US2978744A - Method and apparatus for forming fibers - Google Patents
Method and apparatus for forming fibers Download PDFInfo
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- US2978744A US2978744A US533289A US53328955A US2978744A US 2978744 A US2978744 A US 2978744A US 533289 A US533289 A US 533289A US 53328955 A US53328955 A US 53328955A US 2978744 A US2978744 A US 2978744A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/06—Manufacture of glass fibres or filaments by blasting or blowing molten glass, e.g. for making staple fibres
Definitions
- This invention relates to method and apparatus for forming fibers and more especially to a method and apparatus for forming fine fibers by direct engagement of gaseous attenuating blasts with fine streams or primaries of molten fiber-forming mineral material.
- Fibers have heretofore been formed by several methods utilizing blasts of gases for attenuating heat-softenable mineral material to fibers.
- One of the earlier methods of forming slag or mineral wool comprised fiowing a comparatively large stream of molten slag or argillaceous rock from a furnace and directing a jet of steam against the stream, atomizing the stream to form relatively coarse fibers commercially known as slag or rock wool.
- the fibers made by this method were not only very coarse but the end product contained a major proportion of unfiberized material in the form of pellets or shot.
- Glass wool has been manufactured in substantial cornmercial quantities by flowing a plurality of streams verti-' cally from a forehearth and directing steam or com pressed air blasts downwardly in the general direction of flow of the streams and engaging the streams to form fibers.
- Another method that has 'been used involves forming substantially solid primary filaments from streams of glass or other mineral material and feeding the primary filaments in solid form endwise into an intensely hot gaseous blast whereby the heat of the blast softens the filaments and the velocity of the gases of the blast attenuates the softened material to fibers.
- the streams of molten material have been delivered by gravity into gaseous attenuating mediums, or the streams have first been drawn into solid primary filaments and the solid filaments delivered into an intensely hot blast.
- More recent developments include forming a body of molten mineral material into a plurality of radially projected linear bodies by centrifugal forces and engaging the projected bodies with a gaseous blast to form the radially moving bodies into fine fibers.
- Such method or process involves the use of one or more elements rotating at high speeds and hence requires precision equipment .for its successful operation.
- This method of fiber formation is highly eflicient and produces very fine fibers. It appears that the production of extremely fine fibers from the use of centrifugal units is attributable to the use of comparatively fine primaries or streams of the material delivered to the attenuating blast.
- the present invention embraces the provision of a method and apparatus for forming fine streams, elongated 2,978,744 Patented Apr. 11, 1961 and engaging the streams or primaries by a high velocity gaseous blast to attenuate the streams or primaries to fibers.
- Another object of the invention resides in the provision of forehearth and feeder means maintained under pressure whereby a large number of minute streams or bodies of glass or other heat-sottenable material may be projected at controlled fiow rates from opposed directions into an attenuating blast formed of burned gases of combustion at temperatures well above the attenuating temperature of the glass whereby the streams or bodies are attenuated into fine fibers.
- Another object of the invention resides in the provision of a method and apparatus for attenuating fibers wherein molten fiber-forming material is extruded under pressure under controlled conditions through small openings forming fine primary'filaments or bodies which are engaged by a high velocity gaseous blast to form fibers without the use of moving or rotating elements or mechanism.
- Still another object of the invention is the provision of a method and apparatus of forming fibers wherein a comparatively large number of pressureextruded bodies of fiber-forming material are delivered into an attenuating blast wherein comparatively large quantities of fiberforming material are converted to fine fibers with a minimum expenditude of attenuating energy.
- Figure l is a vertical sectional view showing a form of apparatus for carrying out the method of the invention.
- Figure 2 is an enlarged detail sectional view of a portion of the apparatus shown in Figure 1;
- Figure 3 is a bottom plan view of the arrangement shown in Figure 2;
- Figure 4 is a vertical sectional view illustrating another form of'apparatus for carrying out the method of the invention.
- Figure 5 is a bottom plan view of the arrangement shown in Figure 4.
- Figure 6 is an elevational sectional view with certain parts shown in section of another form of apparatus for carrying'out the method of the invention.
- Figure 7 is a bottom plan view of the filament fiber-forming apparatus shown in Figure 6;
- Figure 8' is a view similar to Figure 7 illustrating an and arrangement for delivering an annular-attenuating blast
- Figure 9 is an elevational view with certain parts shown in section of another form of apparatus for'carry ing h artist at h i im Figure is an enlarged sectional view of a portion of the apparatus shown in Figure 9;
- Figure 11 is a bottom plan view of the filament and fibenforming apparatus shown in Figure 9, and
- Figure 12 is a sectional view of a furnace, forehearth and feeder construction for delivering fiber forming material under pressure to an attenuating blast.
- the forms of apparatus illustrated are especially adaptable for forming fine primary filaments, streams or elongated bodies of molten glass which are projected into an attenuating blast and thereby attenuated to very fine fibers. It is to be understood that the method and apparatus of the invention may be used for forming primary filaments and fibers from other heat-softenable materials such as fusible rock, slag or other thermoplastic or wherever the method and arrangement may be found to have utility.
- Figures 1 through 3 illustrate one form of apparatus for carrying out the method of the invention.
- Numeral it designates a melting furnace, tank or receptacle in which is maintained a supply of molten fiber forming material 11 such as glass, slag, fusible rock or other heat softenable mineral material from which fibers may be formed by attenuation.
- molten fiber forming material 11 such as glass, slag, fusible rock or other heat softenable mineral material from which fibers may be formed by attenuation.
- the furnace or receptacle It ⁇ may be formed with a metal casing 12 which is lined with suitable refractory 14 capable of withstanding the high temperatures of the molten glass or other fiber-forming material.
- the furnace or receptacle 10 forms a confined zone or chamber 18 containing the supply of fiber forming material and pressure is impressed in the chamber 18 so that the supply of molten glass or other material is main tained under a static pressure in order to facilitate satisfactory extrusion of the material through comparatively small orifices.
- a means is provided for feeding raw glass batch 20 or other composition of fiber-forming material to be introduced into the chamber 18 and therein reduced to a molten state or condition.
- a cylindrical tube 22 extends from the furnace 10 and disposed interiorly of the tube 22 is a material feeding means in the form of a screw or member 24 which is snugly but rotatably disposed in the tube 22 to prevent reduction in pressure within the chamber 18. It is to be understood that. other forms of means for introducing raw batch into the furnace may be employed if desired.
- the batch feeding means or screw 24 shown in the embodiment in Figure 1 is driven by a motor (not shown) or other suitable means at a speed to deliver or convey the batch 25 into the furnace 10 substantially at the rate that the molten material is extruded from the furnace in a manner hereinafter described.
- a wall or dam 19 in the furnace having an opening through which the glass flows assists in refining the molten glass.
- the batch, after delivery into the chamber 18, may be rendered molten by the application of heat, and burners or heating means 2% may be utilized for this purpose.
- the burners or heating means 28 may be connected with a source (not shown) of combustible mixture such as fuel gas and air delivered to the burners under pressure, the combustible mixture being ignited and burned within the chamber 18.
- the pressure of the burning gases and products of combustion may be utilized to pressurize the chamber 18 or pressure may be impressed in chamber 18 by the introduction of other gases through a ductor tube such as tube 30.
- a regulating valve. 32 which may be manually controlled or an automatic pressure regulator may be employed to regulate the flow of gases under pressure into the chamber '18.
- I V V f When burners 28 are utilized to deliv'er combustible mixture into the chamber 18 to be burned therein, a vent means maybe provided for.th'e chamber 18 equipped with a valve for maintaining the desired 'pressu're' in the chamber.
- the upper wall of the furnace or receptacle 10 is provided with a vent tube 34 equipped with a valve 36 which may be manually or automatically controlled for maintaining a constant pressure in the chamber.
- Figures 1, 2 and 3 illustrate an arrangement for projecting or extruding streams or, primaries of the molten fiber forming material into an attenuating blast in which the molten streams or primaries are attenuated to fibers.
- walls 44 Depending from the furnace 10 are walls 44) and 41 providing, in effect, a forehearth defining a passage, chamber or well 42 arranged to receive molten material from the supply 11 in the chamber 18, The
- a feeder 44 which may be formed of high temperature resistant metal such as platinum rhodium, platinum iridium or other suitable metal or alloy capable of withstanding the high temperatures of the molten material.
- the feeder 44 is formed with orifice means for exuding or extruding fine streams of molten fiber-forming material contained in the passage or chamber 42.
- the feeder 44 is formed with the plurality of tips, nozzles or projections 46, each of which is formed with a small orifice or outlet 48 through which a stream 50 of molten fiber fornu ing material is delivered or extruded under pressure,
- the streams 50 also referred to herein as primaries, primary filaments or elongated bodies, are projected in a substantially horizontal direction or plane as shown in Figures 1 and 2.
- a current of electrical energy may be delivered through the metal feeder 44 to control or regulate the viscosity of the molten material in the feeder so that the material may be extruded at a viscosity to provide primaries most satisfactory for attenuation to fibers.
- the streams 50 under the influence of the substantially constant static pressure in the chamber 18, are projected in a substantially rectilinear direction-for some distance beyond the outlets 48 in the tips 46.
- the streams or primaries 50 are delivered endwise into an attenuating blast.
- a burner having a metal casing 56, the burner being formed with a combustion chamber or confined zone 57 in which a combustible mixture is adapted to be substantially coma pletely burned.
- the chamber 57 is defined by walls59 of suitable refractory capable of withstanding the high temperature of the burning gases in thechamber, the temperature of the'gases being 3000 F. or higher.
- a lower wall of the chamber 57 is.provided with a restricted orifice or outlet 60 which, as shown in Figure 3, is of elongated rectangular character.
- the burner 55 is connected with a tube 62, the latter being connected with supply of combustible mixture such as fuel gas and air. Any suitable fuel gas may be used such as methane, ethane or propane, and the combustible mixture is. delivered by the tube or duct 62 into 'a manifold chamber or passage 64.
- a rear wall 66 of the chamber 57 adjacent the mixture inlet or manifold chamber 64 is formed with plurality small perforations or passages 68 through which the mixture is conveyed into the chamber 57.
- the perforated wall 66 forms a fire or protective screen to avoid or prevent preignition ofithe mixture in the passage 64 or the duct 62.
- the fuel and air mixture may be deliveredinto the chamber'57 under a comparative low pressure of from three to 10 lbs. p.s.i.
- the combus tible mixture is ignited in the chamber 57v and is sub,-
- the blast B from the orifice 60 is projected downwardly in a direction substantially normal to the endtvgise delivery of the primaries or streams 50 into the ast.
- the streams or primaries 50 are attenuated by the blast B to fine fibers F. While the primaries or streams 50 are in a flowable condition as they enter the blast, there may be some chilling or cooling of the streams and increase in viscosity by the air fiow induced by the blast through the space 43 between a wall of the burner and wall 41 of the well 42.
- the increase in viscosity or thickened condition of the streams entering the attenuating blast B provides in each stream a nub or inertia zone from which fibers may be drawn, the heat of the gases of the blast elevating the temperature of the material of the streams whereby the extremities of the streams in the blast are softened or conditioned so that they are drawn by the blast into long fine fibers.
- fine streams or primaries 50 may be delivered into the high temperature blast B so that the extremely fine fibers of a diameter of two microns or less may be economically produced in commercial quantities. While it is advantageous to utilize a blast of a temperature above the attenuating temperature of the fiber forming material in order to form fine fibers, it is to be understood that the streams or primaries 50 may be delivered into a blast of steam or compressed air moving in a direction normal or perpendicular to the paths of the primaries projected from the outlets or orifice 48. However, fibers attenuated by steam or air blasts are usually not as fine as those produced by the hot blast method.
- the newly formed fibers F entrained in the blast move downwardly as shown in Figure l and may be collected in a mass 69 upon the upper flight 70 of an endless foraminous conveyor 71, the flight 70 moving in a righthand direction as-viewed in Figure 1.
- a box or receptacle 73 may be disposed beneath the upper flight 70 of the conveyor in the path of the descending fibers F providing a chamber 74.
- a duct 75 connects the chamber 74 with a suction blower (not shown) for establishing a suction or subatmospheric pressure in chamber 74 to assist in collecting the fibers upon the conveyor flight 70 and to convey away spent gases of the attenuating blast.
- the mass 69 of fibers may be passed between compression or sizing rolls 77 for predetermining the thickness of the mat M formed from the fibers.
- applicators 80 may be disposed adjacent opposite sides of the descending fibers F for projecting binder 82 or other fiber coating material on to the fibers.
- the binder may be of any type but a thermo-setting material is preferred such as phenol formaldehyde or urea formaldehyde.
- the mat of fibers treated with the bonding agent or material may be conveyed through an oven or curing zone to set the binder in the fibrous mat.
- the bathe '45 may be secured to the casing wall of the burner 55 and may be made adjustable if desired.
- Figures. 4 and 5 illustrate modified form of apparatus for forming heat-softenable mineral material tofibers.
- Burner 78 is similar to the burner 55 and is inclusive of a metal'casing' 79 in which is formed a combustion zone of chamber 83 defined by walls 84 of refractory.
- the lower wall of the chamber 83 is formed with a restricted outlet or orifice 86 which is of elongated character as shown in Figure 5.
- the burner 78 is connected with a tube or pipe 88 adapted to convey a combustible mixture of fuel gas and air into the combustion chamber or confined zone 83.
- the rear wall 89 of the combustion chamber 83 is formedwith a plurality of small openings or passages to convey the mixture into the chamber, the perforated wall providing a fire screen to prevent preignition of the mixture in the inlet 87 and the supply pipe 88.
- the burner 78 is deposed between the downwardly extending material conveying passages or wells 42a and 42b as shown in Figure 4.
- a wall of each of the depending portions of the receptacle defining the chambers 42a and 42b is provided with a feeder or bushing 92 which may be made of metal or alloy capable of withstanding the intense heat of the molten material.
- a feeder or bushing 92 which may be made of metal or alloy capable of withstanding the intense heat of the molten material.
- Such alloys as platinum rhodium or platinum iridium have been found satisfactory for the purpose.
- Each of the feeders 92 is formed with a plurality of tips, nozzles or projections 94 and each of the tips is provided with an orifice or outlet 96 through which molten material from the wells 42a and 42b is projected or exuded in a fine stream 50.
- the projections or tips 94 are disposed so as to project the streams 50 in substantially horizontal directions and endwise into the downwardly projected blast as shown in Figure 4.
- the groups of projections 94 of the feeders are disposed in opposed relation whereby the streams 50 from the groups of tips are projected in opposite directions in entering the blast.
- each orifice 96 of one group is disposed in alignment with an orifice 96 in the opposite group, but it is to be understood that the orifices of one group may be disposed. in staggered relation with respect to the orifices in the'opposite group i so that each stream of molten material may enter a different zone of the blast.
- molten material may be introduced into a single elongated blast projected through the slot or restricted orifice 86.
- the pressure impressed upon the supply of molten material is effective on the material in the wells 42a and 42b and feeders 92 to project the streams 50 endwise into the blast at a substantial velocity.
- the inner walls 76 of the well constructions are disposed in close relation to the side walls of the burner casing 79 in order to restrict the how of induced air along the blast.
- casings 76a and 76b may be spaced at greater distances from the burnerwall and bafiles or other means may be disposed between the burner walls and the casings 76a and 76b for restricting and controlling the flow of induced air alongthe blast.
- the induced air chills the streams 50 rendering them more viscous.
- the viscous condition of the streams or primaries 50 may be controlled and the streams or primaries delivered into the blast under optimum conditions to obtain the most efficient attenuation of the streams or primaries.
- Figures 6 and 7 illustrate another form of apparatus for delivering streams or primaries of molten material in radial directions into a substantially annular gaseous attenuating blast.
- This arrangement is inclusive of a pressurized melting furnace, tank or receptacle 100 in which is contained a supply of molten fiber forming material 1111.
- the glass or other mineral fiber-forming material may be introduced into the furnace in the shape of preformed spheres or marbles 102.
- a tube 104 extending upwardly from the furnace contains a supply of glass marbles.
- a member 105 associated with the furnace 100 is provided with a rotary valve 197 adapted to successively deliver the marbles from the tube 104 through a passage 108 into the furnace without afi'ecting the pressure in the melting chamber 112.
- Heating means in the form of burners 110 are disposed in the chamber 112 for melting the marbles.
- Pressure above atmospheric pressure is impressed in the chamber 112. This may be accomplished by the pres sure of the burning gases from the burners 110 which may be supplemented by gases under pressure introduced into the chamber through a pipe or duct 114.
- a valve 115 is associated with a pipe 114 for controlling the flow of pressure gases into the closed pressurized chamber 112.
- the forehearth 120 in the embodiment illustrated depends from the furnace construction .1110.
- the forehearth 120 extends downwardly and outwardly in an annular formation providing an annularly shaped Well 124.
- a portion 123 is formed with an annularly shaped feeder 126.
- the feeder 126 is fashioned with a plurality of outwardly and radially extending tips or projections 128 each of which is formed with an orifice 130 through which streams 50b are projected under the influence of superatmospherlc pressure on the supply of glass or other material in the chamber 112.
- a substantially annular gaseous blast is provided adapted to engage the streams 59b to attenuate the streams to fibers.
- the blast establishing means is inclusive of four burners 135 each being shaped as a circular ring sector, which in assembled relation provide a substantially annular burner arrangement.
- Each of the burners 135 includes a metal casing 137, the interior which is lined with refractoryj139 shaped to define an internal combustion chamber or confined zone 14th.
- a wall of each burner is formed with a restricted outlet or orifice means 142 of arcuate shape through which burned gases or products of combustion from the chamber 140 are discharged as a high velocity blast of a temperatureabove the attenuating temperature of the fiber forming material.
- a combustible mixture is delivered into the combustion chamber 140 of each burner "through tubes 145 which are connected with a supply of combustible mixture such as fuel gas and air.
- the mixture is burned in the chamber 140 under confined conditions, the burning gases undergoing great expansion attaining a temperature of 3000 F. or more before they are discharged at high velocities through the restricted orifice 142.
- the several arcuately shaped orifices in effect provide a substantially annular blast.
- the annular blast emanating from the orifice means 142 of the burners engages the streams or primaries from the orifices 13%) in. a direction substantially normal to the flow of the streams from the annular feeder 126.
- the amount'of air flow induced by the velocity of the gaseous blast may-becontrolled byan annular plate O u 148 disposed in the path of fiow of air between the feeder 126 and the inner walls of the burner casings 137.
- the width of the plate 148 and its position, may be varied or adjusted to provide the desired restriction to the induced air flow.
- the streams 50b move radially in substantially horizontal directions under the influence of the pressure impressed on the molten material.
- the attenuated fibers are entrained in the annular blast and are carried downwardly by the blast in the form of the circular cylindrically shaped beam or column 150 of fibers.
- the fibers of the beam may be collected upon an upper flight of a foraminous conveyor of the character shown in the Figure 1.
- a suction chamber 74' is provided beneath the conveyor flight 70' in order to assist in collecting the fibers on the conveyor and to carry away spent gases of the blast.
- Figure 8 is a bottom plan view of an arrangement simliar to that shown in Figure 7 with the burner construction formed as a continuous annulus.
- the burner 135 is formed with a continuous annular-shaped combustion chamber from which burned gases or products of combustion are discharged through a continuous annularly shaped restricted orifice 152.
- Streams of molten fiber-forming material are delivered through the orifices formed in projections 128 in the manner shown in Figure 6.
- Combustible mixture is introduced into the combustion chamber of the burner 135' through pipes connected with a supply of fuel gas and air.
- the streams 50b are attenuated by the annular blast from the orifice 152 in the same manner described in connection with Figures 6 and 7. i
- FIG 9 is a view similar to Figure 1 illustrating another form of apparatus'for carrying on the method of the invention.
- the melting, furnace 10c in which glass batch is adapted to be melted is arranged to receive glass batch through the use of means such as those illustrated in Figures 1 and 6.
- the furnace 10c is provided with a forehearth or depending portion 155.
- the construction 1155 is formed with leg portions 158 and 159.
- the portion 158 is formed with a downwardly extending passage 160 and the portion 159 is formed with a similarly shaped downwardly extending passage 162.
- the depending portions 158 and 159 support an annularlyshaped portion 161.
- the portion 161 is formed with anannular chamber 163 which is in communication with both passages or wells 161 and 162 and receive through which the molten material in the annular chamber 163 is extruded under pressure to form streams or primaries 500 of the fiber-forming material.
- the molten material in the passages or chambers 160 and 162 and the annular chamber 163 is under a pressure greater than the normal head of glass in the chambers 160 and 162.
- the portion 155 of the forehearth is formedwith a circular cylindrical chamber or bore 174.
- Extending through an opening in the upper wall of the melting furnace 10c is a shaft 176 which is equipped with a collar 177 to position the rod or shaft The shaft 176 extends into the chamber 174 and is equipped with a' pair of propeller or screw-like members 180 and 182. .
- the blades of members 181) and 182 are of a spiral pitch such that rotation of members 180 and 182 inthe proper direction impresses downwardly acting pressure upon the glass or other molten fiber forming material contained in the passages or chambers 160, 162
- The-shaft 176 may bedrivenby any electric otor (not shown) or by other suitable means torotate the members 130 and 182.
- hearth are pressurized in any suitable manner. burning gases from the burners 220 and 222 may be uti- Through this arrangement, a substantial pressure is exerted upon the glass or molten material contained in the annular feeder 164, the pressure being effective to extrude the fine streams 500 in substantially horizontal directions into an attenuating blast as illustrated in Figure 10.
- the pressure may be controlled by regulating the speed of rotation of the members 180 and 182.
- a burner or blast producing means 186 Arranged in the space between the depending leg portions 158 and 159 of the material feeding means is a burner or blast producing means 186.
- the burner 186 is inclusive of a metal shell 188 which is lined with a high temperature refractory 189 defining a combustion chamber or confined zone 190.
- the rear of the burner is provided with a member 193 formed with a manifold chamber 195 into which a combustible mixture is delivered through a mixture supply pipe 197.
- a rear wall 200 of the chamber 190 is formed with a large number of small channels or passages 202 through which the mixture is delivered into the chamber 190, the wall 200 forming a fire screen to avoid preignition in the manifold 195.
- the depending end zone of the burner 186 is formed with a circular orifice 205 of restricted character in that its cross sectional area is one-quarter to oneeighth of the cross sectional area of the chamber 190.
- the combustible mixture is delivered to the combustion chamber 190 under a comparably low pressure and is substantially completely burned within the chamber 190.
- the burning gases undergo great expansion and are heated to a temperature of 3000 F. or more which is above the attenuating temperature of the glass.
- the burned gases are projected from the chamber 190 through the restricted orifice 205 to form a substantially circular cylindrical blast B2 into which the streams or primaries 500 are projected, the blast moving downwardly in a direction substantially normal to the plane of the paths om movement of the streams 500 into the blast.
- the streams or primaries 50c are attenuated to fine fibers by the heat and velocity of the gases of the blast.
- the attenuated fibers F are entrained in the downwardly projected blast and are collected upon the upper flight 700 of a foraminous conveyor in the manner described in connection with the form of the apparatus shown in Figure 1.
- a suction chamber 74c is disposed beneath the fiber collecting region to assist in collecting the fibers and to carry awa spent gases of the blast.
- pressurizing means 180 and 182 shown in Figure 9 may be used with the other forms of apparatus disclosed.
- the batch or glass feeding means and the pressurizing means shown in Figures 1 and 6 may be utilized in the construction shown in Figure 9 in lieu of or supplementing the mechanical pressurizing means shown in Figure 9.
- Figure 12 illustrates another form of apparatus of the invention.
- the melting furnace 210 is provided with a horizontally extending forehearth construction 212.
- Glass batch is introduced into the chamber 214 of the furnace through a tube or pipe 216 provided with a pair of spaced valves 218 operable to admit the material into the chamber without appreciable variation of pressure in the chamber.
- Burners 220 or other suitable heating means are utilized to reduce the batch material to a molten state.
- Additional burners or heating means 222 may be disposed in the forehearth in order to maintain the glass at the desired viscosity therein.
- the furnace and fore- The lized for the purpose, or gases under pressure may be conveyed intothe chamber 214 by means of a pipe 226.
- Valve means 228-associated with the pipe 226, which pressure regulating type, may be used to control or regulate the pressure in the chamber 214.
- a depending wall portion 230 disposed between the furnace chamber 214 and the forehearth forms a skimmer block, the molten material flowing through the passage 232 from melting chamber into the forehearth.
- One or more vent openings 234 may be formed in the Wall 230 for equalizing the pressures in the chamber 214 and in the forehearth 212.
- a wall of the forehearth 212 is provided with a feeder or bushing 236 having nozzles or projections 238 through which streams or primaries 50d are projected into a blast B3.
- the blast is formed of combustible gases burned within a chamber or confined zone 57d of a burner 55d.
- the burner illustrated in Figure 12 is of the same construction as the burner 55 shown in Figure l.
- the streams or primaries 50d are attenuated to fibers by the intensely hot, high velocity blast B3 in the same manner that the streams 50 are attenuated to fibers in the form of the apparatus shown in Figure 1.
- a cur- ,rent of electrical energy may be passed therethrough to heat the material in the feeder in order to accurately control the viscosity of the glass or other molten material at its zone of discharge. While several means of establishing pressure on the glass supply have been shown and described herein, it is to be understood that any suitable pressure establishing means may be used.
- the pressure impressed on the glass supply should be sufiicient to project the streams or primaries in substantially horizontal directions so that the primaries are delivered into the blast in directions substantially normal to the path of travelof the gases of the blast.
- a method of producing fibers from heat-softenable, fiber-forming material including the steps of establishing a quantity of the fiber-forming material in a molten condition in a stationary chamber, impressing pressure effective on molten material in the chamber, projecting a plurality of streams of the molten material from the chamber by the pressure impressed on the molten material, establishing a high velocity gaseous blast wherein the gases of the blast move in directions normal to the projected streams and in engagement with the streams, the pressure on the molten material being ofsufiicient magnitude to project the streams by their energy of mo tion into the gaseous blast, and attenuating the material of the streams to fibers by the gaseous blast.
- a method of producing fibers from heat-softenable, fiber-forming material including the steps of establishing a quantity of the fiber-forming material in a molten condition in a stationary chamber, impressing fluid pressure effective on the molten material in the chamber, projecting a plurality of streams of the molten material fromthe chamber in substantially horizontal directions by the pressure on the molten material in the chamber, establishing a high velocity gaseous blast wherein the gases of the blast move in directions normal to the paths of the projected streams and in engagement with the streams, the pressure effective on the streams of molten material being of sufiicient magnitude to project the 'streams at substantial velocities by their energy of motion into the gases of the blast, and attenuating the material of the streams to fibers by the gaseous blast.
- a stationary receptacle adapted to contain a quantity .OfrnOltBfl fiber-forming material
- a method of producing fibers from heat-softenable, fiber-forming mineral material including the steps of establishing a supply of molten mineral material in a relatively stationary confined zone, impressing fluid pressure in the confined zone above the supply of molten material, regulating the pressure in the confined zone, establishing a high velocity gaseous blast of a temperature above the attenuating temperature of the material, projecting streams of the molten material substantially horizoually from the pressurized supply under influence of the regulated pressure into the gases of the blast moving in a substantially vertical direction, the regulated pressure effective on the streams of molten mineral material being of sufficient magnitude to project the streams at substantial velocities by their energy of motion into the gases of the blast whereby the forces of the balst continuously attenuate the horizontally projected streams into fibers of varying lengths.
- a method of producing fibers from heat-softenable mineral material including the-steps of establishing a supply of molten mineral material, impressing fiuid pressure on the molten mineral material, establishing a high velocity gaseous attenuating blast of generally rectangular cross section, projecting streams of the molten mineral material substantially horizontally from the pressurized supply into one side of the blast in directions supply of molten mineral material, impressng pressure on the molten mineralmaterial," establishing a down wardly directed high velocity gaseous attenuating blast of generally rectangular cross section, projecting streams of the molten mineral material from the pressurized supply into both sides of the blast in directions generally normalto the direction of movement of the gases of-the blast, the pressure on the molten mineral material being of sufficient magnitude to project the streams by their energyofvmotion into the gaseous blast'whereby the streams are continuously attenuated to fibers.
- a method of producing fibers from heat-softenabl mineral material including the steps of establishing a supply of molten mineral material in a stationary chant ber, impressing pressure on the molten mineral material in the chamber, establishing a downwardly-directed gaseous blast '"of high velocity, and project-ing streams' of 12 the molten material radially into the blast in directions substantially normal to the path of the blast, the pressure on the molten mineral material being'of' sufficient magnitude to project the streams by their energy of motion into the gaseous blast whereby the blast continuously attenuates the projected streams to fibers.
- a method of producing fibers from heat-softenable 'rnine'ral material including the steps of establishing a supply of moltenmineral material in a stationary cham ber, impressing pressure on the molten mineral material in the chamber, establishing asubstantially circular cy- :lindrical gaseous blast of high velocity, and projecting streams of the molten material from the pressurized supply radially into the blast in directions substantially normal to the axis of the blast, the pressure on the molten mineral material being of sutficient magnitude to -project the streams by their energy of motion into the gaseous blast whereby the blast continuously attenuates the projected streams to fibers.
- a method of producing fibers from heat-softenable mineral material including establishing a-supply of molten mineral material in a stationary chamber, impressing pressure on the supply, providing a generally annularly-shaped, high velocity gaseous blast of a temperature above the attenuating temperature of the material, projecting streams of the molten material from the pressurized supply in generally radial directions into the annularly-shaped blast, the pressure on the molten mineral material being of sufiicient magnitude to project the streams by their energy of motion into the gaseous blast whereby the streams are continuously attenuated to fibers by the velocity of the gases of the blast.
- Apparatus of the character disclosed in combination, a stationary receptacle adapted to contain a supply of molten fiber-forming material, a stationary feeder arranged to receive molten mineral from the supply, pressurizing means for maintainingpressure on the material in the feeder, means for regulating the pressure in the feeder, said feeder being formed with a plurality of orifices in a side wall thereof through which streams of 'molten material are projected substantially horizontally of the feeder by the pressure on the material, means for establishing a high velocity blast, said pressurizing means velocity of the blast.
- Apparatus of the character disclosed in combination, a receptacleadapted to contain a supply of molten fiber-forming material, means for establishing a high velocity gaseous blast, a feeder disposed at each side of the blast adapted to receive molten material from the supply, means for impressing pressure on the material in the feeders, said feeders being formed with orifices molten fiber-forming material, a.
- stationary feeder associated with the tank and adapted to receive molten 'material from the tank, pressurizing means for'im-pressing pressure on thematerial in the feeder, said feeder being formed with a plurality of orifices in a side wall thereof through which streams of the molten material are projected in generally horizontal directions by the pressure on the material, an internal combustion chamber in which a combustible mixture is adapted to be burned, a wall of the chamber having a restricted orifice through which the gases of combustion are discharged as a high velocity blast of a temperature above the attenuating temperature of the fiber-forming material, said pressurizing means being adapted to establish sufiicient pressure efiective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the blast, said blast engaging the streams in a direction normal to the paths of the streams for attenuating the same to fibers.
- Apparatus of the character disclosed in combination, a stationary tank adapted to contain a supply of molten fiber-forming material, means for impressing pressure on the material, a feeder associated with the tank and adapted to receive molten material from the tank, said feeder having a plurality of orifices arranged in an annular pattern through which streams of the material are projected in radial directions, means for burning a combustible mixture in a chamber, said chamber having a wall formed therein through which the burned gases are discharged as a high velocity blast of a temperature above the attenuating temperature of the material into engagement with the radially moving streams, said pressure impressing means being adapted to establish sufficient pressure effective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the blast whereby the streams are attenuated into fibers by the blast.
- Apparatus of the character disclosed in combination, a stationary tank adapted to contain a supply of molten fiber-forming material, a plurality of feeders associated with the tank and adapted to receive molten material from the tank, means for impressing pressure on the material in the feeders, each of said feeders being formed with a plurality of orifices through which streams of the molten material are projected in substantially horizontal directions by the pressure on the material, an internal combustion chamber in which a combustible mixture is adapted to be burned, a wall of the chamber having a restricted orifice through which the gases of combustion are discharged as a high velocity blast of a temperature above the attenuating temperature of the fiber forming material, said pressure impressing means 14 being adapted to establish sufiicient pressure eflective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the blast, said blast engaging the streams projected from the feeders to attenuate the streams to fibers.
- Apparatus of the character disclosed in combination, a stationary tank adapted to contain a supply of molten fiber-forming material, means for impressing pressure on the supply in the tank, a feeder associated with the tank and adapted to receive molten material from the tank, said feeder having a plurality of orifices arranged to an annular pattern through which streams or" the material are projected in radial directions under the pressure in the tank, means for establishing an annularly shaped high velocity gaseous blast of a temperature above the attenuating temperature of the material, said pressure impressing means being adapted to establish suflicient pressure effective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the annularly shaped blast, said annularly shaped blast engaging the radially moving streams to attenuate the streams to fibers.
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Description
April 11, 1961 c. F. SCHROEDER 2,978,744
METHOD AND APPARATUS FOR FORMING FIBERS Filed Sept. 9, 1955 6 Sheets-Sheet 1 INVENTOR. CHARLES FSCHROEDER ATTYS.
April 11, 1961 c. F. SCHROEDER METHOD AND APPARATUS FOR FORMING FIBERS 6 Sheets-Sheet 2 Filed Sept. 9, 1955 INVENTOR.
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S Y T T A April 11, 1961 c. F. SCHROEDER METHOD AND APPARATUS FOR FORMING FIBERS 6 Sheets-Sheet 3 Filed Sept. 9, 1955 5 w W w 57 m fi/I d M 08 M I m m: v%. 2 I i TL 6 m 5 g d mm MA 3 v J u ..l .v 2 mwm I 0 5 0 n 1 M a IN VEN TOR. Fl 6 6 CHARLES E SCHROEDER BY i W AT T YS.
April 11, 1961 c. F. SCHROEDER 2,
METHOD AND APPARATUS FOR FORMING FIBERS Filed Sept. 9, 1955 6 Sheets-Sheet 4 INVENTOR. CHA RLES F SCHROEDER FIGS AT T YS.
April 11, 1961 c. F. SCHROEDER METHOD AND APPARATUS FOR FORMING FIBERS 6 Sheets-Sheet 5 Filed Sept. 9, 1955 IN VEN TOR. CHARLES H SCHROEDER April 11, 1961 c. F. SCHROEDER 2,978,744
METHOD AND APPARATUS FOR FORMING FIBERS File d Sept. 9, 1955 6 Sheets-Sheet 6 163 4 INVENTOR.
CHARLES F. SCHHOEDER United States Charles F. Schroeder, Toledo, Ohio, assignor to Owens- Corning Fiberglas Corporation, a corporation of Delaware Filed Sept. 9, 1955, Ser. No. 533,289
16 Claims. (Cl. 18-25) This invention relates to method and apparatus for forming fibers and more especially to a method and apparatus for forming fine fibers by direct engagement of gaseous attenuating blasts with fine streams or primaries of molten fiber-forming mineral material.
Fibers have heretofore been formed by several methods utilizing blasts of gases for attenuating heat-softenable mineral material to fibers. One of the earlier methods of forming slag or mineral wool comprised fiowing a comparatively large stream of molten slag or argillaceous rock from a furnace and directing a jet of steam against the stream, atomizing the stream to form relatively coarse fibers commercially known as slag or rock wool. The fibers made by this method were not only very coarse but the end product contained a major proportion of unfiberized material in the form of pellets or shot.
Glass wool has been manufactured in substantial cornmercial quantities by flowing a plurality of streams verti-' cally from a forehearth and directing steam or com pressed air blasts downwardly in the general direction of flow of the streams and engaging the streams to form fibers.
Another method that has 'been used involves forming substantially solid primary filaments from streams of glass or other mineral material and feeding the primary filaments in solid form endwise into an intensely hot gaseous blast whereby the heat of the blast softens the filaments and the velocity of the gases of the blast attenuates the softened material to fibers.
In such prior processes as have been used commercially, the streams of molten material have been delivered by gravity into gaseous attenuating mediums, or the streams have first been drawn into solid primary filaments and the solid filaments delivered into an intensely hot blast.
More recent developments include forming a body of molten mineral material into a plurality of radially projected linear bodies by centrifugal forces and engaging the projected bodies with a gaseous blast to form the radially moving bodies into fine fibers. Such method or process involves the use of one or more elements rotating at high speeds and hence requires precision equipment .for its successful operation. This method of fiber formation is highly eflicient and produces very fine fibers. It appears that the production of extremely fine fibers from the use of centrifugal units is attributable to the use of comparatively fine primaries or streams of the material delivered to the attenuating blast. The controlled or substantially constant pressure exerted by centrifugal forces of rotation of an element'or spinner efiects extrusion of the fiber-forming material into extremely fine elongated bodies of lesser diameters than primaries or elongated bodies obtained from streams of glass motivated solely by gravity. 7
The present invention embraces the provision of a method and apparatus for forming fine streams, elongated 2,978,744 Patented Apr. 11, 1961 and engaging the streams or primaries by a high velocity gaseous blast to attenuate the streams or primaries to fibers.
Another object of the invention resides in the provision of forehearth and feeder means maintained under pressure whereby a large number of minute streams or bodies of glass or other heat-sottenable material may be projected at controlled fiow rates from opposed directions into an attenuating blast formed of burned gases of combustion at temperatures well above the attenuating temperature of the glass whereby the streams or bodies are attenuated into fine fibers.
Another object of the invention resides in the provision of a method and apparatus for attenuating fibers wherein molten fiber-forming material is extruded under pressure under controlled conditions through small openings forming fine primary'filaments or bodies which are engaged by a high velocity gaseous blast to form fibers without the use of moving or rotating elements or mechanism.
Still another object of the invention is the provision of a method and apparatus of forming fibers wherein a comparatively large number of pressureextruded bodies of fiber-forming material are delivered into an attenuating blast wherein comparatively large quantities of fiberforming material are converted to fine fibers with a minimum expenditude of attenuating energy.
Further objects and advantages are within the scope of this invention such as relate to the arrangement, opera; tion and function of the related elements of the structure, to various details of construction and to combinations of parts, elements per se, and to economies of manufacture and numerous other features as will be apparent from a consideration of the specification and drawing of a form of the invention, which may be preferred, in which:
Figure l is a vertical sectional view showing a form of apparatus for carrying out the method of the invention;
Figure 2 is an enlarged detail sectional view of a portion of the apparatus shown in Figure 1;
Figure 3 is a bottom plan view of the arrangement shown in Figure 2;
Figure 4 is a vertical sectional view illustrating another form of'apparatus for carrying out the method of the invention;
Figure 5 is a bottom plan view of the arrangement shown in Figure 4;
Figure 6 is an elevational sectional view with certain parts shown in section of another form of apparatus for carrying'out the method of the invention;
Figure 7 is a bottom plan view of the filament fiber-forming apparatus shown in Figure 6;
Figure 8' is a view similar to Figure 7 illustrating an and arrangement for delivering an annular-attenuating blast;
' Figure 9 is an elevational view with certain parts shown in section of another form of apparatus for'carry ing h artist at h i im Figure is an enlarged sectional view of a portion of the apparatus shown in Figure 9;
Figure 11 is a bottom plan view of the filament and fibenforming apparatus shown in Figure 9, and
Figure 12 is a sectional view of a furnace, forehearth and feeder construction for delivering fiber forming material under pressure to an attenuating blast.
The forms of apparatus illustrated are especially adaptable for forming fine primary filaments, streams or elongated bodies of molten glass which are projected into an attenuating blast and thereby attenuated to very fine fibers. It is to be understood that the method and apparatus of the invention may be used for forming primary filaments and fibers from other heat-softenable materials such as fusible rock, slag or other thermoplastic or wherever the method and arrangement may be found to have utility.
Referring to the drawings in detail, Figures 1 through 3 illustrate one form of apparatus for carrying out the method of the invention. Numeral it) designates a melting furnace, tank or receptacle in which is maintained a supply of molten fiber forming material 11 such as glass, slag, fusible rock or other heat softenable mineral material from which fibers may be formed by attenuation.
The furnace or receptacle It} may be formed with a metal casing 12 which is lined with suitable refractory 14 capable of withstanding the high temperatures of the molten glass or other fiber-forming material.
The furnace or receptacle 10 forms a confined zone or chamber 18 containing the supply of fiber forming material and pressure is impressed in the chamber 18 so that the supply of molten glass or other material is main tained under a static pressure in order to facilitate satisfactory extrusion of the material through comparatively small orifices. A means is provided for feeding raw glass batch 20 or other composition of fiber-forming material to be introduced into the chamber 18 and therein reduced to a molten state or condition.
As shown in Figure l, a cylindrical tube 22 extends from the furnace 10 and disposed interiorly of the tube 22 is a material feeding means in the form of a screw or member 24 which is snugly but rotatably disposed in the tube 22 to prevent reduction in pressure within the chamber 18. It is to be understood that. other forms of means for introducing raw batch into the furnace may be employed if desired. The batch feeding means or screw 24 shown in the embodiment in Figure 1 is driven by a motor (not shown) or other suitable means at a speed to deliver or convey the batch 25 into the furnace 10 substantially at the rate that the molten material is extruded from the furnace in a manner hereinafter described.
A wall or dam 19 in the furnace having an opening through which the glass flows assists in refining the molten glass. The batch, after delivery into the chamber 18, may be rendered molten by the application of heat, and burners or heating means 2% may be utilized for this purpose. The burners or heating means 28 may be connected with a source (not shown) of combustible mixture such as fuel gas and air delivered to the burners under pressure, the combustible mixture being ignited and burned within the chamber 18. p 7
The pressure of the burning gases and products of combustion may be utilized to pressurize the chamber 18 or pressure may be impressed in chamber 18 by the introduction of other gases through a ductor tube such as tube 30. A regulating valve. 32 which may be manually controlled or an automatic pressure regulator may be employed to regulate the flow of gases under pressure into the chamber '18. I V V f When burners 28 are utilized to deliv'er combustible mixture into the chamber 18 to be burned therein, a vent means maybe provided for.th'e chamber 18 equipped with a valve for maintaining the desired 'pressu're' in the chamber. In Figure 1 the upper wall of the furnace or receptacle 10 is provided with a vent tube 34 equipped with a valve 36 which may be manually or automatically controlled for maintaining a constant pressure in the chamber.
Figures 1, 2 and 3 illustrate an arrangement for projecting or extruding streams or, primaries of the molten fiber forming material into an attenuating blast in which the molten streams or primaries are attenuated to fibers. Depending from the furnace 10 are walls 44) and 41 providing, in effect, a forehearth defining a passage, chamber or well 42 arranged to receive molten material from the supply 11 in the chamber 18, The
The feeder 44 is formed with orifice means for exuding or extruding fine streams of molten fiber-forming material contained in the passage or chamber 42. In the embodiment illustrated in Figures 1, 2 and 3, the feeder 44 is formed with the plurality of tips, nozzles or projections 46, each of which is formed with a small orifice or outlet 48 through which a stream 50 of molten fiber fornu ing material is delivered or extruded under pressure,
The streams 50, also referred to herein as primaries, primary filaments or elongated bodies, are projected in a substantially horizontal direction or plane as shown in Figures 1 and 2. A current of electrical energy may be delivered through the metal feeder 44 to control or regulate the viscosity of the molten material in the feeder so that the material may be extruded at a viscosity to provide primaries most satisfactory for attenuation to fibers.
The streams 50, under the influence of the substantially constant static pressure in the chamber 18, are projected in a substantially rectilinear direction-for some distance beyond the outlets 48 in the tips 46. In the present invention the streams or primaries 50 are delivered endwise into an attenuating blast. As shown in Figures 1 through 3 there is provided a burner having a metal casing 56, the burner being formed with a combustion chamber or confined zone 57 in which a combustible mixture is adapted to be substantially coma pletely burned. The chamber 57 is defined by walls59 of suitable refractory capable of withstanding the high temperature of the burning gases in thechamber, the temperature of the'gases being 3000 F. or higher.
A lower wall of the chamber 57 is.provided with a restricted orifice or outlet 60 which, as shown in Figure 3, is of elongated rectangular character. The burner 55 is connected with a tube 62, the latter being connected with supply of combustible mixture such as fuel gas and air. Any suitable fuel gas may be used such as methane, ethane or propane, and the combustible mixture is. delivered by the tube or duct 62 into 'a manifold chamber or passage 64. A rear wall 66 of the chamber 57 adjacent the mixture inlet or manifold chamber 64 is formed with plurality small perforations or passages 68 through which the mixture is conveyed into the chamber 57.
The perforated wall 66 forms a fire or protective screen to avoid or prevent preignition ofithe mixture in the passage 64 or the duct 62. The fuel and air mixture may be deliveredinto the chamber'57 under a comparative low pressure of from three to 10 lbs. p.s.i. The combus tible mixture is ignited in the chamber 57v and is sub,-
stantially completely burned within the chamber or confinedzone. ,'The burning gases undergo greatexpansion in the V chamber 57, the walls of the chamber being heatedto incandescent which accelerates flame propagation or com; bustion taking place within the chamber. The burned gases are discharged through the restricted orifice or outlet 60 as intensely not high veracity aseous bl'ast amaze;
of a temperature above the attenuating temperature of the fiber forming material. As shown in Figures 1 and 2, the blast B from the orifice 60 is projected downwardly in a direction substantially normal to the endtvgise delivery of the primaries or streams 50 into the ast.
The streams or primaries 50 are attenuated by the blast B to fine fibers F. While the primaries or streams 50 are in a flowable condition as they enter the blast, there may be some chilling or cooling of the streams and increase in viscosity by the air fiow induced by the blast through the space 43 between a wall of the burner and wall 41 of the well 42. The increase in viscosity or thickened condition of the streams entering the attenuating blast B provides in each stream a nub or inertia zone from which fibers may be drawn, the heat of the gases of the blast elevating the temperature of the material of the streams whereby the extremities of the streams in the blast are softened or conditioned so that they are drawn by the blast into long fine fibers.
With the arrangement above described, fine streams or primaries 50 may be delivered into the high temperature blast B so that the extremely fine fibers of a diameter of two microns or less may be economically produced in commercial quantities. While it is advantageous to utilize a blast of a temperature above the attenuating temperature of the fiber forming material in order to form fine fibers, it is to be understood that the streams or primaries 50 may be delivered into a blast of steam or compressed air moving in a direction normal or perpendicular to the paths of the primaries projected from the outlets or orifice 48. However, fibers attenuated by steam or air blasts are usually not as fine as those produced by the hot blast method.
The newly formed fibers F entrained in the blast move downwardly as shown in Figure l and may be collected in a mass 69 upon the upper flight 70 of an endless foraminous conveyor 71, the flight 70 moving in a righthand direction as-viewed in Figure 1. A box or receptacle 73 may be disposed beneath the upper flight 70 of the conveyor in the path of the descending fibers F providing a chamber 74. A duct 75 connects the chamber 74 with a suction blower (not shown) for establishing a suction or subatmospheric pressure in chamber 74 to assist in collecting the fibers upon the conveyor flight 70 and to convey away spent gases of the attenuating blast. The mass 69 of fibers may be passed between compression or sizing rolls 77 for predetermining the thickness of the mat M formed from the fibers.
It may be desirable to apply a binder or other coating material to the newly formed fibers in order to impart mass integrity to the end product. As shown in Figure l, applicators 80 may be disposed adjacent opposite sides of the descending fibers F for projecting binder 82 or other fiber coating material on to the fibers. The binder may be of any type but a thermo-setting material is preferred such as phenol formaldehyde or urea formaldehyde. The mat of fibers treated with the bonding agent or material may be conveyed through an oven or curing zone to set the binder in the fibrous mat.
By regulating the air fiow along the blast, a measure of control may be had over the condition of viscosity of the streams 50. A control over the amount of air ad--,
50. The bathe '45 may be secured to the casing wall of the burner 55 and may be made adjustable if desired.
Figures. 4 and 5 illustrate modified form of apparatus for forming heat-softenable mineral material tofibers.
'In this form of apparatus,'means is provided at each side of a gaseous blast for projecting or extruding streams of molten mineral material such as glass into'the blast.-;- The 6 arrangement shown in Figure 4 may be utilized with a furnace or melting receptacle of the character shown in Figure 1 provided with a second means for delivering an additional group of streams into an attenuating blast. Depending from the furnace or melting receptacle is a forehearth arrangement including two passages, wells or chambers 42a and 42b which are adapted to receive molten glass or other molten mineral material from the melting furnace. The walls defining the passages 42a and 42b are formed of refractory capable of withstanding the intense heat of the molten material. The walls of the passage 42a may be enclosed by a metal casing 76a and the walls defining the passage 42b may be enclosed in'a metal casing 76b.
The adjacent walls of'tlie casings 76a and 76b are spaced to accommodate a blast producing means or internal combustion burner 78. Burner 78 is similar to the burner 55 and is inclusive of a metal'casing' 79 in which is formed a combustion zone of chamber 83 defined by walls 84 of refractory. The lower wall of the chamber 83 is formed with a restricted outlet or orifice 86 which is of elongated character as shown in Figure 5.
The burner 78 is connected with a tube or pipe 88 adapted to convey a combustible mixture of fuel gas and air into the combustion chamber or confined zone 83. The rear wall 89 of the combustion chamber 83 is formedwith a plurality of small openings or passages to convey the mixture into the chamber, the perforated wall providing a fire screen to prevent preignition of the mixture in the inlet 87 and the supply pipe 88.
The burner 78 is deposed between the downwardly extending material conveying passages or wells 42a and 42b as shown in Figure 4. A wall of each of the depending portions of the receptacle defining the chambers 42a and 42b is provided with a feeder or bushing 92 which may be made of metal or alloy capable of withstanding the intense heat of the molten material. Such alloys as platinum rhodium or platinum iridium have been found satisfactory for the purpose.
Each of the feeders 92 is formed with a plurality of tips, nozzles or projections 94 and each of the tips is provided with an orifice or outlet 96 through which molten material from the wells 42a and 42b is projected or exuded in a fine stream 50. The projections or tips 94 are disposed so as to project the streams 50 in substantially horizontal directions and endwise into the downwardly projected blast as shown in Figure 4.
The groups of projections 94 of the feeders are disposed in opposed relation whereby the streams 50 from the groups of tips are projected in opposite directions in entering the blast. As shown in Figure 5, each orifice 96 of one group is disposed in alignment with an orifice 96 in the opposite group, but it is to be understood that the orifices of one group may be disposed. in staggered relation with respect to the orifices in the'opposite group i so that each stream of molten material may enter a different zone of the blast.
Through the arrangement shown in Figures 4 and 5, a large amount of molten material may be introduced into a single elongated blast projected through the slot or restricted orifice 86. The pressure impressed upon the supply of molten material is effective on the material in the wells 42a and 42b and feeders 92 to project the streams 50 endwise into the blast at a substantial velocity. As shown in Figure 4 the inner walls 76 of the well constructions are disposed in close relation to the side walls of the burner casing 79 in order to restrict the how of induced air along the blast. I *1 v 7 It is to be understood that the casings 76a and 76b may be spaced at greater distances from the burnerwall and bafiles or other means may be disposed between the burner walls and the casings 76a and 76b for restricting and controlling the flow of induced air alongthe blast.
The induced air, as previously mentioned in connection s s-rem with the form of the apparatus shown in Figures 1 through 3, chills the streams 50 rendering them more viscous. Thus by restricting and Controlling the induced air, the viscous condition of the streams or primaries 50 may be controlled and the streams or primaries delivered into the blast under optimum conditions to obtain the most efficient attenuation of the streams or primaries.
Figures 6 and 7 illustrate another form of apparatus for delivering streams or primaries of molten material in radial directions into a substantially annular gaseous attenuating blast. This arrangement is inclusive of a pressurized melting furnace, tank or receptacle 100 in which is contained a supply of molten fiber forming material 1111. In the melting furnace illustrated, the glass or other mineral fiber-forming material may be introduced into the furnace in the shape of preformed spheres or marbles 102.
A tube 104 extending upwardly from the furnace contains a supply of glass marbles. A member 105 associated with the furnace 100 is provided with a rotary valve 197 adapted to successively deliver the marbles from the tube 104 through a passage 108 into the furnace without afi'ecting the pressure in the melting chamber 112. Heating means in the form of burners 110 are disposed in the chamber 112 for melting the marbles.
Pressure above atmospheric pressure is impressed in the chamber 112. This may be accomplished by the pres sure of the burning gases from the burners 110 which may be supplemented by gases under pressure introduced into the chamber through a pipe or duct 114. A valve 115 is associated with a pipe 114 for controlling the flow of pressure gases into the closed pressurized chamber 112.
The forehearth 120 in the embodiment illustrated depends from the furnace construction .1110. The forehearth 120 extends downwardly and outwardly in an annular formation providing an annularly shaped Well 124. A portion 123 is formed with an annularly shaped feeder 126. The feeder 126 is fashioned with a plurality of outwardly and radially extending tips or projections 128 each of which is formed with an orifice 130 through which streams 50b are projected under the influence of superatmospherlc pressure on the supply of glass or other material in the chamber 112.
A substantially annular gaseous blast is provided adapted to engage the streams 59b to attenuate the streams to fibers. As shown in Figure 7, the blast establishing means is inclusive of four burners 135 each being shaped as a circular ring sector, which in assembled relation provide a substantially annular burner arrangement. Each of the burners 135 includes a metal casing 137, the interior which is lined with refractoryj139 shaped to define an internal combustion chamber or confined zone 14th.
A wall of each burner is formed with a restricted outlet or orifice means 142 of arcuate shape through which burned gases or products of combustion from the chamber 140 are discharged as a high velocity blast of a temperatureabove the attenuating temperature of the fiber forming material. A combustible mixture is delivered into the combustion chamber 140 of each burner "through tubes 145 which are connected with a supply of combustible mixture such as fuel gas and air.
The mixture is burned in the chamber 140 under confined conditions, the burning gases undergoing great expansion attaining a temperature of 3000 F. or more before they are discharged at high velocities through the restricted orifice 142. As shown in Figure '7, the several arcuately shaped orifices in effect provide a substantially annular blast. The annular blast emanating from the orifice means 142 of the burners engages the streams or primaries from the orifices 13%) in. a direction substantially normal to the flow of the streams from the annular feeder 126.
' The amount'of air flow induced by the velocity of the gaseous blast may-becontrolled byan annular plate O u 148 disposed in the path of fiow of air between the feeder 126 and the inner walls of the burner casings 137. The width of the plate 148 and its position, may be varied or adjusted to provide the desired restriction to the induced air flow. The streams 50b move radially in substantially horizontal directions under the influence of the pressure impressed on the molten material.
The attenuated fibers are entrained in the annular blast and are carried downwardly by the blast in the form of the circular cylindrically shaped beam or column 150 of fibers. The fibers of the beam may be collected upon an upper flight of a foraminous conveyor of the character shown in the Figure 1. A suction chamber 74' is provided beneath the conveyor flight 70' in order to assist in collecting the fibers on the conveyor and to carry away spent gases of the blast.
Figure 8 is a bottom plan view of an arrangement simliar to that shown in Figure 7 with the burner construction formed as a continuous annulus. The burner 135 is formed with a continuous annular-shaped combustion chamber from which burned gases or products of combustion are discharged through a continuous annularly shaped restricted orifice 152. Streams of molten fiber-forming material are delivered through the orifices formed in projections 128 in the manner shown in Figure 6. Combustible mixture is introduced into the combustion chamber of the burner 135' through pipes connected with a supply of fuel gas and air. The streams 50b are attenuated by the annular blast from the orifice 152 in the same manner described in connection with Figures 6 and 7. i
Figure 9 is a view similar to Figure 1 illustrating another form of apparatus'for carrying on the method of the invention. The melting, furnace 10c in which glass batch is adapted to be melted is arranged to receive glass batch through the use of means such as those illustrated in Figures 1 and 6. The furnace 10c is provided with a forehearth or depending portion 155. The construction 1155 is formed with leg portions 158 and 159. The portion 158 is formed with a downwardly extending passage 160 and the portion 159 is formed with a similarly shaped downwardly extending passage 162. The depending portions 158 and 159 support an annularlyshaped portion 161. The portion 161 is formed with anannular chamber 163 which is in communication with both passages or wells 161 and 162 and receive through which the molten material in the annular chamber 163 is extruded under pressure to form streams or primaries 500 of the fiber-forming material.
The molten material in the passages or chambers 160 and 162 and the annular chamber 163 is under a pressure greater than the normal head of glass in the chambers 160 and 162. The portion 155 of the forehearth is formedwith a circular cylindrical chamber or bore 174. Extending through an opening in the upper wall of the melting furnace 10c is a shaft 176 which is equipped with a collar 177 to position the rod or shaft The shaft 176 extends into the chamber 174 and is equipped with a' pair of propeller or screw- like members 180 and 182. .The blades of members 181) and 182 are of a spiral pitch such that rotation of members 180 and 182 inthe proper direction impresses downwardly acting pressure upon the glass or other molten fiber forming material contained in the passages or chambers 160, 162
and 163. The-shaft 176 may bedrivenby any electric otor (not shown) or by other suitable means torotate the members 130 and 182.
hearth are pressurized in any suitable manner. burning gases from the burners 220 and 222 may be uti- Through this arrangement, a substantial pressure is exerted upon the glass or molten material contained in the annular feeder 164, the pressure being effective to extrude the fine streams 500 in substantially horizontal directions into an attenuating blast as illustrated in Figure 10. The pressure may be controlled by regulating the speed of rotation of the members 180 and 182.
Arranged in the space between the depending leg portions 158 and 159 of the material feeding means is a burner or blast producing means 186. The burner 186 is inclusive of a metal shell 188 which is lined with a high temperature refractory 189 defining a combustion chamber or confined zone 190. The rear of the burner is provided with a member 193 formed with a manifold chamber 195 into which a combustible mixture is delivered through a mixture supply pipe 197. A rear wall 200 of the chamber 190 is formed with a large number of small channels or passages 202 through which the mixture is delivered into the chamber 190, the wall 200 forming a fire screen to avoid preignition in the manifold 195.
The depending end zone of the burner 186 is formed with a circular orifice 205 of restricted character in that its cross sectional area is one-quarter to oneeighth of the cross sectional area of the chamber 190. The combustible mixture is delivered to the combustion chamber 190 under a comparably low pressure and is substantially completely burned within the chamber 190. The burning gases undergo great expansion and are heated to a temperature of 3000 F. or more which is above the attenuating temperature of the glass.
The burned gases are projected from the chamber 190 through the restricted orifice 205 to form a substantially circular cylindrical blast B2 into which the streams or primaries 500 are projected, the blast moving downwardly in a direction substantially normal to the plane of the paths om movement of the streams 500 into the blast. The streams or primaries 50c are attenuated to fine fibers by the heat and velocity of the gases of the blast.
As shown in Figure 9, the attenuated fibers F are entrained in the downwardly projected blast and are collected upon the upper flight 700 of a foraminous conveyor in the manner described in connection with the form of the apparatus shown in Figure 1. A suction chamber 74c is disposed beneath the fiber collecting region to assist in collecting the fibers and to carry awa spent gases of the blast.
It is to be understood that the pressurizing means 180 and 182 shown in Figure 9 may be used with the other forms of apparatus disclosed. The batch or glass feeding means and the pressurizing means shown in Figures 1 and 6 may be utilized in the construction shown in Figure 9 in lieu of or supplementing the mechanical pressurizing means shown in Figure 9. I
Figure 12 illustrates another form of apparatus of the invention. In this form, the melting furnace 210 is provided with a horizontally extending forehearth construction 212. Glass batch is introduced into the chamber 214 of the furnace through a tube or pipe 216 provided with a pair of spaced valves 218 operable to admit the material into the chamber without appreciable variation of pressure in the chamber. Burners 220 or other suitable heating means are utilized to reduce the batch material to a molten state.
Additional burners or heating means 222 may be disposed in the forehearth in order to maintain the glass at the desired viscosity therein. The furnace and fore- The lized for the purpose, or gases under pressure may be conveyed intothe chamber 214 by means of a pipe 226.
Valve means 228-associated with the pipe 226, which pressure regulating type, may be used to control or regulate the pressure in the chamber 214. A depending wall portion 230 disposed between the furnace chamber 214 and the forehearth forms a skimmer block, the molten material flowing through the passage 232 from melting chamber into the forehearth. One or more vent openings 234 may be formed in the Wall 230 for equalizing the pressures in the chamber 214 and in the forehearth 212.
A wall of the forehearth 212 is provided with a feeder or bushing 236 having nozzles or projections 238 through which streams or primaries 50d are projected into a blast B3. The blast is formed of combustible gases burned within a chamber or confined zone 57d of a burner 55d. The burner illustrated in Figure 12 is of the same construction as the burner 55 shown in Figure l. The streams or primaries 50d are attenuated to fibers by the intensely hot, high velocity blast B3 in the same manner that the streams 50 are attenuated to fibers in the form of the apparatus shown in Figure 1.
In all forms of feeder construction illustrated, a cur- ,rent of electrical energy may be passed therethrough to heat the material in the feeder in order to accurately control the viscosity of the glass or other molten material at its zone of discharge. While several means of establishing pressure on the glass supply have been shown and described herein, it is to be understood that any suitable pressure establishing means may be used. The pressure impressed on the glass supply should be sufiicient to project the streams or primaries in substantially horizontal directions so that the primaries are delivered into the blast in directions substantially normal to the path of travelof the gases of the blast.
It is apparent that, within the scope of the invention, modifications and diiferent arrangements may be made other than is herein disclosed, and the present disclosure is illustrative merely, the invention comprehending all variations thereof.
I claim:
1. A method of producing fibers from heat-softenable, fiber-forming material including the steps of establishing a quantity of the fiber-forming material in a molten condition in a stationary chamber, impressing pressure effective on molten material in the chamber, projecting a plurality of streams of the molten material from the chamber by the pressure impressed on the molten material, establishing a high velocity gaseous blast wherein the gases of the blast move in directions normal to the projected streams and in engagement with the streams, the pressure on the molten material being ofsufiicient magnitude to project the streams by their energy of mo tion into the gaseous blast, and attenuating the material of the streams to fibers by the gaseous blast.
2. A method of producing fibers from heat-softenable, fiber-forming material including the steps of establishing a quantity of the fiber-forming material in a molten condition in a stationary chamber, impressing fluid pressure effective on the molten material in the chamber, projecting a plurality of streams of the molten material fromthe chamber in substantially horizontal directions by the pressure on the molten material in the chamber, establishing a high velocity gaseous blast wherein the gases of the blast move in directions normal to the paths of the projected streams and in engagement with the streams, the pressure effective on the streams of molten material being of sufiicient magnitude to project the 'streams at substantial velocities by their energy of motion into the gases of the blast, and attenuating the material of the streams to fibers by the gaseous blast.
v3. Apparatus of the character disclosed, in combination; a stationary receptacle adapted to contain a quantity .OfrnOltBfl fiber-forming material, a, stationary feeder associated with the receptacle provided with a plurality of orifices through which streams 'of the material f are pro: jected, means for establishing a high velocity gaseous blast wherein the gases of the blast move in directions tion, a stationary receptacle adapted to contain a quantity of molten fiber-forming material, a stationary feeder associated with the receptacle provided with a plurality oforifices through which streams of the material are projected in substantially horizontal directions, means for establishing a high velocity gaseous blast wherein the gases of the blast move in directions substantially normal to the paths of the projected streams, and pressurizing means associated with the molten material'arranged to establish sufiicient pressure etfective on the molten material at the region of the orifices to project the streams at substantial velocities by their energy of motion through the blast-induced air stream into the blast whereby the streams are attenuated into fibers by the blast.
5. A method of producing fibers from heat-softenable, fiber-forming mineral material including the steps of establishing a supply of molten mineral material in a relatively stationary confined zone, impressing fluid pressure in the confined zone above the supply of molten material, regulating the pressure in the confined zone, establishing a high velocity gaseous blast of a temperature above the attenuating temperature of the material, projecting streams of the molten material substantially horizoually from the pressurized supply under influence of the regulated pressure into the gases of the blast moving in a substantially vertical direction, the regulated pressure effective on the streams of molten mineral material being of sufficient magnitude to project the streams at substantial velocities by their energy of motion into the gases of the blast whereby the forces of the balst continuously attenuate the horizontally projected streams into fibers of varying lengths.
6. A method of producing fibers from heat-softenable mineral material including the-steps of establishing a supply of molten mineral material, impressing fiuid pressure on the molten mineral material, establishing a high velocity gaseous attenuating blast of generally rectangular cross section, projecting streams of the molten mineral material substantially horizontally from the pressurized supply into one side of the blast in directions supply of molten mineral material, impressng pressure on the molten mineralmaterial," establishing a down wardly directed high velocity gaseous attenuating blast of generally rectangular cross section, projecting streams of the molten mineral material from the pressurized supply into both sides of the blast in directions generally normalto the direction of movement of the gases of-the blast, the pressure on the molten mineral material being of sufficient magnitude to project the streams by their energyofvmotion into the gaseous blast'whereby the streams are continuously attenuated to fibers.
8. A method of producing fibers from heat-softenabl mineral material including the steps of establishing a supply of molten mineral material in a stationary chant ber, impressing pressure on the molten mineral material in the chamber, establishing a downwardly-directed gaseous blast '"of high velocity, and project-ing streams' of 12 the molten material radially into the blast in directions substantially normal to the path of the blast, the pressure on the molten mineral material being'of' sufficient magnitude to project the streams by their energy of motion into the gaseous blast whereby the blast continuously attenuates the projected streams to fibers.
9. A method of producing fibers from heat-softenable 'rnine'ral material including the steps of establishing a supply of moltenmineral material in a stationary cham ber, impressing pressure on the molten mineral material in the chamber, establishing asubstantially circular cy- :lindrical gaseous blast of high velocity, and projecting streams of the molten material from the pressurized supply radially into the blast in directions substantially normal to the axis of the blast, the pressure on the molten mineral material being of sutficient magnitude to -project the streams by their energy of motion into the gaseous blast whereby the blast continuously attenuates the projected streams to fibers.
10. A method of producing fibers from heat-softenable mineral material including establishing a-supply of molten mineral material in a stationary chamber, impressing pressure on the supply, providing a generally annularly-shaped, high velocity gaseous blast of a temperature above the attenuating temperature of the material, projecting streams of the molten material from the pressurized supply in generally radial directions into the annularly-shaped blast, the pressure on the molten mineral material being of sufiicient magnitude to project the streams by their energy of motion into the gaseous blast whereby the streams are continuously attenuated to fibers by the velocity of the gases of the blast.
11. Apparatus of the character disclosed, in combination, a stationary receptacle adapted to contain a supply of molten fiber-forming material, a stationary feeder arranged to receive molten mineral from the supply, pressurizing means for maintainingpressure on the material in the feeder, means for regulating the pressure in the feeder, said feeder being formed with a plurality of orifices in a side wall thereof through which streams of 'molten material are projected substantially horizontally of the feeder by the pressure on the material, means for establishing a high velocity blast, said pressurizing means velocity of the blast.
12. Apparatus of the character disclosed, in combination, a receptacleadapted to contain a supply of molten fiber-forming material, means for establishing a high velocity gaseous blast, a feeder disposed at each side of the blast adapted to receive molten material from the supply, means for impressing pressure on the material in the feeders, said feeders being formed with orifices molten fiber-forming material, a. stationary feeder associated with the tank and adapted to receive molten 'material from the tank, pressurizing means for'im-pressing pressure on thematerial in the feeder, said feeder being formed with a plurality of orifices in a side wall thereof through which streams of the molten material are projected in generally horizontal directions by the pressure on the material, an internal combustion chamber in which a combustible mixture is adapted to be burned, a wall of the chamber having a restricted orifice through which the gases of combustion are discharged as a high velocity blast of a temperature above the attenuating temperature of the fiber-forming material, said pressurizing means being adapted to establish sufiicient pressure efiective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the blast, said blast engaging the streams in a direction normal to the paths of the streams for attenuating the same to fibers.
14. Apparatus of the character disclosed, in combination, a stationary tank adapted to contain a supply of molten fiber-forming material, means for impressing pressure on the material, a feeder associated with the tank and adapted to receive molten material from the tank, said feeder having a plurality of orifices arranged in an annular pattern through which streams of the material are projected in radial directions, means for burning a combustible mixture in a chamber, said chamber having a wall formed therein through which the burned gases are discharged as a high velocity blast of a temperature above the attenuating temperature of the material into engagement with the radially moving streams, said pressure impressing means being adapted to establish sufficient pressure effective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the blast whereby the streams are attenuated into fibers by the blast.
15. Apparatus of the character disclosed, in combination, a stationary tank adapted to contain a supply of molten fiber-forming material, a plurality of feeders associated with the tank and adapted to receve molten material from the tank, means for impressing pressure on the material in the feeders, each of said feeders being formed with a plurality of orifices through which streams of the molten material are projected in substantially horizontal directions by the pressure on the material, an internal combustion chamber in which a combustible mixture is adapted to be burned, a wall of the chamber having a restricted orifice through which the gases of combustion are discharged as a high velocity blast of a temperature above the attenuating temperature of the fiber forming material, said pressure impressing means 14 being adapted to establish sufiicient pressure eflective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the blast, said blast engaging the streams projected from the feeders to attenuate the streams to fibers.
16. Apparatus of the character disclosed, in combination, a stationary tank adapted to contain a supply of molten fiber-forming material, means for impressing pressure on the supply in the tank, a feeder associated with the tank and adapted to receive molten material from the tank, said feeder having a plurality of orifices arranged to an annular pattern through which streams or" the material are projected in radial directions under the pressure in the tank, means for establishing an annularly shaped high velocity gaseous blast of a temperature above the attenuating temperature of the material, said pressure impressing means being adapted to establish suflicient pressure effective on the material at the region of the orifices to project the streams at substantial velocities through the blast induced air stream into the annularly shaped blast, said annularly shaped blast engaging the radially moving streams to attenuate the streams to fibers.
References Cited in the file of this patent UNITED STATES PATENTS 282,579 Small Aug. 7, 1883 2,450,363 Slayter et al. Sept. 28, 1948 2,453,864 Schlehr Nov. 16, 1948 2,491,889 Bennett et al. Dec. 20, 1949 2,511,381 Stevens June 13, 1950 2,518,744 Barnard --Aug. 15, 1950 2,526,775 Slayter et al. Oct. 24, 1950 2,578,100 Stalego Dec. 11, 1951 2,614,619 Fuller Oct. 21, 1952 2,624,912 Heymes et al. Jan. 13, 1953 2,635,285 Toulmin Apr. 21, 1953 2,717,416 Fletcher Sept. 13, 1955 FOREIGN PATENTS 877,043 France Aug. 24, 1942 674,334 Germany Apr. 12, 1939 914,424 Germany July 1, 1954
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US533289A US2978744A (en) | 1955-09-09 | 1955-09-09 | Method and apparatus for forming fibers |
DEO5064A DE1052072B (en) | 1955-09-09 | 1956-08-25 | Method and device for the production of fibers from heat-softenable fiber-forming minerals |
GB26581/56A GB793913A (en) | 1955-09-09 | 1956-08-30 | Process and apparatus for forming fibres |
FR1157909D FR1157909A (en) | 1955-09-09 | 1956-09-06 | Method and apparatus for forming fibers |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US533289A US2978744A (en) | 1955-09-09 | 1955-09-09 | Method and apparatus for forming fibers |
Publications (1)
Publication Number | Publication Date |
---|---|
US2978744A true US2978744A (en) | 1961-04-11 |
Family
ID=24125303
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US533289A Expired - Lifetime US2978744A (en) | 1955-09-09 | 1955-09-09 | Method and apparatus for forming fibers |
Country Status (4)
Country | Link |
---|---|
US (1) | US2978744A (en) |
DE (1) | DE1052072B (en) |
FR (1) | FR1157909A (en) |
GB (1) | GB793913A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3077093A (en) * | 1959-12-03 | 1963-02-12 | Pittsburgh Plate Glass Co | Method for forming glass fibers |
US4343640A (en) * | 1981-03-20 | 1982-08-10 | Manville Service Corporation | Attenuation burner for forming fibers |
CN108083656A (en) * | 2017-12-29 | 2018-05-29 | 通鼎互联信息股份有限公司 | A kind of nitrogen guiding device |
CN108315829A (en) * | 2018-04-24 | 2018-07-24 | 苏州大学 | Aeration type electrostatic spinning apparatus and spinning process |
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US2450363A (en) * | 1944-04-27 | 1948-09-28 | Owens Corning Fiberglass Corp | Method and apparatus for making fine glass fibers |
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- 1955-09-09 US US533289A patent/US2978744A/en not_active Expired - Lifetime
-
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- 1956-08-25 DE DEO5064A patent/DE1052072B/en active Pending
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- 1956-09-06 FR FR1157909D patent/FR1157909A/en not_active Expired
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US282579A (en) * | 1883-08-07 | Apparatus for and process of making comminuted solder | ||
DE674334C (en) * | 1936-12-05 | 1939-04-12 | Glasfabrik Wilhelmshuette G M | Method for winding glass threads onto a winding drum |
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US4343640A (en) * | 1981-03-20 | 1982-08-10 | Manville Service Corporation | Attenuation burner for forming fibers |
CN108083656A (en) * | 2017-12-29 | 2018-05-29 | 通鼎互联信息股份有限公司 | A kind of nitrogen guiding device |
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CN108315829A (en) * | 2018-04-24 | 2018-07-24 | 苏州大学 | Aeration type electrostatic spinning apparatus and spinning process |
Also Published As
Publication number | Publication date |
---|---|
GB793913A (en) | 1958-04-23 |
DE1052072B (en) | 1959-03-05 |
FR1157909A (en) | 1958-06-05 |
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