US3733484A

US3733484A - Control for electron microprobe

Info

Publication number: US3733484A
Application number: US00872061A
Authority: US
Inventors: M Bayard
Original assignee: WALTER C MC CRONE ASSOCIATES I
Current assignee: WALTER C MC CRONE ASSOCIATES I; WALTER C MC CRONE ASSOCIATES INC US
Priority date: 1969-10-29
Filing date: 1969-10-29
Publication date: 1973-05-15
Anticipated expiration: 1990-05-15

Abstract

An electron microprobe has a holder for a sample to be analyzed. The holder is movable along an X-axis and a Y-axis, each at right angles to the electron beam directed at the sample. Drives, each including an electric motor, are operatively connected to the holder to adjust the position of the holder along the respective axis. There are also electron beam position controls for positioning the beam in a path oriented as desired with respect to the X and Y axes. An electron beam current control enables the quantity of electrons in the beam to be adjusted. A third drive includes an electric motor, and is connected to a reflector to position the reflector with respect to the X-rays emitted from the sample, and with respect to X-ray detectors. The controls and drives are connected to a control matrix through which signals are supplied to the respective controls and drives, as dictated by a computer. Each of the controls and drives produces an analogue feedback signal indicative of the setting thereof. These feedback signals are sent to a selector matrix from which a specific signal is selected, as dictated by the computer, with the selected signal being delivered to the computer through an analogue to digital converter. The X-ray detectors also produce signals which are ultimately delivered to the computer either directly or through the analogue to digital converter. By appropriately programming the computer, the apparatus automatically analyzes the sample for constituents as desired.

Description

United States Patent 1 Bayard May 15, 1973 s I [75] Inventor:

[ CONTROL FOR ELECTRON MICROPROBE Michael A. Bayard, Chicago, ill.

I [73] Assignee: Walter C. McCrone Associates, Inc.,

Chicago, Ill.

[22] Filed: Oct. 29, 1969 [21] Appl. No.: 872,061

Primary ExaminerWilliam F. Lindquist Attorney- Ddrbo, Bobertson 8; \{andenburgh 7 57 ABSTRACT An electron microprobe has a holderfor a sample to be analyzed. The holder is movable along an X-axis and a Y-axis, each at right angles to the electron beam directed at the sample. Drives, each including an electric motor, are operatively connected to the holder to adjust the position of the holder along the respective axis. There are also electron beam position controls for positioning the beam in a path oriented as desired with respect to the X; and Y axes. An electron beam current control enables. the quantity of electrons in the beam to be adjusted. A third drive includes an electric motor, and is connected to a reflector to position the reflector with'respect to the X-rays emitted from the sample, and with respect to X-ray detectors. The controls and drives are connected to a control matrix through which signals are supplied to the respective controls and drives, as dictated by a computer. Each of the controls and drives produces an analogue feedback signal indicative of the setting thereof. These feedback signals are sent to a selector matrix from which a specific signal is selected, as dictated by the computer, with the selected signal being delivered to the computer through an analogue to digital converter. The X-ray detectors also produce signals which are ultimately delivered to the computer either directly or through the analogue to digital converter.

'By appropriately programming the computer, the apparatus automatically analyzes the sample for constituents as desired.

7 Claims, 3 Drawing Figures CONTROL MA TR! X MANuAi UI/ER K/U/ COMPUT ER 58 ANA! (mus "I Dl i/ T/lL (UNI/ERTER mmmnwm 51m 3. 1 33 48 1 SHEET 1 OF 3 5? BIZ/[AM 539 X A X/S BEAM CONTROL Y-Axls BEAM CONTROL DETECTORS v v SAMPLE 6J3 V CURRENT w 32 MEANS r CONTROL 65 .SELE

MANUAL CTOR MATRIX OVER RIDE PROGRAM -215 i MA TR/X 5% AMA 1.0605 COMPUTER 4: T0 DIGITAL 1 CONVERTER .519

'Zf-L 5d @39 216-- READ T 13 7&6 gm

Jig/ya 1 CONTROL FOR ELECTRON MICROPROBE BACKGROUND OF THE INVENTION Electron microprobes are employed to make composition analyses of various samples, i.e. small areas of a metal surface, occlusions in a polished section, small areas in thin sections, free particles mounted on a substrate, etc. Under the prior art practices, these analyses require constant attention by a qualified operator. Once the raw data is obtained by the operator, the operator must spend a substantial amount of time reducing the raw data to useful analytical answers. Following these practices, a skilled operator cannot be expected to make complete quantitative analysis of more than about three to four samples per day. The electron microprobe is an expensive piece of equipment and the cost of the time of a skilled operator is not insubstantial. Thus, not only is the amount of analytical output relatively small, but the cost per analysis is relatively high.

Utilizing the present invention, the operator need only work about an hour a day to do to a hundred times as much work as he previously accomplished in 8 hours. The operator can analyze 32 samples per 8 hour day using the spectrometers of the microprobe, and can analyze as many as 400 a day using the nondispersive detector. Furthermore, during an eight hour day during which analyses are being made, perhaps seven-eighths of the operators time can be devoted to activities other than overseeing the analyses that are taking place. lt is possible for the apparatus to be set up in the evening to carry out analyses overnight. In the morning when the operator returns to work, the results of those analyses (the raw data which has been reduced to useful analytical answers) is waiting for him.

SUMMARY OF THE INVENTION The present invention relates to a unique combination of a microprobe and controls therefor which will automatically carry out analyses of samples and produce refined analytical answers.

DESCRIPTION OF THE DRAWINGS FIG. 1 is a diagrammatic representation of an electron microprobe having the automatic control apparatus of the present invention;

FIG. 2 is a schematic drawing of the control and feedback apparatus for one of the sample holder drives; and

FIG. 3 is a partial schematic diagram illustrating the control and feedback for one of the electron beam positioning controls.

DESCRIPTION OF SPECIFIC EMBODIMENT Essentially, an electron microprobe comprises a cathode from which an electron beam 16 is emitted, with the electrons being driven towards a sample 17. The impact of the electrons on the sample produce a secondary emission of X-rays which are indicated on FIG. 1 by the dot-dash line 18. The X-rays are picked up and directed by a reflector 19 to X-ray detectors 20 incorporated in a probe 21. I

The position at which the beam 16 impacts on the sample 17 is controlled in two ways. A relatively coarse control is obtained by reason of the fact that the holder 24, on which the sample 17 is mounted, is movable along an X-axis and along a Y-axis, both at right angles to the line of beam 16. As an aid to illustration, various axes are identified herein as X and Y axes, but these are solely to facilitate understanding of the apparatus. Thus, as indicated by arrow 25, holder 24 is movable along an X-axis. It is also movable along a Y-axis as indicated by arrow 26. The fine control of the position at which the beam strikes the sample is obtained by using magnetic fields to align the position of the electron beam 16. Thus, there are a pair of deflecting coils 27 positioned to produce a magnetic field, when energized, to align the beam 16 along the X-axis. There are also similar coils 28 which produce a magnetic field for aligning the beam along the Y-axis.

The angle at which the X-ray beam 18 will be emitted from the sample 17 depends upon the element upon which the beam impacts. Thus, for one element being struck by the electrons, the X-rays emitted therefrom will be in the form of an inverted cone having a first specific central angle; while, for another element, the central angle of the cone will be a second specific angle. The illustrated line 18 from the sample 17 to the reflector 19 is but one line extending from the apex of one of the cones and there are a multitude of similar lines at other positions about that one cone. The reflector 19 is movable with respect to these cones, as indicated by the arrow 29, so that it will pick up and direct to probe 21 X-rays of the cone having a particular central angle. Thus, for a specific setting of the position of reflector 19, it will be known that the probe is receiving X-rays produced by a particular element at the point of impact on sample 17.

The quantity of that element present at the particular point will be roughly indicated by the current flowing between the sample and ground, and can be measured by a sample current detecting means 32. In effect, this detector is nothing more than a refined current measuring apparatus (e.g. meter). A more accurate measurement of the quantity of the element present is obtained by measuring the quantity of X-rays along path 18 by means of the X-ray detectors 20. These detectors take two forms, often simultaneously incorporated in a single probe; namely, (1) a ratemeter and (2) a scaler. The scaler produces a digital output signal in relation to time. The ratemeter produces a voltage signal. Both, of course, have values indicative of the quantity of X- rays received.

An actual spectrometer will have various other components which are inconsequential so far as the explanation of the present invention is concerned. For example, the electron beam 16 will be in an enclosure in which there is a relatively low air pressure maintained so as not to interfere with the movement of the electron beam; various provisions will be made for accelerating the electron beam; etc. Also, in the conventional spectrometer, there are three probes 21. Each probe is associated with a respective reflector 19, individually movable. These are each positioned at different radial positions about the axis of beam 16 and thus pick up various portions of the cones of emitted X-rays. The purpose of using three, rather than only one illustrated, is merely to permit simultaneous examination for different elements at the point of impact of the electron beam. So far as the present invention is concerned, a description of the apparatus in connection with one of these probes and its associated reflector will fully explain the manner in which the invention is employed in connection with each of the two others.

The exact manner in which the holder 24 is movably mounted and traversed is not consequential. The mechanism for doing this includes a lead screw 33 (threaded rod) operatively connected to holder 24 so that a rotation of the lead screw in one direction or the other will move holder 24 in one direction or the other along the X-axis. Similarly, a lead screw 34 is operatively connected so that its rotation will move the holder along the Y-axis. A third lead screw 35 is operatively connected to reflector 19 so that itsrotation will move the reflector to various positions transversely to the various cones of the X-rays to obtain the desired positioning of the reflector to reflect the X-rays in a particular cone from a specific element.

In the present invention an X-axis drive apparatus, generally 36, is connected to lead screw 33. A Y-axis drive apparatus, generally 37, is connected to lead screw 34, and a reflector drive apparatus, generally 38, is connected to lead screw 35. These drives 36, 37, 38 position the respective lead screws in response to input signals on

lines

41, 42 and 43 respectively. Each drive apparatus includes a mechanism (hereinafter described) for producing feedback signals indicative of the then position of the drive. These feedback signals appear on output lines 44-46 respectively.

A beam control apparatus, generally 49, is connected to deflecting coils 28. A similar beam control apparatus, generally 50, is connected to deflecting coils 27. Each of these controls adjusts the current flow through the respective coils so as to obtain the desired positioning of the electron beam 16. The control of this current by

controls

49 and 50 is dictated by a signal on

input lines

51 and 52 respectively. Each control apparatus also includes means for providing a feedback signal indicative of the current control setting. These feedback signals appear on

output lines

53 and 54 respectively. Similarly, there is a-beam current control apparatus, generally 56, operatively connected to cathode to regulate the magnitude of electron beam 16. This magnitude is dictated by an input signal on line 57. The setting of the control is indicated by a feedback signal on output line 58.

Each of the input lines 41, 42, 43, 51, 52, 57 are connected to a control matrix, generally 60, which produces signals to the respective apparatus as dictated by a computer, generally 61. Through line 59, computer 61 dictates what signal and to which apparatus the control matrix 60 shall send a signal. The feedback signals on

lines

44, 45, 46, 53, 54, 58 are sent to a selector matrix, generally 62. The selector matrix also receives a signal from the sample current means 32 over output line 63. It receives a voltage signal from the ratemeter in probe 21 over output line 64. Under the dictation of computer 61, as indicated by line 65, the selector matrix sends the feedback signal from one of these components from which is receives feedback signals to an analogue to digital converter (sometimes called a digital voltmeter) generally 66, as indicated by connecting line 67. The converter changes the analogue feedback signal it receives to a digital signal and sends it to a computer on line 68. The digital signal from the sealer in probe 21 is delivered directly to the computer 61 on line 69. The probe also includes a timer in conjunction with the sealer and the time signal therefrom is sent to the computer 61 on line 70, whereby the computer has the time base against which the scaler digital signal is read.

Lines

68, 69 and 70 are informational inputs for the computer.

As illustrative of each of the lead

screw drive devices

36, 37, 38, and the matrixes connected thereto, FIG. 2 illustrates the structure and operation of the X-axi's drive 36. This drive apparatus is divided into two components one of which (36a) does the driving, and the other of which (36b) provides the feedback signal.

The drive component 36a comprises a reversible synchronous motor 73, the output shaft of which is connected to a brake 74. The motor shaft is also connected to a clutch and then through a two-speed transmission 76 to lead screw 33. The brake is employed to obtain the quick stopping of the output shaft when the motor 73 is deenergized. The clutch 75 is employed to connect and disconnect the motor from the transmission 76. The transmission 76 can be set to obtain rapid rotation or a comparatively slow rotation of lead screw 33 for either a quick traversal of holder 24 or a slow traversal thereof.

The control matrix 60 comprises a plurality of substantially identical control segments, only one of which 60a is illustrated in FIG. 2. The number of such control segments that are employed will depend upon the number of control functions to be achieved. In actual embodiments of the present invention, nine such control segments are used providing a total of 81 input signals to various devices. Not all of these input signals are actually used, however.

The control matrix segment 60a comprises four bistable flip-flops -83, which receive control signals from computer 61 through lines 59a 59d respectively. There is also a clock 89 which receives a signal from the computer over line 59e. Line 91 carries signals from clock 89 to each of the flip-flops and to the computer. The output signals from the flip-flops proceed to decoder 92 over lines 93-96. Decoder 92 has nine output lines 98-106, each leading to an amplifier 107. The nine amplifiers have nine output lines 1 10-1 18 leading to the solenoids a 128a of relays which also include switches 120b 128b actuated by the respective solenoid. Preferably, these are reed relays, but various forms of relays or solid state switches could be employed as an alternative. The input line 41, illustrated in FIG. 1, is actually made up of a number of separate lines (41a 41 f in FIG. 2) corresponding to the number of functions or types of actuations incorporated in the drive apparatus 36. Lines 41a and 41b are connected to switches l20b and 121b respectively to energize the motor for forward or reverse operation respectively. The switches are also connected to one side of the source of alternating current 130, the other side being grounded. Line 410 is connected to switch 122b;. line 41d is connected to switch l23b; line 412 is connected to switch 124b,- and line 41 f is connected to switch 125b. The other side of switches 122b 125b are connected to a direct current source 131. Thus, for example, when switch 122); is closed brake 74 will be energized from source 131; etc.

A signal on line 59a to flip-flop 80 is indicative of the number 1; a signal on line 59b to flip-flop 82 is indicative of the number 2; a signal on line 59c to flip-flop 82 is indicative of the number 4; and a signal on line 5911 to flip-flop 83 is indicative of the number 8. If two or more flip-flops simultaneously receive signals from the computer, their respective numbers are added by decoder 92 to produce a signal on the line that equals the sum of the flip-flop numbers. Thus, for example, if brake 74 were to be energized, coincident signals would be received by flipflops 80 and 81. At the appropriate time clock 89 would be actuated to tell

flipflops

80 and 81 to release their respective signals to decoder 92 and to clear themselves. The simultaneous signals on

lines

93 and 94 would cause decoder 92 to produce an output signal on line 100 indicative of the sum 3. Through the respective amplifier 107, solenoid 122a would be energized to close switch 122b and energize brake 74.

For purposes of simplification, all of these relays have been shown as single acting relays. In some instances, however, they would be of the latching type with two coils, one of which was energized to latch the relay switch closed and the other of which was energized to unlatch the relay and open the switch. The respective coils would be connected to separate outputs on decoder 92 (through respective amplifiers) to be actuated independently when signals were received from the decoder.

Like the control matrix 60, the selector matrix 62 is divided into a number of segments, one of which 62a is illustrated in FIG. 2. Again, there are four outputs 65a 65d to the four flip-flops 139-142 respectively.

A clock 144 receives a signal from the computer over line e and delivers a signal to the flip-flops and to the computer over line 146. Each flip-flop has an output line to decoder 147, the four lines being numbered 148-150 respectively. There are nine output lines -163 from decoder 147 to nine amplifiers 107. In turn the nine amplifiers 107 have nine output lines -173 to the nine relay solenoids a 183a. Each solenoid is part of a relay including switches l75b 183b respectively. One side of each of the switches is connected to line 67. The other side of each of the switches is connected to receive one of the analogue feedback signals from a control apparatus.

In FIG. 2, that portion of the drive apparatus 36 that provides the feedback signal is identified as 36b. This includes a potentiometer 185 having a slider or pick-off 186. Slider 186 is coupled to lead screw 33 so that the slider is moved along the potentiometer resistance in accordance with the rotation of the lead screw. Assume that the lead screw 33 is effective in moving holder 24 through the length D of the lead screw, then slider 186 is coupled so that it moves the full length of. the resistance of potentiometer 185 during the course of the effective operation of the lead screw through the dimension D. Thus, for example, if it takes 270 turns of the lead screw 33 to move the holder 24 through the dimension D, then slider 186 moves one two-hundredseventieth of the length of the resistance of the potentiometer 185 during each rotation of the lead screw. A wire 188 connects one side of the potentiometer resistance to a direct current source of electric power (e.g. 131). The other side of the potentiometer and the source of power are grounded. Thus a voltage will be obtained at slider 186 (in relation to ground), which is indicative of the position of the slider on the potentiometer, and thus indicative of the position of the holder 24 along the lead screw 33.

To obtain even more accurate resolution of the position of the holder along the lead screw, a second potentiometer 190 has a slider 191 which is coupled through the gearing arrangement 192 to the lead screw 33. P0- tentiometer 190 is capable of continuous rotation and the slider 191 thereof is geared to lead screw 33 in a way such that it turns much more rapidly in relation to the rotation of lead screw 33 than is the movement of slider 186 for a given amount of rotation of the lead screw. For example, slider 191 could rotate through two revolutions of the potentiometer resistance for each revolution of lead screw 33. A continuously rotating potentiometer does have a gap in its path of movement, at which gap the slider is not in contact with the potentiometer resistance. To overcome this problem in actual practice, two such potentiometers 190 are ganged together but aligned so that their gaps are offset from each other. Thus it is possible to avoid a loss of signal at the gap. For the purposes of simplifying the illustration, only a single potentiometer 190 is shown in FIG. 2.

Again, wire 188 connects to one side of potentiometer resistance 190 so that a voltage is impressed across the potentiometer. Thus the voltage appearing at line 44b (in relation to ground) is indicative of the position of slider 191 on the resistance. Utilizing this arrangement, an accuracy in one part in four thousand as to the position of lead screw 43 is obtained without having to use gearing connecting the potentiometers to the lead screw which has an accuracy greater than one percent. In an actual embodiment, the potentiometer 185 was a lO-turn potentiometer and was gear connected to lead screw 33.

To rea the position of lead screw 33, the computer first sends out a signal to flip-flop 139. Upon the actuation of clock 144, a signal indicating the number 1 is received by decoder 147. In turn, the decoder sends out a signal on its number 1 line, i.e. line 155. Solenoid 175 is thereby energized to close switch 175b. Over line 67 a voltage is obtained by the converter 66 indicative of the position of the slider 186 on the coarse potentiometer 185. Converter 66 changes this voltage signal into a digital signal and sends it to computer 61 over line 68. Next the computer reads the fine potentiometer 190. To do this, a signal is sent by the computer over line 65b to flip-flop 140. In turn, the decoder 147 sends a signal over lines 156 and 166 to solenoid 176a. This results in a closing of switch 176b. Now a voltage is obtained at line 67 (switch 17512 having opened in the meantime), indicative of the position of the slider 191 on its resistance.

FIG. 3 illustrates the construction and operation of the X-axis beam control apparatus 50 in relation to the computer. The same arrangement would be used for the Y-axis beam control 49, and a similar arrangement for the electron beam current control 56.

The beam control apparatus 50 includes a potentiometer 200 having a slider 20] connected to motor 202 through a gear box 203. A comparable (or actually the same one) gear box 204 connects a slider 205 of potentiometer 206 to motor 202. The resistance of both of the potentiometers are connected to a suitable source of direct current, e.g. source 131, so that a voltage is impressed thereacross. Thus the voltage at the

sliders

201 and 205 will vary, depending upon the position of the slider on the potentiometer resistance.

Slider 201 is connected through an amplifier 210 to the deflection coils 27. Amplifier 210 adjusts the magnitude of the current flow through coils 27 in relation to the input potential of the amplifier as picked off by slider 201. Slider 205 is connected by line 54 to switch 183b of the selector matrix section 62a. Lines 52a and 52b connect the reversible motor 202 to switches 126k and 12712 respectively of control matrix section 60a. Thus motor 202 is energized from source 130 in a forward or reverse direction, depending upon the closing of

switches

126b and 127b. If, for example, slider 201 is to be moved in one direction along its resistance by closing switch 126b, a signal indicative of the number 7 is sent from the computer to the flip-flops (i.e. signals sent out by the computer on

lines

59a, 59b and 590). Upon the clock 89 directing that these signals be transmitted to the decoder 92, signals are sent to the decoder on

lines

93, 94 and 95. In response thereto, the decoder 92 sends out a signal on line 104, through the respective amplifier 107 and through line 116 to solenoid 126a. This closes switch 126b to energize motor 202 for rotation in the desired direction.

In response to the actuation of the motor moving slider 201, a corresponding movement of slider 205 results. Thus, a potential will be obtained on line 54 indicative of the position of

sliders

205 and 201 on their respective resistances (and corresponding to the current flow through coils 27). To read this signal the computer sends out signals to the decoder 147 which sends a signal on its number 9 line to energize relay solenoid 183a. The voltage picked off by slider 205 then is transmitted through closed switch 183b to converter 66. Converter 66 sends a corresponding signal in digital form to computer 61.

Assume that it was desired to see what transition elements were located at a particular area on a sample and then to find all other areas of the sample that were similar in composition over a 2 X 2 millimeter area with a resolution of ten micrometers. The initial area of the sample would have been initially selected by an individual looking at the sample through an optical microscope. This microscope would have a holder identical to 24 so that the coordinate would be the same for both holders when the sample was transferred from one to the other. Assume that the initially selected area had coordinates of X-1999 and Y-2999. The program (in english) to the computer would be substantially as follows:

Store X position of 1999.

Read in the actual X position on X-axis drive 36b.

Match to the X position in store.

If different, move the drive (lead screw 33) fast if the difference is greater than 10 units, or slow if the difference is less than 10 units, until a match is obtained with the X in the store.

Repeat the foregoing for Y position.

Analyze for the various transition elements by moving the reflector 19 to the required position for each and reading in and storing the results from each position as detected by the probe 21.

As to each of these, recall the reflector position for the particular element. Move the reflector to that position. Read the feedback from the reflector drive apparatus. If match is obtained, then read the ratemeter reading from probe 21 and store. Then move the reflector 19 to the position for obtaining a background reading on the same element. Check the feedback signal from the reflector drive apparatus 38 to make sure that the reflector is in the correct position. If match is obtained, read the ratemeter reading from probe 21 and subtract from the ratemeter reading obtained for the element as initially read. Store the difference. Repeat the same procedure for each of the other elements.

Recall the readings for each of the intensities and if any are above a predetermined minimum, store the element and quantity.

Step the holder in the X direction 10 micrometers. Read the feedback to assure that the new position is correct.

Reposition reflector 19 for each of the elements, and take ratemeter readings (as outlined above). Store the readings for only those positions where the element readings match.

Repeat, in a plurality of steps, the X movements of 10 micrometers and make-the same readings at each stop until a total travel of 2 millimeters has been accomplished.

Step the Y-axis drive 37 ten micrometers. Read in the feedback signal from drive 37 to make sure that the right position has been obtained.

Now repeat the stepping of the X-axis movements and take readings at each stop (as previously outlined) until a 2 millimeter travel has been achieved.

Repeat the last two actions until the total coverage over the entire 2 millimeter area (in 10 micrometer increments) has been achieved.

Type out each position in readout 216 where a match was obtained corresponding to the readings of the initially selected position.

Various refinements, not illustrated, can be incorporated into the apparatus. Such as, for example, limit switches on the movement of the holder in relation to the lead screws so that exceeding the desired limit of movement will shut down the apparatus. A further refinement would be to read the actual electron beam current and if it dropped below a given minimum, as for example due to filament burnout, the apparatus would be shut down.

I claim:

1. In an electron microprobe apparatus for use with a source of power for analyzing a sample mounted on a movable holder by producing a secondary emission of X-rays from the sample by impacting an electron beam thereupon and for use with computer means for producing actuating signals and control signals and having an informational input, wherein the apparatus includes a cathode device for producing said electron beam, an X-axis beam control device between the cathode device and the sample for controlling the orientation of the beam along an X-axis transverse thereto, a Y-axis beam control device between the cathode device and the sample for controlling the orientation of the beam along a Y-axis transverse thereto, an X-axis holder control device for controlling the position of the holder along a first axis transverse to the beam, a Y-axis holder control device for controlling the position of the holder along a second axis transverse to the beam, an X-ray detector, and an adjustable device for picking up the secondary emission and separating it into components and directing selected components to said detector,

the combination therewith of:

a plurality of power driven means connected to said devices for controlling the setting of the respective devices and for producing electrical feedback signals in analogue form representative of the contro settings of the devices;

control matrix means connected between the computer means and the power driven means for directing actuating signals from the computer means to the respective power driven means as dictated by control signals from the computer means; an analogue to digital converter having an analogue input and a digital output, said digital output being connected to said informational input of the computer means; selector matrix means connected to said power driven means for receiving said feedback signals, to said computer means for receiving control signals and to the input of said converter for selecting a feedback signal as dictated by a control signal from V the computer means and delivering said selected signal to said converter so that said selected signal is delivered to said computer means by said converter in digital form, said matrix means comprising a plurality of switches each having an operating element, a plurality of electric circuits, each circuit connecting a respective switch and a respective device to the source of power, said switches being controllable between a first state at which each switch energizes the respective device through the respective electric circuit and a second state at which said respective device is deenergized, and means operatively connecting said each of said switches to said computer means to actuate the operating element of a respective switch as dictated by a control signal from the computer means; a beam control device connected to said cathode device for controlling the emission of electrons from the cathode device and one of said power driven means connected to said emission control device to control said emission; and a sample current measuring device for producing an output signal indicative of the current flow from the sample to ground, said current measuring device being connected to said selector matrix means; said X-ray detector including a ratemeter and a scaler each producing output signals, said ratemeter being connected to said selector matrix means to deliver its output signal thereto, said ratemeter being connected to said computer means to deliver its output signal thereto; each of the X-axis holder control device and the Y- axis holder control device including a rotatable threaded shaft which rotates a given number of turns to traverse the holder through its maximum range of movement; and each of the power driven means connected to said holder control devices comprising: an electric motor connected to the control matrix means to be operated in accordance with signals from the control matrix,

means operatively connecting said motor to said shaft for driving the shaft in accordance with the operation of the motor,

a first potentiometer having a contact movable within a given range on the potentiometer, said contact being connected to said selector matrix means, means operatively connecting said movable contact and said shaft for moving the movable contact within said range on said potentiometer in response to said shaft rotating said given number of turns,

second potentiometer means having contact means movable repetitively through a given range on the second potentiometer, said contact means being connected to said selector matrix means,

gearing means operatively connecting said movable contact means of the second potentiometer means and said shaft for moving said contact means through a greater portion of its range in response to a given rotation of the shaft when the portion of the range of the first potentiometer traversed by the contact thereof in response to the same given rotation of the shaft, and means connecting said potentiometer and potentiometer means to said source of power for imposing a voltage across the potentiometer and the potentiometer means, whereby voltages are obtained at said contact and said contact means which together are indicative of the holder position along the respective axis. 2. In the combination as set forth in claim 1, wherein at least one of said control devices comprises a control potentiometer having a movable slider; and

said power driven means connected to said one control device comprises:

an electric motor connected to said control matrix to be operated in accordance with signals from the control matrix, means connecting said motor to said slider for positioning said slider in response to operation of the motor; a feedback potentiometer having a movable pickoff member, said movable pickoff member being connected to said selector matrix,

means connecting said motor and said pickoff member for positioning the pickoff member in response to the operation of the motor, and means connecting said feedback potentiometer to said source of power for imposing a voltage across the feedback potentiometer, whereby a voltage is obtained at said pickoff member indicative of the position of said slider. 3. In a microprobe apparatus for analyzing a sample mounted on a movable holder by producing a secondary emission from the sample by impacting a primary beam thereupon and for use with computer means for producing actuating signals and control signals and having an informational input, wherein the apparatus 5 includes an emitter device for producing said primary beam, an X-axis beam control device between the emitter device and the sample for controlling the orientation of the beam along an X-axis transverse thereto, a Y-axis beam control device between the emitter device and the sample for controlling the orientation of the beam along a Y-axis transverse thereto, an X-axis holder control device for controlling the position of the holder along a first axis transverse to the beam, a Y-axis holder control device for controlling the position of the holder along a second axis transverse to the beam, a secondary emission detector, and an adjustable device for picking up the secondary emission and separating it into components and directing selected components to said detector,

the combination therewith of:

a plurality of power driven means connected to said devices for controlling the respective devices and for producing analogue feedback signals representative of the control settings of the devices;

control matrix means connected between the computer means and the power driven means for directing actuating signals from the computer means 11 Y to the respective power driven means as dictated by control signals from the computer means;

an analogue to digital converter. having an analogue input and a digital output, said digital output being connected to said informational input of the computer means; and

selector matrix means connected to said power driven means for receiving said feedback signals, to said computer means for receiving control signals and to the input of said converter for selecting a feedback signal as dictated by a control signal from the computer means and delivering said selected signal to said converter so that said selected signal is delivered to said computer means by said converter in digital form;

each of the X-axis holder control device and the Y- axis holder control device includes a rotatable threaded shaft which rotates a given number of turns to traverse the holder through its maximum range of movement; and

each of the power driven means connected to said holder control devices comprises:

an electric motor connected to the control matrix means to be operated in accordance with signals from the control matrix;

means operatively connecting said motor to said shaft for driving the shaft in accordance with the operation of the motor;

a first potentiometer having a contact movable within a given range on the potentiometer, said contact being connected to said selector matrix means,

means operatively connecting said movable contact and said shaft for moving the movable contact within said range on said potentiometer in response to said shaft rotating said given number of turns,

gearing means operatively connecting, said movable contact means of the second potentiometer means and said shaft for moving said contact means through a greater portion of its range in response to a given rotation of the shaft than the portion of the range of the first potentiometer traversed by the contact thereof in response to the same given rotation of the shaft, and

means connecting said potentiometer and potentiometer means to a source of power for imposing a voltage across the potentiometer and the potentiometer means,

whereby voltages are obtained at said contact and said contact means which together are'indicative of the holder position along the respective axis.

4. In the combination as set forth in claim 3, wherein at least one of said control devices comprises a control potentiometer having a movable slider; and said power driven means connected to said one control device comprises:

an electric motor connected to said control matrix to be operated in accordance with signals from the control matrix,

means connecting said motor to said slider for positioning said slider in response to operation of the motor,

a feedback potentiometer having a movable pickoff member, said movable pickofi member being connected to said selector matrix,

means connecting said motor and said pickoff member for positioning the pickoff member in response to the operation of the motor, and

means connecting said feedback potentiometer to said source of power for imposing a voltage across the feedback potentiometer,

whereby a voltage is obtained at said pickoff member indicative of the position of said slider.

5. In the combination as set forth in claim 4, wherein said matrix means comprises a plurality of switches each having an operating element, a plurality of electric circuits, each circuit connecting a respective switch and a respective device to the source of power, said switches being controllable between a first state at which each switch energizes the respective device through the respective electric circuit and a second state at which said respective device is deenergized, and means operatively connecting said each of said switches to said computer means to actuate the operating element of a respective switch as dictated by a control signal from the computer means.

6. In the combination as set forth in claim 4, wherein said apparatus is an electron microprobe, with said primary beam being an electron beam, said apparatus has a cathode for emitting said beam, said apparatus includes a beam control device connected to said cathode for controlling the emission of electrons from the cathode and one of said power driven means connected to said emission control device to control said emission, said apparatus has a sample current measuring device for producing an output signal indicative of the current flow from the sample to ground, said current measuring device being connected to said selector matrix means, said secondary emission is X-rays, said secondary emission detector is an X-ray detector including a ratemeter and a scaler each producing output signals, said ratemeter being connected to said selector matrix means to deliver its output signal thereto, said ratemeter being connected to said computer means to deliver its output signal thereto.

7. In the combination as set forth in claim 3, wherein said apparatus is an electron microprobe, with said primary beam being an electron beam, said apparatus has a cathode for emitting said beam, said apparatus includes a beam control device connected to said cathode for controlling the emission of electrons from the cathode and one of said power driven means connected to said emission control device to control said emission, said apparatus has a sample current measuring device for producing an output signal indicative of the current flow from the sample to ground, said current measuring device being connected to said selector matrix means, said secondary emission is X-rays, said secondary emission detector is an X-ray detector including a ratemeter and a scaler each producing output signals, said ratemeter being connected to said selector matrix means to deliver its output signal thereto, said ratemeter being connected to said computer means to deliver its output signal thereto.

Claims

1. In an electron microprobe apparatus for use with a source of power for analyzing a sample mounted on a movable holder by producing a secondary emission of X-rays from the sample by impacting an electron beam thereupon and for use with computer means for producing actuating signals and control signals and having an informational input, wherein the apparatus includes a cathode device for producing said electron beam, an X-axis beam control device between the cathode device and the sample for controlling the orientation of the beam along an X-axis transverse thereto, a Y-axis beam control device between the cathode device and the sample for controlling the orientation of the beam along a Y-axis transverse thereto, an X-axis holder control device for controlling the position of the holder along a first axis transverse to the beam, a Y-axis holder control device for controlling the position of the holder along a second axis transverse to the beam, an X-ray detector, and an adjustable device for picking up the secondary emission and separating it into components and directing selected components to said detector, the combination therewith of: a plurality of power driven means connected to said devices for controlling the setting of the respective devices and for producing electrical feedback signals in analogue form representative of the control settings of the devices; control matrix means connected between the computer means and the power driven means for directing actuating signals from the computer means to the respective power driven means as dictated by control signals from the computer means; an analogue to digital converter having an analogue input and a digital output, said digital output being connected to said informational input of the computer means; selector matrix means connected to said power driven means for receiving said feedback signals, to said computer means for receiving control signals and to the input of said converter for selecting a feedback signal as dictated by a control signal from the computer means and delivering said selected signal to said converter so that said selected signal is delivered to said computer means by said converter in digital form, said matrix means comprising a plurality of switches each having an operating element, a plurality of electric circuits, each circuit connecting a respective switch and a respective device to the source of power, said switches being controllable between a first state at which each switch energizes the respective device through the respective electric circuit and a second state at which said respective device is deenergized, and means operatively connecting said each of said switches to said computer means to actuate the operating element of a respective switch as dictated by a control signal from the computer means; a beam control device connected to said cathode device for controlling the emission of electrons from the cathode device and one of said power driven means connected to said emission control device to control said emission; and a sample current measuring device for producing an output signal indicative of the current flow from the sample to ground, said current measuring device being connected to said selector matrix means; said X-ray detector including a ratemeter and a scaler each producing output signals, said ratemeter being connected to said selector matrix means to deliver its output signal thereto, said ratemeter being connected to said computer means to deliver its output signal thereto; each of the X-axis holder control device and the Y-axis holder control device including a rotatable threaded shaft which rotates a given number of turns to traverse the holder through its maximum range of movement; and each of the power driven means connected to said holder control devices comprising: an electric motor connected to the control matrix means to be operated in accordance with signals from the control matrix, means operatively connecting said motor to said shaft for driving the shaft in accordance with the operation of the motor, a first potentiometer having a contact movable within a given range on the potentiometer, said contact being connected to said selector matrix means, means operatively connecting said movable contact and said shaft for moving the movable contact within said range on said potentiometer in response to said shaft rotating said given number of turns, second potentiometer means having contact means movable repetitively through a given range on the second potentiometer, said contact means being connected to said selector matrix means, gearing means operatively connecting said movable contact means of the second potentiometer means and said shaft for moving said contact means through a greater portion of its range in response to a given rotation of the shaft when the portion of the range of the first potentiometer traversed by the contact thereof in response to the same given rotation of the shaft, and means connecting said potentiometer and potentiometer means to said source of power for imposing a voltage across the potentiometer and the potentiometer means, whereby voltages are obtained at said contact and said contact means which together are indicative of the holder position along the respective axis.

2. In the combination as set forth in claim 1, wherein at least one of said control devices comprises a control potentiometer having a movable slider; and said power driven means connected to said one control device comprises: an electric motor connected to said control matrix to be operated in accordance with signals from the control matrix, means connecting said motor to said slider for positioning said slider in response to operation of the motor; a feedback potentiometer having a movable pickoff member, said movable pickoff member being connected to said selector matrix, means connecting said motor and said pickoff member for positioning the pickoff member in response to the operation of the motor, and means connecting said feedback potentiometer to said source of power for imposing a voltage across the feedback potentiometer, whereby a voltage is obtained at said pickoff member indicative of the position of said slider.

3. In a microprobe apparatus for analyzing a sample mounted on a movable holder by producing a secondary emission from the sample by impacting a primary beam thereupon and for use with computer means for producing actuating signals and control signals and having an informational input, wherein the apparatus includes an emitter device for producing said primary beam, an X-axis beam control device between the emitter device and the sample for controlling the orientation of the beam along an X-axis transverse thereto, a Y-axis beam control device between the emitter device and the sample for controlling the orientation of the beam along a Y-axis transverse thereto, an X-axis holder control device for controlling the position of the holder along a first axis transverse to the beam, a Y-axis holder control device for controlling the position of the holder along a second axis transverse to the beam, a secondary emission detector, and an adjustable device for picking up the secondary emission and separating it into components and directing selected components to said Detector, the combination therewith of: a plurality of power driven means connected to said devices for controlling the respective devices and for producing analogue feedback signals representative of the control settings of the devices; control matrix means connected between the computer means and the power driven means for directing actuating signals from the computer means to the respective power driven means as dictated by control signals from the computer means; an analogue to digital converter having an analogue input and a digital output, said digital output being connected to said informational input of the computer means; and selector matrix means connected to said power driven means for receiving said feedback signals, to said computer means for receiving control signals and to the input of said converter for selecting a feedback signal as dictated by a control signal from the computer means and delivering said selected signal to said converter so that said selected signal is delivered to said computer means by said converter in digital form; each of the X-axis holder control device and the Y-axis holder control device includes a rotatable threaded shaft which rotates a given number of turns to traverse the holder through its maximum range of movement; and each of the power driven means connected to said holder control devices comprises: an electric motor connected to the control matrix means to be operated in accordance with signals from the control matrix; means operatively connecting said motor to said shaft for driving the shaft in accordance with the operation of the motor; a first potentiometer having a contact movable within a given range on the potentiometer, said contact being connected to said selector matrix means, means operatively connecting said movable contact and said shaft for moving the movable contact within said range on said potentiometer in response to said shaft rotating said given number of turns, second potentiometer means having contact means movable repetitively through a given range on the second potentiometer, said contact means being connected to said selector matrix means, gearing means operatively connecting said movable contact means of the second potentiometer means and said shaft for moving said contact means through a greater portion of its range in response to a given rotation of the shaft than the portion of the range of the first potentiometer traversed by the contact thereof in response to the same given rotation of the shaft, and means connecting said potentiometer and potentiometer means to a source of power for imposing a voltage across the potentiometer and the potentiometer means, whereby voltages are obtained at said contact and said contact means which together are indicative of the holder position along the respective axis.

4. In the combination as set forth in claim 3, wherein at least one of said control devices comprises a control potentiometer having a movable slider; and said power driven means connected to said one control device comprises: an electric motor connected to said control matrix to be operated in accordance with signals from the control matrix, means connecting said motor to said slider for positioning said slider in response to operation of the motor, a feedback potentiometer having a movable pickoff member, said movable pickoff member being connected to said selector matrix, means connecting said motor and said pickoff member for positioning the pickoff member in response to the operation of the motor, and means connecting said feedback potentiometer to said source of power for imposing a voltage across the feedback potentiometer, whereby a voltage is obtained at said pickoff member indicative of the position of said slider.