US328611A - Process of remelting soap - Google Patents

Process of remelting soap Download PDF

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US328611A
US328611A US328611DA US328611A US 328611 A US328611 A US 328611A US 328611D A US328611D A US 328611DA US 328611 A US328611 A US 328611A
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soap
steam
melted
coils
scrap
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen

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  • the object of my invention is to provide for the much more rapid remelting of soap-scrap or broken soap than can be done with processes and apparatus heretofore used, and to avoid all danger of injuring the soap, by preventing the excessive condensation therein 4of the steam used as a remelting agent, and to i provide an apparatus adapted to be worked by unskilled labor, and by use of which the. melted soap will be discharged lin as good or better condition as when placed therein to be melted.
  • Figure l is a central vertical sectional elevation of a soap-remelting apparatus constructed in accordance with my invention.
  • Fig. 2 is a sectional plan view taken on the line x, Fig. 1.
  • Fig. 3 is an enlarged plan view with the cover of the melting-vessel removed.
  • Fig. 4 is a sectional elevation of part of the upper compound soap supporting and heating coil and steam-jet of the vessel, and
  • Fig. 5 is an under side view of the same.
  • My invention is an improvement on the invention described in aforesaid Letters Patent.
  • the Whitaker apparatus consists of a melting-vessel with a bottom outlet closed by a valve, and provided with a steam-pipe in the form of a ring perforated to discharge the steannand held horizontally at or near the bottom of the vessel, and above the ring is 6o placed a spiral horizontally-arranged imperforate pipe-coil, which connects with a vertical coil rising some distance into the meltingvessel, and between the perforated lower ring and the upper heating-coils is placed a diaphragni in the form of a sieve.
  • the soap scrap to be melted is thrown into the upper part of the vessel, and is partially melted by sliding down and between the vertical and upper horizontal coils, through which large 7o unmelted pieces of soap fall onto the sievediaphragm, which holds them until melted, the melted soap flowing through the diaphragm and from the botton of the vessel when the valve is opened.
  • the sieve-diaphragm is necessary in this apparatus, and greatly retards the passage of the melted soap therefrom, and it is evident that the steam discharges into the melted soap where it is not needed, and the steam issuing from the ring 8o can only reach the cold hard soap by boiling the iiuid or melted soap, which damages the soap by condensing into it a considerable amount of water, which can be removed only by remaking the soap, thus rendering the re4 85 melter useless.
  • the letter A indicates a vessel or caldron of suitable capacity, and having a bottom tapering toward an Outlet, a, which may be closed bya valve or cutvot'f, B, of any approved construction.
  • the vessel has a removable cover, o 5 C, and a jacket, D.
  • Inside of the vessel A are set quite closely aseries of vertically ranging and communicating coils, E, of pipe, which connect by a pipe, c, with a horiZon-.
  • the vertical coils E, I support in any suitable manner the horizontally-arranged tubular coils H I, which consist each of a series of pipes having connecting-bends of short radius, and the pipes of both coils are connccted, so that steam admitted to the coil H through a connecting-pipe, J,will pass through said coil H and thence to and through the lower coil, I.
  • the pipes of the compound coil H I are so crossed or disposed relatively to each other that they together form a tubular grating having interstices too small to allow the hard soap-scrap placed on it to pass through, but permitting free passage of the melted soap through the grating upon the heating-coils below.
  • the pipes of the compoundcoil grating preferably the lower pipes, I-have formed in them a series of orifices, as at yi, at the under side, (see Figs. 4 and 5,) and these orifices are of such number and area that the steam will pass through them in jets and with consider able force to impinge on the pipe-coils E or E F below.
  • the operation is as follows: The soap-scrap and broken soap to be melted is placed in the vessel A upon the compound tubular grating H I, as at L in Fig. I, the cover C is put on the vessel, and its outlet a is closed by the cutoli B.
  • the distinguishing features of my invention may briey be stated as follows: The continuous use of open steam to melt the soap, and between the cold soap-scrap and the melted soap, and yet not in the body of the melted soap; the use of steam -jets blowing downward upon the lower coils to keep them at all times clear and free from incrustations to get the full benefit of their heat for drying and evaporating the moisture from the melted soap, and to rapidly force the melted soap from the vessel; the escape of the steam,after doing its work, along with the melted soap, but not condensed in it as water, and the superior quality of the iinished soap,which is free from excess of water, the soap being dried by the lo was coils instead of being melted thereby,as formerly was done.
  • the jets of steam may be caused to issue from pipes arranged separate from the tubular grating H I, and so as to direct the steam-jets on the lower coils, E or E F, substantially in the manner above described-but the grating, as shown, combines in a very sin1- ple arrangement a support for the soap-scrap, a heater to help melt the scrap and the nozzles through which the steam-jets issue upon the lower coils and the melted soap.
  • the vessel A and its interior pipe, coils may quickly and thoroughly be cleaned by continuing for a time the steam-discharge from the orifices t', as will readily be understood.

Description

(No Model.) 2 Sheets-Sheet 1.
J. G. RALNSTON.
PROCESS OF REMBLTING SOAP.
No. 328,611. d Patented Oct. 20, 1885.
ATTORNEYS.
Nv VETEHS Plwm-uuwgnplmr, washington. D. C.
(No Model.) l 2 Sheets-Sheet 2. J. C. RALsToN.
PROCESS OF RBMELTING SOAP.
No. 328,611. Patented oct. 20, 1885.
Figi
DTVENTOR:
ATTORNEYS.
N Pneus. mmnhugmhn, wmangwn. uc.
UNITED STATES PATENT GEEICE.
JOHN o. EALSTON, OE TOLEDO, OHIO, ASSIGNOE To EOEEET EEEELANE, OE
EOSTON, MASSACHUSETTS;
PROCESS OF REMELTING SOAP.
SPECIFICATION forming part of Letters Patent No. 328,611, dated October 20, 1885.
Application filed October 29,1884.
.To all whom it may concern:
Be it known that I, JOHN C. RALsToN, of Toledo, in the county of Lucas and State of Ohio, have invented a new and Improved Process of and Apparatus for Remelting Soap, of which the following is affull, clear, and eX- act specilication.
The object of my invention is to provide for the much more rapid remelting of soap-scrap or broken soap than can be done with processes and apparatus heretofore used, and to avoid all danger of injuring the soap, by preventing the excessive condensation therein 4of the steam used as a remelting agent, and to i provide an apparatus adapted to be worked by unskilled labor, and by use of which the. melted soap will be discharged lin as good or better condition as when placed therein to be melted.
The invention will tirst be described, and then pointed out in the claims.
Reference is to be had to the accompanying drawings, forming part of this specification, in which similar letters of reference Vindicate corresponding parts in all the figures.
Figure lis a central vertical sectional elevation of a soap-remelting apparatus constructed in accordance with my invention. Fig. 2 is a sectional plan view taken on the line x, Fig. 1. Fig. 3 is an enlarged plan view with the cover of the melting-vessel removed. Fig. 4 is a sectional elevation of part of the upper compound soap supporting and heating coil and steam-jet of the vessel, and Fig. 5 is an under side view of the same.
The chief disadvantages in the practical operation of apparatus heretofore constructed for remeltng the scraps or broken soap, produced by cutting blocks or masses of soap into 40 bars or shaping the soap into cakes, have been their slowness of operation and the danger of spoiling the soap, which frequently occurs by allowing the discharge of steam for too long a time in the melted soap, which condenses therein to such an extent as to require the soap to be returned to the kettles to be remade.
An apparatus of this class, which is extensively used, but is open to the above-named 5o objections, is shown in a United States Pat- Serial No. 146,755. (No model.)
ent granted to Daniel Whitaker on the 1st day of August, 1876, and numbered 180,688.
My invention is an improvement on the invention described in aforesaid Letters Patent.
The Whitaker apparatus consists of a melting-vessel with a bottom outlet closed by a valve, and provided with a steam-pipe in the form of a ring perforated to discharge the steannand held horizontally at or near the bottom of the vessel, and above the ring is 6o placed a spiral horizontally-arranged imperforate pipe-coil, which connects with a vertical coil rising some distance into the meltingvessel, and between the perforated lower ring and the upper heating-coils is placed a diaphragni in the form of a sieve. The soap scrap to be melted is thrown into the upper part of the vessel, and is partially melted by sliding down and between the vertical and upper horizontal coils, through which large 7o unmelted pieces of soap fall onto the sievediaphragm, which holds them until melted, the melted soap flowing through the diaphragm and from the botton of the vessel when the valve is opened. The sieve-diaphragm is necessary in this apparatus, and greatly retards the passage of the melted soap therefrom, and it is evident that the steam discharges into the melted soap where it is not needed, and the steam issuing from the ring 8o can only reach the cold hard soap by boiling the iiuid or melted soap, which damages the soap by condensing into it a considerable amount of water, which can be removed only by remaking the soap, thus rendering the re4 85 melter useless.
The drawings represent a preferred construction of apparatus by which I carry out myinvention, and which I will describe briefly as follows:
The letter A indicates a vessel or caldron of suitable capacity, and having a bottom tapering toward an Outlet, a, which may be closed bya valve or cutvot'f, B, of any approved construction. The vessel has a removable cover, o 5 C, and a jacket, D. Inside of the vessel A are set quite closely aseries of vertically ranging and communicating coils, E, of pipe, which connect by a pipe, c, with a horiZon-.
tally-disposed pipe-coil, F, placed below the roo coils E, and a pipe, f, at the end of coil F, connects it in turn with the jacket D, which may have any suitable valved or other' outlet, d,
for the escape of the heating medium,when desired.
As thus far described there is nothing new in the construction.
Above the vertical coils E, I support in any suitable manner the horizontally-arranged tubular coils H I, which consist each of a series of pipes having connecting-bends of short radius, and the pipes of both coils are connccted, so that steam admitted to the coil H through a connecting-pipe, J,will pass through said coil H and thence to and through the lower coil, I.
The pipes of the compound coil H I are so crossed or disposed relatively to each other that they together form a tubular grating having interstices too small to allow the hard soap-scrap placed on it to pass through, but permitting free passage of the melted soap through the grating upon the heating-coils below.
The pipes of the compoundcoil gratingpreferably the lower pipes, I-have formed in them a series of orifices, as at yi, at the under side, (see Figs. 4 and 5,) and these orifices are of such number and area that the steam will pass through them in jets and with consider able force to impinge on the pipe-coils E or E F below.
The operation is as follows: The soap-scrap and broken soap to be melted is placed in the vessel A upon the compound tubular grating H I, as at L in Fig. I, the cover C is put on the vessel, and its outlet a is closed by the cutoli B. Steam now is admitted under full pressureto the upper compound soapsupporting tubular grating, H I, and to the lower coils, E F, and the open steam, rushing downward from the orifices t' of the grating H I, quickly fills the lower part ofthe meltingvessel A and ascends to the soap-scrap on the grating, which latter also gives off its heat to the scrap, which at once is softened, and melts and forces its way through the grating by its own gravity, aided by the weight of the mass above, and the melted soap falls in streams, as at Z l, upon the lower coils, E, toward the outlet a, which now is opened, and jets of steam from the grating, impinging on the surface of the downwardly-dowing streams of melted soap, force the melted soap rapidly down the vertical coils E and through the coil F, the steam-jets acting to prevent the formation of a hard, dry, soapy crust on the lower coils and keeping them clear, so that their full heat-radiating effect may be utilized in drying out of the down-flowing melted soap any moisture it may have absorbed by contact with the open steam by which it was melted, and a continuous stream of remelted soap issues from the outlet a, and with it the steam, which reaches the air in an uncondensed state, and the steam does not condense to any hurtful degree in the soap,which is discharged at the proper consistency and in fit condition to produce, when formed into bars or cakes, a soap of the highest market value for the materials employed in making it, and some kinds of soap are materially improved by the remelting process.
It is evident that the soap-melting is practically continuous, and the apparatus needs no further attention than to keep the vessel full of scrap above the grating H I, and to handle the melted soap in the usual manner as it passes from the melting-vessel, which may easily be done by unskilled labor.
The distinguishing features of my invention may briey be stated as follows: The continuous use of open steam to melt the soap, and between the cold soap-scrap and the melted soap, and yet not in the body of the melted soap; the use of steam -jets blowing downward upon the lower coils to keep them at all times clear and free from incrustations to get the full benefit of their heat for drying and evaporating the moisture from the melted soap, and to rapidly force the melted soap from the vessel; the escape of the steam,after doing its work, along with the melted soap, but not condensed in it as water, and the superior quality of the iinished soap,which is free from excess of water, the soap being dried by the lo wer coils instead of being melted thereby,as formerly was done.
It is evident that other arrangements of apparatus than that above described-may be employed in carrying out my invention-as, for instance, the jets of steam may be caused to issue from pipes arranged separate from the tubular grating H I, and so as to direct the steam-jets on the lower coils, E or E F, substantially in the manner above described-but the grating, as shown, combines in a very sin1- ple arrangement a support for the soap-scrap, a heater to help melt the scrap and the nozzles through which the steam-jets issue upon the lower coils and the melted soap.
Vhenthe work of melting the soap-serap is finished, the vessel A and its interior pipe, coils may quickly and thoroughly be cleaned by continuing for a time the steam-discharge from the orifices t', as will readily be understood.
Although I have herein more particularly described my apparatus as operated by the use of steam, it is evident that hot air might be substituted for steam without departing from my invention.
Having thus described my invention, I claim as new and desire to secure by Letters Patent- 1. The method herein described of melting soap-scrap, consisting in subjecting the scrap to the action of'heat and open steam simulta neously to soften and melt the same and then subjecting the melted soap to the action of heatto remove the surplus moisture, as set forth.
2. The method herein described of melting soap-scrap, consisting in subjecting the scrap tothe action ofheat and steam simultaneously,
IOO
IIO
then subjecting the melted scrap to the action of jets of open steam, and. finally subjecting the same to the action of heat, as set forth.
3. The method herein described of keeping the heating-pipes clear of crust, which consists in subjecting the melted soap and the eX- terior surfaces of the heating-pipes to the action of downward jets of steam during the descent of the soap, as set forth.
4. The method herein described of producing a continuous rapid delivery of the nished soap from the meIting-VeSSeLWhich consists in JOHN C. RALSTON.
Witnesses:
EDWARD H. RHoADns, ELIsHA B. SOUTHARD.
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