US3521326A - Powder metallurgy press apparatus - Google Patents

Powder metallurgy press apparatus Download PDF

Info

Publication number
US3521326A
US3521326A US719414A US3521326DA US3521326A US 3521326 A US3521326 A US 3521326A US 719414 A US719414 A US 719414A US 3521326D A US3521326D A US 3521326DA US 3521326 A US3521326 A US 3521326A
Authority
US
United States
Prior art keywords
powder
die
housing
temperature
powder metallurgy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US719414A
Inventor
Richard E Rice
George Warren Webb
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Comstock and Wescott Inc
Original Assignee
Comstock and Wescott Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US633781A external-priority patent/US3386821A/en
Application filed by Comstock and Wescott Inc filed Critical Comstock and Wescott Inc
Application granted granted Critical
Publication of US3521326A publication Critical patent/US3521326A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B30PRESSES
    • B30BPRESSES IN GENERAL
    • B30B11/00Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
    • B30B11/02Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses using a ram exerting pressure on the material in a moulding space
    • B30B11/027Particular press methods or systems
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously

Definitions

  • Objects of the invention are to provide apparatus which operates continuously, which makes complete articles with a single piece of equipment, which requires relatively low temperatures and short times, which requires no sintering operation of the conventional type, which requires relatively very small floor area, which eliminates in-process inventories of partially completed parts, which produces high densities with relatively low-pressure presses, which permits the use of the lowest priced powders, and which results in improved overall manufacturing economy.
  • the iron powder is compressed to form a compacted article which is then quenched, characterized in that the powder is compressed while at a temperature of the order of 1100 F. to 1300 F. and the article is quenched quickly while it retains the metastable quality existing at said temperature, whereby strong articles of high density may be produced quickly with only one pressing operation and with inexpensive powder which does not contain carbon.
  • the aforesaid temperature is approximately 1200 F.
  • the die in which the powder is compressed should be pre- 3,521,326 Patented Jul 21, 1970 heated to the aforesaid temperature. While the powder may be heated in the die it is preferably preheated to the aforesaid temperature before introduction into the die.
  • the powder may be poured into the die or it may J be precompacted to form a briquette.
  • a special feature of the invention resides in the timing of three critical operations of the method, carried out in sequence, namely heating the powder, its compaction, and its cooling.
  • the invention involves the discovery that with ferrous metal composed of powder particles which will pass through a 20 mesh sieve and wtihin the powder particles a crystal size which is customarily referred to as fine grain, the superior mechanical properties which are associated with fine grain size can be preserved to a worth-while degree through the hot pressing operation in spite of the fact that the pressing temperature is in the range ordinarily used for annealing the ferrous metal.
  • the compacted articles By pressing within the aforesaid temperature range the compacted articles have very superior qualities, such as fine grain, high density and exceptional strength. Quick quenching preserves the metastable quality existing at the pressing temperature and prevents the fine metal crystals from growing.
  • the apparatus comprises a die, a closed housing surrounding the die, the housing having an inlet through which the die may be charged with powder, means for compacting the powder in the die to form said compact, the housing having an outlet, a tank of quenching liquid which seals said outlet, and means for ejecting the compact through said outlet and liquid, whereby articles of high quality may be formed rapidly and continually.
  • the aforesaid compacting and ejecting means extend through sealed openings in the housing so as to be operated from outside the housing, andthe housing contains means for heating the die to the aforesaid temperature.
  • the apparatus should have means for keeping the housing filled with inert gas.
  • FIG. 1 is a vertical section showing the parts in position to charge the die
  • FIG. 2 is a plan view of the die from the line 22 of FIG. 1;
  • FIG. 3 is a view like FIG. 1 showing the parts in compressing position
  • FIG. 4 is a similar section showing the parts in ejecting position.
  • the particular embodiment of the invention chosen for the purpose of illustration comprises a die 1 such as described and claimed in copending application Ser. No. 633,780, now Pat. No. 3,461,507, filed on Apr. 26, 1967, the die consisting of two sections held together by a wire winding 2.
  • the die is surrounded by a housing 3 having a removable bottom 4.
  • the die is mounted on the bottom 4 by means of a casing 6 held in place by screws 7.
  • Between the casing and housing is a cylindrical space for a heating coil 8.
  • the die has an axial opening 9 in which the powder is compacted by plungers 11 and 12 extending through sealed openings in the housing. With the parts in the position shown in FIG.
  • the die is charged with powder from hopper 13 by means of a screw 14 extending through a tube 16 sealed in an opening in the side of the housing.
  • a heating coil 17 Surrounding the tube is a heating coil 17 for heating the powder to the pressing temperature or nearly thereto.
  • the powder is guided into the die by chute 18.
  • the plunger 11 is advanced from the position shown in FIG. 1 to the position shown in FIG. 3 to form the compacted article A.
  • plunger 11 is retracted and the plunger 12 is advanced to the position shown in FIG. 4'to eject the article from the die, after which the article is discharged from the housing 3 by the following mechanism.
  • a pusher 19 Sliding over the top of the die is a pusher 19 actuated by a cylinder 21 and a piston connected to the pusher by a piston rod 22.
  • the pusher When fluid is admitted to the cylinder the pusher is advanced from the position shown in FIGS. 1 and 3 to the position shown in FIG. 4, thereby depositing the article A on a belt 23 which carries the article to a pool of quenching liquid in a tank 24 which forms a part of housing 3 and which is sealed from the outside atmosphere.
  • the articles are removed from the pool by a screw conveyor 26.
  • the housing and tank are preferably kept full of an inert gas through an inlet 27 and an outlet 28.
  • this method is characterized by the fact that it employs only a single hot-pressing operation at a moderately elevated temperature and moderate pressure and does not require a sintering operation.
  • a uniqueness of the new process resides in the fact that the entire operation, from raw metal powder to finished article, is carried out in a very short time.
  • the transit time of material through the process is of the order of seconds rather than hours as in conventional powder metal processing. It thus becomes possible to produce finished powder metal parts by a continuous process within a single piece of equipment of moderate size.
  • apparatus for hot-pressing iron powder to form a compact and then quenching the compact, apparatus comprising a die, a closed housing surrounding the die, the housing having an inlet through which the die may be charged with powder, means for compacting the powder in the die to form said compact, the housing having an outlet, a tank of quenching liquid which seals said outlet, and means for ejecting the compact through said outlet and liquid, whereby articles of high quality may be formed rapidly and continually.
  • Apparatus according to claim 1 further characterized by means for keeping the housing filled with inert gas.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Powder Metallurgy (AREA)

Description

July 21, 1970 'R. E. RICE im. 3,521,326
POWDER METALLURGY PRESS APPARATUS OriginalFiled April 26, 1967 vmoooooomu 1 United States Patent US. Cl. 1816.5 4 Claims ABSTRACT OF THE DISCLOSURE Apparatus for making articles of powdered iron which involves only a single pressing at moderate temperature with inexpensive powder containing no carbon, quick quenching and no sintering.
This application is a division of application Ser. No. 633,781, filed Apr. 26, 1967, now Pat. No. 3,386,821, June 4, 1968.
In the conventional processes of making metal parts by powder metallurgy methods, it is usual to compact the metal powder in a pressing operation carried out at room temperature. In order to strengthen the parts, they are then subjected to a sintering operation at a high temperature in a protective atmosphere for an extended period of time. Following this they may be further compressed in a coining or sizing operation to further densify them and to improve the uniformity of dimensional tolerances. In order to improve the mechanical strengths of the parts additions of alloying elements may be used; for example, a few percent of copper powder is often introduced and during sintering temperatures suflicient to melt the copper powder may be employed. Since copper has a relatively high melting point, 1981 F., this requires a costly furnacing operation. Another method by which compacts may be strengthened is through the use of an infiltration operation which involves heating a porous iron compact in contact with a carefully metered quantity of copper. The temperature is sufiicient to melt the copper and allow it to permeate the porous iron structure and to partially alloy with the iron. All of these operations are essentially batch type. Equipment for sintering is expensive, requires considerable floor space and involves relatively high maintenance costs. Processes which involve two pressing operations ordinarily require two complete sets of tooling which adds appreciably to the piece cost.
Objects of the invention are to provide apparatus which operates continuously, which makes complete articles with a single piece of equipment, which requires relatively low temperatures and short times, which requires no sintering operation of the conventional type, which requires relatively very small floor area, which eliminates in-process inventories of partially completed parts, which produces high densities with relatively low-pressure presses, which permits the use of the lowest priced powders, and which results in improved overall manufacturing economy.
According to this invention the iron powder is compressed to form a compacted article which is then quenched, characterized in that the powder is compressed while at a temperature of the order of 1100 F. to 1300 F. and the article is quenched quickly while it retains the metastable quality existing at said temperature, whereby strong articles of high density may be produced quickly with only one pressing operation and with inexpensive powder which does not contain carbon. Preferably the aforesaid temperature is approximately 1200 F. The die in which the powder is compressed should be pre- 3,521,326 Patented Jul 21, 1970 heated to the aforesaid temperature. While the powder may be heated in the die it is preferably preheated to the aforesaid temperature before introduction into the die. The powder may be poured into the die or it may J be precompacted to form a briquette.
A special feature of the invention resides in the timing of three critical operations of the method, carried out in sequence, namely heating the powder, its compaction, and its cooling. The invention involves the discovery that with ferrous metal composed of powder particles which will pass through a 20 mesh sieve and wtihin the powder particles a crystal size which is customarily referred to as fine grain, the superior mechanical properties which are associated with fine grain size can be preserved to a worth-while degree through the hot pressing operation in spite of the fact that the pressing temperature is in the range ordinarily used for annealing the ferrous metal. While it is customary to anneal metal powders prior to compaction when they are to be pressed cold and even when they are to be hot pressed, in practicing this invention such annealing is to be avoided since it causes crystal growth and leads to less desirable mechanical properties in the finished article.
By pressing within the aforesaid temperature range the compacted articles have very superior qualities, such as fine grain, high density and exceptional strength. Quick quenching preserves the metastable quality existing at the pressing temperature and prevents the fine metal crystals from growing.
The apparatus comprises a die, a closed housing surrounding the die, the housing having an inlet through which the die may be charged with powder, means for compacting the powder in the die to form said compact, the housing having an outlet, a tank of quenching liquid which seals said outlet, and means for ejecting the compact through said outlet and liquid, whereby articles of high quality may be formed rapidly and continually. Preferably the aforesaid compacting and ejecting means extend through sealed openings in the housing so as to be operated from outside the housing, andthe housing contains means for heating the die to the aforesaid temperature. The apparatus should have means for keeping the housing filled with inert gas.
For the purpose of illustration a typical example of the invention is illustrated diagrammatically in the accompanying drawing in which FIG. 1 is a vertical section showing the parts in position to charge the die;
FIG. 2 is a plan view of the die from the line 22 of FIG. 1;
FIG. 3 is a view like FIG. 1 showing the parts in compressing position; and
FIG. 4 is a similar section showing the parts in ejecting position.
The particular embodiment of the invention chosen for the purpose of illustration comprises a die 1 such as described and claimed in copending application Ser. No. 633,780, now Pat. No. 3,461,507, filed on Apr. 26, 1967, the die consisting of two sections held together by a wire winding 2. The die is surrounded by a housing 3 having a removable bottom 4. The die is mounted on the bottom 4 by means of a casing 6 held in place by screws 7. Between the casing and housing is a cylindrical space for a heating coil 8. The die has an axial opening 9 in which the powder is compacted by plungers 11 and 12 extending through sealed openings in the housing. With the parts in the position shown in FIG. 1 the die is charged with powder from hopper 13 by means of a screw 14 extending through a tube 16 sealed in an opening in the side of the housing. Surrounding the tube is a heating coil 17 for heating the powder to the pressing temperature or nearly thereto. The powder is guided into the die by chute 18. After the die is charged with the desired amount of powder the plunger 11 is advanced from the position shown in FIG. 1 to the position shown in FIG. 3 to form the compacted article A. Then plunger 11 is retracted and the plunger 12 is advanced to the position shown in FIG. 4'to eject the article from the die, after which the article is discharged from the housing 3 by the following mechanism.
Sliding over the top of the die is a pusher 19 actuated by a cylinder 21 and a piston connected to the pusher by a piston rod 22. When fluid is admitted to the cylinder the pusher is advanced from the position shown in FIGS. 1 and 3 to the position shown in FIG. 4, thereby depositing the article A on a belt 23 which carries the article to a pool of quenching liquid in a tank 24 which forms a part of housing 3 and which is sealed from the outside atmosphere. The articles are removed from the pool by a screw conveyor 26. The housing and tank are preferably kept full of an inert gas through an inlet 27 and an outlet 28.
From the foregoing it will be understood that this method is characterized by the fact that it employs only a single hot-pressing operation at a moderately elevated temperature and moderate pressure and does not require a sintering operation. Thus it makes possible a unique continuous single-step manufacturing process which has substantial advantages over the conventional multi-step processes. A uniqueness of the new process resides in the fact that the entire operation, from raw metal powder to finished article, is carried out in a very short time. The transit time of material through the process is of the order of seconds rather than hours as in conventional powder metal processing. It thus becomes possible to produce finished powder metal parts by a continuous process within a single piece of equipment of moderate size. Ordinary inexpensive commercial iron powders can be used to produce parts of excellent mechanical properties, and very superior mechanical properties can be obtained by the use of the somewhat more expensive electrolytic iron powders. Also from the foregoing it will be evident that articles may be formed continually by repeating the aforesaid steps of charging, compressing and ejecting. It will also be evident that the articles may be quenched quickly while they retain the metastable quality existing at the compression temperature.
It should be understood that the present disclosure is for the purpose of illustration only and that this invention includes all modifications and equivalents which fall with in the scope of the appended claims.
We claim:
1. For hot-pressing iron powder to form a compact and then quenching the compact, apparatus comprising a die, a closed housing surrounding the die, the housing having an inlet through which the die may be charged with powder, means for compacting the powder in the die to form said compact, the housing having an outlet, a tank of quenching liquid which seals said outlet, and means for ejecting the compact through said outlet and liquid, whereby articles of high quality may be formed rapidly and continually.
2. Apparatus according to claim 1 wherein said compacting and ejecting means extend through sealed openings in the housing so as to be operated from outside the housing.
3. Apparatus according to claim 1 further characterized by means for keeping the housing filled with inert gas.
4. Apparatus according to claim 1 wherein the housing contains means for heating the die to the aforesaid temperature.
References Cited UNITED STATES PATENTS 741,752 10/1903 Acklin 164128 X 1,779,534 10/1930 Eppensteiner et al. 164-128 X 2,882,143 4/1959 Schmidt et al 1816.5 X 3,052,919 9/1962 Rayburn 18-16 3,129,463 4/1964 Gill et al 18-16 3,277,524 10/ 1966 Silver.
3,343,209 9/ 1967 Solomir et al.
J. HOWARD FLINT, JR., Primary Examiner U.S. Cl. X.R.
US719414A 1967-04-26 1968-04-08 Powder metallurgy press apparatus Expired - Lifetime US3521326A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US633781A US3386821A (en) 1967-04-26 1967-04-26 Powder metallurgy
US71941468A 1968-04-08 1968-04-08

Publications (1)

Publication Number Publication Date
US3521326A true US3521326A (en) 1970-07-21

Family

ID=27091975

Family Applications (1)

Application Number Title Priority Date Filing Date
US719414A Expired - Lifetime US3521326A (en) 1967-04-26 1968-04-08 Powder metallurgy press apparatus

Country Status (1)

Country Link
US (1) US3521326A (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3832107A (en) * 1973-06-29 1974-08-27 United Aircraft Corp Apparatus for making articles from particulate matter
US3986803A (en) * 1975-12-04 1976-10-19 United Technologies Corporation Cover positioning device for container in a compacting press
US3988088A (en) * 1975-12-04 1976-10-26 United Technologies Corporation Press for particulate material
US4005956A (en) * 1973-04-11 1977-02-01 Inoue-Japax Research Incorporated Powder activation and integrated powder metallurgy system
JPS531608A (en) * 1976-06-29 1978-01-09 Chiaki Tamura Method and apparatus for effcting quenching simultaneously with union by sintering
US4140453A (en) * 1977-09-23 1979-02-20 Westinghouse Electric Corp. Press apparatus enclosure arrangement
US4362484A (en) * 1980-11-07 1982-12-07 Ecobric Foundry Limited Apparatus for hot briquetting of ferrous or non-ferrous metallic particles
US4364893A (en) * 1981-06-15 1982-12-21 Application Engineering Corporation Mold atmosphere control system
EP0875368A2 (en) * 1997-04-30 1998-11-04 GKN Sinter Metals Limited Apparatus for feeding moulding material
US5840348A (en) * 1995-09-15 1998-11-24 Ultrapure Systems, Inc. Automated carbon block molding machine and method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US741752A (en) * 1901-03-05 1903-10-20 Heyl And Patterson Apparatus for casting metals.
US1779534A (en) * 1928-02-13 1930-10-28 American Metal Co Ltd Method of casting and rolling copper
US2882143A (en) * 1953-04-16 1959-04-14 Nat Lead Co Continuous process for the production of titanium metal
US3052919A (en) * 1960-05-09 1962-09-11 Western Electric Co Article-forming apparatus
US3129463A (en) * 1961-09-28 1964-04-21 Scully Anthony Corp Compacting press
US3277524A (en) * 1962-10-17 1966-10-11 United Aircraft Corp Method of and apparatus for compacting ferrite particles
US3343209A (en) * 1963-03-27 1967-09-26 Alusuisse Apparatus for the manufacture of dense sintered articles

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US741752A (en) * 1901-03-05 1903-10-20 Heyl And Patterson Apparatus for casting metals.
US1779534A (en) * 1928-02-13 1930-10-28 American Metal Co Ltd Method of casting and rolling copper
US2882143A (en) * 1953-04-16 1959-04-14 Nat Lead Co Continuous process for the production of titanium metal
US3052919A (en) * 1960-05-09 1962-09-11 Western Electric Co Article-forming apparatus
US3129463A (en) * 1961-09-28 1964-04-21 Scully Anthony Corp Compacting press
US3277524A (en) * 1962-10-17 1966-10-11 United Aircraft Corp Method of and apparatus for compacting ferrite particles
US3343209A (en) * 1963-03-27 1967-09-26 Alusuisse Apparatus for the manufacture of dense sintered articles

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4005956A (en) * 1973-04-11 1977-02-01 Inoue-Japax Research Incorporated Powder activation and integrated powder metallurgy system
US3832107A (en) * 1973-06-29 1974-08-27 United Aircraft Corp Apparatus for making articles from particulate matter
US3986803A (en) * 1975-12-04 1976-10-19 United Technologies Corporation Cover positioning device for container in a compacting press
US3988088A (en) * 1975-12-04 1976-10-26 United Technologies Corporation Press for particulate material
JPS531608A (en) * 1976-06-29 1978-01-09 Chiaki Tamura Method and apparatus for effcting quenching simultaneously with union by sintering
US4140453A (en) * 1977-09-23 1979-02-20 Westinghouse Electric Corp. Press apparatus enclosure arrangement
FR2404285A1 (en) * 1977-09-23 1979-04-20 Westinghouse Electric Corp ENCLOSURE FOR PRESS OPERATING IN A HAZARDOUS ENVIRONMENT
US4362484A (en) * 1980-11-07 1982-12-07 Ecobric Foundry Limited Apparatus for hot briquetting of ferrous or non-ferrous metallic particles
US4364893A (en) * 1981-06-15 1982-12-21 Application Engineering Corporation Mold atmosphere control system
US5840348A (en) * 1995-09-15 1998-11-24 Ultrapure Systems, Inc. Automated carbon block molding machine and method
EP0875368A2 (en) * 1997-04-30 1998-11-04 GKN Sinter Metals Limited Apparatus for feeding moulding material
EP0875368A3 (en) * 1997-04-30 1998-11-25 GKN Sinter Metals Limited Apparatus for feeding moulding material

Similar Documents

Publication Publication Date Title
DE2200066A1 (en) Process for the production of metal-ceramic objects
US2123416A (en) graham
US3521326A (en) Powder metallurgy press apparatus
EP0397513A1 (en) Consolidation of powder aluminum and aluminum alloys
US3779747A (en) Process for heating and sintering ferrous powder metal compacts
US2746741A (en) Apparatus for the production of wrought metal shapes from metal powder
US4274875A (en) Powder metallurgy process and product
US3120436A (en) Powdered metal article and method of making
US3144328A (en) Method of producing porous sintered tantalum anodes
US3386821A (en) Powder metallurgy
US5053192A (en) Method for making products from powdered materials
US4452756A (en) Method for producing a machinable, high strength hot formed powdered ferrous base metal alloy
US3544392A (en) Process for making high quality hotworked products from aluminum base alloy powders
DE2915831C2 (en)
US2782110A (en) Metal-ceramic bonded granular material
US3356495A (en) Method for producing high density tungsten ingots
US2561583A (en) Method of making articles from metal powder
US3212876A (en) Method for the production of iron powder from sponge iron
GB1590953A (en) Making articles from metallic powder
EP0054404A1 (en) Method of forming an article
US4270951A (en) Sintering of coated briquette
US3453103A (en) Method of sintering nickel-bronze articles
US2835573A (en) Hot pressing with a temperature gradient
JPS6111282B2 (en)
US2556921A (en) Gold beryllium alloy and method of making same