US3531299A - Process of washing and filling containers with beverage using inert gas - Google Patents
Process of washing and filling containers with beverage using inert gas Download PDFInfo
- Publication number
- US3531299A US3531299A US732400A US3531299DA US3531299A US 3531299 A US3531299 A US 3531299A US 732400 A US732400 A US 732400A US 3531299D A US3531299D A US 3531299DA US 3531299 A US3531299 A US 3531299A
- Authority
- US
- United States
- Prior art keywords
- beverage
- container
- bottle
- filling
- washing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C7/00—Concurrent cleaning, filling, and closing of bottles; Processes or devices for at least two of these operations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B31/00—Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B31/00—Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
- B65B31/04—Evacuating, pressurising or gasifying filled containers or wrappers by means of nozzles through which air or other gas, e.g. an inert gas, is withdrawn or supplied
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/06—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus using counterpressure, i.e. filling while the container is under pressure
- B67C3/10—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus using counterpressure, i.e. filling while the container is under pressure preliminary filling with inert gases, e.g. carbon dioxide
Definitions
- a process for filling a container with a beverage which process comprises the steps of washing the container, introducing nitrogen into the container simultaneously with the washing water used in said washing step, and displacing the nitrogen by introducing the beverage into the container.
- the bottle is washed with nitrogen immediately preceding the filling.
- the container is preferably a bottle or can while the beverage is preferably beer.
- the nitrogen gas may be introduced into the container in various ways, for example, centrally through a spraying nozzle and surrounded by an annular stream of washing water delivered by the same nozzle.
- the nitrogen gas is held, according to a following feature of the invention, at an overpressure in the bottle or the can, and driven out by the beverage pouring in during the filling.
- the oxygen which might be dissolved in the beer is liberated by the interaction between the beer pouring in in a thin film along the bottle wall, according to a known process, and then driven out together with the nitrogen gas.
- the beverage is allowed to flow from a filling container in the filling machine to the lowerpositioned bottle or can by gravity.
- nitrogen gas is present over the beverage in the filling container.
- the beverage may be pressed from the container by the pressure of the nitrogen gas, so that the beverage neither in the storage containers, nor during the storing up in the bottles or the cans has the opportunity to pick up oxygen.
- the nitrogen gas driven away during the filling may be removed in various manners.
- the nitrogen gas is forced from the bottle or the can to be filled to the gas supply container of the filling machine during the filling step.
- a bottle filled in accordance with the invention may be closed simply or after a foam generation in the bottle neck in which latter event the beer is stored with an extremely low oxygen content.
- FIGS. 1 and 2 illustrate apparatus which may be used for the introduction of wash Water and an inert gas simultaneously into each bottle or container for the beverage.
- FIG. 1 shows two rows of bottles 1 which are placed upside down over respective spraying nozzles 2 of a bottle-washing machine during the bottle-washing operation.
- the side view of FIG. 2 further illustrates each bottle which has been positioned above a respective one of the spray nozzles 2.
- FIG. 3 is a vertical sectional view of a spraying nozzle 2 together with a portion of a bottle 1 which is placed upside down above the nozzle during the washing operation.
- Each nozzle is provided with a central opening 11 for introducing nitrogen gas into the bottle 1 from a source of nitrogen gas designated by the reference numeral 8.
- the spraying nozzle 11 is surrounded by an annular spraying nozzle 9 by means of which the wash Water which is supplied to the nozzle at 10 may be sprayed into the interior of the bottle 1.
- the wash water is introduced into the conduits 4, each of which fits a plurality of nozzles 2.
- a single conduit 6 Disposed between the conduits 4 is a single conduit 6 which supplies nitrogen gas to both of the rows of spraying nozzles, the nitrogen gas being 3 supplied from the conduit 6 to the individual nozzles 2 by means of flexible tubes 7.
- each bottle is thoroughly washed by the wash water entering into the inverted bottle from the nozzle 2, and at the same time is filled with a quantity of nitrogen gas. Any oxygen remaining in the bottle is substantially entirely removed from the bottle during this process.
- the bottle is removed from a position directly above the nozzle, or when the supply of wash water is cut 01?, the Wash water remaining in the bottle runs out by gravity, but the nitrogen stays inside because of its having a lower specific gravity than the surrounding air.
- the bottle is inverted to an upright position and filled with the beverage which displaces the nitrogen then occupying the bottle.
- this filling operation takes place in a nitrogen atmosphere, so that the beverage does not in any way come into contact with oxygen during the filling operation.
- the process of this invention is not limited to the filling of; containers such as bottles or cans with beer, but may also be applied to the filling of containers with other beverages whether or not containing carbon dioxide and whether or not containing alcohol.
- a process for filling a container with a beverage the filling operation being carried out in an atmosphere of nitrogen gas to prevent contact of the beverage with oxygen during the filling operation.
- a process for filling a container with a beverage which comprises the steps of,
Description
Sept. 29, 1970 BENJAMINS 3,531,299-
PROCESS OF WASHING'AND FILLING CONTAINERS WITH BEVERAGE USING INERT GAS Filed May 27, 1968 WASH WATER FZTROGEN GAS fi l-Z 1 25 7 i Mi WK NITROGEN GAS l A INVENTOR WASH WATER I 1O LUCAS BENJAM/NS BY vamkcgwb H18 nrrmwer United States Patent Office 3,531,299 Patented Sept. 29, 1970 3,531,299 PROCESS OF WASHING AND FILLING CON- TAINERS WITH BEVERAGE USING INERT GAS Lucas Benjamins, Clairionlaan 9, Santpoort, Netherlands Continuation-impart of application Ser. No. 500,154, Oct. 21, 1965. This application May 27, 1968, Ser. No. 732,400 Claims priority, application Netherlands, Jan. 5, 1965, 6500035 Int. Cl. A23b 1/14 US. Cl. 99-189 2 Claims ABSTRACT OF THE DISCLOSURE A process for filling a bottle or can with a beverage, particularly beer, including the step of washing the container, introducing nitrogen gas into the container simultaneously with washing water used in the washing step, and displacing the nitrogen by introducing the beverage into the container.
This application is a continuation-in-part of United States application Ser. No. 500,154, filed Oct. 21, 1965.
BACKGROUND OF THE INVENTION In a known process for filling beverage into containers, the air in the container is evacuated and thereafter nitrogen gas is introduced into the container. Alternatively, the air may be flushed out of the container by rinsing out the container with nitrogen gas. These known processes are complicated, and the nitrogen gas introduced into the container is easily contaminated by air left behind in the container or by air which is drawn into the container by the nitrogen flow thereinto.
In processes where the container is rinsed with nitrogen to remove the air, a relatively long rinsing time is necessary and a large quantity of nitrogen gas is required to fill the container with nitrogen with a purity of at least 98%. In this connection, it should be noted that when the container is filled with pure nitrogen, any oxygen which may be dissolved in the beverage is withdrawn from the beverage; in contrast, when filling with impure nitrogen, the impure nitrogen gas only prevents air from entering the container during the introduction of the beverage, but does not affect the oxygen dissolved in the beverage. In the known processes, it is not possible to introduce pure nitrogen into the container during the short time interval which exists in the mechanical bottling processes between the washing of the container and filling with the beverage.
It is an object of the invention to remove the disadvantages of the known method for filling bottles or cans with a beverage.
SUMMARY OF THE INVENTION According to the present invention, there is provided a process for filling a container with a beverage, which process comprises the steps of washing the container, introducing nitrogen into the container simultaneously with the washing water used in said washing step, and displacing the nitrogen by introducing the beverage into the container.
In this manner, the free air present in the bottle is driven out and also the oxygen dissolved in the washing water is liberated by the interaction with the nitrogen gas and then driven out so that the bottle after the washing is filled with nitrogen gas and possibly minute amounts of wash water with a very low oxygen percentage.
According to another feature of the invention, the bottle is washed with nitrogen immediately preceding the filling. The container is preferably a bottle or can while the beverage is preferably beer. The nitrogen gas may be introduced into the container in various ways, for example, centrally through a spraying nozzle and surrounded by an annular stream of washing water delivered by the same nozzle. Preferably, the nitrogen gas is held, according to a following feature of the invention, at an overpressure in the bottle or the can, and driven out by the beverage pouring in during the filling. As a result, the oxygen which might be dissolved in the beer is liberated by the interaction between the beer pouring in in a thin film along the bottle wall, according to a known process, and then driven out together with the nitrogen gas.
According to a known process for filling bottles or cans with beverages, the beverage is allowed to flow from a filling container in the filling machine to the lowerpositioned bottle or can by gravity.
According to a feature of the invention, only, or substantially only, nitrogen gas is present over the beverage in the filling container. The beverage may be pressed from the container by the pressure of the nitrogen gas, so that the beverage neither in the storage containers, nor during the storing up in the bottles or the cans has the opportunity to pick up oxygen. The nitrogen gas driven away during the filling may be removed in various manners.
According to another feature of the invention, the nitrogen gas is forced from the bottle or the can to be filled to the gas supply container of the filling machine during the filling step.
A bottle filled in accordance with the invention may be closed simply or after a foam generation in the bottle neck in which latter event the beer is stored with an extremely low oxygen content.
BRIEF DESCRIPTION OF THE DRAWING DETAILED DESCRIPTION OF THE INVENTION FIGS. 1 and 2 illustrate apparatus which may be used for the introduction of wash Water and an inert gas simultaneously into each bottle or container for the beverage.
' It should be understood that the gas which is to be used must be one which contains substantially no free oxygen, and preferably the gas used is nitrogen. FIG. 1 shows two rows of bottles 1 which are placed upside down over respective spraying nozzles 2 of a bottle-washing machine during the bottle-washing operation. The side view of FIG. 2 further illustrates each bottle which has been positioned above a respective one of the spray nozzles 2.
FIG. 3 is a vertical sectional view of a spraying nozzle 2 together with a portion of a bottle 1 which is placed upside down above the nozzle during the washing operation. Each nozzle is provided with a central opening 11 for introducing nitrogen gas into the bottle 1 from a source of nitrogen gas designated by the reference numeral 8. The spraying nozzle 11 is surrounded by an annular spraying nozzle 9 by means of which the wash Water which is supplied to the nozzle at 10 may be sprayed into the interior of the bottle 1.
For the arrangement shown in FIG. 1, the wash water is introduced into the conduits 4, each of which fits a plurality of nozzles 2. Disposed between the conduits 4 is a single conduit 6 which supplies nitrogen gas to both of the rows of spraying nozzles, the nitrogen gas being 3 supplied from the conduit 6 to the individual nozzles 2 by means of flexible tubes 7.
During the washing operation, each bottle is thoroughly washed by the wash water entering into the inverted bottle from the nozzle 2, and at the same time is filled with a quantity of nitrogen gas. Any oxygen remaining in the bottle is substantially entirely removed from the bottle during this process. When the bottle is removed from a position directly above the nozzle, or when the supply of wash water is cut 01?, the Wash water remaining in the bottle runs out by gravity, but the nitrogen stays inside because of its having a lower specific gravity than the surrounding air. Subsequently, the bottle is inverted to an upright position and filled with the beverage which displaces the nitrogen then occupying the bottle. Preferably, this filling operation takes place in a nitrogen atmosphere, so that the beverage does not in any way come into contact with oxygen during the filling operation.
The process of this invention is not limited to the filling of; containers such as bottles or cans with beer, but may also be applied to the filling of containers with other beverages whether or not containing carbon dioxide and whether or not containing alcohol.
What I claim is:
1. A process for filling a container with a beverage the filling operation being carried out in an atmosphere of nitrogen gas to prevent contact of the beverage with oxygen during the filling operation.
2. A process for filling a container with a beverage which comprises the steps of,
thoroughly washing the container with wash water introduced in the form of an annular stream,
introducing into the container simultaneously with the wash water, and while said container is inverted, nitrogen gas, said nitrogen gas being introduced as a jet internally of the annular stream of wash water,
and while said container is positioned upright introducing the beverage into the container to thereby fill the container and concurrently displace the nitrogen gas.
References Cited UNITED STATES PATENTS 490,524 1/1893 Werner 99-49 X 1,361,498 12/1920 Ruif. 1,608,634 11/1926 Taylor 2179 2,424,049 7/1947 Parker et al 99l82 X 2,897,082 7/1959 Kaiser 99-482 X 2,993,246 7/1961 Haloski et al. 2179 3,088,831 5/1963 Fauth et al. 99-49 X 2,771,645 11/1956 Martin 21-80 2,973,267 2/1961 Keller et a1 99-49 NORMAN YUDKOFF, Primary Examiner F. E. DRUMMOND, Assistant Examiner US. 01. X.R. 2149; 99 2s; 134 22; 141-4, 5
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL6500035A NL6500035A (en) | 1965-01-05 | 1965-01-05 |
Publications (1)
Publication Number | Publication Date |
---|---|
US3531299A true US3531299A (en) | 1970-09-29 |
Family
ID=19792036
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US732400A Expired - Lifetime US3531299A (en) | 1965-01-05 | 1968-05-27 | Process of washing and filling containers with beverage using inert gas |
Country Status (6)
Country | Link |
---|---|
US (1) | US3531299A (en) |
DE (1) | DE1482608C3 (en) |
DK (1) | DK117616B (en) |
ES (1) | ES318213A1 (en) |
GB (1) | GB1096875A (en) |
NL (1) | NL6500035A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6231907B1 (en) * | 1996-03-26 | 2001-05-15 | Pokka Corporation | Method for producing high-quality drinks filled in containers |
US6328928B1 (en) * | 1997-01-07 | 2001-12-11 | Gea Finnah Gmbh | Method and for preparing container for filling, and method of filling container |
US6401730B1 (en) * | 2001-01-17 | 2002-06-11 | Julius Z. Knapp | Container wash system |
US6544473B1 (en) * | 1998-02-19 | 2003-04-08 | Shintaku Kogyo Co., Ltd | Method and apparatus for performing sterilizing treatment on plastic container |
CN102300777A (en) * | 2009-01-30 | 2011-12-28 | 大日本印刷株式会社 | Content filling method, content filling system, and content-containing bottle |
CN102917954A (en) * | 2010-06-07 | 2013-02-06 | 大日本印刷株式会社 | Filling method, filling system and bottle |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE8604295U1 (en) * | 1986-02-18 | 1986-05-15 | Erich Lacher Uhrenfabrik GmbH & Co KG, 7530 Pforzheim | Wrist watch |
EP0447104A1 (en) * | 1990-03-12 | 1991-09-18 | The BOC Group plc | Dissolving a gas in a liquid |
EP0447103A1 (en) * | 1990-03-12 | 1991-09-18 | The BOC Group plc | Dissolving gas in a liquid |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US490524A (en) * | 1893-01-24 | Method of and apparatus for the manufacture and filling of liqufds | ||
US1361498A (en) * | 1916-02-25 | 1920-12-07 | William J Ruff | Method for preserving carbonated beverages |
US1608634A (en) * | 1925-04-24 | 1926-11-30 | Borden Co | Apparatus for sterilizing and drying containers |
US2424049A (en) * | 1941-07-16 | 1947-07-15 | Paul W Bonewitz | Method of cleaning containers |
US2771645A (en) * | 1950-12-04 | 1956-11-27 | Dole Eng Co James | Apparatus for sterilizing food containers |
US2897082A (en) * | 1955-03-11 | 1959-07-28 | Kaiser Bruno | Method for filling containers with carbon - dioxide containing beverages |
US2973267A (en) * | 1957-11-14 | 1961-02-28 | Bruno Kaiser Dr | Method and device for sterile racking hot beverages containing carbon dioxide, especially beer |
US2993246A (en) * | 1957-09-18 | 1961-07-25 | Vacuum Can Company | Spray sterilizer |
US3088831A (en) * | 1960-08-25 | 1963-05-07 | Crown Cork & Seal Co | Air free packaging |
-
1965
- 1965-01-05 NL NL6500035A patent/NL6500035A/xx unknown
- 1965-06-15 GB GB25172/65A patent/GB1096875A/en not_active Expired
- 1965-08-31 DE DE1482608A patent/DE1482608C3/en not_active Expired
- 1965-09-13 DK DK467665AA patent/DK117616B/en unknown
- 1965-09-25 ES ES0318213A patent/ES318213A1/en not_active Expired
-
1968
- 1968-05-27 US US732400A patent/US3531299A/en not_active Expired - Lifetime
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US490524A (en) * | 1893-01-24 | Method of and apparatus for the manufacture and filling of liqufds | ||
US1361498A (en) * | 1916-02-25 | 1920-12-07 | William J Ruff | Method for preserving carbonated beverages |
US1608634A (en) * | 1925-04-24 | 1926-11-30 | Borden Co | Apparatus for sterilizing and drying containers |
US2424049A (en) * | 1941-07-16 | 1947-07-15 | Paul W Bonewitz | Method of cleaning containers |
US2771645A (en) * | 1950-12-04 | 1956-11-27 | Dole Eng Co James | Apparatus for sterilizing food containers |
US2897082A (en) * | 1955-03-11 | 1959-07-28 | Kaiser Bruno | Method for filling containers with carbon - dioxide containing beverages |
US2993246A (en) * | 1957-09-18 | 1961-07-25 | Vacuum Can Company | Spray sterilizer |
US2973267A (en) * | 1957-11-14 | 1961-02-28 | Bruno Kaiser Dr | Method and device for sterile racking hot beverages containing carbon dioxide, especially beer |
US3088831A (en) * | 1960-08-25 | 1963-05-07 | Crown Cork & Seal Co | Air free packaging |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6231907B1 (en) * | 1996-03-26 | 2001-05-15 | Pokka Corporation | Method for producing high-quality drinks filled in containers |
US6328928B1 (en) * | 1997-01-07 | 2001-12-11 | Gea Finnah Gmbh | Method and for preparing container for filling, and method of filling container |
US6544473B1 (en) * | 1998-02-19 | 2003-04-08 | Shintaku Kogyo Co., Ltd | Method and apparatus for performing sterilizing treatment on plastic container |
US6401730B1 (en) * | 2001-01-17 | 2002-06-11 | Julius Z. Knapp | Container wash system |
CN102300777A (en) * | 2009-01-30 | 2011-12-28 | 大日本印刷株式会社 | Content filling method, content filling system, and content-containing bottle |
CN102300777B (en) * | 2009-01-30 | 2015-01-14 | 大日本印刷株式会社 | Content filling method and content filling system |
CN102917954A (en) * | 2010-06-07 | 2013-02-06 | 大日本印刷株式会社 | Filling method, filling system and bottle |
Also Published As
Publication number | Publication date |
---|---|
DE1482608A1 (en) | 1969-04-03 |
NL6500035A (en) | 1965-08-25 |
DE1482608C3 (en) | 1975-09-25 |
GB1096875A (en) | 1967-12-29 |
ES318213A1 (en) | 1966-04-16 |
DK117616B (en) | 1970-05-11 |
DE1482608B2 (en) | 1974-07-18 |
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