US85256A - Improvement in bone-coal and other filters - Google Patents

Improvement in bone-coal and other filters Download PDF

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US85256A
US85256A US85256DA US85256A US 85256 A US85256 A US 85256A US 85256D A US85256D A US 85256DA US 85256 A US85256 A US 85256A
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bone
dust
coal
filters
improvement
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes

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  • the dust presents a greater surface, over which the sirup should pass in its flow through the filter, than an equal weight of coal in larger bits or fragments, it has been found impracticable to use it, for the reason, that, when it becomes fully saturated, it forms a pasty mass, through which the sirup is unable torun with the rapidity requisite for. its practical use and when it may be attempted to hasten orassist the operation by means of'pressure on the surface of the liquor in the filter, or by suction beneath the filtering-material, an opening or channel is forced through the mass, by which the liquor escapes, withoutderiving any benefit from the main body of the coal.
  • the object of my invention is to utilize, for filteringpurposes, the bone-dust thathas been of but little value, and it is accomplished by mixing the bone-dust with fine anthracite coal, or other similar substance or material that is insoluble in the liquid to be filtered, and remains unafiected under the circumstances-of heating, washing, and steaming, to which it may be subjected, except when thereby brought into alcondition more favorable for the intended purpose, and which will hold the particles of the bone-dust apart, and prevent their "orming, either by themselves or with the dividing- .tgent, a paste that is comparatively impervious to the solution or liquidit is desired to filter.
  • the bone-dust is so separated that it'can no longer form a pasty mas'sthat is comparatively impervious'to the fluid to'be filtered, 1
  • the bone-dust may be more thoroughly 1 cleaned by washing and steaming, as a preliminary: to its restoration by fermentation, or acids or other agents.
  • the proportionate quantity of anthracite or other divisor may be adjusted so that'the percolation'will be slow, owing to the preponderance of the bone-dust, or
  • the filtration will be more rapid, and a thicker stratum of the mixed material will be required to retain the liquid in contact with the bone a sufficient time to become thoroughly decolorized.
  • the fine dust of bone-black that would otherwise be useless for I claim, as my inventiona filter, is rendered of value, and advantage may be- Theuseofmlividing-ugent substantiallyztsdescribed, taken of the larger proportion of. surface ziflbrded by in conneetionwith the filtering-material,ibrthe purpose the same weight of dust, compared with bits of greater of filtration.

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtering Materials (AREA)

Description

; cited HENRY TonsTRIcjK,
OF NEW YORK, N. Y.
Letters Patent No. 85,256, dated December 22, 1868.
IMPROVEMENT IN BONE-COAL AND OTHER FILTERS.
The Schedule referred to in these Letters Patent and making part of the same.
- To all whom it may concern Be it known that I, Hiiwnr Tons'rRIo 'of New York, in the county and State of N eW York, have invented a certain new and useful Improvement in Bone- Ooal and other Filters; and I do hereby'declare that the following is a full,.clear, and exact description of the same, and the manner in which it may be applied.
It has hitherto been necessary to carefully sift the bone-coalprepared for filters, such as are commonly used by sugar-refiners, for the purpose of removing the fine dust, and the waste from this cause, occasioned by the repeated and necessary handlings in placing it in the filters and removing it from them, and in rebnrning andsifting, has been a very important element in the cost of the production of refined sugar. Although the dust presents a greater surface, over which the sirup should pass in its flow through the filter, than an equal weight of coal in larger bits or fragments, it has been found impracticable to use it, for the reason, that, when it becomes fully saturated, it forms a pasty mass, through which the sirup is unable torun with the rapidity requisite for. its practical use and when it may be attempted to hasten orassist the operation by means of'pressure on the surface of the liquor in the filter, or by suction beneath the filtering-material, an opening or channel is forced through the mass, by which the liquor escapes, withoutderiving any benefit from the main body of the coal. In a similar manner, when the bone has not been sifted, to remove the dust, the latter fills up the pores or interstices between the larger pieces, and speedily clogs it to a degree that renders the filter practically useless long before the decolorizing and purifying-power of the bone is exhausted.
The object of my invention is to utilize, for filteringpurposes, the bone-dust thathas been of but little value, and it is accomplished by mixing the bone-dust with fine anthracite coal, or other similar substance or material that is insoluble in the liquid to be filtered, and remains unafiected under the circumstances-of heating, washing, and steaming, to which it may be subjected, except when thereby brought into alcondition more favorable for the intended purpose, and which will hold the particles of the bone-dust apart, and prevent their "orming, either by themselves or with the dividing- .tgent, a paste that is comparatively impervious to the solution or liquidit is desired to filter.
To enable others skilled in the arts to which it appertains, to make and, use my invention, I will proceed to describe in detail the manner of carrying'it into effect.
I mix the bone-black as thoroughly and intimately as may be possible, with about the same measure of fine anthracite coal, and, after heating the mixture, place it in a filter, of any ofthe ordinary forms, provided at the bottom with a lining of flannel or felt, to prevent the washing out of the dust.
. The same end may be attained by the employment, as a divisor or separating-agent, instead of fine anthra cite co'al, of any other material with a similar nature,
thatis insoluble, and not acted upon 'in theliquid to be filtered, and under the circumstances incident to filtration and renovation of the bone by steaming and heating, or by fermentation with acids, or other treat ment to which it may be subjected while in use, or for subsequent cleansing.
By the use of a mixing-agent that fulfils these requirements, and the particles of which are of a hard, sharp, and glazed character, the bone-dust is so separated that it'can no longer form a pasty mas'sthat is comparatively impervious'to the fluid to'be filtered, 1
and all portions of its surface are thus brought into efiicient action in the filter.
The same principle may be applied to burnt blood,
or other decolorizing-agent or filtering-medium, in a finely-divided'state, that may be used instead of bonecoal, and which would otherwise pack itself together, so that the fluid to be filtered would fail to passr'eadily through it. The liquor and the filter should be kept heated, to promote its efficiency, and it is'believed that the mixtiu-e of fine anthracite, as described, retains the heat better than bone-coal alone.
I prefer the dust of anthracite as a dividing-agent, on account of its .cheapness, occasioned by the large quantities necessarily produced in the mining and working of coal, for which there has hitherto been no profitable use, and, although its power of decolorizing and sepa rating impurities, as a filter, may not be sufiicient to warrantits separate use for the purpose, its virtue in this respect is an addition to its intended function, of enabling the profitable use of the finedust of burnt bone.
By the admixture of a finely-divided glazed material,
as described, the bone-dust may be more thoroughly 1 cleaned by washing and steaming, as a preliminary: to its restoration by fermentation, or acids or other agents.
The reburning of bone-black dust, also, that has been hitherto impracticable, for the reason that it aggregates into a mass when wet with sirup, and sticks together in irregular lumps, and adheres to the calcinating-vessels, may be accomplished by the addition of a dividingagent, of the'character hereinbefore described, by which means the carbonization may be more perfectly reguq lated and rendered more uniform,-and both the over and the under-calcination, that are so detrimental to .the efiicacy of its action, may be easily avoided.
'The proportionate quantity of anthracite or other divisor may be adjusted so that'the percolation'will be slow, owing to the preponderance of the bone-dust, or
with a larger quantity ofthe divisor, the filtration will be more rapid, and a thicker stratum of the mixed material will be required to retain the liquid in contact with the bone a sufficient time to become thoroughly decolorized.
By the method that has been herein described more particularly'in connection with bone-black, and itscmployment by sugar-refiners, but which is applicable to other material and for other filteIing-purposes, the fine dust of bone-black, that would otherwise be useless for I claim, as my inventiona filter, is rendered of value, and advantage may be- Theuseofmlividing-ugent substantiallyztsdescribed, taken of the larger proportion of. surface ziflbrded by in conneetionwith the filtering-material,ibrthe purpose the same weight of dust, compared with bits of greater of filtration.
size, and a proportionably less amount of bone may be Also, the use of a dividing-egentin reburning or otherused, and, finally, the same method of separating the wise restoring bone-dust;
molecules of dust admits of their complete and uniform HENRY TORSTRICK. renovation or restoration, by Washing, reburning, or Witnesses:
other meems that requires access to every particle of THOMAS DAY,
the fine dust. WM. KEMBLE HALL.
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