US5718939A - Continuous sugar infusion process - Google Patents
Continuous sugar infusion process Download PDFInfo
- Publication number
- US5718939A US5718939A US08/709,727 US70972796A US5718939A US 5718939 A US5718939 A US 5718939A US 70972796 A US70972796 A US 70972796A US 5718939 A US5718939 A US 5718939A
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- United States
- Prior art keywords
- produce
- syrup
- infusing
- water
- infusion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/08—Preserving with sugars
Definitions
- This invention relates generally to a continuous process for infusing fruits and vegetables with sugar. More particularly, the invention is directed to a process for treating the fruits or vegetables with water for a period of time sufficient to cause osmotic rupturing of the cells of the fruits or vegetables which makes the cells more receptive to sugar infusion, followed by infusing the fruits or vegetables with sugar in a stage-wise manner utilizing a concentrated sugar infusion syrup.
- Such a process may consist of charging several hundred gallons of a high Brix syrup (45° to 67°) to a large tank, circulating the syrup, adding more sugar to the syrup, heating the syrup to a temperature from about 100° F. to about 140° F., then immersing the produce therein.
- the syrup is circulated over and through the bed of produce, and the temperature of the system is lowered to an infusion temperature between about 60° F. and about 110° F., depending upon the type of produce being infused. This combination of produce and syrup is maintained within the tank for a period of time ranging from about 3 to about 12 hours.
- the concentrations of sugar in the syrup and the produce will be nearly equal, i.e., within about 5° to about 15° Brix of each other.
- the produce will have been infused with sugar to a level of perhaps 40° to 52° Brix, depending upon the produce being infused.
- the spent infusion syrup is reconcentrated by the evaporation of water therefrom and recycled back to the tank to begin the batch process again.
- Batch infusion processes are disclosed in U.S. Pat. No. 5,000,972 to Nafisi-Movaghar, U.S. Pat. No. 4,713,252 to Ismail, U.S. Pat. No. 4,626,434 to O'Mahony et al., and U.S. Pat. No. 4,256,772 to Shanbhag et al.
- U.S. Pat. No. 5,320,861 to Mantius et al. discloses a two-step process for initially extracting the juice from the fruit then infusing the fruit with sugar.
- the patent states that the post-extraction fruit (prior to the infusion step) has a concentration of fruit juice of about 1% by weight.
- the juice extracted from the fruit is purified and sold, and the soluble sugars contained in the juice are not utilized to infuse the extracted fruit in a subsequent process step.
- the disclosed extraction step is time-consuming, requiring from 90 to 150 minutes, thus resulting in an overall fruit infusion process requiring several hours.
- infusing the treated produce by contacting the treated produce with a concentrated infusion syrup in a stage-wise manner for a time sufficient to prepare an infused produce having a Brix level from about 40° to about 52° and a spent syrup.
- the process for infusing fruits and vegetables comprises the steps of:
- rinsing the infused produce by contacting the infused produce with at least a portion of the waste water, to prepare a rinsed produce and rinse water;
- the process of the present invention are particularly suited for infusing sugar into various fruits and vegetables, to prepare a food product which may be eaten as a snack, mixed with dry breakfast cereals, added to cake mixes, used in confections, etc.
- FIG. 1 is a schematic representation of an infusion process according to the present invention.
- FIG. 2 is a schematic representation of a counter-current infusion process according to the present invention.
- the present invention is directed to a continuous process for infusing sugar into fruits and vegetables, followed by drying.
- Suitable produce for use in practicing the present invention include, but are not necessarily limited to, cherries, cranberries, blueberries, strawberries, peaches, bananas, apples, pineapples, mangos, carrots, beans, peas, potatoes, and the like. This process effectively depresses the water activity of the produce to a level at which most bacteria will not grow.
- the infused produce is rendered microbiologically stable and need not be refrigerated or frozen.
- the process comprises treating the produce for a period of time sufficient to cause osmotic rupturing of at least a portion of the cells within the produce by contacting the produce with water, followed by infusing the treated produce by contacting same with a concentrated sugar infusion syrup in a stage-wise manner.
- a quantity of produce is introduced to a device 12 where it may be treated for a period of time sufficient to cause osmotic rupturing of at least a portion of the cells within the produce, by contacting the produce with water.
- the produce is charged to the device 12 at a rate from about 1,000 pounds per hour to about 6,000 pounds per hour, while water is charged to the device 12 at a rate from about fifty percent (50%) to about three hundred percent (300%) of the produce charge rate.
- the time period sufficient to cause osmotic rupturing of at least a portion of the cells of the produce by contacting the produce with water is generally from about thirty (30) minutes to about three (3) hours.
- the osmotic rupturing is generally carried out at a temperature from about 50° F. to about 100° F. It has been discovered that the osmotic rupturing of a least a portion of the cells of the produce makes the produce more receptive to sugar infusion than simply attempting to infuse the produce by immersing it into an infusion syrup bath.
- This initial step of treating the produce to cause osmotic rupturing is in contrast to prior art processes which treat fruit with water to an extent such that the juice within the fruit is substantially completely extracted from the fruit.
- U.S. Pat. No. 5,320,861 to Mantius et al. discloses water extraction of fruit to the extent that the fruit retains only 1% of its juice content.
- the present invention merely requires that the water contact the produce for a period of time sufficient to cause osmotic rupturing of at least a portion of the cells of the produce.
- the waste water 14 generated by the initial treatment step of the present invention contains only a very minor amount of juice from the produce, i.e., from about one percent (1%) to about five percent (5%) by weight.
- the device 12 utilized to effect the osmotic rupturing of the fruit cells may be any device conventionally known in the art for contacting a bed of produce with a stream of water, such as for example a tank.
- the treating process is carried out by depositing the produce onto a tray with perforated sides and moving flights or onto a porous endless belt, which causes the produce to proceed in a substantially horizontal direction. Water is then sprayed onto the produce from above. The water passes over and through the bed of produce and is collected below the tray or belt. The treated produce 16 is then discharged from the end of the tray or belt, and conveyed to the next process step.
- the process of osmotic rupturing thus effected is known to those involved in molecular biology, but has never been utilized as a preliminary treatment for fruit that is subsequently sugar infused utilizing a stage-wise infusion process.
- the residence time for the produce in any particular stage ranges from about 0.5 hour to about 2 hours.
- the temperature at which the infusion is carried out ranges generally from about 60° F. to about 110° F.
- the treated produce is then conveyed to a stage-wise infusion device 18, comprising a series of step-wise stages.
- Each stage may comprise a pan with moving flights or an endless belt, and an associated infusion syrup spray system, as described hereinabove for the osmotic rupturing treatment device.
- the stages may be configured such that the fruit discharged from any one stage drops by gravity to the beginning of the next stage, while the infusion syrup is directed from a manifold system to each individual stage.
- the infusion syrup flows in a counter-current direction; i.e., the infusion syrup from any one stage is collected and pumped to the previous stage, as illustrated in FIG. 2.
- the treated fruit 16 is infused in a stage-wise, preferably counter-current, process.
- Stage-wise processes are well known to those ordinarily skilled in the art, and do not require further explanation herein.
- a concentrated infusion syrup 20 is introduced to the infusion device 18, generally at a flow rate from about 300 gallons per hour to about 2,000 gallons per hour.
- the concentrated infusion syrup conveniently has a sugar concentration from about 45° to about 72° Brix.
- the Brix scale is a hydrometer scale for sugar solutions so graduated that its readings at a specific temperature represent percentages by weight of the sugar solutions.
- sugar comprises fructose, sucrose, glucose, dextrose, or a mixture thereof.
- the concentrated infusion syrup 20 is sprayed over and through the beds of produce contained in the infusion device 18.
- the liquid collected from the infusion device 18 is spent syrup 22 which is recirculated for use in the produce infusion process.
- spent syrup 22 which is recirculated for use in the produce infusion process.
- the sugar infusion process within the infusion device 18 is most effective when the Brix levels between the syrup and produce at any particular stage are within about 5° to about 20°. Moreover, it is desired to achieve a substantially uniform change in the Brix level of the produce from one stage to the next. A higher yield is achieved when the infusion occurs over an even delta Brix between the produce and syrup in each stage, compared to batch sugar infusion which begins with a high initial Brix level between the produce and syrup and ends with a low delta Brix at the end of the infusion process.
- Infused produce 24 exits from the last stage of the infusion device 18, and is rinsed using at least a portion of the waste water 14 (which has a lower Brix than the infused produce) that is a byproduct of the osmotic rupturing step.
- the rinse flow rate generally ranges from about 500 gallons per hour to about 1,500 gallons per hour.
- This rinsing operation may be carried out in any conventional containment device such as a flume and results in the production of rinsed produce 26 and rinse water 28.
- the rinse water contains syrup removed from the surfaces of the infused produce 24 particles, which syrup is then mixed with the spent syrup 22 exiting from the infusion device 18.
- Sugar is dissolved in the mixture of rinse water 28 and spent syrup 22 by any conventional method such as adding the ingredients to a stirred mixing tank.
- the addition of sugar effectively increases the Brix level, thereby replacing the removed sugar and producing an infusion syrup 30 for use in the infusion process step.
- the infusion syrup 30 is concentrated to remove water therefrom. Such concentration may generally be accomplished by heating the infusion syrup 30 by conventional means to evaporate water therefrom.
- the resultant concentrated infusion syrup 20, having a Brix level from about 45° to about 72°, is then introduced to the infusion device 18.
- Concentrated infusion syrup 20 may be removed from the system as a concentrate 32, for supplying to the manufacturers of flavored food products such as carbonated beverages and candies.
- Adjuvants, such as acids and/or oils may be added to the concentrated infusion syrup 20 for use in the produce infusion process step. For example, glycerine may be added to produce a glycerated product.
- rinsed produce 26 is conveyed through a conventional dryer to prepare dried infused produce, according to the present invention.
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Jellies, Jams, And Syrups (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
Description
Claims (12)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/709,727 US5718939A (en) | 1996-09-09 | 1996-09-09 | Continuous sugar infusion process |
PCT/US1997/015875 WO1998009531A1 (en) | 1996-09-09 | 1997-09-09 | Continuous sugar infusion process |
AU42596/97A AU4259697A (en) | 1996-09-09 | 1997-09-09 | Continuous sugar infusion process |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/709,727 US5718939A (en) | 1996-09-09 | 1996-09-09 | Continuous sugar infusion process |
Publications (1)
Publication Number | Publication Date |
---|---|
US5718939A true US5718939A (en) | 1998-02-17 |
Family
ID=24851089
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US08/709,727 Expired - Lifetime US5718939A (en) | 1996-09-09 | 1996-09-09 | Continuous sugar infusion process |
Country Status (3)
Country | Link |
---|---|
US (1) | US5718939A (en) |
AU (1) | AU4259697A (en) |
WO (1) | WO1998009531A1 (en) |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999035917A1 (en) * | 1998-01-15 | 1999-07-22 | Edward Hirschberg | Methods of infusing phytochemicals, nutraceuticals, and other compositions into food products |
US6254919B1 (en) | 1999-06-29 | 2001-07-03 | Maine Wild Blueberry Company | Preparation of shelf stable blueberries and moist shelf stable blueberry product |
FR2816172A1 (en) * | 2000-11-07 | 2002-05-10 | Doveurope Sa | Starch-based grain preparation for inclusion in food product e.g. ice cream, consists of cooking grain, rinsing and immersion in syrup |
US6440483B1 (en) * | 1999-12-28 | 2002-08-27 | Decas Cranberry Products, Inc. | Method and apparatus for producing a fruit product |
US20030008057A1 (en) * | 2001-04-30 | 2003-01-09 | Hynes Michael P. | Food products |
US20040142072A1 (en) * | 2002-11-06 | 2004-07-22 | Schwarz John C.. | Process and apparatus for infusing cranberry |
US20050249847A1 (en) * | 2004-05-06 | 2005-11-10 | Sinha Nirmal K | Process for producing refrigerated produce |
US20070031552A1 (en) * | 2005-08-05 | 2007-02-08 | Bauman Michael N | Peeled infused dried buoyant cranberries and method for making same |
US20070031553A1 (en) * | 2005-08-05 | 2007-02-08 | Sinha Nirmal K | Scarified infused dried buoyant cranberries and method for making same |
US7625592B1 (en) | 2006-05-24 | 2009-12-01 | Graceland Fruit, Inc. | Process and formulation for dried tomatoes |
US20100173049A1 (en) * | 2007-02-14 | 2010-07-08 | Perdon Alicia A | Reduced sugar raisin and method |
US20220151277A1 (en) * | 2019-03-08 | 2022-05-19 | Jean Marc Tachet Création | Method for enriching food products with proteins and/or with food supplements |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US772018A (en) * | 1903-12-09 | 1904-10-11 | Elizabeth N Alexandrian | Process of preserving citrus fruits. |
US1703730A (en) * | 1925-04-08 | 1929-02-26 | Fraisse Charles | Process for the manufacture of preserved fruit |
US4183963A (en) * | 1976-02-02 | 1980-01-15 | Societe D'assistance Technique Pour Produits Nestle S.A. | Continuous food impregnation |
US4256772A (en) * | 1979-02-12 | 1981-03-17 | General Foods Corporation | Fruit and cereal products and process therefor |
US4350711A (en) * | 1977-01-28 | 1982-09-21 | Rich Products Corporation | Methods of infusing fruits |
US4626434A (en) * | 1983-02-15 | 1986-12-02 | Rich Products Corporation | Fruit infusion using a syrup which has been subjected to enzyme treatment and concentrated |
US4713252A (en) * | 1985-09-12 | 1987-12-15 | Maine Wild Blueberry Co. | Process for producing a semi-moist fruit product and the products therefrom |
US5000972A (en) * | 1989-06-21 | 1991-03-19 | Del Monte Corporation | Method of making dried fruits |
US5320861A (en) * | 1992-01-03 | 1994-06-14 | Ocean Spray Cranberries, Inc. | Fruit extraction and infusion |
-
1996
- 1996-09-09 US US08/709,727 patent/US5718939A/en not_active Expired - Lifetime
-
1997
- 1997-09-09 AU AU42596/97A patent/AU4259697A/en not_active Withdrawn
- 1997-09-09 WO PCT/US1997/015875 patent/WO1998009531A1/en active Application Filing
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US772018A (en) * | 1903-12-09 | 1904-10-11 | Elizabeth N Alexandrian | Process of preserving citrus fruits. |
US1703730A (en) * | 1925-04-08 | 1929-02-26 | Fraisse Charles | Process for the manufacture of preserved fruit |
US4183963A (en) * | 1976-02-02 | 1980-01-15 | Societe D'assistance Technique Pour Produits Nestle S.A. | Continuous food impregnation |
US4350711A (en) * | 1977-01-28 | 1982-09-21 | Rich Products Corporation | Methods of infusing fruits |
US4256772A (en) * | 1979-02-12 | 1981-03-17 | General Foods Corporation | Fruit and cereal products and process therefor |
US4626434A (en) * | 1983-02-15 | 1986-12-02 | Rich Products Corporation | Fruit infusion using a syrup which has been subjected to enzyme treatment and concentrated |
US4713252A (en) * | 1985-09-12 | 1987-12-15 | Maine Wild Blueberry Co. | Process for producing a semi-moist fruit product and the products therefrom |
US5000972A (en) * | 1989-06-21 | 1991-03-19 | Del Monte Corporation | Method of making dried fruits |
US5320861A (en) * | 1992-01-03 | 1994-06-14 | Ocean Spray Cranberries, Inc. | Fruit extraction and infusion |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999035917A1 (en) * | 1998-01-15 | 1999-07-22 | Edward Hirschberg | Methods of infusing phytochemicals, nutraceuticals, and other compositions into food products |
US6254919B1 (en) | 1999-06-29 | 2001-07-03 | Maine Wild Blueberry Company | Preparation of shelf stable blueberries and moist shelf stable blueberry product |
US6880455B1 (en) | 1999-12-28 | 2005-04-19 | Decas Cranberry Products, Inc. | Method and apparatus for producing a fruit product |
US6440483B1 (en) * | 1999-12-28 | 2002-08-27 | Decas Cranberry Products, Inc. | Method and apparatus for producing a fruit product |
US20050186324A1 (en) * | 1999-12-28 | 2005-08-25 | Decas Cranberry Products, Inc. | Method and apparatus for producing a fruit product |
US20040067299A1 (en) * | 2000-11-07 | 2004-04-08 | Andre Granger | Method for preparing a starch-based grain designed to be included in a food product |
FR2816172A1 (en) * | 2000-11-07 | 2002-05-10 | Doveurope Sa | Starch-based grain preparation for inclusion in food product e.g. ice cream, consists of cooking grain, rinsing and immersion in syrup |
WO2002037974A1 (en) * | 2000-11-07 | 2002-05-16 | Mars Incorporated | Method for preparing a starch-based grain designed to be included in a food product |
US20030008057A1 (en) * | 2001-04-30 | 2003-01-09 | Hynes Michael P. | Food products |
US20040142072A1 (en) * | 2002-11-06 | 2004-07-22 | Schwarz John C.. | Process and apparatus for infusing cranberry |
US8178146B2 (en) | 2004-05-06 | 2012-05-15 | Graceland Fruit, Inc. | Process for producing refrigerated produce |
US20050249847A1 (en) * | 2004-05-06 | 2005-11-10 | Sinha Nirmal K | Process for producing refrigerated produce |
US20070031552A1 (en) * | 2005-08-05 | 2007-02-08 | Bauman Michael N | Peeled infused dried buoyant cranberries and method for making same |
US7767242B2 (en) | 2005-08-05 | 2010-08-03 | Kellogg Company | Peeled infused dried buoyant cranberries and method for making same |
US7781008B2 (en) | 2005-08-05 | 2010-08-24 | Kellogg Company | Scarified infused dried buoyant cranberries and method for making same |
US20070031553A1 (en) * | 2005-08-05 | 2007-02-08 | Sinha Nirmal K | Scarified infused dried buoyant cranberries and method for making same |
US7625592B1 (en) | 2006-05-24 | 2009-12-01 | Graceland Fruit, Inc. | Process and formulation for dried tomatoes |
US20100173049A1 (en) * | 2007-02-14 | 2010-07-08 | Perdon Alicia A | Reduced sugar raisin and method |
US20220151277A1 (en) * | 2019-03-08 | 2022-05-19 | Jean Marc Tachet Création | Method for enriching food products with proteins and/or with food supplements |
Also Published As
Publication number | Publication date |
---|---|
WO1998009531A1 (en) | 1998-03-12 |
AU4259697A (en) | 1998-03-26 |
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Legal Events
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AS | Assignment |
Owner name: GRACELAND FRUIT COOPERATIVE, INC., MICHIGAN Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:NUGENT, DUANE C.;REEL/FRAME:008208/0357 Effective date: 19960821 |
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Free format text: PATENTED CASE |
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Year of fee payment: 4 |
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FPAY | Fee payment |
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FPAY | Fee payment |
Year of fee payment: 12 |
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Owner name: CITIZENS BANK, MICHIGAN Free format text: SECURITY AGREEMENT;ASSIGNOR:GRACELAND FRUIT, INC.;REEL/FRAME:027544/0846 Effective date: 20111229 |
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AS | Assignment |
Owner name: GRACELAND FRUIT, INC., MICHIGAN Free format text: RELEASE BY SECURED PARTY;ASSIGNOR:THE HUNTINGTON NATIONAL BANK;REEL/FRAME:060795/0579 Effective date: 20171215 |