US824956A - Depurator for gas. - Google Patents

Depurator for gas. Download PDF

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Publication number
US824956A
US824956A US4012700A US1900040127A US824956A US 824956 A US824956 A US 824956A US 4012700 A US4012700 A US 4012700A US 1900040127 A US1900040127 A US 1900040127A US 824956 A US824956 A US 824956A
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vaseline
gas
chamber
pipe
water
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US4012700A
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George Gregory Smith
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/236Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids specially adapted for aerating or carbonating beverages
    • B01F23/2362Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids specially adapted for aerating or carbonating beverages for aerating or carbonating within receptacles or tanks, e.g. distribution machines

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  • the present invention consists of an improved automatic depurator for acetylene and other gases; and its object is to provide means for urifying and drying the gas. This is attalned by passing the gas coming from the generator once or several times through liquid Vaseline, which will extract all the water and a great many other impurities from the same.
  • the invention also comprises means for reventing the Vaseline from bubbling over lnto the pipe leading to the gasometer and means for regulating the pressure in the de urator so that the water extracted from t e gas will be automatically discharged from the said depurator.
  • Means are also furnished for distributing the gas through the v aseline in finely-divided streams or jets.
  • Figure 1 is a sectional elevation through one form of embodying the invention, and Fig. 2 is a plan of the same.
  • the depurator consists of the housing a, of a suitable material, which is divided into two or more chambers b b.
  • the gas then rises through the vaselin'e into pipe 0, by means of which it passes to the second chamber b.
  • the pipe e dips into the second chamber below the level ofi the Vaseline therein and is also provided with a rose (Z for the purpose hereinbefore set forth.
  • the gas again rises though the vaseline into the pipe g, whence it passes to the gasometer.
  • the vaseline In connection with some gases-such, for instance, as acetylene when the gas is being generated the vaseline is agitated (the gas generation being very energetic) to such an extent that at first an emulsion, or rather a temporary emulsion, is formed, and this causes bubbles of Vaseline to rise in the chambers. These bubbles pass u on the outlet pipes and finally flow into the dip leading to the gasometer. Here they accumulate and finally form a Vaseline seal in the said di which prevents the passage of the gas an form a source of danger.
  • gases such, for instance, as acetylene when the gas is being generated the vaseline is agitated (the gas generation being very energetic) to such an extent that at first an emulsion, or rather a temporary emulsion, is formed, and this causes bubbles of Vaseline to rise in the chambers. These bubbles pass u on the outlet pipes and finally flow into the dip leading to the gasometer. Here they accumulate and finally form a Vaseline seal in the said di which prevent
  • these latter are expanded or enlarged, as at f, nd such enlargements have the effect of causing the bubbles rising to gradually expand therein until theyburst and the Vaseline contained in the same flows back into the depurator.
  • the enlargements f might be of any desired form; but it has been found adas illustrated, since this form seems to .cause the bubbles to burst more quickly than any other form as far as hitherto ascertained.
  • the stand-pipe is made adjustable so that the height of the column of liquid may be adjusted, to the end that the amount ofpressure within the chamber which will be neces-' sary to overbalance the column may be pre,
  • the cham ber will automatically discharge the water through the stand-pipe and the stand-pipe will, through its contained column of liquid, automatically'stop the discharge upon the restoration of the balance to which it has been adjusted.
  • This is effected by means of telescopically-adjustable water-pipes h it, one for each chamber, which pipes are shown as havim bent upper ends.
  • These pipes are guided in the stationary pipes i t', advantageously mounted underneath the cover of the depurator and extending down far. enough to dip into the water below the vaseline, as illustrated.
  • mounting the pipes h 71 telescopically is to enable them to be adjusted by being raised or lowered to keep the water-level beneath the vaseline at a certain predetermined height irrespective of the pressure in the depurator.
  • 722 represents the vaseline layer, and n, the water below the same, and the pipes it should be adjusted so that their ends dip into the wntcr-ql a, care.
  • the pipes it may be ⁇ -'1tlulrawn from the tubes i, through which tubes the vaseline may be poured into the same, and ouf lets Ir /r are provided at the bottoms of the suit] chambers for drawing oil' the water and removing other impurities as may be necessary.
  • liquid vaseline is of particular importance in connection more especially with acetylene.
  • Vaseline has the property not only of drying, but also of purifying acetylene gas. Experiments have shown that it extracts a great many of the phosphoric, as also all benzine, alcohol and the naphthalene and some of the sulfurous impurities from the same. It also eliminates practically all the water, thus producing a welldried gas.
  • a depurator embodying a closed chamber, a' permanent body of precipitating depurant, and adjustable automatic hydrostatic means capable of purging the chamber of precipitate.
  • a depurator of the class specified comprising a series of chambers ;v a well in the lower portion of each chamber; a permanent body of li uid vaseline each chamher; a gas eed pipe opening below the normal surface level of the vaseline in the first chamber a similar pipe leading from the gasspace of one chamber to below the normal surface of the vaseline in the next chamber; an enlargement in each of the pipes for ex panding and breaking bubbles or film carried by the gas; and a discharge-pipe emanating from each well.
  • a depurator of the class specified comprising a series of chambers; a well in the lower portion of each chamber; a permanent body of liquid vaseline within each chamber; a gas-feed pipe openin below the normal surface level of the vaseline in the first chamber a similar pipe leadin from the gas-space of one chamber to below t 1e normal surface of the vaseline in the next chamber an enlargement in each of the pipes for expanding and breaking bubbles or film carried by the gas; .and a discharge-pipe, in communication with each well, containing a column of water and capable of adjusting the height of the same.
  • achamber adapted to hold a depurant
  • a gas-inlet pipe entering said chamber and having its opening below the normal surface levelof the depurant and effective to pass liquid-laden gas into the depne'nthody of liquid Vaseline wltnm the ch amwater, and means for adjusting the height of her, a gas-feed iipe opening below the northe discharge end of said pipe.
  • surface leve of the Vaseline a as-pipe Inwitness whereof I have hereunto'set my leading from the gas-space of such 0 amber, hand in presence of two witnesses.

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  • Chemical Kinetics & Catalysis (AREA)
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Description

No. 824.956. PATENTED JULY 3, 1906.
e. G. SMITH,
DEPURATOR. FOR GAS. APPLIOATION FILED DBO.17. 1900 GEORGE GREGORY SMITH, OF FLORENCE, ITALY.
DEPURATOR Fo e'As.
nose rose.
specification of Letters Patent.
Patented July 3, 1906.
Application filed December 1'7, 1900. Serial No. 40,127.
To alt whom it may concern-J Be it known that I, GEORGE GREGORY SMITH, a citizen of the United States of America, residing at Villa Bel Riposo, San Domenico, Florence, Italy, have invented new and useful Improvements in De urators for Acetylene and other Gases, of w rich the following is a description. The present invention consists of an improved automatic depurator for acetylene and other gases; and its object is to provide means for urifying and drying the gas. This is attalned by passing the gas coming from the generator once or several times through liquid Vaseline, which will extract all the water and a great many other impurities from the same.
The invention also comprises means for reventing the Vaseline from bubbling over lnto the pipe leading to the gasometer and means for regulating the pressure in the de urator so that the water extracted from t e gas will be automatically discharged from the said depurator. Means are also furnished for distributing the gas through the v aseline in finely-divided streams or jets.
In order to render the present specification easily intelligible, reference is had to the accompanying drawings, in which similar letters of reference denote similar parts throughout both views.
Figure 1 is a sectional elevation through one form of embodying the invention, and Fig. 2 is a plan of the same.
The depurator consists of the housing a, of a suitable material, which is divided into two or more chambers b b. A pipe 0, coming from the gas-generator, dips into the fluid Vaseline in the chamber 1) and is provided at its lower end with a rose (1, which serves to distribute the gas in finely-divided streams into the Vaseline. The gas then rises through the vaselin'e into pipe 0, by means of which it passes to the second chamber b. The pipe e dips into the second chamber below the level ofi the Vaseline therein and is also provided with a rose (Z for the purpose hereinbefore set forth. In chamber b the gas again rises though the vaseline into the pipe g, whence it passes to the gasometer.
In connection with some gases-such, for instance, as acetylene when the gas is being generated the vaseline is agitated (the gas generation being very energetic) to such an extent that at first an emulsion, or rather a temporary emulsion, is formed, and this causes bubbles of Vaseline to rise in the chambers. These bubbles pass u on the outlet pipes and finally flow into the dip leading to the gasometer. Here they accumulate and finally form a Vaseline seal in the said di which prevents the passage of the gas an form a source of danger. In order to prevent the Vaseline-bubbles formed by the emulsion from passing into the outlet-pipes, these latter are expanded or enlarged, as at f, nd such enlargements have the effect of causing the bubbles rising to gradually expand therein until theyburst and the Vaseline contained in the same flows back into the depurator. The enlargements f might be of any desired form; but it has been found adas illustrated, since this form seems to .cause the bubbles to burst more quickly than any other form as far as hitherto ascertained.
Since acetylene when newly generated contains a considerable quantity of water and Vaseline possesses the quality or property of extracting practically all the water from the same, a quantity of water would soon be deposited underneath the Vaseline which would cause a total displacement of the latter in a very short time were not means provided for automatically eliminating the suerfluous water, so as to retain the position of the vaseline at substantially the same level throughout.
In the operation of this device several elements and forces are to be reckoned withto wit, a permanent body of liquid Vaseline, gas of constantly-varying pressure passing into and rising through and remaining for a short period above the body of Vaseline, water charged with impurities constantly accumulating above the body of Vaseline and The column of water is contained within an open stand-pipe commumcatmg with the exterior of the chamber, and such column, plus the atmospheric pressure, is capable of withstanding the pressure of the gas upon' the liquids withinthe chamber, accentuated by the accumulation of water, only up to a vantageous to employ the double-cone form,
raising it up and causing it to encroach upon 1 certain point, and then the stand-pipe will permit the escape of a sufficient quantity of surplus water to enable the atmospherically- 1 pressed column to again resist the physical conditions existing within the chamber, and at the moment of cessation of the discharge from the stand-pipe the columnof liquid,
plus the atmospheric pressure, balances the existing condition of the combination of forces within the chamber. The discharge of water is caused by the condition of forces within the chamber overbalancing such col umn. The action is automatic, and since .the accumulation of water reduces the gasspace upon rise of gas-pressure after a certain dimunition of gas-space the surplus water, and only the surplus, will be ejected. This action will go through the stand-pipe. on, provided no unusual accident happens to the machine, year after year.
The stand-pipe is made adjustable so that the height of the column of liquid may be adjusted, to the end that the amount ofpressure within the chamber which will be neces-' sary to overbalance the column may be pre,
- determined, and upon the rise of pressure ily understood.
above such predetermined point the cham ber will automatically discharge the water through the stand-pipe and the stand-pipe will, through its contained column of liquid, automatically'stop the discharge upon the restoration of the balance to which it has been adjusted. This is effected by means of telescopically-adjustable water-pipes h it, one for each chamber, which pipes are shown as havim bent upper ends. These pipes are guided in the stationary pipes i t', advantageously mounted underneath the cover of the depurator and extending down far. enough to dip into the water below the vaseline, as illustrated. The object in. mounting the pipes h 71 telescopically is to enable them to be adjusted by being raised or lowered to keep the water-level beneath the vaseline at a certain predetermined height irrespective of the pressure in the depurator. Thus if the pressure is very high in the depurator the pipe it should be correspondingly raised tov increase the height of the column, and if it is low the pipe may be lowered, as will be read- As illustrated, 722 represents the vaseline layer, and n, the water below the same, and the pipes it should be adjusted so that their ends dip into the wntcr-ql a, care.
must be taken by examining the discharge of thesaid pipes it that no vaseline is discharged and wasted through the same.
The pipes it may be \\-'1tlulrawn from the tubes i, through which tubes the vaseline may be poured into the same, and ouf lets Ir /r are provided at the bottoms of the suit] chambers for drawing oil' the water and removing other impurities as may be necessary.
Although two chambers have been described, it will be obvious that only one, or more than two, might be employed without departing from the spirit of the invention.
The use of liquid vaseline is of particular importance in connection more especially with acetylene. Vaseline has the property not only of drying, but also of purifying acetylene gas. Experiments have shown that it extracts a great many of the phosphoric, as also all benzine, alcohol and the naphthalene and some of the sulfurous impurities from the same. It also eliminates practically all the water, thus producing a welldried gas.
I claim as my invention 1. A depurator embodying a closed chamber, a' permanent body of precipitating depurant, and adjustable automatic hydrostatic means capable of purging the chamber of precipitate.
2. A depurator of the class specified comprising a series of chambers ;v a well in the lower portion of each chamber; a permanent body of li uid vaseline each chamher; a gas eed pipe opening below the normal surface level of the vaseline in the first chamber a similar pipe leading from the gasspace of one chamber to below the normal surface of the vaseline in the next chamber; an enlargement in each of the pipes for ex panding and breaking bubbles or film carried by the gas; and a discharge-pipe emanating from each well. 1
3. A depurator of the class specified comprising a series of chambers; a well in the lower portion of each chamber; a permanent body of liquid vaseline within each chamber; a gas-feed pipe openin below the normal surface level of the vaseline in the first chamber a similar pipe leadin from the gas-space of one chamber to below t 1e normal surface of the vaseline in the next chamber an enlargement in each of the pipes for expanding and breaking bubbles or film carried by the gas; .and a discharge-pipe, in communication with each well, containing a column of water and capable of adjusting the height of the same.
l. In a device of the character specified, the combination of achamber adapted to hold a depurant, a gas-inlet pipe entering said chamber and having its opening below the normal surface levelof the depurant and effective to pass liquid-laden gas into the depne'nthody of liquid Vaseline wltnm the ch amwater, and means for adjusting the height of her, a gas-feed iipe opening below the northe discharge end of said pipe. o ma] surface leve of the Vaseline, a as-pipe Inwitness whereof I have hereunto'set my leading from the gas-space of such 0 amber, hand in presence of two witnesses.
an enlar ement in such pi e for eiffanding GEORGE GREGORY SMITH. and'brea g bubbles or m carrie by the Witnesses: gas, and a dlschargeipe in communication SPIRITO BERNARD,
with the wall adapte to contain a column of i EUGENIA CEooHINI.
US4012700A 1900-12-17 1900-12-17 Depurator for gas. Expired - Lifetime US824956A (en)

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US4012700A US824956A (en) 1900-12-17 1900-12-17 Depurator for gas.
US85545A US850680A (en) 1900-12-17 1901-12-12 Process of purifying gas.

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4305896A (en) * 1975-09-05 1981-12-15 Hitachi, Ltd. Vent exit device for condensing steam
US20060244160A1 (en) * 2002-06-21 2006-11-02 Abolghassem Pakdaman Gas enrichment module

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4305896A (en) * 1975-09-05 1981-12-15 Hitachi, Ltd. Vent exit device for condensing steam
US20060244160A1 (en) * 2002-06-21 2006-11-02 Abolghassem Pakdaman Gas enrichment module
US7377499B2 (en) * 2002-06-21 2008-05-27 Abolghassem Pakdaman Gas enrichment module

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