US3117733A - Method of wet-grinding in a rotary drum - Google Patents

Method of wet-grinding in a rotary drum Download PDF

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Publication number
US3117733A
US3117733A US133559A US13355961A US3117733A US 3117733 A US3117733 A US 3117733A US 133559 A US133559 A US 133559A US 13355961 A US13355961 A US 13355961A US 3117733 A US3117733 A US 3117733A
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mill
slurry
grinding
bodies
speed
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US133559A
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Cleemann Jorgen Olav
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FLSmidth and Co AS
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FLSmidth and Co AS
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls

Definitions

  • non-metallic grinding media in the form of pebbles or to practice autogenous grinding, that is, grinding of the material by means of the material itself in the form of large lumps.
  • autogenous grinding that is, grinding of the material by means of the material itself in the form of large lumps.
  • the use of such non-metallic bodies reduces the capacity of a given mill by from 50% to 70%.
  • the critical speed referred to is the speed of rotation of a mill, at which the centrifugal force required to maintain a grinding body in circular motion at the inner periphery of the mill is equal to the force of gravity and a mathematical expression for such critical speed is where 11 is measured in revolutions per minute and D is the inside diameter of the mill in feet.
  • the present invention is based on observations made in grinding cement raw material slurries at speeds just below or above the critical speed of the mill. In experiments, it has been found that an increase in the output of a mill can be obtained, if the quantity of slurry present in the charge occupies a limited proportion of the voids between the grinding bodies and the slurry has a yield value in the range from 300 to 900 dynes/om.
  • the yield value referred to is a measure of fluidity of the slurry and is a characteristic constant for plastic liquids, of which cement raw material is an example.
  • the yield value of a slurry may be determined by a Stormer viscometer.
  • a charge of non-metallie grinding bodies and a quantity of slurry sufiicient to occupy from 40% to 80% of the voids among the bodies and of a yield value in the range from 300 to 900 dynes/ cm. are introduced into a rotary drum, such as a tube mill, and the drum is rotated at a speed within the range from just below the critical speed to about 150% of the critical speed.
  • Slurry containing particles below a selected size continually withdrawn from the mill and slurry of a yield value within the specified range is introduced into the mill at a rate to maintain the specified quantity of slurry within the mill.
  • the practice of the invention makes it possible to increase the output of a mill of given size to two or more times the output under normal Working conditions so that the output approximates that obtained by the use of iron grinding bodies with the mill operating at a normal speed.
  • the slurry charge is specified as the percentage of the voids in the charge of grinding bodies which the slurry occupies.
  • a mill in which the ratio of length to diameter ranges from 00.5 to 2 and is preferably about 1.
  • a grate-discharge mill may have discharge slots in a plane end wall or through the cylindrical shell of the mill, the slots being of a Width small enough to prevent the grinding bodies from passing but wide enough to permit the ground material to be discharged for collection in a hopper below the mill.
  • Such a mill is to be distinguished from an overflow mill, in which the ground material is discharged through an axial hollow trunnion.
  • Grate-discharge mills which may be advantageously employed in practicing the method, may be divided into two compartments having discharge slots I claim:
  • a method of grinding a slurry of mineral material which comprises introducing into a rotary drum a charge of non-metallic grinding bodies and a quantity of slurry sutficient to occupy from to of the voids among the bodies and of a yield value in the range of 300 to 900 dynes/cm.-, rotating the drum at a speed in the range from just below the critical speed to about of the critical speed, withdrawing from the mill slurry containing particles below a selected size, and introducing into the mill slurry of a yield value within the specified range at a rate sufiicient to maintain the specified quantity of slurry within the mill.

Description

United States Patent 3,117,733 METHOD OF WET-GRINDIN G ]N A ROTARY DRUM This invention relates to the grinding of ores and other mineral materials as practiced in the mining and cement industries and is concerned more particularly with a novel method of wet-grinding such materials in mill drums as part of a tumbling load which includes non-metallic bodies.
In the grinding of minerals in rotary drums, such as tube mills, it is common practice to employ grinding bodies which are usually of steel or cast iron. In the grinding operation, the wear on the grinding bodies forms a considerable part of the total cost, particularly when hard materials are being ground, and the expenditures for metallic grinding bodies may be at least as great as the cost of the power consumed and is frequently considerably greater.
To reduce the cost of grinding by the use of metallic grinding bodies, it is common to use non-metallic grinding media in the form of pebbles or to practice autogenous grinding, that is, grinding of the material by means of the material itself in the form of large lumps. As grinding bodies formed of pebbles or lumps of the material to be ground are of much lower specific gravity than iron bodies, the use of such non-metallic bodies reduces the capacity of a given mill by from 50% to 70%. To compensate for this reduction in capacity, it has become the practice in recent years to increase the speed of rotation of the mill to a value just below the critical speed or to a super-critical speed exceeding the critical speed by from 20% to 50%. The critical speed referred to is the speed of rotation of a mill, at which the centrifugal force required to maintain a grinding body in circular motion at the inner periphery of the mill is equal to the force of gravity and a mathematical expression for such critical speed is where 11 is measured in revolutions per minute and D is the inside diameter of the mill in feet.
The present invention is based on observations made in grinding cement raw material slurries at speeds just below or above the critical speed of the mill. In experiments, it has been found that an increase in the output of a mill can be obtained, if the quantity of slurry present in the charge occupies a limited proportion of the voids between the grinding bodies and the slurry has a yield value in the range from 300 to 900 dynes/om. The yield value referred to is a measure of fluidity of the slurry and is a characteristic constant for plastic liquids, of which cement raw material is an example. The yield value of a slurry may be determined by a Stormer viscometer.
In the practice of the invention, a charge of non-metallie grinding bodies and a quantity of slurry sufiicient to occupy from 40% to 80% of the voids among the bodies and of a yield value in the range from 300 to 900 dynes/ cm. are introduced into a rotary drum, such as a tube mill, and the drum is rotated at a speed within the range from just below the critical speed to about 150% of the critical speed. Slurry containing particles below a selected size continually withdrawn from the mill and slurry of a yield value within the specified range is introduced into the mill at a rate to maintain the specified quantity of slurry within the mill. The practice of the invention makes it possible to increase the output of a mill of given size to two or more times the output under normal Working conditions so that the output approximates that obtained by the use of iron grinding bodies with the mill operating at a normal speed.
In order to show the advantages of the invention, tests were carried out in a mill 600 mm. in diameter and 720 mm. long. The grinding bodies used were pebbles formed of pieces of limestone which had been worn smooth and the entire charge occupied 30% of the total volume of the mill. The material ground was limestone slurry, which had been subjected to primary grinding. In one series of tests, the slurry employed had a yield value of 400 dynes/orn. as determined by a Stormer viscometer, and the power consumption for grinding, which is a measure of the effectiveness of the grinding and indicativeof the mill output, was determined for various slurry charges and varying mill speeds.
In Table I, the slurry charge is specified as the percentage of the voids in the charge of grinding bodies which the slurry occupies.
TABLE I Power Consumption of the Mill in kw. at Varying Slurry Charges and Varying Mill Speeds Speed in percent of critical Slurry Charge, percent It will be observed in Table I that variations in the percentages of the voids in the charge of grinding bodies, which are occupied by the slurry, have little elfect on the power consumption when the mill is rotated at normal speeds. At the critical speed, the power consumption reaches a maximum when the slurry occupies about 60% of the voids in the charge of grinding bodies and it has been found that, at super-critical speeds, the power consumption reaches a maximum when the slurry occupies 60% to 70% of the voids in the charge of grinding bodies.
In another series of tests, the slurry occupied 70% of the voids among the grinding bodies at all times and the yield value of the slurry and the speed of rotation of the mill were varied. The results of these tests are shown in Table II.
TABLE II Consumption in kw. at Various Yield Values and at Varying M ill Speeds An examination of the test results contained in Table II shows that variations in the yield value of the slurry have a comparatively little eifect on the power consumption at normal mill speeds. At the critical speeds and at 140% of the critical speed, the power consumption is a maximum, when the slurry has a yield value of 600 dynes/om. while, with a mill speed of of the critical speed, the
maximum power consumption occurs when the slurry has a yield value of 800 dynes/cm.'-. The test results with the mill operating at critical and super-critical speeds indicate that the yield value of the slurry isof substantial importance. If the slurry has too high a viscosity, the grinding bodies and slurry stick to the mill lining by centrifugal action so that grinding is impossible. The consistency of slurry should, accordingly, be slightly thinner than that which results in the grinding bodies and slurry being held against the mill lining by centrifugal action.
In the practice of the method of the invention, it is desirable that the introduction of Water into the mill be automatically regulated on the basis of a continuous determination of the consistency of the mill slurry and such regulation may be accomplished by the use of the viscometer and associated control devices disclosed in the British patent specification 624,468.
In the practice of the new method, the use of mills of close to a central partition separating the compartments and inlets for feed at opposite ends. The use of the separate discharge outlets from the two compartments permits the consistency of the slurry in the compartments to be separately checked. The material discharged from one compartment may be conveyed to. the inlet of the other or the grinding in either or both compartments may be in closed circuit.
the well-known grate-discharge type is preferred and it is advantageous to employ a mill, in which the ratio of length to diameter ranges from 00.5 to 2 and is preferably about 1. Such a grate-discharge mill may have discharge slots in a plane end wall or through the cylindrical shell of the mill, the slots being of a Width small enough to prevent the grinding bodies from passing but wide enough to permit the ground material to be discharged for collection in a hopper below the mill. Such a mill is to be distinguished from an overflow mill, in which the ground material is discharged through an axial hollow trunnion. Grate-discharge mills, which may be advantageously employed in practicing the method, may be divided into two compartments having discharge slots I claim:
A method of grinding a slurry of mineral material which comprises introducing into a rotary drum a charge of non-metallic grinding bodies and a quantity of slurry sutficient to occupy from to of the voids among the bodies and of a yield value in the range of 300 to 900 dynes/cm.-, rotating the drum at a speed in the range from just below the critical speed to about of the critical speed, withdrawing from the mill slurry containing particles below a selected size, and introducing into the mill slurry of a yield value within the specified range at a rate sufiicient to maintain the specified quantity of slurry within the mill.
References Cited in the file of this patent UNITED STATES PATENTS 2,754,067 Klugh July 10, 1956 2,766,940 Weston Oct. 16, 1956 2,824,701 Vester et a1. Feb. 25, 1958 OTHER REFERENCES Taggart, Handbook of Mineral Dressing, pages 5-122- 5-l25 (copy in Scientific Library).
US133559A 1960-08-29 1961-08-24 Method of wet-grinding in a rotary drum Expired - Lifetime US3117733A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4044107A (en) * 1973-11-16 1977-08-23 Davy Powergas, Inc. Process for the manufacture of wet process phosphoric acid using wet-grinding of the phosphate rock feed
US4287233A (en) * 1979-02-13 1981-09-01 Basf Aktiengesellschaft Manufacture of acicular cobalt-containing magnetic iron oxide
US4613084A (en) * 1983-06-28 1986-09-23 Babcock-Hitachi Kabushiki Kaisha Process for producing a coal-water slurry

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2754067A (en) * 1950-05-26 1956-07-10 Monsanto Chemicals Wet-grinding apparatus
US2766940A (en) * 1954-04-05 1956-10-16 Weston David Ball mill feed control
US2824701A (en) * 1952-11-21 1958-02-25 Smidth & Co As F L Method of and apparatus for multiple stage wet grinding

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2754067A (en) * 1950-05-26 1956-07-10 Monsanto Chemicals Wet-grinding apparatus
US2824701A (en) * 1952-11-21 1958-02-25 Smidth & Co As F L Method of and apparatus for multiple stage wet grinding
US2766940A (en) * 1954-04-05 1956-10-16 Weston David Ball mill feed control

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4044107A (en) * 1973-11-16 1977-08-23 Davy Powergas, Inc. Process for the manufacture of wet process phosphoric acid using wet-grinding of the phosphate rock feed
US4287233A (en) * 1979-02-13 1981-09-01 Basf Aktiengesellschaft Manufacture of acicular cobalt-containing magnetic iron oxide
US4613084A (en) * 1983-06-28 1986-09-23 Babcock-Hitachi Kabushiki Kaisha Process for producing a coal-water slurry

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