US433066A - Process of making soap - Google Patents
Process of making soap Download PDFInfo
- Publication number
- US433066A US433066A US433066DA US433066A US 433066 A US433066 A US 433066A US 433066D A US433066D A US 433066DA US 433066 A US433066 A US 433066A
- Authority
- US
- United States
- Prior art keywords
- soap
- making soap
- making
- needles
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title description 18
- 239000000344 soap Substances 0.000 title description 16
- 238000009835 boiling Methods 0.000 description 14
- 239000011347 resin Substances 0.000 description 12
- 229920005989 resin Polymers 0.000 description 12
- 239000000835 fiber Substances 0.000 description 8
- 238000007127 saponification reaction Methods 0.000 description 8
- 239000000463 material Substances 0.000 description 6
- 239000003513 alkali Substances 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 230000005484 gravity Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 241001237728 Precis Species 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 235000021028 berry Nutrition 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000009938 salting Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/02—Boiling soap; Refining
Definitions
- This invention relates to an improved process of manufacturing soap; and it consists in the novel steps hereinafter set forth, and particularly defined by the claims.
- I proceed as follows: I first take pineneedles, generally considered a waste material, but containing considerable resin, which I have found to be especially useful in the manufacture of soap. I treat these needles so as to extract therefrom the resin, preferably by first crushing the same to loosen the silicious coating or covering, and then boiling them from one to five hours in an alkaline solution of suitable strength. The crushing opens the needles, so that the alkali may readily act upon the interior thereof, and the boiling extracts therefrom the resin. The specific gravity of the solution varies, so that it cannot be precis 31y stated, and I do not wish to restrict myself to any particular specific gravity.
- a fatty substance is then mixed with this solution in proportions found to be most desirable, and both are then boiled from an hour and a half to two hours, or until a viscid emulsion capable of being drawn out into threads or ribbons is produced.
- a further quantity of the solution is added gradually for the purpose of making the separation more complete and with constant stirring during the addition, so as to insure thorough contact.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
UNITED STATES PATENT ()FFICE.
JOHN B. N. BERRY, OF BALTIMORE, MARYLAND.
PROCESS OF MAKING SOAP.
SPEGIFIGATION forming part of Letters Patent No. 483,066, dated July 29, 1890.
Application filed August l la, 1889. Serial No. 320,756- (Spccimcna) To all whom it may concern:
Be it known that I, JOHN B. N. BERRY, a citizen of the United States, residing at Baltiinore,in the State of Maryland, have invented certain new and useful Improvements in the Process of Making Soap, of which the follow ing is a specification.
This invention relates to an improved process of manufacturing soap; and it consists in the novel steps hereinafter set forth, and particularly defined by the claims.
In carrying out my invention I proceed as follows: I first take pineneedles, generally considered a waste material, but containing considerable resin, which I have found to be especially useful in the manufacture of soap. I treat these needles so as to extract therefrom the resin, preferably by first crushing the same to loosen the silicious coating or covering, and then boiling them from one to five hours in an alkaline solution of suitable strength. The crushing opens the needles, so that the alkali may readily act upon the interior thereof, and the boiling extracts therefrom the resin. The specific gravity of the solution varies, so that it cannot be precis 31y stated, and I do not wish to restrict myself to any particular specific gravity. After the needles have been thus boiled in the alkaline solution for a sufficient length of time to extract therefrom all the resin contained therein, which is taken up by the alkali, the refuse material-namely, the pine-needle fiber-is then removed from the solution or liquor, and may be afterward used for purposes to which it may be found adapted. A fatty substance is then mixed with this solution in proportions found to be most desirable, and both are then boiled from an hour and a half to two hours, or until a viscid emulsion capable of being drawn out into threads or ribbons is produced. At this stage a further quantity of the solution is added gradually for the purpose of making the separation more complete and with constant stirring during the addition, so as to insure thorough contact. The
further steps in the process are such as are nsuallyemployedin soap-making and understood by those skilled in the art, the usual salting'out process being employed to separate the spent lye. Although not absolutely necessaryit is preferred to add the fatty substance and proceed with the subsequent steps immediately after the complete extraction of the resin from the needles before precipitation or evaporation has had time to take place. 7 The product is specially fitted for cleaning harness and other like uses.
What I claim as new is 1. The herein-described process of making soap, which consists in treating pine-needles in an alkaline solution to extract the resin therefrom, removing the fibers, adding fatty materials to the liquor, and subsequently treating the mass to produce saponification, as set forth.
2. The herein-described process of making soap, which consists in first treating pineneedles to loosen their outer coating, next boiling the same in an alkaline solution, removing the fibers, and subsequentlytreating the resultingliquor to produce saponification, as set forth.
3. The herein-described process of making soap, which consists in treating pine-needles to loosen their covering, boiling the same in an alkaline solution, removing the fibers, adding the fatty material to said solution, and treating the mass to produce saponification, as set forth.
4. The herein-described process of making soap, which consists in treating pine-needles to loosen their covering, boiling the same in an alkaline solution, removing the fibers, adding the fatty material to said solution before cooling of the latter, and immediately treating the mass to produce saponification,as set forth.
In testimony whereof I afiix my signature in presence of two witnesses.
JOHN B. N. BERRY. Witnesses:
H. OTIS GRAY, WILLIAM J. GASCOYNE.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US433066A true US433066A (en) | 1890-07-29 |
Family
ID=2501969
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US433066D Expired - Lifetime US433066A (en) | Process of making soap |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US433066A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1868560A2 (en) * | 2005-03-17 | 2007-12-26 | Caper Naum Vista Olive Oil Market Ltd. | Soaps from organic residues and method of producing the same |
-
0
- US US433066D patent/US433066A/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1868560A2 (en) * | 2005-03-17 | 2007-12-26 | Caper Naum Vista Olive Oil Market Ltd. | Soaps from organic residues and method of producing the same |
| EP1868560A4 (en) * | 2005-03-17 | 2014-06-11 | Caper Naum Vista Olive Oil Market Ltd | Soaps from organic residues and method of producing the same |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US433066A (en) | Process of making soap | |
| US2300749A (en) | Manufacture of soap | |
| US2678326A (en) | Method of refining oils with polycarboxylic acids | |
| US547122A (en) | Process of purifying vegetable oils | |
| US441462A (en) | Method of treating parchmentized-fiber waste | |
| US153707A (en) | Improvement in the processes of treating sponge for upholstering purposes | |
| US2069823A (en) | Waterproofing materials and processes for producing the same | |
| US601603A (en) | Process of decomposing fats or oils into fatty acids and glycerin | |
| US506051A (en) | Process of treating black-ash residuum of wood-pulp manufacture | |
| US2000562A (en) | Process of removing resin from sulphite cellulose | |
| US664437A (en) | Treating white lead. | |
| US450120A (en) | Process of extracting palmetto fiber | |
| US1115500A (en) | Process of preparing vegetable fibers. | |
| US968438A (en) | Process for the manufacture of bleached soap. | |
| US259755A (en) | William green | |
| US2022738A (en) | Bleaching of fatty acids, oils, and fats | |
| US2415140A (en) | Triglyceride refining process | |
| US475395A (en) | Process of recovering grease | |
| US1257080A (en) | Process of treating cotton-stalks. | |
| US776187A (en) | Process of reclaiming rubber from vulcanized-rubber waste. | |
| US549532A (en) | Chusetts | |
| US823053A (en) | Process of recovering rubber from rubber waste. | |
| US1116343A (en) | Process of preparing vegetable fibers. | |
| US101175A (en) | Improvement in the manufacture of xyloidine and its compound | |
| US1009019A (en) | Process of separating hair from haircloth. |