US6517679B1 - Method for determination of an irreversible stretch and of a dynamic modulus of elasticity - Google Patents

Method for determination of an irreversible stretch and of a dynamic modulus of elasticity Download PDF

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Publication number
US6517679B1
US6517679B1 US09/623,205 US62320500A US6517679B1 US 6517679 B1 US6517679 B1 US 6517679B1 US 62320500 A US62320500 A US 62320500A US 6517679 B1 US6517679 B1 US 6517679B1
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United States
Prior art keywords
tension
measurement
elasticity
dynamic modulus
carried out
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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US09/623,205
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English (en)
Inventor
Harri Mustonen
Pekka Pakarinen
Mika Tammenoja
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Valmet Technologies Oy
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Metso Paper Oy
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Assigned to VALMET CORPORATION reassignment VALMET CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: PAKARINEN, PEKKA, TAMMENOJA, MIKA, MUSTONEN, HARRI
Assigned to METSO PAPER, INC. reassignment METSO PAPER, INC. CHANGE OF NAME (SEE DOCUMENT FOR DETAILS). Assignors: VALMET CORPORATION
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Publication of US6517679B1 publication Critical patent/US6517679B1/en
Assigned to VALMET TECHNOLOGIES, INC. reassignment VALMET TECHNOLOGIES, INC. CHANGE OF NAME (SEE DOCUMENT FOR DETAILS). Assignors: METSO PAPER, INC.
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08—Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21G—CALENDERS; ACCESSORIES FOR PAPER-MAKING MACHINES
    • D21G9/00—Other accessories for paper-making machines
    • D21G9/0009—Paper-making control systems
    • D21G9/0027—Paper-making control systems controlling the forming section
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21G—CALENDERS; ACCESSORIES FOR PAPER-MAKING MACHINES
    • D21G9/00—Other accessories for paper-making machines
    • D21G9/0009—Paper-making control systems
    • D21G9/0036—Paper-making control systems controlling the press or drying section
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/34—Paper
    • G01N33/346—Paper paper sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65H—HANDLING THIN OR FILAMENTARY MATERIAL, e.g. SHEETS, WEBS, CABLES
    • B65H2515/00—Physical entities not provided for in groups B65H2511/00 or B65H2513/00
    • B65H2515/30—Forces; Stresses
    • B65H2515/37—Elasticity modulus
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02—Details not specific for a particular testing method
    • G01N2203/026—Specifications of the specimen
    • G01N2203/0262—Shape of the specimen
    • G01N2203/0278—Thin specimens
    • G01N2203/0282—Two dimensional, e.g. tapes, webs, sheets, strips, disks or membranes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S162/00—Paper making and fiber liberation
    • Y10S162/09—Uses for paper making sludge
    • Y10S162/10—Computer control of paper making variables
    • Y10S162/11—Wet end paper making variables

Definitions

  • the invention concerns a method for determination of an irreversible stretch and of a dynamic modulus of elasticity from a paper web.
  • the invention also concerns a method for the control of a papermaking process.
  • the tension of the web is measured by, in the vicinity of the moving web, fitting a measurement rib, which has a face that is curved in the running direction of the web and in which rib there are pressure metering detectors placed in holes.
  • An air cushion is formed between the moving web and the curved face, in which cushion the air pressure is directly proportional to the tension of the web.
  • the tension of the web is measured indirectly by metering the pressure in the air cushion.
  • a method for measurement of a tension profile is described, which method is based on the speed of propagation of a plane wave.
  • an acoustic impulse is produced in the web, and the travel time of the impulse is measured by means of a microphone.
  • the object of the present invention is to provide a novel method for determination of an irreversible stretch and of a dynamic modulus of elasticity from a paper web.
  • the aim of the method in accordance with the method is to provide a possibility for rapid adjustment of the regulation parameters employed in the manufacture of paper after determination of the quantities concerned.
  • the method in accordance with the invention for determination of an irreversible stretch and of a dynamic modulus of elasticity from a paper web is mainly characterized in that the method comprises the following steps:
  • the paper web is subjected to an on-line measurement of its cross-direction tension profile at two or more different tension levels
  • the dynamic modulus of elasticity is determined from each fitted curve.
  • the method in accordance with the invention for the control of a papermaking process is mainly characterized in that, in said method, the method in accordance with the invention for determination of an irreversible stretch and of a dynamic modulus of elasticity from a paper web is employed for regulation of the dynamic modulus of elasticity and/or of the irreversible stretch.
  • the measurement results of a number of measured tension profiles are fitted together. From the fitted result thus formed, it is possible to determine the irreversible stretch and the modulus of elasticity of the paper web.
  • a particular advantage of the present invention is the rapidity of the method of measurement as well as the possibility of integrating the measurement procedure on-line in the rest of the control system of the paper machine.
  • FIG. 1 illustrates a location of an apparatus for measurement of tension profile in a paper machine.
  • FIG. 2 illustrates a result of measurement of a tension profile at three different levels of tension.
  • FIG. 3 illustrates the principle of fitting together of measurement points.
  • FIG. 4 illustrates a profile of modulus of elasticity of a paper web.
  • FIG. 5 illustrates a profile of irreversible stretch of a paper web.
  • FIG. 1 shows a typical location of an apparatus 10 for measurement of the tension profile in a paper machine.
  • the measurement apparatus has been fitted in the dry end of the paper machine between a calender 20 and a reel-up 30 .
  • the measurement data 1 concerning the tension profile are passed along a bus to a data processing equipment 14 .
  • the tension profile is measured at different tension levels so that the stretch of the paper web W between the calender 20 and the reel-up 30 is adjusted.
  • a change in the stretch is produced so that the web W speeds in the calender nip and in the reeling nip are altered. In this way, a difference in speed is produced between the calender and the reel-up.
  • v 2 web speed in the reeling nip.
  • the data processing equipment 14 gives commands concerning the regulation of the different speeds to the regulation units 12 and 13 for the drives whose speeds can be regulated.
  • the regulation unit 12 controls the calender nip, and the regulation unit 13 controls the reeling nip.
  • the data processing equipment 14 computes the profiles 15 of irreversible stretch and of dynamic modulus of elasticity by means of the fitting method that will be described later. These profiles can be displayed in a display apparatus 17 , which can be, e.g., a display monitor or a printer.
  • the profiles 15 are used for making the regulations of the papermaking process by means of the control unit 16 of the paper machine.
  • the control unit 16 can be based on automatic feedback regulation and/or on manual regulation.
  • FIG. 2 shows a measurement result obtained by means of the apparatus 10 for measurement of the tension profile, wherein the tension profile has been measured at three different known tension levels T 1 (y), T 2 (y) and T 3 (y), which levels correspond to the values of relative stretch ⁇ 1 , ⁇ 2 and ⁇ 3 .
  • the vertical axis represents the tension as the units N/m (newtons per metre).
  • the horizontal axis represents the location y in the cross direction of the paper web, the unit being mm (millimetre). In this example, the width of the paper web is 7 meters.
  • the tension values T 1 (1000), T 2 (1000) and T 3 (1000) corresponding to a cross-direction distance of 1000 mm of the paper web have been indicated in respect of each graph of tension profile T 1 (y), T 2 (y) and T 3 (y).
  • FIG. 3 illustrates the principle with which the tension values measured with each stretch value ⁇ 1 , ⁇ 2 and ⁇ 3 are fitted in the curve. This fitting is carried out at each point of measurement of the tension profile.
  • the fitting of a straight line at the measurement points is carried out, for example, by making use of the method of fitting of the least squares.
  • the equation of the straight line drawn in FIG. 3 has the following form:
  • m(y) basis weight profile [kg/sq.m]
  • FIG. 4 shows the CD profile of the dynamic modulus of elasticity E of the paper web determined in the way described above.
  • the vertical axis represents the elasticity module E, whose unit is sq.m/s 2
  • the horizontal axis represents the location on the paper web W in the CD direction.
US09/623,205 1998-02-25 1999-02-22 Method for determination of an irreversible stretch and of a dynamic modulus of elasticity Expired - Fee Related US6517679B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI980428A FI103610B1 (fi) 1998-02-25 1998-02-25 Palautumattoman venymän ja dynaamisen kimmomodulin määritysmenetelmä
FI980428 1998-02-25
PCT/FI1999/000138 WO1999044058A1 (en) 1998-02-25 1999-02-22 Method for determination of an irreversible stretch and of a dynamic modulus of elasticity

Publications (1)

Publication Number Publication Date
US6517679B1 true US6517679B1 (en) 2003-02-11

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Family Applications (1)

Application Number Title Priority Date Filing Date
US09/623,205 Expired - Fee Related US6517679B1 (en) 1998-02-25 1999-02-22 Method for determination of an irreversible stretch and of a dynamic modulus of elasticity

Country Status (8)

Country Link
US (1) US6517679B1 (de)
EP (1) EP1066515B1 (de)
AT (1) ATE249625T1 (de)
AU (1) AU2625599A (de)
CA (1) CA2321726C (de)
DE (1) DE69911187T2 (de)
FI (1) FI103610B1 (de)
WO (1) WO1999044058A1 (de)

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004038384A1 (en) * 2002-10-24 2004-05-06 Metso Paper, Inc. Method for determining the modulus of elasticity of paper
US20040163457A1 (en) * 2001-04-25 2004-08-26 Marko Jorkama Measurement of radial modulus of elasticity of paper
US20050137738A1 (en) * 2003-12-22 2005-06-23 3M Innovative Properties Company Real-time determination of web tension and control using position sensors
US20050167460A1 (en) * 2004-02-04 2005-08-04 The Procter & Gamble Company Method of controlling tension in a moving web material
US20050166670A1 (en) * 2004-02-04 2005-08-04 The Procter & Gamble Company Method of determining a modulus of elasticity of a moving web material
WO2009059860A1 (de) * 2007-11-09 2009-05-14 Voith Patent Gmbh Verfahren und vorrichtung zum erfassen eines risses und/oder eines elastizitätsmoduls einer materialbahn
US20100319454A1 (en) * 2009-06-19 2010-12-23 Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Natural Resources Method and system for determining young's modulus and poisson's ratio for a crystalline material
US7891276B2 (en) 2007-08-31 2011-02-22 Kimbelry-Clark Worldwide, Inc. System and method for controlling the length of a discrete segment of a continuous web of elastic material
US8733686B2 (en) 2010-10-25 2014-05-27 The Procter & Gamble Company Alternative apparatus for reducing web feed rate variations induced by parent roll geometry variations
US8733687B2 (en) 2010-10-25 2014-05-27 The Procter & Gamble Company Alternative apparatus for reducing web feed rate variations induced by parent roll geometry variations
US8733685B2 (en) 2010-10-25 2014-05-27 The Procter & Gamble Company Apparatus for reducing web feed rate variations induced by parent roll geometry variations
US8740130B2 (en) 2010-10-25 2014-06-03 The Procter & Gamble Company Alternative method for reducing web feed rate variations induced by parent roll geometry variations
US8757535B2 (en) 2010-10-25 2014-06-24 The Procter & Gamble Company Method for reducing web feed rate variations induced by parent roll geometry variations
US20150308934A1 (en) * 2014-04-25 2015-10-29 Honeywell International Inc. Apparatus and method for stretch measurements of tissue webs
US9434573B2 (en) 2010-10-25 2016-09-06 The Procter & Gamble Company Alternative method for reducing web feed rate variations induced by parent roll geometry variations
US9434572B2 (en) 2010-10-25 2016-09-06 The Procter & Gamble Company Alternative method for reducing web feed rate variations induced by parent roll geometry variations
US20170188051A1 (en) * 2015-12-28 2017-06-29 Ati Technologies Ulc Method and apparatus for determining the severity of corruption in a picture
US9952160B2 (en) * 2014-04-04 2018-04-24 Packaging Corporation Of America System and method for determining an impact of manufacturing processes on the caliper of a sheet material

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI20010852A0 (fi) * 2001-04-25 2001-04-25 Metso Paper Inc Paperin tangentiaalisen kimmomodulin mittaus
FI111193B (fi) * 2001-12-19 2003-06-13 Metso Paper Automation Oy Menetelmä ja laitteisto liikkuvan rainan kireyden mittaamiseksi
DE10249396A1 (de) * 2002-10-23 2004-05-06 Voith Paper Patent Gmbh Anordnung zur indirekten oder direkten Erfassung eines lokalen Bahnzugs einer laufenden Materialbahn an wenigstens einer Bahn-Querposition
DE102005058142A1 (de) * 2005-12-06 2007-06-21 Voith Patent Gmbh Verfahren zur Bestimmung einer Dehnungseigenschaft einer Papierbahn
DE102008021445B4 (de) * 2008-04-29 2016-03-24 Robert Bosch Gmbh Bahnverarbeitende Maschine und Verfahren zu deren Steuerung

Citations (15)

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Publication number Priority date Publication date Assignee Title
US2755032A (en) 1951-12-17 1956-07-17 Beloit Iron Works Tension regulator and guide and control means therefor
US3057574A (en) 1960-08-08 1962-10-09 Beloit Iron Works Web tension control means
US3718037A (en) 1969-11-24 1973-02-27 Cons Paper Bahamas Ltd Paper machine tension tester
US3933035A (en) 1973-09-19 1976-01-20 J. Bobst & Fils S.A. Installation for continuous measurement of the elastic coefficient of a traveling strip, wire or ribbon
EP0311507A2 (de) 1987-10-05 1989-04-12 Measurex Corporation Anordnung zur kontinuierlichen Bestimmung der Papierkraft
US4866984A (en) 1985-10-04 1989-09-19 Measurex Corporation Sensor and system for continuous determination of paper strength
US5026458A (en) * 1990-08-31 1991-06-25 Kimberly-Clark Corporation Method for controlling basis weight in the production of stretchable webs
US5029469A (en) * 1988-06-17 1991-07-09 Measurex Corporation Sheet tension sensor
US5104488A (en) * 1987-10-05 1992-04-14 Measurex Corporation System and process for continuous determination and control of paper strength
US5269883A (en) * 1990-08-31 1993-12-14 Kimberly-Clark Corporation Method for controlling basis weight in the production of stretchable webs
GB2281632A (en) 1993-09-02 1995-03-08 Czeslaw Golebiowski Tension measurement of elogate moving members
US5649448A (en) 1994-05-16 1997-07-22 Valmet Corporation System for overall control of different transverse profiles in a paper web manufactured in a board of paper machine and/or treated in a finishing machine
US5658432A (en) * 1995-08-24 1997-08-19 Measurex Devron Inc. Apparatus and method of determining sheet shrinkage or expansion characteristics
EP0826821A2 (de) 1996-08-30 1998-03-04 Voith Sulzer Papiermaschinen Gesellschaft mbH Regeleinrichtung mit einer Sensoren-Mehrzahl
US5891306A (en) * 1996-12-13 1999-04-06 Measurex Corporation Electromagnetic field perturbation sensor and methods for measuring water content in sheetmaking systems

Patent Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2755032A (en) 1951-12-17 1956-07-17 Beloit Iron Works Tension regulator and guide and control means therefor
US3057574A (en) 1960-08-08 1962-10-09 Beloit Iron Works Web tension control means
US3718037A (en) 1969-11-24 1973-02-27 Cons Paper Bahamas Ltd Paper machine tension tester
US3933035A (en) 1973-09-19 1976-01-20 J. Bobst & Fils S.A. Installation for continuous measurement of the elastic coefficient of a traveling strip, wire or ribbon
US4866984A (en) 1985-10-04 1989-09-19 Measurex Corporation Sensor and system for continuous determination of paper strength
EP0311507A2 (de) 1987-10-05 1989-04-12 Measurex Corporation Anordnung zur kontinuierlichen Bestimmung der Papierkraft
US5013403A (en) * 1987-10-05 1991-05-07 Measurex Corporation Process for continuous determination of paper strength
US5104488A (en) * 1987-10-05 1992-04-14 Measurex Corporation System and process for continuous determination and control of paper strength
US5029469A (en) * 1988-06-17 1991-07-09 Measurex Corporation Sheet tension sensor
US5026458A (en) * 1990-08-31 1991-06-25 Kimberly-Clark Corporation Method for controlling basis weight in the production of stretchable webs
US5269883A (en) * 1990-08-31 1993-12-14 Kimberly-Clark Corporation Method for controlling basis weight in the production of stretchable webs
GB2281632A (en) 1993-09-02 1995-03-08 Czeslaw Golebiowski Tension measurement of elogate moving members
US5649448A (en) 1994-05-16 1997-07-22 Valmet Corporation System for overall control of different transverse profiles in a paper web manufactured in a board of paper machine and/or treated in a finishing machine
US5658432A (en) * 1995-08-24 1997-08-19 Measurex Devron Inc. Apparatus and method of determining sheet shrinkage or expansion characteristics
EP0826821A2 (de) 1996-08-30 1998-03-04 Voith Sulzer Papiermaschinen Gesellschaft mbH Regeleinrichtung mit einer Sensoren-Mehrzahl
US5891306A (en) * 1996-12-13 1999-04-06 Measurex Corporation Electromagnetic field perturbation sensor and methods for measuring water content in sheetmaking systems

Cited By (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040163457A1 (en) * 2001-04-25 2004-08-26 Marko Jorkama Measurement of radial modulus of elasticity of paper
WO2004038384A1 (en) * 2002-10-24 2004-05-06 Metso Paper, Inc. Method for determining the modulus of elasticity of paper
US7162932B2 (en) * 2002-10-24 2007-01-16 Metso Paper, Inc. Method for determining the modulus of elasticity of paper
US20060037389A1 (en) * 2002-10-24 2006-02-23 Marko Jorkama Method for Determining the Modulus of Elasticity of Paper
US20050137738A1 (en) * 2003-12-22 2005-06-23 3M Innovative Properties Company Real-time determination of web tension and control using position sensors
US6985789B2 (en) 2003-12-22 2006-01-10 3M Innovative Properties Company Real-time determination of web tension and control using position sensors
WO2005078408A1 (en) * 2004-02-04 2005-08-25 The Procter & Gamble Company A method of determining a modulus of elasticity of a moving web material
WO2005077798A1 (en) * 2004-02-04 2005-08-25 The Procter & Gamble Company A method of controlling tension in a moving web material
US6991144B2 (en) 2004-02-04 2006-01-31 The Procter & Gamble Company Method of controlling tension in a moving web material
US6993964B2 (en) 2004-02-04 2006-02-07 The Procter & Gamble Company Method of determining a modulus of elasticity of a moving web material
US20050166670A1 (en) * 2004-02-04 2005-08-04 The Procter & Gamble Company Method of determining a modulus of elasticity of a moving web material
US20050167460A1 (en) * 2004-02-04 2005-08-04 The Procter & Gamble Company Method of controlling tension in a moving web material
AU2005213633B2 (en) * 2004-02-04 2008-03-06 The Procter & Gamble Company A method of determining a modulus of elasticity of a moving web material
US8196497B2 (en) 2007-08-31 2012-06-12 Kimberly-Clark Worldwide, Inc. System and method for controlling the length of a discrete segment of a continuous web of elastic material
US7891276B2 (en) 2007-08-31 2011-02-22 Kimbelry-Clark Worldwide, Inc. System and method for controlling the length of a discrete segment of a continuous web of elastic material
WO2009059860A1 (de) * 2007-11-09 2009-05-14 Voith Patent Gmbh Verfahren und vorrichtung zum erfassen eines risses und/oder eines elastizitätsmoduls einer materialbahn
US20100319454A1 (en) * 2009-06-19 2010-12-23 Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Natural Resources Method and system for determining young's modulus and poisson's ratio for a crystalline material
US8733686B2 (en) 2010-10-25 2014-05-27 The Procter & Gamble Company Alternative apparatus for reducing web feed rate variations induced by parent roll geometry variations
US8733687B2 (en) 2010-10-25 2014-05-27 The Procter & Gamble Company Alternative apparatus for reducing web feed rate variations induced by parent roll geometry variations
US8733685B2 (en) 2010-10-25 2014-05-27 The Procter & Gamble Company Apparatus for reducing web feed rate variations induced by parent roll geometry variations
US8740130B2 (en) 2010-10-25 2014-06-03 The Procter & Gamble Company Alternative method for reducing web feed rate variations induced by parent roll geometry variations
US8757535B2 (en) 2010-10-25 2014-06-24 The Procter & Gamble Company Method for reducing web feed rate variations induced by parent roll geometry variations
US9434573B2 (en) 2010-10-25 2016-09-06 The Procter & Gamble Company Alternative method for reducing web feed rate variations induced by parent roll geometry variations
US9434572B2 (en) 2010-10-25 2016-09-06 The Procter & Gamble Company Alternative method for reducing web feed rate variations induced by parent roll geometry variations
US9952160B2 (en) * 2014-04-04 2018-04-24 Packaging Corporation Of America System and method for determining an impact of manufacturing processes on the caliper of a sheet material
US10184897B2 (en) 2014-04-04 2019-01-22 Packaging Corporation Of America System and method for determining an impact of manufacturing processes on the caliper of a sheet material
US20150308934A1 (en) * 2014-04-25 2015-10-29 Honeywell International Inc. Apparatus and method for stretch measurements of tissue webs
US9816906B2 (en) * 2014-04-25 2017-11-14 Honeywell International Inc. Apparatus and method for stretch measurements of tissue webs
US20170188051A1 (en) * 2015-12-28 2017-06-29 Ati Technologies Ulc Method and apparatus for determining the severity of corruption in a picture
US10334276B2 (en) * 2015-12-28 2019-06-25 Ati Technologies Ulc Method and apparatus for determining the severity of corruption in a picture
US20190268622A1 (en) * 2015-12-28 2019-08-29 Ati Technologies Ulc Method and apparatus for determining the severity of corruption in a picture
US10771818B2 (en) * 2015-12-28 2020-09-08 Ati Technologies, Ulc Method and apparatus for determining the severity of corruption in a picture

Also Published As

Publication number Publication date
FI980428A0 (fi) 1998-02-25
AU2625599A (en) 1999-09-15
CA2321726C (en) 2006-12-19
ATE249625T1 (de) 2003-09-15
CA2321726A1 (en) 1999-09-02
DE69911187T2 (de) 2004-04-29
WO1999044058A1 (en) 1999-09-02
EP1066515B1 (de) 2003-09-10
FI103610B (fi) 1999-07-30
DE69911187D1 (de) 2003-10-16
EP1066515A1 (de) 2001-01-10
FI103610B1 (fi) 1999-07-30

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