US851381A - Composition of matter and process of making the same. - Google Patents
Composition of matter and process of making the same. Download PDFInfo
- Publication number
- US851381A US851381A US32088306A US1906320883A US851381A US 851381 A US851381 A US 851381A US 32088306 A US32088306 A US 32088306A US 1906320883 A US1906320883 A US 1906320883A US 851381 A US851381 A US 851381A
- Authority
- US
- United States
- Prior art keywords
- adhesive
- same
- making
- matter
- sulfite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title description 23
- 239000000203 mixture Substances 0.000 title description 7
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 20
- 230000001070 adhesive effect Effects 0.000 description 16
- 239000000853 adhesive Substances 0.000 description 15
- 239000011276 wood tar Substances 0.000 description 10
- 239000007788 liquid Substances 0.000 description 9
- 230000007935 neutral effect Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 238000000197 pyrolysis Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- 239000002023 wood Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 230000001066 destructive effect Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000011269 tar Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- -1 lime or magnesia Chemical compound 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000012749 thinning agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
Definitions
- My invention relates to compositions of matter having adhesive properties, and contion of matter.
- wood tar (or pitch) is meant the heavy liquid byroduct from the condensed products of the estructive distillation of woody tissues in the manufacture of pyroligneous acid and methyl alcohol &c.
- My invention comprises further the method or process of making this improved composi-
- the sul te process which consists in boiling Wood and other fibres under pressure in a solution containing sulfurous acid and a base, such as lime or magnesia
- waste sulfite liquor is roduced that hitherto has had little value, esides'being highly 0b 'ectionable in a number of ways and. very iffioult of disposal.
- I may add the wood tar at the same density as the concentrated sulfite liquor, which compound thus formed is ready for practical use, or may, if desired for any urpose, be subsequently reduced in density i br practical use by the addition ingredients may emade condition in which the material may, under some circumstances, be employed? For many purposes the density may be reduced by heat and this will" ermit a better admixture with the materia to be bri netted.
- e combined mixture is preferably sub- 4 jected to the action of heat to insure the inti-. mate and com lete admixture of the in edients thereof, a though substantially sat1sfactory results can be secured by mixing the ingredients at ordinary temperatures.
- An adhesive-comprisin lose elements of wood in so li uid byroduct from the tiIlation o Woody tissue.
- An adhesive comprising a sulfite solution of the non-celluloseelements of wood uid from the destructive distillation of woo y tissue.
- An adhesive comprising sulfite liquor and the liquid by-product from the destructive distillation of woody tissue.
- An adhesive comprising concentrated sulfite liquor and the condensed liquid from the destructive distillation of Woody tissue.
- An adhesive comprising a neutral, undecomposed and concentrated mass of sulfite the non-celluution, and the destructive discommonly known as wood decomposed and concentrated mass ssnssi roduct resulting "'13.
- the process herein described of'mak-' lation of woody ing an adhesive said process consisting in concentrating sulfite liquor, adding to a quantity of the same a certain quantity of wood tar, and then incorporating said materials by the agency of heat? 14.
- the process herein described of making an adhesive said process consisting in concentrating sulfite liquor, and adding to a certain quantity of the same an equal quantity of wood tar.
- An adhesive comprising a neutral, undecomposed and concentrated mass of sulfite liquor, and wood tar.
- An adhesive comprising a neutral, un-
- a liquid adhesive comprising a mass of neutral, unde'composed and concentrated sulfite liquor, and wood tar.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Civil Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Description
JACOB s. RoBEsoN,
PROCESS COMPANY, OF NEw JERSEY.
OF CAMDEN, NEW JERSEY, ASSIGNOR TO ROBESON CAMDEN, ,NEW' JERSEY, A CORPORATION or COMPOSITION OF MATTER AND PROCESS OF MAKING THE SAME- Specification of Letters Patent.
Patented April 23, 1907.
Application filed June 8,1906. Serial No. 320,888.
To all whom it may concern:
Be it known that I, JACOB S. ROBESON, a
3 citizen of the United States, and a resident of Camden, Camden county, New Jersey, have invented an Improved Composition of Mat- .ter and Process of Making the Same, of which the following is a specification.
My invention relates to compositions of matter having adhesive properties, and contion of matter.
sists of an improved com mass of sulfite liquor an as the material particularly from coni erous woods is sometimes called. By the term wood tar, (or pitch) is meant the heavy liquid byroduct from the condensed products of the estructive distillation of woody tissues in the manufacture of pyroligneous acid and methyl alcohol &c. I
My invention comprises further the method or process of making this improved composi- In the manufacture of cellulose or pa er pulp under what is known as the sul te process, which consists in boiling Wood and other fibres under pressure in a solution containing sulfurous acid and a base, such as lime or magnesia, a vast quantity of'awatery mixture known as waste sulfite liquor is roduced that hitherto has had little value, esides'being highly 0b 'ectionable in a number of ways and. very iffioult of disposal.
Incarrying the method or process of my present invention into eflect, I em loy a concentrated or evaporated solution o the same; preferring to use a neutral, undecom osed and concentrated mass of this waste made in accordance with a method I have developed for utilizing such material.- In my patent, N o. 833,634,,dated October 16, 1906,
have set forth a process of treating this raw waste liquor, by renderin neutral with the aid of mill: of lime or other suitable alkaline material, and then quickly concentrating such neutralized body in 'vacuo, without decomposition, to a desirable it substantially density.
In thepreferred method or recess of makmg my improved compoun I propose to .use this substantially neutral, undecomposed and concentrated mass of sulfite liquor made forth, and to -1n accordance with the process above set aquant-ity of this liquor at a ound comprising a Wood tar, or itch,
combination of the in a relatively thin quor tissue, and the condensed li density of about 30 B., I add the same quantity by volume of Wood tar, ofsubstantially the same density.
In practice I have found that the emulsion formed by this combination of theneutral and concentrated waste sulfite liquor, and the by-product tar, roduces a composition of matter having a hesive properties of a high degree, and possesses the further characteristic of being non-hygroscopic; rendering it highly valuable for use as a binder in the briquetting of all forms of in0rganic.mineral matter, notably the ores of the various metals, particularlly iron ore, and all forms of carbonaceous fue I may add the wood tar at the same density as the concentrated sulfite liquor, which compound thus formed is ready for practical use, or may, if desired for any urpose, be subsequently reduced in density i br practical use by the addition ingredients may emade condition in which the material may, under some circumstances, be employed? For many purposes the density may be reduced by heat and this will" ermit a better admixture with the materia to be bri netted.
e combined mixture is preferably sub- 4 jected to the action of heat to insure the inti-. mate and com lete admixture of the in edients thereof, a though substantially sat1sfactory results can be secured by mixing the ingredients at ordinary temperatures.
claim:
1. An adhesive-comprisin lose elements of wood in so li uid byroduct from the tiIlation o Woody tissue.
2. An adhesive comprising a sulfite solution of the non-celluloseelements of wood uid from the destructive distillation of woo y tissue.
3. An adhesive comprising sulfite liquor and the liquid by-product from the destructive distillation of woody tissue.
' 4. An adhesive comprising concentrated sulfite liquor and the condensed liquid from the destructive distillation of Woody tissue.
5. An adhesive comprising a neutral, undecomposed and concentrated mass of sulfite the non-celluution, and the destructive discommonly known as wood decomposed and concentrated mass ssnssi roduct resulting "'13. The process herein described of'mak-' lation of woody ing an adhesive, said process consisting in concentrating sulfite liquor, adding to a quantity of the same a certain quantity of wood tar, and then incorporating said materials by the agency of heat? 14. The process herein described of making an adhesive, said process consisting in concentrating sulfite liquor, and adding to a certain quantity of the same an equal quantity of wood tar.
15. The process ing an adhesive, said process consisting in concentrating sulfite li uor, adding thereto a uantity of the liquid y-product from the estructive distillation of woody tissue, and incorporating said products in a homogene- Bous body by the agency of heat.
16. The process herein described of making an adhesive, said process consisting in concentrating sulfite liquor, adding thereto a quantity of wood tar, and incorporating said products in a homogeneous body by the agency of heat. a
In testimony whereof, I have signed my liquor, and the liquid byfrom the destructlve disti tissue. 1
'6. q A liquid adhesive com rising a mass of chemically unaltered sulfite iquor andwood tar. v
.7."An adhesive comprising concentrated sulfite liquor and wood tar, in equal proportions. 7
8. An adhesive comprising a neutral, undecomposed and concentrated mass of sulfite liquor, and wood tar.
9. An adhesive comprising a neutral, un-
liquor, the liquid byroduet resulting from the destructive distil ation of woody tissue, and an aqueous thinning agent.
,7 10. A liquid adhesive comprising a mass of neutral, unde'composed and concentrated sulfite liquor, and wood tar. I
11. The process herein described of making an adhesive, said process consisting in concentrating sulfite liquor, and then adding thereto a quantity of the liquid by-product from the destructive distillation of woody tissue. 7 name to this specification, in the presence of 12. The process heie-in described of maktwo'subscribing witnesses. in an adhesive, sai rocess consisting in, co iicentrating sulfite liguor, and adding to a JACOB ROBESON' certain quantity of the same an equal quan- I Witnesses: I
\ MURRAY C. BOYER, l
tity of the li uid by-Q roduct from the de- Jos. H. KL IN. I
structive disti ation o woody tissue.
herein described of mak-
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US32088306A US851381A (en) | 1906-06-08 | 1906-06-08 | Composition of matter and process of making the same. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US32088306A US851381A (en) | 1906-06-08 | 1906-06-08 | Composition of matter and process of making the same. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US851381A true US851381A (en) | 1907-04-23 |
Family
ID=2919839
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US32088306A Expired - Lifetime US851381A (en) | 1906-06-08 | 1906-06-08 | Composition of matter and process of making the same. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US851381A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3903025A (en) * | 1973-11-06 | 1975-09-02 | Gen Refractories Co | Method for cold molding pitch bonded refractory |
| US4017433A (en) * | 1973-11-06 | 1977-04-12 | General Refractories Company | Pitch water soluble resin and alkyd resin as binder composition for refractory particles |
| US5916826A (en) * | 1997-12-05 | 1999-06-29 | Waste Technology Transfer, Inc. | Pelletizing and briquetting of coal fines using binders produced by liquefaction of biomass |
| US6506223B2 (en) | 1997-12-05 | 2003-01-14 | Waste Technology Transfer, Inc. | Pelletizing and briquetting of combustible organic-waste materials using binders produced by liquefaction of biomass |
| US20100083504A1 (en) * | 2004-04-06 | 2010-04-08 | The Boeing Company | Methods of manufacturing structural panels |
-
1906
- 1906-06-08 US US32088306A patent/US851381A/en not_active Expired - Lifetime
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3903025A (en) * | 1973-11-06 | 1975-09-02 | Gen Refractories Co | Method for cold molding pitch bonded refractory |
| US4017433A (en) * | 1973-11-06 | 1977-04-12 | General Refractories Company | Pitch water soluble resin and alkyd resin as binder composition for refractory particles |
| US5916826A (en) * | 1997-12-05 | 1999-06-29 | Waste Technology Transfer, Inc. | Pelletizing and briquetting of coal fines using binders produced by liquefaction of biomass |
| US6506223B2 (en) | 1997-12-05 | 2003-01-14 | Waste Technology Transfer, Inc. | Pelletizing and briquetting of combustible organic-waste materials using binders produced by liquefaction of biomass |
| US20100083504A1 (en) * | 2004-04-06 | 2010-04-08 | The Boeing Company | Methods of manufacturing structural panels |
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