US4008A - Improvement w the manufacture of oil from resin - Google Patents
Improvement w the manufacture of oil from resin Download PDFInfo
- Publication number
- US4008A US4008A US4008DA US4008A US 4008 A US4008 A US 4008A US 4008D A US4008D A US 4008DA US 4008 A US4008 A US 4008A
- Authority
- US
- United States
- Prior art keywords
- oil
- improvement
- manufacture
- resin
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title description 4
- 239000011347 resin Substances 0.000 title 2
- 229920005989 resin Polymers 0.000 title 2
- 239000002253 acid Substances 0.000 description 16
- 238000000034 method Methods 0.000 description 12
- 238000004821 distillation Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 210000003414 Extremities Anatomy 0.000 description 2
- 206010022000 Influenza Diseases 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 229910052570 clay Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 150000002894 organic compounds Chemical class 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 230000000630 rising Effects 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
Definitions
- TafijiZZ uglbona it may concern:
- the fire must then be withdrawn-fron1 .B,- and the, still allowed to cool for four hours.
- the plug is thenwithdrawn from the short pipe 0, No. 1, and the pitchy residuum will flow into any convenient vessel placed to receive it.
- the mixture of oil and acid produced at the commencement "of the operation is allowed to separate in the,
- the process, as in the first case, must be discontinued when the green color makes its appearance in the, oil; time being allowed for cooling the apparatus as before. The pitchy.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Description
W. T. GLOUGH.
MAKING OIL.
' 2 Sheets-Sheet I.
Patented Apr. 22, 1845.
mmllmli WHHIIH STATES f OFFICEO WILLIAM iii. onoun, or orr'y, I NEW JERSEY.
sta caafi orming part amt-es Patent No. 4,0018, dated April2'2, 1845. I
TafijiZZ uglbona it may concern:
. i-Be it'known that I; Wi I A'MT, Qnouefl, 'of' J ersey fGijJY j i i a the Statet of; Jersey, have: ,scovereda process not hitherto known for manufacturing adstfulbihyas hereiu de scribedi'f' 4, v 1
,IThe oil' is aj mpoundof carb'oniand hyd rog'enyiwliich pipe t .by..tiie dry distillation ot 1 esin ,"-oifromzthe residual tarry liquids :otI"ihe-' j!-rosiugas worksfil .T.-I' place tweli e from thetrosinf igasiworks; in the still A, No: 1,' th roughjthecharging-dooi- 3-,:(thef'stilhvtith it's condensers-may be made of cast or wroughtironyor any'jother suitable material,)=the'cover for wliicli is'thenscrewed firmly into its place,
the-outer side of which -has been-previously smai'ediwithdoam 'or' clay or any other sui-table material;torrpreventthe escape of oil-i I ne;. distillation.- Fire is then; "placed in'fthe rumJce B, No. Zthe' flame and" vapeegunmgr heafii'rbmzwhitzh rise-through the openings M in the'fi're arch L, into the flues G, circulating round each half of the still A,- and terminating' ip he flue 0, communicatingtwith the chimney of the works: In the flue Othere mustbe adampernearthe chimney, or inany 5 convenient place, to regulate the heat during the process of. distillation. During-the early part of th'e"di'stil1ation a quantity of. acid mixed with adark colored oilvisi discharged from-the pipe G-into'the fupne'lL attached tothe pipe 1?, contained in the cooling-trough ,L, which I keep filled with cold water, and thence into a receiver placed at theextremjjty, of -P, and atlthesame time acid and asmall portion ofoil are discharged by the pipe H from therpo'st condejnserll into-the spout mend thence intoareceiver. The pipe'N on the top of the condenser F allows the uncon; densable-igases togesoape during the process.
When about fifty gallons inalll of this mixture ot oil and acid'liaye-been obtained frouijtlie pipes H and G,ioil of abrown'ish red color,
but nearlyl'fi ee from acid isdischarged by f Barticiilar attention' must now be" paid to i the fi're,in:B,-in order 't-hat'thstream of oil whichfiows' from -G' maybe continued as regular'a's pnssiblefiay to the extent of twenty five g'allpns per hour. V If the fire is urged too t- I e pipe 'G,c and.auerysmall portion of acid strong,jrosin in'an undecomposed state will 'be distilled'over along with the .oil, which considerably injures the'subsequent operations. I lation may be known by the oil assuming a light greenish tin-t. The fire must then be withdrawn-fron1 .B,- and the, still allowed to cool for four hours. The plug is thenwithdrawn from the short pipe 0, No. 1, and the pitchy residuum will flow into any convenient vessel placed to receive it. The mixture of oil and acid produced at the commencement "of the operation is allowed to separate in the,
vessels-in which it has been received, and-the oil rising to thesurface of the acid is decanted and m'ixed with the. oil obtained during the remainder of the'distil-lation to be again introduced into the still fora secondoperation,
in the c'arly"stage "of which a portionof oil.
will. distill 'ofx er mixed with acid whichjnustf *neanoweirtosinister beidi when the oil is free froniacid, (which may be ascertained by its havinglost the peculiar sour smell resulting fromjts' admixture with that organic compound.) 'it'may be run into any convenient receiver placed at the extremity of the pipe P. The process, as in the first case, must be discontinued when the green color makes its appearance in the, oil; time being allowed for cooling the apparatus as before. The pitchy.
residuum is to be discharged at O, the redistiyllation to be continued until the oil is of the desired purity;- p
I do not claim the particular form or description' of apparatus still, or retorts as set iorth in the drawings Nos. 1 What I; claim is?- V 1. The process or mode of producing the American oil, as setforth'in the above specification' and drawings. Such apparatus may be Tmodiliedor varied, as" circumstances may require, from'time to time, when deemed "expedient. v
2. The process, as
ne emaboveset forth, at
producing the. substance which-kl denominatei J Arms 0. BELL.
The period for suspending-the distil-- and 2- herewith.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US4008A true US4008A (en) | 1845-04-22 |
Family
ID=2064308
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US4008D Expired - Lifetime US4008A (en) | Improvement w the manufacture of oil from resin |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US4008A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2010253376A (en) * | 2009-04-24 | 2010-11-11 | Musashi Eng Co Ltd | Nozzle rotation mechanism and coating device provided with the same |
| JP2011500645A (en) * | 2007-10-17 | 2011-01-06 | ティクセル | Composition for the treatment of multiple sclerosis |
| JP2011512092A (en) * | 2008-02-11 | 2011-04-14 | テレフオンアクチーボラゲット エル エム エリクソン（パブル） | Techniques for soft bit scaling |
| JP2012105072A (en) * | 2010-11-10 | 2012-05-31 | Fujitsu Ten Ltd | Antenna |
| JP2012110619A (en) * | 2010-11-26 | 2012-06-14 | National Institute Of Advanced Industrial Science & Technology | Footrest mounting structure of wheelchair |
| JP2012164004A (en) * | 2011-02-03 | 2012-08-30 | Canon Inc | Control device, control method and program |
| JP2013544598A (en) * | 2010-11-23 | 2013-12-19 | カーディアック ペースメイカーズ， インコーポレイテッド | Foldable antenna for implantable medical device |
| JP5662484B2 (en) * | 2011-02-04 | 2015-01-28 | 富士電機株式会社 | Battery-powered gas alarm and its control device |
-
0
- US US4008D patent/US4008A/en not_active Expired - Lifetime
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011500645A (en) * | 2007-10-17 | 2011-01-06 | ティクセル | Composition for the treatment of multiple sclerosis |
| JP2011512092A (en) * | 2008-02-11 | 2011-04-14 | テレフオンアクチーボラゲット エル エム エリクソン（パブル） | Techniques for soft bit scaling |
| JP2010253376A (en) * | 2009-04-24 | 2010-11-11 | Musashi Eng Co Ltd | Nozzle rotation mechanism and coating device provided with the same |
| JP2012105072A (en) * | 2010-11-10 | 2012-05-31 | Fujitsu Ten Ltd | Antenna |
| JP2013544598A (en) * | 2010-11-23 | 2013-12-19 | カーディアック ペースメイカーズ， インコーポレイテッド | Foldable antenna for implantable medical device |
| JP2012110619A (en) * | 2010-11-26 | 2012-06-14 | National Institute Of Advanced Industrial Science & Technology | Footrest mounting structure of wheelchair |
| JP2012164004A (en) * | 2011-02-03 | 2012-08-30 | Canon Inc | Control device, control method and program |
| JP5662484B2 (en) * | 2011-02-04 | 2015-01-28 | 富士電機株式会社 | Battery-powered gas alarm and its control device |
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