US3144381A - Continuously operable vertical digester for cooking pre-impregnated fibrous raw materials - Google Patents

Continuously operable vertical digester for cooking pre-impregnated fibrous raw materials Download PDF

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US3144381A
US3144381A US123162A US12316261A US3144381A US 3144381 A US3144381 A US 3144381A US 123162 A US123162 A US 123162A US 12316261 A US12316261 A US 12316261A US 3144381 A US3144381 A US 3144381A
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digester
shaft
raw materials
fibrous raw
cooking
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US123162A
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Simon Ludwig
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JM Voith AG
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JM Voith AG
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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C7/00Digesters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01BBOILING; BOILING APPARATUS ; EVAPORATION; EVAPORATION APPARATUS
    • B01B1/00Boiling; Boiling apparatus for physical or chemical purposes ; Evaporation in general

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  • This invention relates to a continuously operable vertical digester for cooking pro-impregnated fibrous raw materials for the manufacture of chemical or semi-chemical pulp at temperatures over 100 C. and under pressure.
  • the invention relates to a continuously operable vertical digester for cooking pro-impregnated fibrous raw materials for the manufacture of chemical or semi-chemical woodpulp at temperatures above 100 C. and under pressure, which digester comprises a centrically mounted, driven vertical shaft, a digester bottom having one or more discharge openings which are suitably connected to one or more cylindrical or conical screw-type extruders or the like and/ or a disintegrator, which digester is characterized in that the shaft extends throughout the digester vessel Patented Aug; 11, 1964 from top to bottom and is mounted in known manner in an axial bearing on the cover of the vessel and guided in a radial bearing below the bottom of the vessel, and that a discharge device carrying the entire pulp column is supported by the shaft next to the digester bottom.
  • the diameter of the shaft may be larger at the top end than at the bottom end of the digester.
  • the shaft may be hollow and formed with holes, through which the steam introduced into the shaft enter
  • FIG. 1 is a longitudinal sectional view showing one embodiment of a digester according to the invention.
  • FIG. 2 is a sectional view taken on line ab of FIG. 1.
  • FIGS. 3, 4 and 5 are diagrammatic views showing modifications.
  • the vertical cylindrical digester 1 operates continuously in the vapor phase and serves for cooking pre-impregnated fibrous raw materials for manufacturing chemical or semi-chemical pulp at temperatures over C. and under pressure.
  • the digester may also be used for pretreating any fibrous raw material.
  • the material to be cooked is introduced into the digester 1 from a hopper 35.
  • the Weight of the material 3 to be cooked in the digester loads the rotating outlet device 4, which is secured to a continuous, vertical shaft 5 having a controllable speed.
  • the shaft 5 is supported by an axial bearing (step bearing) 6 carried on the cover of the digester 1.
  • a lower bearing 7 also disposed outside the digester serves as a guide bearing for the shaft. Owing to this arrangement the continuous vertical shaft 5 is stressed only in tension and torsion rather than in fiexion because the load of the discharge device 4 is uniformly divided by the material 3 to be boiled. For this reason the volume of the digester may be large without involving structural difficulties because the digester having a given height may be given an appropriate diameter.
  • the material 3 to be boiled must slowly descend in the digester 1. This descent must be uniform in order to ensure a uniform cooking.
  • the discharge device 4 must continuously and uniformly remove the cooked material from the digester.
  • the chips of raw material descend in the digest 1 under the action of the force of gravity, which can act on the material 3 being cooked without hindrance in all cross-sections unless the chips form bridges.
  • the available cross-section of the digest 1 must be downwardly enlarged in known manner to provide for a progressive relief of the chips of raw material.
  • the digester is provided with a device 8 of any known type for indicating the level of the material to be cooked. It is also suitable to provide the continuous vertical shaft 5 at its top end with stirring arms 9 for leveling the material 3 to be cooked.
  • a steam pipe 11 is connected to the digester approximately in the middle and also below the outlet device 4, e.g. by means of a ring conduit provided with a plurality of supply connections, in order to equalize the steam pressure in the digester.
  • automatic device 12 is provided to eliminate air and gasses from the digester 1.
  • the shaft is hollow and provided with holes, steam can be supplied also from the top by means of the conduit indicated with dash-and-dot lines.
  • the rotating outlet device 4 driven by the shaft 5 at, e.g. 20-30 revolutions per minute, consists of a disc 13 having approximately the same diameter as the bottom of the digester, and two or more stirring arms 14 which are disposed below the disc 13 and curved opposite to the direction of rotation 15.
  • the stirring arms 14 are rigidly secured to the underside of the disc 13.
  • Pegs or pins 16 in the form of pyramids, cones, prisms, cylinders or the like are secured to the top face of the disc 13.
  • the disc 13 is also formed with through holes 17. During the rotation of the outlet device 4, the pins mix the cooked chips of the raw material.
  • these chips are comminuted to some extent at the cooking temperature because the weight of the material 3 being cooked presses the cooked material onto the disc 13. Owing to the friction between the chips and between the chips and the digester wall the material being cooked cannot rotate in synchronism with the disc 13. Owing to the pressure exerted by the material 3 being cooked on the top face of the disc 13 and owing to the force of gravity, the cooked and comminuted raw material falls through the holes 17 into the space between the disc and the digester bottom, in which space the stirrer arms 14 rotate in the direction 15. They are preferably curved opposite to the direction of rotation.
  • the material is urged outwardly towards the discharge opening 19 in the direction of the arrow 18 and flows through a discharge conduit 20 into a conical or cylindrical screw-type extruder 21, which is radially or tangentially disposed.
  • the rotating screw 22 which is driven, e.g. by an electric motor having a controllable speed, compresses the material and feeds it to the adjustable discharge opening 23, through which it is extruded from the extruder 21.
  • the material is blown out in the direction of the arrow 24 by means of steam.
  • the shaft 5 is connected by a clutch 27 to a stub shaft of the transmission 28, which is driven by an additional electric motor.
  • FIG. 3 shows another design of the digester providing for a relief of the chips of the raw material in the digester.
  • the digester 1a is assembled from a plurality of relatively short cylindrical parts. The diameter of each part is larger than that of the part preceding in the direction of flow. This digester provides for a stepwise enlargement of the free cross-section of the digester.
  • FIG. 4 shows another form of the digester 1b, which has the shape of an upright cone providing for a continuous increase of the free cross-section of the digester from top to bottom to afford a progressive relief of the chips of the raw material.
  • FIG. 5 shows a digester in which features of the digesters of FIGS. 3 and 4 are combined.
  • This digester 10 consists of a plurality of conical parts and the top diameter of each part is larger than the bottom diameter of the part preceding in the direction of flow. This provides for an increase of the free cross-section of the digester in the downward direction and for a stepwise and continuous relief of the raw material.
  • the digester may have a conical shaft 5 (FIG. 1) or a cylindrical shaft 5a (FIG. 3), 5b (FIG. 4) or 5c (FIG. 5).
  • This conical or cylindrical shaft is desirably provided with a plurality of projections, pins or the like, which extend substantially at right angles to the shaft and prevent a formation of bridges by the material being cooked.
  • the invention provides an arrangement of the shaft and of the discharge device carried thereby in which the shaft is stressed only in tension and possibly in torsion and the bearings disposed outside the digester are exposed only to the environmental temperature and are easily accessible for maintenance.
  • the features of the invention enable the construction of reliable digesters having a large volume without involving design difficulties.
  • V/hat is claimed is:
  • a vertical digester for the continuous cooking of preimpregnated fibrous raw materials in the manufacture of pulp at temperatures above C. and under pressure, comprising a digester vessel adapted to contain a pulp column and having a top and a bottom, said bottom having at least one outlet, a vertical shaft coaxially disposed in and extending throughout said digester vessel and through the top and bottom thereof, an axial thrust bearing for said shaft located above said top, a radial bearing for said shaft disposed below said bottom, drive means for rotating said shaft in said axial and radial bearings, a discharge device fixed to and carried by said shaft above and adjacent to said bottom, said discharge device comprising a disc secured to said shaft having perforations as well as projections provided on its top face and having approximately the same diameter as the digester bottom, and at least two stirrer arms rigidly secured to said disc on the underside thereof and serving for pushing the digested chips collected at the bottom of the vessel radially outwards.
  • a vertical digester for the continuous cooking of preimpregnated fibrous raw materials in the manufacture of pulp at temperatures above 100 C. and under pressure, comprising a digester vessel adapted to contain a pulp column and having a top and a bottom, said bottom having at least one outlet, a vertical shaft coaxially disposed in and extending throughout said digester vessel and through the top and bottom thereof, an axial thrust bearing for said shaft located above said top, a radial bearing for said shaft disposed below said bottom, drive means for rotating said shaft in said axial and radial bearings, a discharge device fixed to and carried by said shaft above and adjacent to said bottom and the diameter of said shaft being larger at the top than at the bottom of said digester vessel.
  • a vertical digester for the continuous cooking of preimpregnated fibrous raw materials in the manufacture of pulp at temperatures above 100 C. and under pressure, comprising a digester vessel adapted to contain a pulp column and having a top and a bottom, said bottom having at least one outlet, a vertical shaft coaxially disposed in and extending throughout said digester vessel and through the top and bottom thereof, an axial thrust bearing for said shaft located above said top, a radial bearing for said shaft disposed below said bottom, drive means for rotating said shaft in said axial and radial bearings, a discharge device fixed to and carried by said shaft above and adjacent to said bottom, said shaft being hollow and provided with holes so that steam can pass through said holes into the interior of said digester vessel.

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Description

Aug. 11, 1964 1.. SIMON 3,144,381
CONTINUOUSLY OPERABLE VERTICAL DIGESTER FOR COOKING PRE-IMPREGNATED FIBROUS RAW MATERIALS Filed July 11, 1961 2 Sheets-Sheetv 1 FIG. 7
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wow/e SIMON y MvM A 7 TORNEYS Aug. 11, 1964 SIMON 3,144,381
CONTINUOUSLY OPERABLE VERTICAL DIGESTER FOR cooxmc PRE-IMPREGNATED FIBROUS RAW MATERIALS Filed July 11, 1961 2 Sheets-Sheet 2 I 1 E g l FIGS 11 5:21-51? 6 i:
II R
INVENTOR L up WIG S/MON y ATTORNEYS United States Patent 3,144,381 CONTHJUOUSLY OPERABLE VERTICAL DI- GESTER FOR COOKING PRE-IMPREG- NATED FIBROUS RAW MATERIALS Ludwig Simon, St. Polten, Austria, assignor to J. M.
Voith Aktiengesellschaft, St. Polten, Austria, a corporation of Austria Filed July 11, 1961, Ser. No. 123,162 Claims priority, application Austria July 20, 1960 5 Claims. (Cl. 162-237) This invention relates to a continuously operable vertical digester for cooking pro-impregnated fibrous raw materials for the manufacture of chemical or semi-chemical pulp at temperatures over 100 C. and under pressure.
It is an object of the invention to provide a digester which is suitable for a continuous cooking operation in the vapor phase.
It is desired in industry to increase the productivity of labor and to save raw materials. In long years of research, the semi-chemical process has been developed in the pulp industry in order to reduce the raw materials required in the manufacture of pulp and to reduce also the price of the various products. The next step was the continuous digestion by cooking in the vapor phase, using pre-impregnated raw material. This resulted in a considerable reduction in steam consumption compared to cooking in a liquid phase and in a reduction of labor costs compared to the discontinuous operation. In addition, the cooking temperature was increased above the usual temperature to enable a better utilization of a given digester volume by a reduction of the cooking time. For the same reason, the surplus of digester chemicals has been used with good results.
There is an additional measure which can be adopted to reduce the costs of the manufacture of pulp from preimpregnated raw materials. This consists in the use of digesters having a large Volume.
Several proposals have already been made to achieve this aim. Most digesters of the type mentioned initially hereinbefore are provided adjacent to the bottom with stirrer arms, scrapers, spiral scraper blades or the like for loosening the material and subsequently to effect or facilitate its discharge. A considerable portion of the pulp column rests on these means so that they are under a high pressure load as they rotate together with parts of the pulp column. Some of the digesters designed according to known proposals are hardly suitable for this function. The relatively short shafts used to rotate said means are under compressive stress and it is not possible owing to the high temperature to provide bearings within the digester or the discharge region thereof in order to reduce the buckling stress acting on the shaft.
Vertical digesters have been disclosed which comprise a shaft extending throughout the height of the digester. In addition to other disadvantages inherent in part of these digesters, their main disadvantage resides in the provision of shaft bearings inside the digester. The function and life of these hearings are adversely affected by the existing temperature conditions.
All these difficulties have been eliminated by the invention. As has been mentioned initially hereinbefore, the invention relates to a continuously operable vertical digester for cooking pro-impregnated fibrous raw materials for the manufacture of chemical or semi-chemical woodpulp at temperatures above 100 C. and under pressure, which digester comprises a centrically mounted, driven vertical shaft, a digester bottom having one or more discharge openings which are suitably connected to one or more cylindrical or conical screw-type extruders or the like and/ or a disintegrator, which digester is characterized in that the shaft extends throughout the digester vessel Patented Aug; 11, 1964 from top to bottom and is mounted in known manner in an axial bearing on the cover of the vessel and guided in a radial bearing below the bottom of the vessel, and that a discharge device carrying the entire pulp column is supported by the shaft next to the digester bottom. In a preferred embodiment, the diameter of the shaft may be larger at the top end than at the bottom end of the digester. The shaft may be hollow and formed with holes, through which the steam introduced into the shaft enters the interior of the digester.
Further advantages and details of the invention will be explained with reference to the accompanying drawings, in which FIG. 1 is a longitudinal sectional view showing one embodiment of a digester according to the invention.
FIG. 2 is a sectional view taken on line ab of FIG. 1.
FIGS. 3, 4 and 5 are diagrammatic views showing modifications.
The drawings and the following specification disclose also features that are not a part of the invention but are required to understand the same and in any case suitable.
The vertical cylindrical digester 1 operates continuously in the vapor phase and serves for cooking pre-impregnated fibrous raw materials for manufacturing chemical or semi-chemical pulp at temperatures over C. and under pressure. The digester may also be used for pretreating any fibrous raw material.
The material to be cooked is introduced into the digester 1 from a hopper 35. The Weight of the material 3 to be cooked in the digester loads the rotating outlet device 4, which is secured to a continuous, vertical shaft 5 having a controllable speed. The shaft 5 is supported by an axial bearing (step bearing) 6 carried on the cover of the digester 1. A lower bearing 7 also disposed outside the digester serves as a guide bearing for the shaft. Owing to this arrangement the continuous vertical shaft 5 is stressed only in tension and torsion rather than in fiexion because the load of the discharge device 4 is uniformly divided by the material 3 to be boiled. For this reason the volume of the digester may be large without involving structural difficulties because the digester having a given height may be given an appropriate diameter.
As is known per se, the material 3 to be boiled must slowly descend in the digester 1. This descent must be uniform in order to ensure a uniform cooking. The discharge device 4 must continuously and uniformly remove the cooked material from the digester. The chips of raw material descend in the digest 1 under the action of the force of gravity, which can act on the material 3 being cooked without hindrance in all cross-sections unless the chips form bridges. To fulfil this requirement, the available cross-section of the digest 1 must be downwardly enlarged in known manner to provide for a progressive relief of the chips of raw material.
In the embodiment shown in FIGURE 1 this results from the shape of the continuous vertical shaft 5, the the diameter of which at the top end of the digester 1 is larger than at the lower end of the digester at the outlet device 4.
The digester is provided with a device 8 of any known type for indicating the level of the material to be cooked. It is also suitable to provide the continuous vertical shaft 5 at its top end with stirring arms 9 for leveling the material 3 to be cooked.
Steam at more than 100-200 C. is introduced through the steam supply conduit 10 into the digester 1 to heat the material to be cooked. A steam pipe 11 is connected to the digester approximately in the middle and also below the outlet device 4, e.g. by means of a ring conduit provided with a plurality of supply connections, in order to equalize the steam pressure in the digester. An
automatic device 12 is provided to eliminate air and gasses from the digester 1.
If, in accordance with the invention, the shaft is hollow and provided with holes, steam can be supplied also from the top by means of the conduit indicated with dash-and-dot lines.
The rotating outlet device 4 driven by the shaft 5 at, e.g. 20-30 revolutions per minute, consists of a disc 13 having approximately the same diameter as the bottom of the digester, and two or more stirring arms 14 which are disposed below the disc 13 and curved opposite to the direction of rotation 15. The stirring arms 14 are rigidly secured to the underside of the disc 13. Pegs or pins 16 in the form of pyramids, cones, prisms, cylinders or the like are secured to the top face of the disc 13. The disc 13 is also formed with through holes 17. During the rotation of the outlet device 4, the pins mix the cooked chips of the raw material.
At the same time, these chips are comminuted to some extent at the cooking temperature because the weight of the material 3 being cooked presses the cooked material onto the disc 13. Owing to the friction between the chips and between the chips and the digester wall the material being cooked cannot rotate in synchronism with the disc 13. Owing to the pressure exerted by the material 3 being cooked on the top face of the disc 13 and owing to the force of gravity, the cooked and comminuted raw material falls through the holes 17 into the space between the disc and the digester bottom, in which space the stirrer arms 14 rotate in the direction 15. They are preferably curved opposite to the direction of rotation. Owing to the shape of the stirrer arms 14, the material is urged outwardly towards the discharge opening 19 in the direction of the arrow 18 and flows through a discharge conduit 20 into a conical or cylindrical screw-type extruder 21, which is radially or tangentially disposed.
The rotating screw 22, which is driven, e.g. by an electric motor having a controllable speed, compresses the material and feeds it to the adjustable discharge opening 23, through which it is extruded from the extruder 21. The material is blown out in the direction of the arrow 24 by means of steam.
The shaft 5 is connected by a clutch 27 to a stub shaft of the transmission 28, which is driven by an additional electric motor.
FIG. 3 shows another design of the digester providing for a relief of the chips of the raw material in the digester. To this end, the digester 1a is assembled from a plurality of relatively short cylindrical parts. The diameter of each part is larger than that of the part preceding in the direction of flow. This digester provides for a stepwise enlargement of the free cross-section of the digester.
FIG. 4 shows another form of the digester 1b, which has the shape of an upright cone providing for a continuous increase of the free cross-section of the digester from top to bottom to afford a progressive relief of the chips of the raw material.
FIG. 5 shows a digester in which features of the digesters of FIGS. 3 and 4 are combined. This digester 10 consists of a plurality of conical parts and the top diameter of each part is larger than the bottom diameter of the part preceding in the direction of flow. This provides for an increase of the free cross-section of the digester in the downward direction and for a stepwise and continuous relief of the raw material.
According to the invention the digester may have a conical shaft 5 (FIG. 1) or a cylindrical shaft 5a (FIG. 3), 5b (FIG. 4) or 5c (FIG. 5). This conical or cylindrical shaft is desirably provided with a plurality of projections, pins or the like, which extend substantially at right angles to the shaft and prevent a formation of bridges by the material being cooked.
The invention provides an arrangement of the shaft and of the discharge device carried thereby in which the shaft is stressed only in tension and possibly in torsion and the bearings disposed outside the digester are exposed only to the environmental temperature and are easily accessible for maintenance. As contrasted with known designs, the features of the invention enable the construction of reliable digesters having a large volume without involving design difficulties.
V/hat is claimed is:
1. A vertical digester for the continuous cooking of preimpregnated fibrous raw materials in the manufacture of pulp at temperatures above C. and under pressure, comprising a digester vessel adapted to contain a pulp column and having a top and a bottom, said bottom having at least one outlet, a vertical shaft coaxially disposed in and extending throughout said digester vessel and through the top and bottom thereof, an axial thrust bearing for said shaft located above said top, a radial bearing for said shaft disposed below said bottom, drive means for rotating said shaft in said axial and radial bearings, a discharge device fixed to and carried by said shaft above and adjacent to said bottom, said discharge device comprising a disc secured to said shaft having perforations as well as projections provided on its top face and having approximately the same diameter as the digester bottom, and at least two stirrer arms rigidly secured to said disc on the underside thereof and serving for pushing the digested chips collected at the bottom of the vessel radially outwards.
2. A digester as set forth in claim 1 wherein the diameter of said shaft is larger at the top than at the bottom of said digester vessel.
3. A digester as set forth in claim 1 wherein said shaft is hollow and provided with holes so that steam can pass through said holes into the interior of said digester vessel.
4. A vertical digester for the continuous cooking of preimpregnated fibrous raw materials in the manufacture of pulp at temperatures above 100 C. and under pressure, comprising a digester vessel adapted to contain a pulp column and having a top and a bottom, said bottom having at least one outlet, a vertical shaft coaxially disposed in and extending throughout said digester vessel and through the top and bottom thereof, an axial thrust bearing for said shaft located above said top, a radial bearing for said shaft disposed below said bottom, drive means for rotating said shaft in said axial and radial bearings, a discharge device fixed to and carried by said shaft above and adjacent to said bottom and the diameter of said shaft being larger at the top than at the bottom of said digester vessel.
5. A vertical digester for the continuous cooking of preimpregnated fibrous raw materials in the manufacture of pulp at temperatures above 100 C. and under pressure, comprising a digester vessel adapted to contain a pulp column and having a top and a bottom, said bottom having at least one outlet, a vertical shaft coaxially disposed in and extending throughout said digester vessel and through the top and bottom thereof, an axial thrust bearing for said shaft located above said top, a radial bearing for said shaft disposed below said bottom, drive means for rotating said shaft in said axial and radial bearings, a discharge device fixed to and carried by said shaft above and adjacent to said bottom, said shaft being hollow and provided with holes so that steam can pass through said holes into the interior of said digester vessel.
References Cited in the file of this patent UNITED STATES PATENTS 1,415,433 Engel May 9, 1922 2,027,131 Upton Jan. 7, 1936 2,516,447 Burling July 25, 1950 2,540,706 Beck Feb. 6, 1951 2,858,211 Durant Oct. 28, 1958 2,960,161 Richter Nov. 15, 1960

Claims (1)

  1. 5. A VERTICAL DIGESTER FOR THE CONTINUOUS COOKING OF PREIMPREGNATED FIBROUS RAW MATERIALS IN THE MANUFACTURE OF PULP AT TEMPERATURES ABOVE 100*C. AND UNDER PRESSURE, COMPRISING A DIGESTER VESSEL ADAPTED TO CONTAIN A PULP COLUMN AND HAVING A TOP AND A BOTTOM, SAID BOTTOM HAVING AT LEAST ONE OUTLET, A VERTICAL SHAFT COAXIALLY DISPOSED IN AND EXTENDING THROUGHOUT SAID DIGESTER VESEL AND THROUGH THE TOP AND BOTTOM THEREOF, AND AXIAL THRUST BEARING FOR SAID SHAFT LOCATED ABOVE SAID TOP, A RADIAL BEARING FOR SAID SHAFT DISPOSED BELOW SAID BOTTOM DRIVE MEANS FOR ROTATING SAID SHAFT IN SAID AXAIL AND RADIAL BEARINGS, A DISCHARGE DEVICE FIXED TO AND CARRIED BY SAID SHAFT ABOVE AND ADJACENT TO SIAD BOTTOM, SAID SHAFT BEING HOLLOW AND PROVIDED WITH HOLES SO THAT STEAM CAN PASS THROUGH SAID HOLES INTO THE INTERIOR OF SAID DIGESTER VESSEL.
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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1415433A (en) * 1919-12-16 1922-05-09 Engel Henri Apparatus for the extraction of oils and the like
US2027131A (en) * 1931-07-28 1936-01-07 Charles B Upton Cooker
US2516447A (en) * 1947-02-24 1950-07-25 Elmer R Burling Method and apparatus for chemical treatment
US2540706A (en) * 1947-05-22 1951-02-06 Texas Co Process and apparatus for effecting catalytic reactions
US2858211A (en) * 1956-02-13 1958-10-28 Condi Engineering Corp Apparatus for wood chip digestion
US2960161A (en) * 1957-05-16 1960-11-15 John C F C Richter Device for discharging materials from vessels

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1415433A (en) * 1919-12-16 1922-05-09 Engel Henri Apparatus for the extraction of oils and the like
US2027131A (en) * 1931-07-28 1936-01-07 Charles B Upton Cooker
US2516447A (en) * 1947-02-24 1950-07-25 Elmer R Burling Method and apparatus for chemical treatment
US2540706A (en) * 1947-05-22 1951-02-06 Texas Co Process and apparatus for effecting catalytic reactions
US2858211A (en) * 1956-02-13 1958-10-28 Condi Engineering Corp Apparatus for wood chip digestion
US2960161A (en) * 1957-05-16 1960-11-15 John C F C Richter Device for discharging materials from vessels

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FR1295266A (en) 1962-06-01

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