US565361A - John a - Google Patents
John a Download PDFInfo
- Publication number
- US565361A US565361A US565361DA US565361A US 565361 A US565361 A US 565361A US 565361D A US565361D A US 565361DA US 565361 A US565361 A US 565361A
- Authority
- US
- United States
- Prior art keywords
- adhesive
- pound
- compounds
- john
- glycerin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000853 adhesive Substances 0.000 description 34
- 230000001070 adhesive Effects 0.000 description 28
- 150000001875 compounds Chemical class 0.000 description 28
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 12
- 235000011187 glycerol Nutrition 0.000 description 12
- 239000000463 material Substances 0.000 description 12
- 239000000126 substance Substances 0.000 description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N D-Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 6
- 108010010803 Gelatin Proteins 0.000 description 6
- 229920000715 Mucilage Polymers 0.000 description 6
- CVHZOJJKTDOEJC-UHFFFAOYSA-N Saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 description 6
- 229940081974 Saccharin Drugs 0.000 description 6
- 239000008273 gelatin Substances 0.000 description 6
- 229920000159 gelatin Polymers 0.000 description 6
- 235000019322 gelatine Nutrition 0.000 description 6
- 235000011852 gelatine desserts Nutrition 0.000 description 6
- 239000008103 glucose Substances 0.000 description 6
- 239000003230 hygroscopic agent Substances 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 235000019204 saccharin Nutrition 0.000 description 6
- 239000000901 saccharin and its Na,K and Ca salt Substances 0.000 description 6
- 241000370092 Actiniopteris Species 0.000 description 4
- 230000002421 anti-septic Effects 0.000 description 4
- 239000004568 cement Substances 0.000 description 4
- 239000003292 glue Substances 0.000 description 4
- NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
- 238000003892 spreading Methods 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 2
- 235000004310 Cinnamomum zeylanicum Nutrition 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- 239000004375 Dextrin Substances 0.000 description 2
- 241000206672 Gelidium Species 0.000 description 2
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 2
- 240000005147 Syzygium aromaticum Species 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 235000017803 cinnamon Nutrition 0.000 description 2
- 230000002939 deleterious Effects 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- 108010059642 isinglass Proteins 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910052627 muscovite Inorganic materials 0.000 description 2
- 230000001473 noxious Effects 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 230000002335 preservative Effects 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000004642 transportation engineering Methods 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09H—PREPARATION OF GLUE OR GELATINE
- C09H5/00—Stabilisation of solutions of glue or gelatine
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L89/00—Compositions of proteins; Compositions of derivatives thereof
Definitions
- My invention relates to that class of adhesives that is most widely recognized by the terms mucilage or cements, being intended for the uses to which these articles are adapted and applied; but unlike most of these preparations my adhesive is a solid substance, though it is designed to supplant the mucilage bottle and brush and for many purposes the more expensive liquid cements and glues.
- a further object of my invention is the preparation of a stronger and more effective adhesive than merely dissolved gums and the like, and more convenient in all respects of transportation or shipment, exposure for sale, and safety and ease of application in practical use.
- these compounds When cooled, these compounds form a soft flexible elastic mass not unlike very soft rubber or the material of printers rollers, and when formed into sticks or pencils of convenient size, usually by pouring while hot into suitable cylindrical envelops, it produces a very serviceable article for use, as the end of the pencil is admirably adapted to spreading a thin coat of the adhesive upon any surfaces it is designed to unite.
- These compounds are difficultly soluble or are, in other words, too slowly soluble to adapt them to the many little uses that arise at the desk, such as gumming an imperfect envelop or stamp or a wrapper or label or mending a torn document or note, because too much time is required to moisten and dissolve the material sufficiently to coat the surfaces to be united.
- the compounds described become, moreover, of a tougher and still more insoluble consistency as they slowly harden with lapse of time, and though retaining a certain degree of flexibility they redissolve with much difficulty, requiring both time and the application of heat for the process.
- an adhesive compound preferably in stick form, being of a permanently plastic nature and composed of a suitable adhesive, saccharin matter, a suitable hygroscopic agent, and an antiseptic or preservative material in substantially the proportions specified.
- An adhesive compound composed of a suitable adhesive, saccharin matter, glycerin,
- An adhesive compound composed of a suitable adhesive, saccharin matter, glycerin, a hygroscopic agent, and an antiseptic ele- JOHN A. LINK. In presence of- FLoRINn A. ALT-BRIGHT, M. A. POLLARD.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Adhesives Or Adhesive Processes (AREA)
Description
UNITED STATES PATENT ()FFICE.
JOHN A. LINK, OF IVASHINGTON, DISTRICT OF COLUMBIA, ASSIGNOR OF NINE-SIXTEENTHS TO CAMPBELL CARRINGTON AND ALEXANDER R.
HULLOWNY, OF SAME PLACE.
MUCILAGE.
SPECIFICATION forming part of Letters Patent No. 565,361, dated August 4, 1896.
Application filed May 16, 1896. Serial No. 591,864. (No specimens.)
To all whom it may concern.-
Be it known that I, JOHN A. LINK, a citizen of the United States, residing at Washington, District of Columbia, have invented certain new and useful Improvements in Adhesive Compounds; and I do hereby declare the following to be a specification thereof.
My invention relates to that class of adhesives that is most widely recognized by the terms mucilage or cements, being intended for the uses to which these articles are adapted and applied; but unlike most of these preparations my adhesive is a solid substance, though it is designed to supplant the mucilage bottle and brush and for many purposes the more expensive liquid cements and glues.
A further object of my invention is the preparation of a stronger and more effective adhesive than merely dissolved gums and the like, and more convenient in all respects of transportation or shipment, exposure for sale, and safety and ease of application in practical use.
To these ends and in preparation of my compound I take of gelatin or glue one pound, of glucose one-half pound, and of glycerin three-fourths of a pound. I dilute and heat these together over a vapor bath and then pour into molds to cool. Or I may take of gelatin and glycerin each one pound and of glucose and sugar each one-half pound and melt together as described. When cooled, these compounds form a soft flexible elastic mass not unlike very soft rubber or the material of printers rollers, and when formed into sticks or pencils of convenient size, usually by pouring while hot into suitable cylindrical envelops, it produces a very serviceable article for use, as the end of the pencil is admirably adapted to spreading a thin coat of the adhesive upon any surfaces it is designed to unite. These compounds, however, are difficultly soluble or are, in other words, too slowly soluble to adapt them to the many little uses that arise at the desk, such as gumming an imperfect envelop or stamp or a wrapper or label or mending a torn document or note, because too much time is required to moisten and dissolve the material sufficiently to coat the surfaces to be united. For practical use a touch to the tongue or to a damp sponge must suffice, and a single application of the pencil by rubbing it across the surfaces should spread the proper quantity of the dissolved material to insure the best results, any material too refractory to use as above described being unsuitable for the purpose.
The compounds described become, moreover, of a tougher and still more insoluble consistency as they slowly harden with lapse of time, and though retaining a certain degree of flexibility they redissolve with much difficulty, requiring both time and the application of heat for the process. I therefore add a strongly hygroscopic element or substance to the compound in such quantity as to retain a permanently greater percentage of water in combination, as well as to insure more instant solubility when moisture is appliedthat is to say, the material is maintained in a soft, viscid, and tenacious consistency and at once combines at the surface with adclitionalmoisture when this is applied, so that a portion of the adhesive instantly adheres to anything it touches.
I find that four to six ounces of the nitrate of ammonium,when added to either of the compounds I have named, secures the results desired. The compound remains permanently moist and adhesive in consistency, only requiring additional moisture to dilute it sufficiently for spreading evenly; but these compounds, especially in the moistened condition described, are very subject to fermentative and putrefactive changes, and quickly become offensive unless preserved against these, and I therefore add, say, of acetic acid, one ounce; carbolic acid, one ounce; oil of myrbane, one ounce, or in place of this last an equal quantity of the oil of cinnamon or cloves or any highly aromatic essential oil or substance. I have found these sufficient to wholly prevent and resist deleterious or noxious changes in these compounds.
As another example, I take of gelatin or isinglass, one pound; of glucose, dextrin, or sugar, one pound, and of glycerin one pound, and to these Iadd, of acetic acid, of carbolic acid, and of an essential oil, each, one ounce. Lastly, I add six ounces of the nitrate of am- Ice monium; but I do not limit my invention to these compounds or to these proportions, as I employ any suitable group of adhesives which when diluted and softened with Water and glycerin, and combined With a more highly hygroscopic substance and preserved by means of any effective agency, are Well Within the scope of said invention.
Having thus described my invention, What I claim is 1. As a new article of manufacture, an adhesive compound preferably in stick form, being of a permanently plastic nature and composed of a suitable adhesive, saccharin matter, a suitable hygroscopic agent, and an antiseptic or preservative material in substantially the proportions specified.
2. An adhesive compound composed of a suitable adhesive, saccharin matter, glycerin,
and a hygroscopic agent in substantially the portions specified.
3. An adhesive compound composed of a suitable adhesive, saccharin matter, glycerin, a hygroscopic agent, and an antiseptic ele- JOHN A. LINK. In presence of- FLoRINn A. ALT-BRIGHT, M. A. POLLARD.
Publications (1)
Publication Number | Publication Date |
---|---|
US565361A true US565361A (en) | 1896-08-04 |
Family
ID=2634075
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US565361D Expired - Lifetime US565361A (en) | John a |
Country Status (1)
Country | Link |
---|---|
US (1) | US565361A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2467715A (en) * | 1946-03-08 | 1949-04-19 | Nat Starch Products Inc | Manufacture of animal glue jellies |
US2531715A (en) * | 1948-04-28 | 1950-11-28 | Nat Starch Products Inc | Manufacture of animal glue jellies |
US5209776A (en) * | 1990-07-27 | 1993-05-11 | The Trustees Of Columbia University In The City Of New York | Tissue bonding and sealing composition and method of using the same |
-
0
- US US565361D patent/US565361A/en not_active Expired - Lifetime
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2467715A (en) * | 1946-03-08 | 1949-04-19 | Nat Starch Products Inc | Manufacture of animal glue jellies |
US2531715A (en) * | 1948-04-28 | 1950-11-28 | Nat Starch Products Inc | Manufacture of animal glue jellies |
US5209776A (en) * | 1990-07-27 | 1993-05-11 | The Trustees Of Columbia University In The City Of New York | Tissue bonding and sealing composition and method of using the same |
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