US3042557A - Method of heating the interior of an enclosure - Google Patents

Method of heating the interior of an enclosure Download PDF

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US3042557A
US3042557A US806946A US80694659A US3042557A US 3042557 A US3042557 A US 3042557A US 806946 A US806946 A US 806946A US 80694659 A US80694659 A US 80694659A US 3042557 A US3042557 A US 3042557A
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tube
fuel
inside surface
charge
heating
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US806946A
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Roy L Chenault
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United States Steel Corp
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United States Steel Corp
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/34Methods of heating
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/08Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for tubular bodies or pipes

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  • An object of the invention is to provide a heating method which momentarily develops an extremely high temperature within an enclosure, useful for example for casehardening the inside surface of a metal tube.
  • a further object is to provide an improved casehardening method applicable to metal tubes in which the inside surface of the tube is heated momentarily above its critical temperature and immediately quenched by conduction of heat to other regions of the tube.
  • a more specific object is to provide an improved casehardening method in which a suitable fuel is charged into a tube along with sufiicient oxygen for complete combustion, the ends of the tube are sealed, and the charge ignited, whereby the inside surface is heated momentarily above its critical temperature and immediately quenched by conduction of heat away from this surface.
  • FIGURE 1 is a somewhat diagrammatic longitudinal sectional view of a tube prepared for heating in accordance with my method.
  • FIGURE 2 is a similar view showing a modification.
  • FlGURE 1 shows a metal tube which contains a finely divided solid fuel charge 1'2, for example aluminum or magnesium in powder or wool form.
  • a gaseous fuel such as propane or butane, or other recently developed high energy solid, liquid or gaseous fuels.
  • Plugs 13 and 14 are fitted into the left and right ends respectively of the tube.
  • Plug 13 contains a bore 15 into which is threaded a pipe 16 containing a valve 17.
  • the tube is evacuated and charged through pipe 16 with a calculated quantity of oxygen for complete combustion of the fuel, after which valve 17 is closed. if a gaseous fuel is used, it is also introduced through pipe 16.
  • Plug 14 contains a bore 18 and counterbore 19.
  • a cap 20 is threadedly engaged with plug 14 and covers the countcrbore.
  • the cap contains a bore 21 into which is fitted an electrically insulating seal 22, an electrode 23 and an ignition means 24, such as a conventional photographic flash bulb illustrated for igniting solid fuels.
  • the cap and electrode are connected to a suitable current source indicated at 25 for firing the flash bulb.
  • the tube When the fuel charge 12 is in powder form, the tube is mounted in a conventional lathe or equivalent mechanism for spinning it on its longitudinal axis and thus distributing the powder uniformly over the inside surface by centrifugal force.
  • the end of bore 21 contains an intermediate igniter 26 preferably of ahuninum or magnesium wool.
  • the flash bulb 24 fires, it ignites the intermediate igniter, which in turn ignites the fuel charge.
  • the fuel charge is aluminum or magnesium wool, it is not necessary to rotate the tube and the intermediate igniter can be omitted, since the fuel charge is exposed directly to the flash bulb.
  • Another possibility with a powdered fuel charge is to direct the bore 21 obliquely at the charge to expose the charge directly to the flash bulb and again omit the intermediate igniter.
  • the ignition means 24 can be a conventional spark plug.
  • the purpose of mounting the ignition means in a separate chamber provided by the counterbo-re 1 and cap 20 is that otherwise the high temperature developed when the fuel burns tends to fuse the base and seal. Thus considerable trouble would be encountered in reconditioning the equipment for further use.
  • FIGURE 2 shows a modification in which an auxiliary chamber 27 is connected to pipe 16 at the left end of tube 10.
  • This chamber can contain part of the oxygen supply and thus lower the pressure within the tube 16 while maintaining the necessary quantity of oxygen.
  • An auxiliary oxygen supply can also serve as a means to regulate the rate of burning and thus control both maximum temperature and maximum pressure obtained for a given fuel charge representing a given amount of energy to be dissipated.
  • the range of aluminum or magnesium for pnactical use as fuel in casehardening the inside of a steel tube is about 10 to grams per square foot of surface.
  • the lower limit of the fuel charge is determined by the minimum which produces a useful hardness increase and may involve an extremely thin case.
  • the upper limit of the charge is determined by the maximum which does not cause burning or fusing of the tube surface.
  • the oxygen charged preferably is substantially the quantity required for complete combustion of the fuel without appreciable excess.
  • the case characteristics can be varied by varying the size and shape of powdered fuel particles, as well as the quantity. In general coarser mesh powder burns more slowly than finer mesh, and granular particles more slowly than flaky.
  • the tube can be quenched in water or oil if more rapid cooling is needed.
  • My instantaneous heating method also produces momentary high pressures within an enclosure at the same instant the temperature is high. Such pressure may also have a beneficial effect along with the temperature.
  • An example is when my heating method is used in the coating of a surface with high melting point enamels, plastics or the like. Such coatings are used to make porous materials impermeable, and the application of pressure along with temperature tends to force the sealing material into the pores of the surface to produce a better bond and a more permanent coating.
  • My method may also be utilized to induce chemical reactions that occur under the simultaneous application of high pressure and high temperature.
  • Example I As a specific example of my method, I selected a tube of A.I.-S.I. 1045 steel 10 inches long, 1 /2. inches inside diameter, and having an initial hardness of 20 to 25 Reel- Well C. I introduced a fuel charge of 4 grams of minus 60 mesh powdered aluminum along with oxygen at a pressure of p.s.i.g. at 75 F. I prepared the tube as shown in FIGURE 1, spun it in a lathe to distribute the fuel charge, and fired the ignition means. Subsequently I found that the inner surface of the tube had acquired areas hardened to about 55 to 65 Rockwell C.
  • Example 11 As a further example, I introduced to a similar tube a fuel charge of 8 grams of minus 60 mesh powdered magnesium along with oxygen at a pressure of p.s.i.g. at 75 F. I prepared the tube, spun it and fired the ignition means as in the first example. Subsequently I found that the inner surface had acquired a case approximately & inch deep with a hardness of about 55 to 65 Rockwell C. I found magnesium preferable to aluminum for the reason that I was able to attain a more uniform case with magnesium. I attribute this result to the higher melting point of MgO (5072 F.) compared with Al O (3722 F). The latter forms droplets which tend to create hot spots when they solidify. This characteristic is not observed with MgO, presumably because of its higher melting point.
  • a method of casehardening the inside surface of a metal tube comprising introducing to the tube a fuel charge along with sufficient oxygen for complete combustion of the fuel, sealing the ends of the tube, igniting the charge to heat the inside surface momentarily above its critical temperature, and quenching the inside surface by conduction of heat therefrom.
  • a method of casehardening the inside surface of a steel tube comprising introducing to the tube a finely divided solid fuel charge of the group consisting of aluminum, magnesium and combinations thereof in the amount of to 75 grams of fuel per square foot of surface, along with suflicient oxygen for complete combustion of the fuel, sealing the ends of the tube, igniting the charge to heat the inside surface momentarily above its critical temperature, and quenching the inside surface by conduction of heat therefrom.
  • a method of casehardening the inside surface of a steel tube comprising introducing to the tube a finely divided powdered solid fuel charge of the group consisting of aluminum, magnesium and combinations thereof in the amount of 10 to grams of fuel per square foot of surface, along with sufficient oxygen for complete combustion of the fuel, sealing the ends of the tube, spinning the tube on its longitudinal axis to distribute the fuel charge over the inside surface, igniting the charge to heat the inside surface momentarily above its critical temperature, and quenching the inside surface by conduction of heat therefrom.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Liquid Carbonaceous Fuels (AREA)

Description

July 3, 1962 R. CHENAULT 3,042,557
METHOD OF HEATING THE INTERIOR OF AN ENCLOSURE Filed April 16, 1959 IN V EN TOR.
ROY I. CHE/VAULT ATT'ORNEY 3,042,557 Patented July 3, 1962 3,042,557 METHOD OF HEATING THE INTERIOR OF AN ENCLOSURE Roy L. Chenault, Seneca, Pa., assignor to United States Steel Corporation, a corporation of New Jersey Filed Apr. 16, 1959, Ser. No. 806,946 3 Claims. (Cl. 148-144) This invention relates to an improved method of heating the interior of an enclosure.
An object of the invention is to provide a heating method which momentarily develops an extremely high temperature within an enclosure, useful for example for casehardening the inside surface of a metal tube.
A further object is to provide an improved casehardening method applicable to metal tubes in which the inside surface of the tube is heated momentarily above its critical temperature and immediately quenched by conduction of heat to other regions of the tube.
A more specific object is to provide an improved casehardening method in which a suitable fuel is charged into a tube along with sufiicient oxygen for complete combustion, the ends of the tube are sealed, and the charge ignited, whereby the inside surface is heated momentarily above its critical temperature and immediately quenched by conduction of heat away from this surface.
In the drawing:
FIGURE 1 is a somewhat diagrammatic longitudinal sectional view of a tube prepared for heating in accordance with my method; and
FIGURE 2 is a similar view showing a modification.
FlGURE 1 shows a metal tube which contains a finely divided solid fuel charge 1'2, for example aluminum or magnesium in powder or wool form. Alternatively I can substitute a gaseous fuel, such as propane or butane, or other recently developed high energy solid, liquid or gaseous fuels. Plugs 13 and 14 are fitted into the left and right ends respectively of the tube. Plug 13 contains a bore 15 into which is threaded a pipe 16 containing a valve 17. The tube is evacuated and charged through pipe 16 with a calculated quantity of oxygen for complete combustion of the fuel, after which valve 17 is closed. if a gaseous fuel is used, it is also introduced through pipe 16. Plug 14 contains a bore 18 and counterbore 19. A cap 20 is threadedly engaged with plug 14 and covers the countcrbore. The cap contains a bore 21 into which is fitted an electrically insulating seal 22, an electrode 23 and an ignition means 24, such as a conventional photographic flash bulb illustrated for igniting solid fuels. The cap and electrode are connected to a suitable current source indicated at 25 for firing the flash bulb.
When the fuel charge 12 is in powder form, the tube is mounted in a conventional lathe or equivalent mechanism for spinning it on its longitudinal axis and thus distributing the powder uniformly over the inside surface by centrifugal force. In this event the end of bore 21 contains an intermediate igniter 26 preferably of ahuninum or magnesium wool. When the flash bulb 24 fires, it ignites the intermediate igniter, which in turn ignites the fuel charge. When the fuel charge is aluminum or magnesium wool, it is not necessary to rotate the tube and the intermediate igniter can be omitted, since the fuel charge is exposed directly to the flash bulb. Another possibility with a powdered fuel charge is to direct the bore 21 obliquely at the charge to expose the charge directly to the flash bulb and again omit the intermediate igniter. When a gaseous fuel is used, the ignition means 24 can be a conventional spark plug. The purpose of mounting the ignition means in a separate chamber provided by the counterbo-re 1 and cap 20 is that otherwise the high temperature developed when the fuel burns tends to fuse the base and seal. Thus considerable trouble would be encountered in reconditioning the equipment for further use.
FIGURE 2 shows a modification in which an auxiliary chamber 27 is connected to pipe 16 at the left end of tube 10. This chamber can contain part of the oxygen supply and thus lower the pressure within the tube 16 while maintaining the necessary quantity of oxygen. An auxiliary oxygen supply can also serve as a means to regulate the rate of burning and thus control both maximum temperature and maximum pressure obtained for a given fuel charge representing a given amount of energy to be dissipated.
The range of aluminum or magnesium for pnactical use as fuel in casehardening the inside of a steel tube is about 10 to grams per square foot of surface. The lower limit of the fuel charge is determined by the minimum which produces a useful hardness increase and may involve an extremely thin case. The upper limit of the charge is determined by the maximum which does not cause burning or fusing of the tube surface. The oxygen charged preferably is substantially the quantity required for complete combustion of the fuel without appreciable excess. The case characteristics can be varied by varying the size and shape of powdered fuel particles, as well as the quantity. In general coarser mesh powder burns more slowly than finer mesh, and granular particles more slowly than flaky. The tube can be quenched in water or oil if more rapid cooling is needed.
My instantaneous heating method also produces momentary high pressures within an enclosure at the same instant the temperature is high. Such pressure may also have a beneficial effect along with the temperature. An example is when my heating method is used in the coating of a surface with high melting point enamels, plastics or the like. Such coatings are used to make porous materials impermeable, and the application of pressure along with temperature tends to force the sealing material into the pores of the surface to produce a better bond and a more permanent coating. My method may also be utilized to induce chemical reactions that occur under the simultaneous application of high pressure and high temperature.
Example I As a specific example of my method, I selected a tube of A.I.-S.I. 1045 steel 10 inches long, 1 /2. inches inside diameter, and having an initial hardness of 20 to 25 Reel- Well C. I introduced a fuel charge of 4 grams of minus 60 mesh powdered aluminum along with oxygen at a pressure of p.s.i.g. at 75 F. I prepared the tube as shown in FIGURE 1, spun it in a lathe to distribute the fuel charge, and fired the ignition means. Subsequently I found that the inner surface of the tube had acquired areas hardened to about 55 to 65 Rockwell C.
Example 11 As a further example, I introduced to a similar tube a fuel charge of 8 grams of minus 60 mesh powdered magnesium along with oxygen at a pressure of p.s.i.g. at 75 F. I prepared the tube, spun it and fired the ignition means as in the first example. Subsequently I found that the inner surface had acquired a case approximately & inch deep with a hardness of about 55 to 65 Rockwell C. I found magnesium preferable to aluminum for the reason that I was able to attain a more uniform case with magnesium. I attribute this result to the higher melting point of MgO (5072 F.) compared with Al O (3722 F). The latter forms droplets which tend to create hot spots when they solidify. This characteristic is not observed with MgO, presumably because of its higher melting point.
From the foregoing description it is seen that my invention affords a simple and effective method of flash-heating the interior of an enclosure. The method is especially If: applicable to casehardening as described in the examples, although it may have other applications.
While I have shown and described certain preferred embodiments of my invention, it is apparent that other modifications may arise. Therefore, I do not wish to be limited to the disclosure set forth but only by the scope of the appended claims.
I claim:
1. A method of casehardening the inside surface of a metal tube comprising introducing to the tube a fuel charge along with sufficient oxygen for complete combustion of the fuel, sealing the ends of the tube, igniting the charge to heat the inside surface momentarily above its critical temperature, and quenching the inside surface by conduction of heat therefrom.
2. A method of casehardening the inside surface of a steel tube comprising introducing to the tube a finely divided solid fuel charge of the group consisting of aluminum, magnesium and combinations thereof in the amount of to 75 grams of fuel per square foot of surface, along with suflicient oxygen for complete combustion of the fuel, sealing the ends of the tube, igniting the charge to heat the inside surface momentarily above its critical temperature, and quenching the inside surface by conduction of heat therefrom.
3. A method of casehardening the inside surface of a steel tube comprising introducing to the tube a finely divided powdered solid fuel charge of the group consisting of aluminum, magnesium and combinations thereof in the amount of 10 to grams of fuel per square foot of surface, along with sufficient oxygen for complete combustion of the fuel, sealing the ends of the tube, spinning the tube on its longitudinal axis to distribute the fuel charge over the inside surface, igniting the charge to heat the inside surface momentarily above its critical temperature, and quenching the inside surface by conduction of heat therefrom.
References Cited in the file of this patent UNITED STATES PATENTS 829,117 Maxim Aug. 21, 1906 2,318,145 Emery et al May 4, 1943 2,448,203 Africano Aug. 31, 1948 2,464,179 Hickman et al Mar. 8, 1949 2,596,981 Ohennault et a1 May 20, 1952 2,669,511 Whitney Feb. 16, 1954 OTHER REFERENCES Johnson: Metal Working and Heat-Treatment Manual, Volume III, Lib. Call No. TS 205 vc; pages 89, 106, 107, and 121, dated 1948.

Claims (1)

1. A METHOD OF CASEHARDENING THE INSIDE SURFACE OF A METAL TUBE COMPRISING INTRODUCING TO THE TUBE A FUEL CHARGE ALONG WITH SUFFICIENT OXYGEN FOR COMPLETE COMBUSTION OF THE FUEL, SEALING THE ENDS OF THE TUBE, IGNITING THE CHARGE TO HEAT THE INSIDE SURFACE MOMENTARILY ABOVE ITS CRITIAL TEMPERATURE, AND QUENCHING THE INSIDE SURFACE BY CONDUCTION OF HEAT THEREFROM.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3421953A (en) * 1966-10-07 1969-01-14 Atomic Energy Commission Carbide deposition on tantalum
US4503959A (en) * 1981-08-28 1985-03-12 Dana Corporation Clutch lever and adjustment method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US829117A (en) * 1904-05-24 1906-08-21 Du Pont Powder Co Erosion-meter.
US2318145A (en) * 1939-10-30 1943-05-04 Axelson Mfg Co Method of flame hardening tubular structures
US2448203A (en) * 1946-01-18 1948-08-31 Us Sec War Powder tester
US2464179A (en) * 1943-09-02 1949-03-08 Clarence N Hickman Smokeless powder tester
US2596981A (en) * 1949-10-05 1952-05-20 United States Steel Corp Method for nitriding metallic surfaces
US2669511A (en) * 1950-04-06 1954-02-16 Jr Loren L Whitney Method for refining ferrous metals

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US829117A (en) * 1904-05-24 1906-08-21 Du Pont Powder Co Erosion-meter.
US2318145A (en) * 1939-10-30 1943-05-04 Axelson Mfg Co Method of flame hardening tubular structures
US2464179A (en) * 1943-09-02 1949-03-08 Clarence N Hickman Smokeless powder tester
US2448203A (en) * 1946-01-18 1948-08-31 Us Sec War Powder tester
US2596981A (en) * 1949-10-05 1952-05-20 United States Steel Corp Method for nitriding metallic surfaces
US2669511A (en) * 1950-04-06 1954-02-16 Jr Loren L Whitney Method for refining ferrous metals

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3421953A (en) * 1966-10-07 1969-01-14 Atomic Energy Commission Carbide deposition on tantalum
US4503959A (en) * 1981-08-28 1985-03-12 Dana Corporation Clutch lever and adjustment method

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