US6744503B2 - Monitoring of vapor phase polycyclic aromatic hydrocarbons - Google Patents
Monitoring of vapor phase polycyclic aromatic hydrocarbons Download PDFInfo
- Publication number
- US6744503B2 US6744503B2 US10/022,239 US2223901A US6744503B2 US 6744503 B2 US6744503 B2 US 6744503B2 US 2223901 A US2223901 A US 2223901A US 6744503 B2 US6744503 B2 US 6744503B2
- Authority
- US
- United States
- Prior art keywords
- optical probe
- electromagnetic radiation
- radiation
- polycyclic aromatic
- monitoring apparatus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related, expires
Links
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/64—Fluorescence; Phosphorescence
- G01N21/6408—Fluorescence; Phosphorescence with measurement of decay time, time resolved fluorescence
Landscapes
- Health & Medical Sciences (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
Description
Claims (39)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/022,239 US6744503B2 (en) | 2001-12-20 | 2001-12-20 | Monitoring of vapor phase polycyclic aromatic hydrocarbons |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/022,239 US6744503B2 (en) | 2001-12-20 | 2001-12-20 | Monitoring of vapor phase polycyclic aromatic hydrocarbons |
Publications (2)
Publication Number | Publication Date |
---|---|
US20030117619A1 US20030117619A1 (en) | 2003-06-26 |
US6744503B2 true US6744503B2 (en) | 2004-06-01 |
Family
ID=21808569
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/022,239 Expired - Fee Related US6744503B2 (en) | 2001-12-20 | 2001-12-20 | Monitoring of vapor phase polycyclic aromatic hydrocarbons |
Country Status (1)
Country | Link |
---|---|
US (1) | US6744503B2 (en) |
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20030178578A1 (en) * | 2002-03-14 | 2003-09-25 | Govind Rao | Device for discrimination of fluorescence lifetimes and uses therefor |
US20060185687A1 (en) * | 2004-12-22 | 2006-08-24 | Philip Morris Usa Inc. | Filter cigarette and method of making filter cigarette for an electrical smoking system |
US20070210262A1 (en) * | 2006-03-10 | 2007-09-13 | Interocean Systems, Inc. | Non-contact oil spill detection apparatus and method |
US20080117951A1 (en) * | 2006-11-16 | 2008-05-22 | University Of South Florida | Thermally Compensated Dual-Probe Fluorescence Decay Rate Temperature Sensor and Method of Use |
US9790834B2 (en) | 2014-03-20 | 2017-10-17 | General Electric Company | Method of monitoring for combustion anomalies in a gas turbomachine and a gas turbomachine including a combustion anomaly detection system |
US9791351B2 (en) | 2015-02-06 | 2017-10-17 | General Electric Company | Gas turbine combustion profile monitoring |
US11250681B2 (en) | 2012-02-13 | 2022-02-15 | Johnson Controls Fire Protection LP | Combustion product detection |
US11636870B2 (en) | 2020-08-20 | 2023-04-25 | Denso International America, Inc. | Smoking cessation systems and methods |
US11760169B2 (en) | 2020-08-20 | 2023-09-19 | Denso International America, Inc. | Particulate control systems and methods for olfaction sensors |
US11760170B2 (en) | 2020-08-20 | 2023-09-19 | Denso International America, Inc. | Olfaction sensor preservation systems and methods |
US11813926B2 (en) | 2020-08-20 | 2023-11-14 | Denso International America, Inc. | Binding agent and olfaction sensor |
US11828210B2 (en) | 2020-08-20 | 2023-11-28 | Denso International America, Inc. | Diagnostic systems and methods of vehicles using olfaction |
US11881093B2 (en) | 2020-08-20 | 2024-01-23 | Denso International America, Inc. | Systems and methods for identifying smoking in vehicles |
US11932080B2 (en) | 2020-08-20 | 2024-03-19 | Denso International America, Inc. | Diagnostic and recirculation control systems and methods |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7632012B2 (en) * | 2005-09-01 | 2009-12-15 | Siemens Energy, Inc. | Method of measuring in situ differential emissivity and temperature |
US7997300B1 (en) * | 2006-04-11 | 2011-08-16 | The United States Of America As Represented By The Secretary Of The Army | Aerosol inlet flow modulator |
DE102009017932B4 (en) * | 2009-04-20 | 2010-12-09 | Gröger & Obst Vertriebs- und Service GmbH | A method for the continuous quantitative determination of an oxidizable chemical compound in an assay medium |
EP2587154A1 (en) * | 2011-10-24 | 2013-05-01 | Alstom Technology Ltd | Method for data acquisition from a combustion process |
US9282260B2 (en) | 2012-04-05 | 2016-03-08 | Baker Hughes Incorporated | Visualizing polynuclear aromatic hydrocarbons within the near infrared spectrum |
CN104267140B (en) * | 2014-09-30 | 2017-01-25 | 福建中烟工业有限责任公司 | Tobacco pyrolysis and combustion reactor, analysis system and method |
CN106289882B (en) * | 2016-07-19 | 2018-09-18 | 天津大学 | A kind of laboratory flames quartz probe on-line period system and sampling method |
CN108012054B (en) * | 2017-11-21 | 2020-04-14 | 西安理工大学 | Shooting trigger system suitable for ultra-high-speed camera in brittle material research |
CN112749906A (en) * | 2021-01-14 | 2021-05-04 | 云南中烟工业有限责任公司 | Sensory evaluation method for spectrum data of cigarette mainstream smoke |
KR102374932B1 (en) * | 2021-02-09 | 2022-03-16 | 대윤계기산업 주식회사 | System for Polycyclic Aromatic Hydrocarbon Concentration Measurement |
Citations (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3749495A (en) | 1971-11-17 | 1973-07-31 | Monitor Labs Inc | Gas analyzer utilizing infrared emission from gaseous molecules |
US3788752A (en) | 1972-03-03 | 1974-01-29 | Perkin Elmer Corp | Gas flow controller for a heated sample cell |
US3975098A (en) | 1975-08-05 | 1976-08-17 | Applied Photophysics Limited | Spectrofluorimeter |
US4432225A (en) * | 1982-04-26 | 1984-02-21 | The United States Of America As Represented By The United States Department Of Energy | Detection system for a gas chromatograph |
US4569592A (en) * | 1981-12-11 | 1986-02-11 | Hitachi, Ltd. | Plasma monitor |
US4577109A (en) * | 1980-10-06 | 1986-03-18 | Regents Of The University Of California | Remote multi-position information gathering system and method |
US4679939A (en) | 1985-12-23 | 1987-07-14 | The United States Of America As Represented By The Secretary Of The Air Firce | In situ small particle diagnostics |
USRE32598E (en) | 1975-12-11 | 1988-02-09 | Feature extraction system for extracting a predetermined feature from a signal | |
US5220172A (en) * | 1991-09-23 | 1993-06-15 | The Babcock & Wilcox Company | Fluorescence analyzer for lignin |
US5477218A (en) | 1993-01-07 | 1995-12-19 | Hochiki Kabushiki Kaisha | Smoke detecting apparatus capable of detecting both smoke fine particles |
US5684580A (en) * | 1995-05-01 | 1997-11-04 | Ashland Inc. | Hydrocarbon analysis and control by raman spectroscopy |
US5748311A (en) | 1996-03-11 | 1998-05-05 | Hamann; Oliver | Apparatus and method of particle geometry measurement by speckle pattern analysis |
US5793478A (en) | 1996-11-19 | 1998-08-11 | Sandia Corporation | Apparatus for measuring particle properties |
US5880830A (en) | 1997-01-29 | 1999-03-09 | Greenvision Systems Ltd. | Spectral imaging method for on-line analysis of polycyclic aromatic hydrocarbons in aerosols |
US5993194A (en) | 1996-06-21 | 1999-11-30 | Lemelson; Jerome H. | Automatically optimized combustion control |
US6008894A (en) * | 1998-07-28 | 1999-12-28 | The United States Of America As Represented By The United States Department Of Energy | Remote adjustable focus Raman spectroscopy probe |
US6008895A (en) * | 1996-08-13 | 1999-12-28 | Deutsches Zentrum Fuer Luft -Und Raumfahrt E.V. | Stoichiometric ratio measuring device |
US6091843A (en) | 1998-09-03 | 2000-07-18 | Greenvision Systems Ltd. | Method of calibration and real-time analysis of particulates |
US6576911B1 (en) * | 2000-10-19 | 2003-06-10 | General Electric Company | Method and apparatus for nondestructive determination of polymer hydrolytic stability |
-
2001
- 2001-12-20 US US10/022,239 patent/US6744503B2/en not_active Expired - Fee Related
Patent Citations (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3749495A (en) | 1971-11-17 | 1973-07-31 | Monitor Labs Inc | Gas analyzer utilizing infrared emission from gaseous molecules |
US3788752A (en) | 1972-03-03 | 1974-01-29 | Perkin Elmer Corp | Gas flow controller for a heated sample cell |
US3975098A (en) | 1975-08-05 | 1976-08-17 | Applied Photophysics Limited | Spectrofluorimeter |
USRE32598E (en) | 1975-12-11 | 1988-02-09 | Feature extraction system for extracting a predetermined feature from a signal | |
US4577109A (en) * | 1980-10-06 | 1986-03-18 | Regents Of The University Of California | Remote multi-position information gathering system and method |
US4569592A (en) * | 1981-12-11 | 1986-02-11 | Hitachi, Ltd. | Plasma monitor |
US4432225A (en) * | 1982-04-26 | 1984-02-21 | The United States Of America As Represented By The United States Department Of Energy | Detection system for a gas chromatograph |
US4679939A (en) | 1985-12-23 | 1987-07-14 | The United States Of America As Represented By The Secretary Of The Air Firce | In situ small particle diagnostics |
US5220172A (en) * | 1991-09-23 | 1993-06-15 | The Babcock & Wilcox Company | Fluorescence analyzer for lignin |
US5477218A (en) | 1993-01-07 | 1995-12-19 | Hochiki Kabushiki Kaisha | Smoke detecting apparatus capable of detecting both smoke fine particles |
US5684580A (en) * | 1995-05-01 | 1997-11-04 | Ashland Inc. | Hydrocarbon analysis and control by raman spectroscopy |
US5748311A (en) | 1996-03-11 | 1998-05-05 | Hamann; Oliver | Apparatus and method of particle geometry measurement by speckle pattern analysis |
US5993194A (en) | 1996-06-21 | 1999-11-30 | Lemelson; Jerome H. | Automatically optimized combustion control |
US6008895A (en) * | 1996-08-13 | 1999-12-28 | Deutsches Zentrum Fuer Luft -Und Raumfahrt E.V. | Stoichiometric ratio measuring device |
US5793478A (en) | 1996-11-19 | 1998-08-11 | Sandia Corporation | Apparatus for measuring particle properties |
US5880830A (en) | 1997-01-29 | 1999-03-09 | Greenvision Systems Ltd. | Spectral imaging method for on-line analysis of polycyclic aromatic hydrocarbons in aerosols |
US6008894A (en) * | 1998-07-28 | 1999-12-28 | The United States Of America As Represented By The United States Department Of Energy | Remote adjustable focus Raman spectroscopy probe |
US6091843A (en) | 1998-09-03 | 2000-07-18 | Greenvision Systems Ltd. | Method of calibration and real-time analysis of particulates |
US6576911B1 (en) * | 2000-10-19 | 2003-06-10 | General Electric Company | Method and apparatus for nondestructive determination of polymer hydrolytic stability |
Non-Patent Citations (16)
Title |
---|
A.D. Campiglia et al., "Fiber Optic Sensor for Laser-Induced Room-Temperature Phosphorescence Detection of Polycyclic Aromatic Compounds", Talanta 43 (1996), pp 1805-1814, The International Journal of Pure and Applied Analytical Chemistry, Amsterdam, The Netherlands. |
Brian M. Cullum et al., "High-Temperature Fluorescence Measurements and Instrumentation for Polyaromatic Hydrocarbons (PAH): A Review", Journal of Polycyclic Aromatic Compounds, vol. 18, No. 1, pp. 25-47 (2000). |
Christopher L. Stevenson et al., "Analysis of Polynuclear Aromatic Compounds Using Laser-Excited Synchronous Fluorescence", Analytica Chimica Acta, 303 (1995), pp. 247-253. |
Christopher L. Stevenson et al., "Laser-Excited Synchronous Luminescence Spectroscopy", Applied Spectroscopy, vol. 47, No. 4, 1993, pp. 430-435. |
J. C. Andrea et al., "Applications of Fast Fourier Transform to Deconvolution in Single Photon Counting", J. Phys Chem., vol. 83, p. 2285 (1979). |
J.P. Alarie et al. "A Fiber-Optic Cyclodextrin-Based Sensor", Talanta, vol. 38, No. 5, pp. 529-534, 1991, printed in Great Britain. |
R. P. Cooney et al., "The Sit Image Vidicon as a Gas-Phase Fluorescence Detector for Gas Chromatography", Analytica Chimica Acta 89 (1977), pp. 9-19. |
T. Vo-Dinh et al., "Detection of Polyaromatic Compounds Using Antibody-Based Fiberoptics Fluoroimmunosensors", Polynuclear Aromatic Hydrocarbons: Measurements, Means, and Metabolism, Battelle Press, International Symposium on Polynuclear Aromatic Hydrocarbons, Gaithersburg, MD, 1987, pp. 965-979. |
T. Vo-Dinh et al., "Immunosensors: Principles and Applications", Immunomethods 3, pp. 85-92 (1993). |
T. Vo-Dinh et al., "Screening Polynuclear Aromatic Pollutants in Ambient and Indoor Air by Synchronous Luminescence", 79th Annual Meeting of the Air Pollution Control Association Minneapolis, Minnesota, Jun. 22-27, 1986, 86-32.2, pp. 1-8. |
T. Vo-Dinh et al., Screening Air Samples for Polynuclear Aromatic Compounds: A Field Study, Specialty Conference on Measurement and Monitoring of Non-Criteria (Toxic) Contaminants, Air Pollution Control Assoc., Chicago IL, Mar. 23-4, 1983, 12 pages. |
Tuan Vo-Dinh et al., "Laser-Induced Room-Temperature Phosphorescence Detection of Benzo[a]pyrene-DNA Adducts", American Chemical Society, Analytical Chemistry, vol. 59, No. 8, Apr. 15, 1987, pp. 1093-1095. |
Tuan Vo-Dinh, "Development of a Dosimeter for Personnel Exposure to Vapors of Polyaromatic Pollutants", Environmental Science & Technology, vol. 19, No. 10, pp. 997-1003, Oct. 1985. |
Tuan Vo-Dinh, "Fluorescence Line-Narrowing Spectrometry of Polycyclic Compounds on Filter Paper Substrates", American Chemical Society, Analytical Chemistry, vol. 58, No. 14, Dec. 1986, pp. 3135-3139. |
Tuan Vo-Dinh, "Significance of Chemical Analysis of Polycyclic Aromatic Compounds and Related Biological Systems", Chemical Analysis of Polycyclic Aromatic Compounds, 1989, pp. 1-30. |
Zhenhuan Chi et al., "Laser-Induced Fluorescence Studies of Polycyclic Aromatic Hydrocarbons (PAH) Vapors at High Temperatures", Spectrochimica Acta, Part A, vol. 57, pp. 1377-1384 (2001). |
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7041986B2 (en) * | 2002-03-14 | 2006-05-09 | University Of Maryland Baltimore County | Device for discrimination of fluorescence lifetimes and uses therefor |
US20030178578A1 (en) * | 2002-03-14 | 2003-09-25 | Govind Rao | Device for discrimination of fluorescence lifetimes and uses therefor |
US20060185687A1 (en) * | 2004-12-22 | 2006-08-24 | Philip Morris Usa Inc. | Filter cigarette and method of making filter cigarette for an electrical smoking system |
US20070210262A1 (en) * | 2006-03-10 | 2007-09-13 | Interocean Systems, Inc. | Non-contact oil spill detection apparatus and method |
US7688428B2 (en) * | 2006-03-10 | 2010-03-30 | Interocean Systems, Inc. | Non-contact oil spill detection apparatus and method |
US20080117951A1 (en) * | 2006-11-16 | 2008-05-22 | University Of South Florida | Thermally Compensated Dual-Probe Fluorescence Decay Rate Temperature Sensor and Method of Use |
US7789556B2 (en) * | 2006-11-16 | 2010-09-07 | University Of South Florida | Thermally compensated dual-probe fluorescence decay rate temperature sensor and method of use |
US11250681B2 (en) | 2012-02-13 | 2022-02-15 | Johnson Controls Fire Protection LP | Combustion product detection |
US9790834B2 (en) | 2014-03-20 | 2017-10-17 | General Electric Company | Method of monitoring for combustion anomalies in a gas turbomachine and a gas turbomachine including a combustion anomaly detection system |
US9791351B2 (en) | 2015-02-06 | 2017-10-17 | General Electric Company | Gas turbine combustion profile monitoring |
US11636870B2 (en) | 2020-08-20 | 2023-04-25 | Denso International America, Inc. | Smoking cessation systems and methods |
US11760169B2 (en) | 2020-08-20 | 2023-09-19 | Denso International America, Inc. | Particulate control systems and methods for olfaction sensors |
US11760170B2 (en) | 2020-08-20 | 2023-09-19 | Denso International America, Inc. | Olfaction sensor preservation systems and methods |
US11813926B2 (en) | 2020-08-20 | 2023-11-14 | Denso International America, Inc. | Binding agent and olfaction sensor |
US11828210B2 (en) | 2020-08-20 | 2023-11-28 | Denso International America, Inc. | Diagnostic systems and methods of vehicles using olfaction |
US11881093B2 (en) | 2020-08-20 | 2024-01-23 | Denso International America, Inc. | Systems and methods for identifying smoking in vehicles |
US11932080B2 (en) | 2020-08-20 | 2024-03-19 | Denso International America, Inc. | Diagnostic and recirculation control systems and methods |
Also Published As
Publication number | Publication date |
---|---|
US20030117619A1 (en) | 2003-06-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US6744503B2 (en) | Monitoring of vapor phase polycyclic aromatic hydrocarbons | |
US5759859A (en) | Sensor and method for detecting trace underground energetic materials | |
Sgro et al. | UV-visible spectroscopy of organic carbon particulate sampled from ethylene/air flames | |
US6762836B2 (en) | Portable laser plasma spectroscopy apparatus and method for in situ identification of deposits | |
US7088435B2 (en) | Controlled substance detection and identification system | |
US7619742B2 (en) | High-speed spectrographic sensor for internal combustion engines | |
US5786893A (en) | Raman spectrometer | |
Radziemski et al. | Laser-induced breakdown spectroscopy: time-resolved spectrochemical applications | |
Lazic et al. | Analysis of explosive and other organic residues by laser induced breakdown spectroscopy | |
US20040155202A1 (en) | Methods and apparatus for molecular species detection, inspection and classification using ultraviolet fluorescence | |
US5826214A (en) | Hand-held probe for real-time analysis of trace pollutants in atmosphere and on surfaces | |
Bauer et al. | Pulsed laser surface fragmentation and mid-infrared laser spectroscopy for remote detection of explosives | |
Liangying et al. | Analysis of pulverized coal by laser-induced breakdown spectroscopy | |
Hartland et al. | Fourier transform dispersed fluorescence spectroscopy: Observation of new vibrational levels in the 5000–8000 cm− 1 region of a ̃ 1 A 1 CH2 | |
JP6581786B2 (en) | Drug detection device | |
Yang et al. | Mid-infrared emission from laser-induced breakdown spectroscopy | |
EP0015284A1 (en) | Flameless emission spectroscope apparatus and sample introduction method for same. | |
WO2003027650A2 (en) | Method for detection and discrimination of polycyclic aromatic hydrocarbons (pahs) and monoaromatics based on laser-induced breakdown spectroscopy (libs) | |
EP3441750A1 (en) | Method for isotopic measurement | |
JP3858844B2 (en) | Gas monitoring apparatus and gas monitoring method for underground fixation of carbon dioxide gas | |
Tripathi et al. | An optical sensor for multi-species impurity monitoring in hydrogen fuel | |
Petrucci et al. | Analytical and spectroscopic characterization of double-resonance laser-induced fluorescence of gold atoms in a graphite furnace and in a flame | |
Wang et al. | Selective detection of organophosphate nerve agents using microplasma device | |
Ciucci et al. | Laser-induced breakdown spectroscopy: a new and powerful technique for pollutant diagnostics | |
Hartford Jr et al. | Optical instrumentation for on-line analysis of chemical processes |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
AS | Assignment |
Owner name: PHILIP MORRIS INCORPORATED, NEW YORK Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:UT-BATTELLE, LLC;REEL/FRAME:012777/0184 Effective date: 20020320 Owner name: UT-BATTELLE, LLC, TENNESSEE Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:VO-DINH, TUAN;REEL/FRAME:012777/0202 Effective date: 20020322 Owner name: PHILIP MORRIS INCORPORATED, NEW YORK Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:HAJALIGOL, MOHAMMAD R.;REEL/FRAME:012777/0224 Effective date: 20020215 |
|
AS | Assignment |
Owner name: PHILIP MORRIS USA INC., VIRGINIA Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:PHILIP MORRIS INCORPORATED;REEL/FRAME:015548/0195 Effective date: 20030115 |
|
AS | Assignment |
Owner name: ENERGY, U.S., DEPARTMENT OF, DISTRICT OF COLUMBIA Free format text: CONFIRMATORY LICENSE;ASSIGNOR:PHILIP MORRIS INCORPORATED;REEL/FRAME:014901/0694 Effective date: 20040630 |
|
FEPP | Fee payment procedure |
Free format text: PAYOR NUMBER ASSIGNED (ORIGINAL EVENT CODE: ASPN); ENTITY STATUS OF PATENT OWNER: LARGE ENTITY |
|
FPAY | Fee payment |
Year of fee payment: 4 |
|
REMI | Maintenance fee reminder mailed | ||
LAPS | Lapse for failure to pay maintenance fees | ||
STCH | Information on status: patent discontinuation |
Free format text: PATENT EXPIRED DUE TO NONPAYMENT OF MAINTENANCE FEES UNDER 37 CFR 1.362 |
|
FP | Lapsed due to failure to pay maintenance fee |
Effective date: 20120601 |