.
The charge containers I4 are connected to the upper generators l5, and the lower end of the upper generator is connected to the second generator 16 such generator being connected to the lower generator that discharges into a receiving tank lS. The connections shown in detail by Fig. 8 of'the drawings comprise sections of wooden pipe I9 and 2O that are connected by a larger section 2l, the lower pipe 2() has attached thereto a leather apvalve 22 which opens upward and when closed will rest upon the upper end of the pipe, such valves have attached thereto blocks as shown. Below the valves 22 the tubes are apertu-red to provide bearings for spindles 23 that carry pins 24, the heads of the spindles project beyond the pipes 2l and carry an arm 25 to which the valve raising or opening mechanism is attached. By the arrangement shown the valves may be raised from their seats with very little effort, and there is no liability of leakage or the spindles jamming by the wood swelling or contracting. The valves for the horizontal pipes are constructed in the same manner as the valves for the vertical pipes, see Fig. 7 of the drawings.
In horizontal alinement with the connections 26, 27
and 28 between the 4chargers and the generators, are
shafts or rock- bars 29, 30 and 3l they being of suilicient length to extend across one of the horizontal series of generators, and each of the shafts carry arms 32, such arms being connected to the arms 25 of the valves 2G, 27 and 28 by rods 33 so that when the shafts are turned the valves will be opened. The shafts or rock-bars each carry a disk or wheel 34, about which passes a flexible connection 35, to one end of which a weight 3G is secured and to the other end is secured a receptacle 37, which when empty is over-balanced by the weight.
The receptacles 37 are provided with a valved outlet opening and below the receptacles there are pans 38 from which depend pipes or spouts, such pans having upward extending pins that are intended to engage the valves and raise the same when the receptacles are lowered so that any and all liquid contained in the receptacles will be discharged. Each receptacle 37 has an outward projecting pin or stud 39 that is adapted to engage a pivoted catch-and-release-bar 40 that is so constructed and positioned that the same will hold the receptacle 37 when it has been filled and lowered to turn the shaft and operate the valves.
The shafts may be rocked or turned by any suitable mechanical means and they can be coupled so that they will be turned successively or one after the other, the periods intervening between the operating oi the valves being under the control oi time mechanism, an independent water supply, or an attendant, in practice we prefer to use the devices shown, as the pivoted catch and release bars 40 are simple and effective.
In practice the closed charge containers I4 are connected together by pipes 4l located slightly below the upper ends of the kegs or chargers 14, the last of the series of chargers having an air outlet pipe 48, that extends upward above the normal level of the liquid in the supply tank. The kegs or chargers are filled through a pipe 42, the pipe having a valve 43 that may be adjusted so that the chargers may be iilled within a certain period of time, and when the chargers have all been filled from the supply tank 9, the overflow will pass from the first charger through the pipe 44, that leaves the same at a higher level than the pipe 41, the
overflow being discharged into the receptacle 37. When the amount of liquid in the receptacle 37 is sufficient to overcome the weight and the friction of the parts the receptacle will be lowered, its downward movement turning the shaft so that the valve from the supply tank will be closed and all of the valves between the chargers andthe upper generators will be opened, to admit a predetermined quantity of alcoholic solution to each of the upper Series of generators. When the rst receptacle falls or is lowered its outward projecting pin 39, will engage the upper end of the catch-and-release-bar 40 pushing the same out of its path, so that the hook will engage the pin and hold the receptacle lowered. When the contents of the upper receptacle has flowed therefrom and passed into the receptacle below such receptacle on its downward movement will engage the catch-and-release-bar below its pivot to disengage the hook from the upper receptacle, which is then raised by the weight to turn the shaft to its initial position opening the supply and cutting off the chargers from the generators. The action is repeated so that the shafts 3() and 31 are operated to successively connect the generators 16 and 17. The receptacle that engages the disk or wheel on shaft 31 engages a catch-and-release 45 and when the contents of the receptacle 46 is discharged the weight will return such receptacle to its normal position. The shaft 47 may be connected to the outlet pipes of the lower generator, when the same have valves, but in practice such pipes are usually open as they lead directly into the storage tank. The receptacles may be suitably guided and the pins 39 not only engage the hooks but also serve as a stop to limit the swing of the catch-and-release-bars in `one direction. The overflow that is used to operate the automatic valve opening mechanism is usually discharged into a waste pipe or sewer but if desired it may be collected in a tank and returned to the supply tank 9,
The outlet openings for the receptacles 37 may be of such construction that the out-flow Inay be regulated to hold the receptacle down for the period of time desired, for instance the upper receptacle may have a comparatively small discharge opening so that the valves will be held open for quite a long period of time while the chargers are emptying themselves into the upper generators, and the counter weights on the second and third receptacles may be varied so that less liquid will be required to cause the receptacles to descend, and as to such details our invention may be modified or varied to meet such requirements as may arise. l
ln practice the generators which contain shavings are charged with an alcoholic solution to saturate the shavings, and vinegar' cultures are introduced, they propagating on the shavings, and as air is introduced into the generators the alcohol before becoming vinegar is converted into aldehyde, and it is upon the aldehyde that the bacteria feed. The generators are closed in order to prevent the introduction of bacteria not essential in converting low wines into vinegar. When the generators are in condition for use the alcoholic solution is pumped or fed from a still into the supply tank 9, and such solution contains not more than 25 of alcohol. When the generators have been charged air at the proper temperature is forced into the generators and the temperature therein will be raised and aldehydic vapors will be given off, these vapors being condensed and pumped back into the supply tank instead of being allowed to escape into the atmosphere; the saving of the aldehydic vapors not only results in enriching the low wine with aldehyde which is a desirable element in the manufacture of vinegar', but avoids contamination of the atmosphere about the generators, and incidentally the propagation of germs that are not necessary or helpful in the conversion of alcohol into vinegar'.
Referring .to the drawings, particularly Figs. 2 and 3, the tank 9 is supplied with an alcoholic liquidithrough the'pipe 10, and with aldehyde or condensed alcoholic vapors that arise from oxidation of the alcohol, the vapors being expelled from the generators by the air that is forced therein, the vapors being Condensed and then carried from the condenser to the supply tank.
In the production of vinegar with our apparatus, and with proper cultures upon the shavings in the generators, and with a supply of filtered air, the temperature in the upper generator will be about 90D F., and in the next generator below about 80 F., and in the last or lower generator about 7 6 F., the largest amount of aldehyde being recovered from the first generator, and by rising closed generators and saving the products that are usually lost by evaporation we are able to convert the alcoholic solution into very strong and pure vinegar. The pipe 42 having a valve 43, enters the first of a series of charge containers, and as each of the containers are being filled the air therefrom escapes through a vent or air outlet pipe 48. When all of the chargers are filled the liquid will fiow out ofthe first container into the upper bucket or receptacle 37. The time required to fill the receptacle depends either upon the adjustment of the valve 43 or upon the size of the bucket 37. l1`he receptaele or bucket is held raised by a counterweight 36, and when such weight is overcome the receptacle will be lowered and its downward movement actuates a' rock-shaft 29 that has an arm, movement of the arm in the proper direction closing a valve in the supply-pipe thatV enters the chargers, movement of the rock-shaft and other arms thereon opening the valves in the connections between the charge containers and the upper generators. As the liquid flows out of the charge containers, air will be drawn into the chargers through the vent-pipe, and such air will be forced out of the chargers when they are refilled.
When the first or upper receptacle descends it is held down by the catch 40 and when its contents is discharged into the next receptacle beneath, such receptacle descends and releases the catch from the upper receptacle, the downward movement of the second receptacle opening the previously closed valves in the connections between the generators 15 and 1G. The downward movement of the secon d receptacle or bucket releases the catch that holds down the first bucket, and when the rock-shaft 30 is turned the valves between the generators 15 and 16 are opened to allow the low grade vinegar to pass from the first generators, on the upper floor, to the generators on the next lower floor, the operation being repeated the third or lower of the vertical series of generators discharging the finished product into a receiving tank 18.
The generators are of the closed type, and filtered air is forced into each generator through pipes 12, such pipes being connected with an air supply pipe 13. The vapors that are given ott by the oxidation o the alcohol and the air that is forced into the generators passout oi' the generators through pipes that lead to a condenser, and the condensed products are pumped into the supply tank. The quantity lost by evaporation when open generators are used amounts to about 15%, and this waste is saved lby the use of the apparatus shown.
The valves between the chargers and the generators are opened and closed successively or one after the other, and when the Supply valve to the chargers is properly adjusted the process is practically automatic.
We claim.
l.. ln an apparatus of the character set forth, a supply tank, a plurality of-charge containers connected therewith, a plurality of generators connected to the charge containers, a valve or cut-oit in the connection between each ot' the charge containers and each of the generators, means tor connecting the valves or cutotfs to each other, and means for actuating the connection when a charge has been admitted to the containers.
L. ln a vinegar apparatus, a supply tank, a horizontal series of charge containers connected to the supply tank, a vertical series of generators connected with the charge containers. valves in the connections between the charge containers and the upper generators ot' a series, rockshafts connected to each of the valves, an overflow pipe from one of the charge containers and receiving means for the overflow operatively connected with the rock-shafts.
I. In a vinegarI apparatus, a supply tank, a plurality oi. charge containers connected with the supply tank and to each other so that the charge containers will be filled successively, a vertical series of generators, valved pipes for connecting the charge containers and thenpper generators, valved pipes between each of the generators constituting a vertical series, a series ot rock-shafts one for each horizontal series ol valves.r connections between the rockshafts and the valves. and automatic means for successively openingl the horizontal series of valves. substantially as shown and for the purpose set forth.
el. In a vinegar apparatus. a plurality of generators, closed chargers maintained above the generators, a supply tankfa pipe leading from the supply tank to "one of the chargers, pipes connecting the chargers so that they will be iilled successively, an overflow through which liquid passes irom the chargers when all have been filled, and means operated bysuch overflow for establishing communication between the chargers and the generators.
5. lu a vinegar apparatus the combination of a receptacle that is adapted to receive a predetermined quantity of liquid in a certain time, means for operatively connecting such receptacle with valve operatingl mechanism, means i'or holding the receptacle in its lowered position, and means for releasing the holding means when the contents of the receptacle have been discharged therefrom.
G. 'lhe combination with a supply tank, a series of chargers and generators that are supplied therefrom, means for connecting valves in the connections between the generators and the valves between the chargers and the upper series of generators, a rock shat't ior cach horizontal series ot' valves, receptacles connected with each oi the rock shafts, an overflow connected with one of the chargers and adapted to discharge into the upper receptacle, means for holding the receptacle lowered and other means for releasing the receptacle when the contents thereoi has been discharged.
T. In a vinegar apparatus, a supply tank, a series of charge containers in communication with the supply tank, an air-outlet pipe attached to one of the charge containers, an overflow pipe from one of the charge containers, a ver tical series oi generators below each charge container, valved connections between the charge containers and the upper series of generators. valved connections between the generators constituting a vertical series, a series ot' rockshafts, connections between such rock-shafts and the 75 valves. and means t'or turning automatically the rock shai'ts to open the valves when the charge containers have been tilled, substantially as set forth.
EUGENE A. SPINK. JAMES W. NORTON. Witnesses:
WM. J NnALn, EUGENE W, JOHNSON.
US34831606A 1906-12-17 1906-12-17 Vinegar apparatus. Expired - Lifetime US863949A (en)

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