US2717962A - Electric discharge devices - Google Patents
Electric discharge devices Download PDFInfo
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- US2717962A US2717962A US528818A US52881844A US2717962A US 2717962 A US2717962 A US 2717962A US 528818 A US528818 A US 528818A US 52881844 A US52881844 A US 52881844A US 2717962 A US2717962 A US 2717962A
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/26—Mass spectrometers or separator tubes
- H01J49/28—Static spectrometers
- H01J49/30—Static spectrometers using magnetic analysers, e.g. Dempster spectrometer
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- a further object of the invention is to provide an arc discharge device with an improved electrode arrangement for increasing the life of the arc cathode.
- a calutron ion source is provided with an improved electron source including a filamentary cathode, a plate-like arc cathode, and a control electrode arranged in alignment with the magnetic field of the calutron, the arc.
- cathode being positioned immediately above a collimating electrode of the ion source are chamber, which chamber contains a vapor through which an arc discharge is established.
- the electron source of the ion source unit of a calutron consisted of a directly heated cathode and entailed many disadvantages. Inasmuch as a low voltage and high current is required to bring the filamentary cathode to thermionic emission, regulation and adjustment thereof is difiicult. Further, the physical configuration and position of such cathode exposes it to positive ion bombardment and rapid deterioration.
- the filamentary cathode is shielded from positive ion bombardment by the plate-like arc cathode which can more easily withstand the positive ion bombardment and resulting deterioration.
- the filamentary cathode is brought to thermionic emission, an adjustable potential is applied to the are cathode with respect to the filamentary cathode and an adjustable bias is applied to the control electrode, which, if of proper geometry and disposition, will draw very little current.
- the adjustment and regulation of the improved electron source is both simple and eflicient.
- FIG. 1 is a diagrammatic plan view of a calutron into which there may be incorporated an ion source embodying the present invention
- Fig. 2 is a diagrammatic sectional view of the calutron taken along the line 2-2 in Fig. 1
- Fig. 3 is a schematic perspective view of the electrode arrangement in a calutron ion source embodying the present invention
- Fig. 4 is a longitudinal sectional view of a calutron ion source embodying the present invention
- Fig. 5 is a front elevacation of Ernest 0. Lawrence, Serial No.
- Such a calutron essentially comprises means for vaporizing a quantity of material containing an element that is to be enriched with a selected one of its several isotopes; means for subjecting the vapor to ionization, whereby at least a portion of the vapor is ionized causing ions of the several isotopes of the element to be produced; electrical means for segregating the ions from the un-ionized vapor and for accelerating the segregated ions to relatively high velocities; electromagnetic means for deflecting the ions along curved paths, the radii of curvature of the paths of the ions being proportional to the square roots of the masses of the ions, whereby the ions are concentrated in accordance with their masses; and means for de-ionizing A and collecting the ions of the selected isotope thus concentrated, thereby to produce a deposit of the element enriched with the selected isotope.
- the magnetic field structure including upper and lower pole pieces 11 and 12, provided with substantially fiat parallel spaced apart pole faces, and a tank 13 disposed between The pole pieces 11 and 3.2 carry windings, not shown, which are adapted to be energized in order to produce a substantialiy uniform and relatively strong magnetic field therebetween, which magnetic field passes through the tank
- the tank 13 is of tubular configuration, being substantially crescentshaped in plan, and comprising substantially flat parallel spaced-apart top and bottom walls 14 and 15, upstanding curved inner and outer side walls 16 and 17, and end walls 18 and 19.
- the end walls 18 and 19 close the opposite ends of the tubular tank 13 and are adapted to be removably secured in place, whereby the tank 13 is hermetically sealed.
- vacuum pumping apparatus is associated with the tank 13, whereby the interior of the tank 13 may be evacuated to a pressure of the order of lO to 10' mm. Hg.
- the component parts of the tank 13 are formed of steel, the top and bottom walls 14 and 15 thereof being spaced a short distance from the pole faces of the upper and lower pole pieces 11 and 12 respectively, the tank 13 being retained in such position in any suitable manner, whereby the top and bottom walls 14 and 15 constitute in effect pole pieces with respect to the interior of the tank 13, as explained more fully hereinafter.
- the removable end wall 18 suitably supports a source unit 2% comprising a charge receptacle 21 and a communicating arc-block 22.
- An electric heater 23 is arranged in heat exchange relation with the charge receptacle 21 and is adapted to be connected to a suitable source of heater supply, whereby the charge receptacle 21 may be appropriately heated, the charge receptacle 21 being formed of steel or the like.
- the arc-block 22 is formed, at least partially, of carbon or graphite and is substantially C-shaped in plan, an upstanding slot 24 being formed in the wall thereof remote from the charge receptacle 21.
- the arc-block 22 is of hollow construction, the cavity therein communicating with the interior of the charge receptacle 21.
- the removal end wall 18 carries a filamentary cathode 25 adapted to be connected to a suitable source of filament suply, the filamentary cathode 25 overhanging the upper end of the arc-block 22 and arranged in alignment with respect to the upper end of the cavity formed therein.
- the arc-block 22 carries an anode 26 disposed adjacent the lower end thereof and arranged in alignment with respect to the cavity formed therein.
- the arc-block 22 carries a collimating electrode 27 disposed adjacent the upper end thereof and having an elongated collimating slot 28 formed therethrough and arranged in alignment with respect to the filamentary cathode 25 as Well as the anode 26 and the cavity formed in the arc-block 22.
- Both the anode 26 and the collimating electrode 27 are electrically connected to the source unit 20 which in turn is grounded; likewise, the tank 13 is grounded. Also, the filamentary cathode 25 and the cooperating anode 26 are adapted to be connected to a suitable source of arc supply. It should be noted that the above-described electrode arrangement is disclosed in the copending application of Oppenheimer, Serial No. 523,544, filed February 23, 1944.
- the removable end wall 18 carries ion accelcrating structure 39 formed of carbon or graphite and disposed in spaced-apart relation with respect to the wall of the arc-block 22 in which the slot 24 is formed. More specifically, a slit 40 is formed in the ion accelerating structure 39 and arranged in substantial alignment with respect to the slot 24 formed in the wall of the arc-block 22.
- a suitable source of accelerating electrode supply is adapted to be connected between the arc-block 22 and the ion accelerating structure 39, the positive and negative terminals of the supply mentioned being respectively connected to the arc-block 22 and to the ion accelerating structure 39. Further, the positive terminal of the ion accelerating potential is grounded.
- the removable end wall 19 suitably supports a collector block 29 formed of stainless steel or the like and provided with two laterally spaced-apart cavities or pockets 30 and 31 which respectively communicate with aligned slots 32 and 33 formed in the wall of the collector block 29 disposed remote from the removable end wall 19. It is noted that the pockets 30 and 31 are adapted to receive two constituent isotopes of an element which have been separated in the calutron 10, as explained more fully hereinafter.
- the inner wall 16 suitably supports a tubular liner 34 formed of copper or the like, rectangular in vertical cross-section, disposed within the tank 13 and spaced from the walls 14, 15, 16 and 17.
- tubular liner 34 terminates adjacent the accelerating structure 39; and the other end of the tubular liner 34 terminates adjacent the collector block 29; the tubular liner 34 constituting an electrostatic shield for the high velocity ions traversing the curved paths between the slit 40 formed in the ion accelerating structure 39 and the slots 32 and 33 formed in the collector block 29, as explained more fully hereinafter. Finally, the tubular liner 34 is electrically connected to the ion accelerating structure 39 and to the collector block 29.
- the source unit 20 and the tank 13 are connected to the positive grounded terminal of the accelerating electrode supply; while the ion accelerating structure 39, the tubular liner 34 and the collector block 29 are connected to the ungrounded negative terminal of the accelerating electrode supply; the ion accelerating structure 39, the tubular liner 3-6 and the collector block 29 being electrically insulated from the component parts of the tank 13.
- a charge comprising a compound of the element to be treated is placed in the charge receptacle 21, the compound of the element mentioned being one which may be readily vaporized.
- the end walls 18 and 19 are securely attached to the open ends of the tank 13, whereby the tank 13 is hermetically sealed.
- the various electrical connections are completed and operation of the vacuum pumping apparatus, not shown, associated with the tank 13 is initiated.
- a pressure of the order of 10- to 10 mm. Hg is established within the tank 13, the electric circuits for the windings, not shown, associated with the pole pieces 11 and 12 are closed and adjusted, whereby a predetermined magnetic field is established therebetween traversing the tank 13.
- the electric circuit for the heater 23 is closed, whereby the charge in the charge receptacle 21 is heated and vaporized. The vapor fills the charge receptacle 21 and is conducted into the communicating cavity formed in the arc-block 22.
- the electric circuit for the filamentary cathode 25 is closed, whereby the filamentary cathode is heated and rendered electron emissive. Then the electric circuit between the filamentary cathode 25 and the anode 26 is closed, whereby an arc discharge is struck therebetween, electrons proceeding from the filamentary cathode 25 through the collimating slot 23 formed in the collimating electrode 27 to the anode 26.
- the collimating slot 28 formed in the collimating electrode 27 defines the cross-section of the stream of electrons proceeding into the arc-block 22, whereby the arc discharge has a ribhon-like configuration and breaks up the molecular form of the compound of the vapor to a considerable extent, producing positive ions of the element that is to be enriched with the selected one of its isotopes.
- the electric circuit between the arc-block 22 and the ion accelerating structure 39 is completed, the ion accelerating structure 39 being at a high negative potential with respect to the arc-block 22, whereby the positive ions in the arc-block 22 are attracted by the ion accelcrating structure 39 and accelerated through the voltage impressed therebetween. More particularly the positive ions proceed from the cavity formed in the arc-block 22 through the slot 24 formed in the wall thereof, and across the space between the ion accelerating structure 39 and the adjacent wall of the arc-block 22, and thence through the slit 40 formed in the ion accelerating structure 39 into the interior of the tubular liner 34.
- the high-velocity positive ions form a vertical upstanding ribbon or beam proceeding from the cavity formed in the arc-block 22 through the slot 24 and the aligned slit 40 into the tubular liner 34.
- the collector block 29, as well as the tubular liner 34, is electrically connected to the ion accelerating structure 39, whereby there is an electricfield-free path for the high-velocity positive ions disposed between the ion accelerating structure 39 and the collector block 29 within the tubular liner 34.
- the highvelocity positive ions entering the adjacent end of the liner 34 are deflected from their normal straight-line path and from a vertical plane passing through the slot 24 and the aligned slit 40, due to the efiect of the relatively strong magnetic field maintained through the space within the tank 13 and the liner 34 through which the positive ions travel, whereby the positive ions describe arcs, the radii of which are proportional to the square roots of the masses of the ions and consequently of the isotopes of the element mentioned.
- ions of the relatively light isotope of the elements describe an interior arc of relatively short radius and are focused through the slot 32 into the pocket 30 formed in the collector block 29; whereas ions of the relatively heavy isotope of the element describe an exterior arc of relatively long radius and are focused through the slot 33 into the pocket 31 formed in the collector block 29. Accordingly, the relatively light ions are collected in the pocket 30 and are de-ionized to produce a deposit of the relatively light isotope of the element therein; while the relatively heavy ions are collected in the pocket 31 and are de-ionized to produce a deposit of the relatively heavy isotope of the element therein.
- a calutron especially designed for the production of uranium enriched with the isotope U
- the compound of uranium which is suggested as a suitable charge in the charge receptacle 21 is UCl i, as this compound may be readily vaporized and the molecular form of the vapor may be readily broken up to form positive ions of uranium with great facility.
- uranium enriched with U is collected in the pocket 30 of the collector block 29, and uranium comprising principally U is collected in the pocket 31 of the collector block 29.
- the deposit of uranium collected in the pocket 30 of the collector block 29 contains considerable amounts of U in view of the fact that this isotope comprises the dominant constituent of normal uranium. Furthermore, the deposit of uranium collected in the pocket 30 of the collector block 29 contains a considerably increased amount of U in view of the fact that it is not ordinarily feasible to separate U and U in the production of relatively large quantities of uranium enriched with U for commercial purposes. Accordingly, in this example the uranium deposited in the pocket 30 of the collector block 29 is considerably enriched, both with U and with U and considerably impoverished with respect to U as compared to natural or normal uranium.
- the ion source unit 20 In the operation of the calutron 10, it is highly desirable that a relatively intense stable beam of positive ions be projected by the ion accelerating structure 39, through the liner 34, toward the collector block 29; which operating condition requires that the source unit 20 be productive of a steady and copious supply of positive ions.
- the are discharge through the cavity in the arc-block 22 must be both relatively intense and uniform.
- it is desirable that such an arc discharge should be steady and free from both intensity and position variations in order that the ion source unit 20 be productive of a highly continuous, copious and uniform supply of positive ions.
- the ion source unit 20 should be so constructed and arranged that the parts thereof are subjected to minimum wear and erosion, whereby the unit has a long life and an efficient operating characteristic.
- this ion source unit 100 comprises an electron source 101, a plate-like collimating electrode 124 formed of tungsten, molybdenum, or the like, and a plate-like anode 127 formed of tungsten or the like.
- the electron source 101 and the electrodes 124 and 127 are arranged in alignment with the magnetic field of the calutron, the direction of the field between the north pole and the south pole of the field structure being indicated by the arrow 53.
- a substantially U-shaped filamentary or first cathode 121 formed of tungsten or the like and arranged in a vertical plane parallel to the magnetic field, a platelike are cathode 117 formed of tungsten or the like and positioned above and adjacent to the collimating electrode 124, and a plate-like control electrode 114 formed of tungsten or the like having a longitudinal slot 104 formed therein, the control electrode 114 being disposed between the filamentary cathode 121 and the arc cathode 117.
- the electrodes constituting the ion source unit 100 are all arranged in alignment with the magnetic field 53 of the calutron and that the electrodes 114, 117, 124 and 127 are disposed in planes normal to the magnetic field 53.
- the longitudinal slot 104 formed in the control electrode 114 and a longitudinal slot formed in the collimating electrode 124 are parallel one to the other.
- the filamentary cathode 121 is disposed in a vertical plane and the longitudinal slot 104 formed in the control electrode 114 is of such configuration and is so positioned relative to the filamentary cathode 121 that the projection of the filamentary cathode along the magnetic field entirely passes through the longitudinal slot 104.
- the control electrode 114 is disposed 0.020 below the filamentary cathode 121 control electrode 114 and is of 0.060" thickness, the longitudinal slot 104 formed in the Q electrode 114 being 0.750" x 0.094" and being aligned extends about 0.094" beyond the front edge of the longitudinal slot 104 formed in the control electrode 114.
- the filamentary cathode 121 is connected by way of an adjustable resistor 102a to a suitable source of filament supply indicated as a battery 103a; while the filamentary cathode 121 and the control electrode 114 are respectively connected by way of a potentiometer 130 to the terminals of a suitable source of control electrode supply. Further, the filamentary cathode 121 and the arc cathode 117 are respectively connected by way of a potentiometer 132 to the negative and positive terminals of a suitable source of cathode supply.
- the above connections constitute the electrical arrangement of the electron source 101 of the arc mechanism; whereas the arc cathode 117 and the anode 127 are respectively connected to the negative and positive terminals of a suitable source of arc supply, the collimating electrode also being electrically connected to the anode 127 thus completing the electric network of the ion source unit 100.
- the current flowing through the filamentary cathode 121 is adjusted by means of the adjustable resistor 102a until the filamentary cathode 121 becomes electron emissive.
- the cathode supply circuit is thence completed so that electrons emitted by the filamentary cathode 121 are accelerated to and bombard the arc cathode 117, thereby raising the temperature of the arc cathode 117 to incandescence and to electron emission.
- the control electrode supply circuit is completed thus applying a bias to the control electrode 114.
- the potential of the cathode supply the energy with which the electrons leaving the filamentary cathode 121 bombard the arc cathode 117 may be regulated. Further, by varying the potential of the control electrode supply and consequently the impressed bias on the control electrode 114 with respect to the filamentary cathode 121 the number of electrons which are emitted by the filamentary cathode 121 and bombard the arc cathode 117 may be space charge controlled.
- the control electrode current will be small even though a large positive bias is applied thereto. This feature is of great advantage since the current density of the electron stream bombarding the arc cathode 117 may be simply adjusted with a minimum dissipation of current.
- the electron source arrangement 101 affords u a variable source of electrons for an arc discharge of the ion source unit which requires little additional apparatus of low current carrying capacity.
- the electron emission of the arc cathode 117 may be also adjusted by varying the cathode supply voltage; but since the current output of the cathode supply is substantially high and the voltage swing necessary for a given change in the electron emission of the arc cathode 117 is greater than the voltage swing required on the control electrode 114, this method is not as facile as the method employing the control electrode. However either of these methods of control is easier than the previously used method of control by adjusting a large current in a directly heated cathode. Furthermore, inasmuch as the potential of the control electrode 114 relative to the arc cathode 117 is negative, the electrons emitted from the upper face of the arc cathode 117 will not bombard the control electrode 114.
- the electrons emitted from the lower face of the arc cathode 117 are accelerated toward the collimating electrode 124, some of the electrons passing through the longitudinal slit 125 formed in the collimating electrode 124, which collimating slit defines the cross-section of the ionizing electron stream which is projected into the gaseous region between the collimating electrode 124 and the anode 127.
- the electrons thus projected into the gaseous region between the collimating electrode 124 and the anode 127 result in a discharge therethrough.
- This discharge through this region occurs between the arc cathode 117 and the anode 127 and is of the arc type, being characterized by a high current, a low voltage drop and a luminous plasma.
- Zone of intense ionization having a cross-section of the same shape as the longitudinal slit 125, this zone constituting part of the arc discharge between the arc cathode 117 and the anode 127. It should be noted that the aforesaid zone of intense ionization has a ribbon-like configuration and is believed to be a plasma region with little variation in potential.
- the source unit 100 comprising a charge receptacle 99 and an arc-block 102.
- the charge receptacle 99 comprises wall structure, including a removable cover 101a, defining an upstanding cylindrical cavity 103 therein, that is adapted to receive a removable cylindrical charge bottle 104a containing a charge 105 which is to be vaporized.
- the arc-block 102 comprises wall structure defining an upstanding vapor distributing chamber 106 and an upstanding arc chamber 107 therein, the cavity 103 communicating with the vapor distributing chamber 106 through a tubular member 108 supported by the wall structure of the charge receptacle 99 and the wall structure of the arc-block 102.
- the wall structure of the charge receptacle 99 carries an exteriorly arranged electric heater 109 of any suitable form, whereby the charge receptacle 99 and consequently the charge bottle 104a may be appropriately heated in order to vaporize the charge 105 contained in the charge bottle 104a.
- the wall structure of the arc-block 102 carries an exteriorly arranged electric heater 110 of any suitable form, whereby the arc-block 102, and more particularly the vapor distributing chamber 106 therein, may be heated in order to prevent condensation of the contained vapor, as explained more fully hereinafter.
- the wall structure of the arc block 102 comprises a substantially inverted U-shaped frame member 111, supporting an upstanding baffie plate 112, the frame member 111 and the bafile plate 112 being formed of carbon or graphite.
- the frame member 111 is secured to the wall structure of the arc-block 102 by an arrangement comprising two upstanding strips 113, and comprises a top wall 128, two upstanding substantially parallel spaced-apart side walls 115 and a front wall 116, the front wall 116 having a centrally disposed longitudinal slot 117a formed therein and communicating with the arc chamber 107.
- baflle plate 112 The side edges of the baflle plate 112 are spaced a short distance from the side walls 115 of the frame member 111 in order to provide communication between the vapor distributing chamber 106 and the arc chamber 107, the baffle plate 112 defining the boundary between the chambers mentioned.
- the wall structure of the charge receptacle 99 carries a standard 118 which supports cathode structure 119 in cooperating relationship with respect to the arc-block 102. More particularly, the cathode structure 119 comprises two terminals 120 supporting the opposite ends of the substantially U-shaped filamentary cathode 121, the
- the control electrode 114 is disposed immediately below the filamentary cathode 121 and is connected by way of the lead 115a to a terminal of the control electrode supply, the other terminal of the control electrode supply being connected to the filamentary cathode 121.
- the arc cathode 117 is positioned below the control electrode 114 and the cathode supply is applied between the filamentary cathode 121 and the arc cathode 117 as has been heretofore described. It should be noted that insulating members 129 are inserted between the terminals of the filamentary cathode 121 and the control electrode 114, and between the terminals of the control electrode 114 and the arc cathode 117.
- the central portion of the top wall 128 of the frame member 111 has a transversely extending slot 122 formed therethrough communicating with the arc chamber 107.
- the upper end of the transverse slot 122 is provided with a counterrecess 123 extending thereabout which receives the collimating electrode 124, the collimating electrode 124 having the transversely extending slot 125 formed therethrough, as previously noted, and communicating with the transverse slot 122 formed in the top wall 128 and consequently with the arc chamber 107, the length of the slot 125 being greater than the width of the slot 117a formed in the front wall 116.
- the arc cathode 117 is spaced a short distance above the collimating electrode 124; the filamentary cathode 121, the
- a laterally extending slot 126 is formed in the front wall 116 of the frame member 111 adjacent the lower end thereof, and supports the anode 127 extending into the arc chamber 107 in vertical alignment with the transverse slot 125 formed in the collimating electrode 124.
- the negative and positive terminals of the arc supply are respectively connected to the arc cathode 117 and to the arcblock 102, the anode 127 and the collimating electrode 124 being connected together by the frame member 111, and consequently by way of the arc-block 102 to the positive terminal of the arc supply mentioned, as previously noted.
- the charge receptacle 99 and consequently the charge bottle 104a are heated, whereby the charge 105 is vaporized, filling the cavity 103 in the charge receptacle 99.
- the vapor passes through the tubular member 108 into the vapor distributing chamber 106, whereby this chamber is filled with the vapor.
- the vapor is thoroughly diffused in the vapor distributing chamber 106 and passes around the side edges of the baffle plate 112 into the arc chamber 107, whereby this chamber is filled with the vapor. More particularly, the arc chamber 107 is thoroughly and uniformly filled with the vapor to be ionized, due to the arrangement of the vapor distributing chamber 106 and the baffle plate 112.
- the filamentary cathode 121 When the circuit for the filamentary cathode 121 is completed, the filamentary cathode 121 is heated and rendered electron emissive; and when the arc cathode circuit is completed between the filamentary cathode 121 and the arc cathode 117, electrons are projected from the filamentary cathode 121 through the slot 104 formed in the control electrode 114 and bombard the arc cathode 117 thus rendering the arc cathode 117 electron emissive. Further, the control electrode supply circuit is closed and by varying the potential applied to the control electrode 114 the number of electrons bombarding the arc cathode 117 and consequently the electron emission thereof may be adjusted.
- the are supply circuit is closed and some of the electrons emitted by the arc cathode 117 are projected through the transverse slot 125 formed in the collimating electrode 124' into the arc chamber 107 and proceed toward the anode 127.
- the collimating electrode 124 causes a stream of electrons having a ribbon-like configuration to be projected through the are chamber 107, whereby the vapor in the are chamber 107 is ionized.
- the width of the stream of electrons is greater than the width of the upstanding slot 117a formed in the front wall 116, whereby any vapor flowing through the arc chamber 107 and the slot 117a must traverse the electron stream and thus be subjected to its ionizing influence.
- the positive ions produced in the arc chamber 107 are drawn through the upstanding slot 117a formed in the front wall 116 of the frame member 111 by the associated ion accelerating structure, whereby a beam of positive ions having a substantially ribbon-like configuration is projected into the adjacent end of the associated liner and directed toward the cooperating collector block.
- An ion source unit comprising means for establishing a magnetic field, a substantially U-shaped first cathode, a second cathode disposed transversely of said magnetic field with the discharge path between said cathodes aligned with said magnetic field, an anode mounted parallel to said second cathode with the path therebetween aligned with said magnetic field, a hollow arcblock defining a gaseous region therein positioned between said second cathode and said anode, means for rendering said first cathode electron emissive, means for applying a positive potential to said second cathode relative to said first cathode, whereby electrons emitted by said first cathode bombard said second cathode to raise said second cathode to an electron emissive temperature, a plate-shaped control electrode having an elongated slot with dimensions substantially equal to said first cathode disposed between said cathodes parallel to said first cathode, whereby the electron emission between said cathodes passes through the slot in
- a plate-shaped collimating electrode having an elongated slot disposed transversely of said magnetic field between said second cathode and said anode, the slot of said collirnating electrode being positioned parallel to the slot in said control electrode for defining the cross section of said are, means for maintaining said collimating electrode at the potential of said anode, means for supplying gas to be ionized to said gaseous region, said arc-block having a slit in a wall thereof aligned with said magnetic field, and means for withdrawing a beam of ions from said gaseous region through said slit transversely of said magnetic field.
- An electric discharge device comprising means for establishing a magnetic field, a substantially U-shaped filamentary cathode disposed in alignment with said magnetic field, a plate-shaped cathode disposed transversely of said magnetic field and spaced apart from said filamentary cathode with the path therebetween extending along said magnetic field, means for rendering said filamentary cathode electron emissive, a source of potential for rendering said plate-shaped cathode positive relative to said filamentary cathode, whereby electrons emitted by said filamentary cathode bombard said plate-shaped cathode to raise said plate-shaped cathode to an electron emissive temperature, a plate-shaped control electrode disposed transversely of said magnetic field between said cathode, said control electrode having an elongated slot extended parallel to and aligned with said filamentary cathode and having dimensions substantially equal to said filamentary cathode for defining the cross section of said electron emission between said cathodes, a source of potential connected between said filamentary catho
- An electric discharge device comprising a vacuum envelope, a single gaseous region disposed therein, a filamentary cathode therein, and an anode therein, a second cathode therein disposed intermediate said filamentary cathode and said anode, means for rendering said filamentary cathode electron emissive, means for applying a positive potential to said second cathode relative to said filamentary cathode, whereby electrons emitted by said filamentary cathode create a nonplasma discharge that bombards said second cathode to raise said second cathode to an electron emissive temperature, a control electrode having an elongated slot formed therein positioned between said cathodes, said slot being disposed parallel to said filamentary cathode to limit the bombardment area of said second cathode, means for applying a potential to said control electrode relative to said filamentary cathode,
- an ion source unit comprising a hollow arc block defining a gaseous region and having an elongated exit slit in a front wall thereof, said slit being terminated at one end by an inwardly extended plate electrically conneted to said are block and at the other end by a top wall of said are block having a slot therein, said slot being disposed parallel to said front wall adjacent said slit and aligned with said plate, a substantially U- shaped first cathode disposed external of said are block and parallel to said slot, a plate-shaped second cathode disposed parallel to said slotted top wall and between said slotted top wall and said first cathode, a plate-shaped control electrode having an elongated aperture disposed parallel to said second cathode and between said cathodes,
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Description
Sept. 13, 1955 L. F. wouTE 2,717,962
ELECTRIC DISCHARGE D fEIVICES Filed March 31, 1944 2 Sheets-Sheet l HEATER 6 UPPLY F/LAMENT SUPPLY ARC SUPPLY ACCELERATING ELECTRODE SUPPLY mm Q Ifg. 5'. /O3a /02a o o A30 F ILA/145N7- /04 CONTROL CONT/POL ELECTRODE ELECTRODE H4 SUPPLY HPC CATHODE COLL/MAT/NG CATHODE ELECTRODE SUPPLY A:
+ ELECT/FONS ANOOZ INVENTOR. L0 UIS F. W0 UTERS United States Patent ELECTRIC DISCHARGE DEVICES Louis F. Wouters, Berkeley, Calif., assignor to the Unit-ed States of America as represented by the United States Atomic Energy Commission Application March 31, 1944, Serial No. 528,818
Claims. (Cl. 250-495) tron ion source of improved construction and arrangement that is eflicient in operation and subject to minimum wear and erosion.
A further object of the invention is to provide an arc discharge device with an improved electrode arrangement for increasing the life of the arc cathode.
In carrying out the objects of the present invention, a calutron ion source is provided with an improved electron source including a filamentary cathode, a plate-like arc cathode, and a control electrode arranged in alignment with the magnetic field of the calutron, the arc.
cathode being positioned immediately above a collimating electrode of the ion source are chamber, which chamber contains a vapor through which an arc discharge is established. Heretofore, the electron source of the ion source unit of a calutron consisted of a directly heated cathode and entailed many disadvantages. Inasmuch as a low voltage and high current is required to bring the filamentary cathode to thermionic emission, regulation and adjustment thereof is difiicult. Further, the physical configuration and position of such cathode exposes it to positive ion bombardment and rapid deterioration. With the improved arrangement, the filamentary cathode is shielded from positive ion bombardment by the plate-like arc cathode which can more easily withstand the positive ion bombardment and resulting deterioration. To operate the improved electron source the filamentary cathode is brought to thermionic emission, an adjustable potential is applied to the are cathode with respect to the filamentary cathode and an adjustable bias is applied to the control electrode, which, if of proper geometry and disposition, will draw very little current. The adjustment and regulation of the improved electron source is both simple and eflicient.
The invention, both as to its organization and method of operation, together with other objects and advantages thereof, will best be understood by reference to the following specification taken in connection with the accompanying drawings, in which Figure 1 is a diagrammatic plan view of a calutron into which there may be incorporated an ion source embodying the present invention; Fig. 2 is a diagrammatic sectional view of the calutron taken along the line 2-2 in Fig. 1; Fig. 3 is a schematic perspective view of the electrode arrangement in a calutron ion source embodying the present invention; Fig. 4 is a longitudinal sectional view of a calutron ion source embodying the present invention; Fig. 5 is a front elevacation of Ernest 0. Lawrence, Serial No. 557,784, filed October 9, 1944, now U. S. Patent No. 2,709,222, and is employed to separate the constituent isotopes of an element and, more particularly, to increase the proportion of a selected isotope in an element containing several isotopes in order to produce the element enriched with the selected isotope. For example, the machine is especially useful in producing uranium enriched with U Such a calutron essentially comprises means for vaporizing a quantity of material containing an element that is to be enriched with a selected one of its several isotopes; means for subjecting the vapor to ionization, whereby at least a portion of the vapor is ionized causing ions of the several isotopes of the element to be produced; electrical means for segregating the ions from the un-ionized vapor and for accelerating the segregated ions to relatively high velocities; electromagnetic means for deflecting the ions along curved paths, the radii of curvature of the paths of the ions being proportional to the square roots of the masses of the ions, whereby the ions are concentrated in accordance with their masses; and means for de-ionizing A and collecting the ions of the selected isotope thus concentrated, thereby to produce a deposit of the element enriched with the selected isotope.
Referring now more particulariy to Figs. 1 and 2 of the drawings, there is illustrated a representative example "of a calutron 10 of the character noted, that comprises the pole faces of the pole pieces 11 and 12.
. 13 and the various parts housed therein.
magnetic field structure including upper and lower pole pieces 11 and 12, provided with substantially fiat parallel spaced apart pole faces, and a tank 13 disposed between The pole pieces 11 and 3.2 carry windings, not shown, which are adapted to be energized in order to produce a substantialiy uniform and relatively strong magnetic field therebetween, which magnetic field passes through the tank The tank 13 is of tubular configuration, being substantially crescentshaped in plan, and comprising substantially flat parallel spaced-apart top and bottom walls 14 and 15, upstanding curved inner and outer side walls 16 and 17, and end walls 18 and 19. The end walls 18 and 19 close the opposite ends of the tubular tank 13 and are adapted to be removably secured in place, whereby the tank 13 is hermetically sealed. Also, vacuum pumping apparatus, not shown, is associated with the tank 13, whereby the interior of the tank 13 may be evacuated to a pressure of the order of lO to 10' mm. Hg. Preferably, the component parts of the tank 13 are formed of steel, the top and bottom walls 14 and 15 thereof being spaced a short distance from the pole faces of the upper and lower pole pieces 11 and 12 respectively, the tank 13 being retained in such position in any suitable manner, whereby the top and bottom walls 14 and 15 constitute in effect pole pieces with respect to the interior of the tank 13, as explained more fully hereinafter.
The removable end wall 18 suitably supports a source unit 2% comprising a charge receptacle 21 and a communicating arc-block 22. An electric heater 23 is arranged in heat exchange relation with the charge receptacle 21 and is adapted to be connected to a suitable source of heater supply, whereby the charge receptacle 21 may be appropriately heated, the charge receptacle 21 being formed of steel or the like. The arc-block 22 is formed, at least partially, of carbon or graphite and is substantially C-shaped in plan, an upstanding slot 24 being formed in the wall thereof remote from the charge receptacle 21. Thus, the arc-block 22 is of hollow construction, the cavity therein communicating with the interior of the charge receptacle 21.
Also, the removal end wall 18 carries a filamentary cathode 25 adapted to be connected to a suitable source of filament suply, the filamentary cathode 25 overhanging the upper end of the arc-block 22 and arranged in alignment with respect to the upper end of the cavity formed therein. The arc-block 22 carries an anode 26 disposed adjacent the lower end thereof and arranged in alignment with respect to the cavity formed therein. Also, the arc-block 22 carries a collimating electrode 27 disposed adjacent the upper end thereof and having an elongated collimating slot 28 formed therethrough and arranged in alignment with respect to the filamentary cathode 25 as Well as the anode 26 and the cavity formed in the arc-block 22. Both the anode 26 and the collimating electrode 27 are electrically connected to the source unit 20 which in turn is grounded; likewise, the tank 13 is grounded. Also, the filamentary cathode 25 and the cooperating anode 26 are adapted to be connected to a suitable source of arc supply. It should be noted that the above-described electrode arrangement is disclosed in the copending application of Oppenheimer, Serial No. 523,544, filed February 23, 1944.
Further, the removable end wall 18 carries ion accelcrating structure 39 formed of carbon or graphite and disposed in spaced-apart relation with respect to the wall of the arc-block 22 in which the slot 24 is formed. More specifically, a slit 40 is formed in the ion accelerating structure 39 and arranged in substantial alignment with respect to the slot 24 formed in the wall of the arc-block 22. A suitable source of accelerating electrode supply is adapted to be connected between the arc-block 22 and the ion accelerating structure 39, the positive and negative terminals of the supply mentioned being respectively connected to the arc-block 22 and to the ion accelerating structure 39. Further, the positive terminal of the ion accelerating potential is grounded.
The removable end wall 19 suitably supports a collector block 29 formed of stainless steel or the like and provided with two laterally spaced-apart cavities or pockets 30 and 31 which respectively communicate with aligned slots 32 and 33 formed in the wall of the collector block 29 disposed remote from the removable end wall 19. It is noted that the pockets 30 and 31 are adapted to receive two constituent isotopes of an element which have been separated in the calutron 10, as explained more fully hereinafter. Further, the inner wall 16 suitably supports a tubular liner 34 formed of copper or the like, rectangular in vertical cross-section, disposed within the tank 13 and spaced from the walls 14, 15, 16 and 17. One end of the tubular liner 34 terminates adjacent the accelerating structure 39; and the other end of the tubular liner 34 terminates adjacent the collector block 29; the tubular liner 34 constituting an electrostatic shield for the high velocity ions traversing the curved paths between the slit 40 formed in the ion accelerating structure 39 and the slots 32 and 33 formed in the collector block 29, as explained more fully hereinafter. Finally, the tubular liner 34 is electrically connected to the ion accelerating structure 39 and to the collector block 29. Thus, it will be understood that the source unit 20 and the tank 13 are connected to the positive grounded terminal of the accelerating electrode supply; while the ion accelerating structure 39, the tubular liner 34 and the collector block 29 are connected to the ungrounded negative terminal of the accelerating electrode supply; the ion accelerating structure 39, the tubular liner 3-6 and the collector block 29 being electrically insulated from the component parts of the tank 13.
Considering now the general principle of operation of the calutron 10, a charge comprising a compound of the element to be treated is placed in the charge receptacle 21, the compound of the element mentioned being one which may be readily vaporized. The end walls 18 and 19 are securely attached to the open ends of the tank 13, whereby the tank 13 is hermetically sealed. The various electrical connections are completed and operation of the vacuum pumping apparatus, not shown, associated with the tank 13 is initiated. When a pressure of the order of 10- to 10 mm. Hg is established within the tank 13, the electric circuits for the windings, not shown, associated with the pole pieces 11 and 12 are closed and adjusted, whereby a predetermined magnetic field is established therebetween traversing the tank 13. The electric circuit for the heater 23 is closed, whereby the charge in the charge receptacle 21 is heated and vaporized. The vapor fills the charge receptacle 21 and is conducted into the communicating cavity formed in the arc-block 22. The electric circuit for the filamentary cathode 25 is closed, whereby the filamentary cathode is heated and rendered electron emissive. Then the electric circuit between the filamentary cathode 25 and the anode 26 is closed, whereby an arc discharge is struck therebetween, electrons proceeding from the filamentary cathode 25 through the collimating slot 23 formed in the collimating electrode 27 to the anode 26. The collimating slot 28 formed in the collimating electrode 27 defines the cross-section of the stream of electrons proceeding into the arc-block 22, whereby the arc discharge has a ribhon-like configuration and breaks up the molecular form of the compound of the vapor to a considerable extent, producing positive ions of the element that is to be enriched with the selected one of its isotopes. A more detailed explanation of the operation of the aforesaid arrangement may be had by referring to the copending application of Oppenheimer, Serial No. 523,544, filed Feb. 23, 1944.
The electric circuit between the arc-block 22 and the ion accelerating structure 39 is completed, the ion accelerating structure 39 being at a high negative potential with respect to the arc-block 22, whereby the positive ions in the arc-block 22 are attracted by the ion accelcrating structure 39 and accelerated through the voltage impressed therebetween. More particularly the positive ions proceed from the cavity formed in the arc-block 22 through the slot 24 formed in the wall thereof, and across the space between the ion accelerating structure 39 and the adjacent wall of the arc-block 22, and thence through the slit 40 formed in the ion accelerating structure 39 into the interior of the tubular liner 34. The high-velocity positive ions form a vertical upstanding ribbon or beam proceeding from the cavity formed in the arc-block 22 through the slot 24 and the aligned slit 40 into the tubular liner 34.
As previously noted, the collector block 29, as well as the tubular liner 34, is electrically connected to the ion accelerating structure 39, whereby there is an electricfield-free path for the high-velocity positive ions disposed between the ion accelerating structure 39 and the collector block 29 within the tubular liner 34. The highvelocity positive ions entering the adjacent end of the liner 34 are deflected from their normal straight-line path and from a vertical plane passing through the slot 24 and the aligned slit 40, due to the efiect of the relatively strong magnetic field maintained through the space within the tank 13 and the liner 34 through which the positive ions travel, whereby the positive ions describe arcs, the radii of which are proportional to the square roots of the masses of the ions and consequently of the isotopes of the element mentioned. Thus, ions of the relatively light isotope of the elements describe an interior arc of relatively short radius and are focused through the slot 32 into the pocket 30 formed in the collector block 29; whereas ions of the relatively heavy isotope of the element describe an exterior arc of relatively long radius and are focused through the slot 33 into the pocket 31 formed in the collector block 29. Accordingly, the relatively light ions are collected in the pocket 30 and are de-ionized to produce a deposit of the relatively light isotope of the element therein; while the relatively heavy ions are collected in the pocket 31 and are de-ionized to produce a deposit of the relatively heavy isotope of the element therein.
After all of the charge in the charge receptacle 21 has been vaporized, all of the electric circuits are interrupted and the end wall 18 is removed so that another charge may be placed in the charge receptacle 21 and subsequently vaporized in the manner explained above. After a suitable number of charges have been vaporized in order to obtain appropriate deposits of the isotopes of the element in the pockets 30 and 31 of the collector block 29, the end wall 19 may be removed and the deposits of the collected isotopes in the pockets 30 and 31 in the collector block 29 may be reclaimed.
Of course, it will be understood that the various dimensions of the parts of the calutron 10, the various electrical potentials applied between the various electrical parts thereof, as well as the strength of the magnetic field between the pole pieces 11 and 12, are suitably correlated with respect to each other, depending upon the mass numbers of the several isotopes of the element which is to be treated therein. In this connection reference is again made to the copending application of Ernest 0. Lawrence, for a complete specification of a calutron especially designed for the production of uranium enriched with the isotope U By way of illustration, it is noted that when the calutron is employed in order to produce uranium enriched with U the compound of uranium which is suggested as a suitable charge in the charge receptacle 21 is UCl i, as this compound may be readily vaporized and the molecular form of the vapor may be readily broken up to form positive ions of uranium with great facility. In this case, uranium enriched with U is collected in the pocket 30 of the collector block 29, and uranium comprising principally U is collected in the pocket 31 of the collector block 29. Also, it is noted that from a practical standpoint, the deposit of uranium collected in the pocket 30 of the collector block 29 contains considerable amounts of U in view of the fact that this isotope comprises the dominant constituent of normal uranium. Furthermore,the deposit of uranium collected in the pocket 30 of the collector block 29 contains a considerably increased amount of U in view of the fact that it is not ordinarily feasible to separate U and U in the production of relatively large quantities of uranium enriched with U for commercial purposes. Accordingly, in this example the uranium deposited in the pocket 30 of the collector block 29 is considerably enriched, both with U and with U and considerably impoverished with respect to U as compared to natural or normal uranium.
In the operation of the calutron 10, it is highly desirable that a relatively intense stable beam of positive ions be projected by the ion accelerating structure 39, through the liner 34, toward the collector block 29; which operating condition requires that the source unit 20 be productive of a steady and copious supply of positive ions. To accomplish this end in the source unit 20, the are discharge through the cavity in the arc-block 22 must be both relatively intense and uniform. Moreover, it is desirable that such an arc discharge should be steady and free from both intensity and position variations in order that the ion source unit 20 be productive of a highly continuous, copious and uniform supply of positive ions. Furthermore, the ion source unit 20 should be so constructed and arranged that the parts thereof are subjected to minimum wear and erosion, whereby the unit has a long life and an efficient operating characteristic.
While the source unit in the calutron disclosed in the previously mentioned copending application of Ernest 0. Lawrence is satisfactory in operation, it does not possess the characteristics noted to the extent desired; nor has it the long life required for most efitcient commercial operatiou.
Referring now more particularly to Fig. 3 of the drawings, the electrode arrangement in the calutron ion source unit embodying the features of the present invention is illustrated schematically in perspective. More particularly, this ion source unit 100 comprises an electron source 101, a plate-like collimating electrode 124 formed of tungsten, molybdenum, or the like, and a plate-like anode 127 formed of tungsten or the like. The electron source 101 and the electrodes 124 and 127 are arranged in alignment with the magnetic field of the calutron, the direction of the field between the north pole and the south pole of the field structure being indicated by the arrow 53.
Considering now the electron source 101, there are provided a substantially U-shaped filamentary or first cathode 121 formed of tungsten or the like and arranged in a vertical plane parallel to the magnetic field, a platelike are cathode 117 formed of tungsten or the like and positioned above and adjacent to the collimating electrode 124, and a plate-like control electrode 114 formed of tungsten or the like having a longitudinal slot 104 formed therein, the control electrode 114 being disposed between the filamentary cathode 121 and the arc cathode 117. Further, it should be noted that the electrodes constituting the ion source unit 100 are all arranged in alignment with the magnetic field 53 of the calutron and that the electrodes 114, 117, 124 and 127 are disposed in planes normal to the magnetic field 53. The longitudinal slot 104 formed in the control electrode 114 and a longitudinal slot formed in the collimating electrode 124 are parallel one to the other. Moreover, it should be noted that the filamentary cathode 121 is disposed in a vertical plane and the longitudinal slot 104 formed in the control electrode 114 is of such configuration and is so positioned relative to the filamentary cathode 121 that the projection of the filamentary cathode along the magnetic field entirely passes through the longitudinal slot 104.
Considering now the structure and dimensional details of the electrodes constituting the electron source 101 of the ion source unit 100, highly satisfactory results have been obtained employing a filamentary cathode of circular cross-section having a diameter of 0.050, the length of the central portion being slightly less than 0.750". The control electrode 114 is disposed 0.020 below the filamentary cathode 121 control electrode 114 and is of 0.060" thickness, the longitudinal slot 104 formed in the Q electrode 114 being 0.750" x 0.094" and being aligned extends about 0.094" beyond the front edge of the longitudinal slot 104 formed in the control electrode 114.
The filamentary cathode 121 is connected by way of an adjustable resistor 102a to a suitable source of filament supply indicated as a battery 103a; while the filamentary cathode 121 and the control electrode 114 are respectively connected by way of a potentiometer 130 to the terminals of a suitable source of control electrode supply. Further, the filamentary cathode 121 and the arc cathode 117 are respectively connected by way of a potentiometer 132 to the negative and positive terminals of a suitable source of cathode supply. The above connections constitute the electrical arrangement of the electron source 101 of the arc mechanism; whereas the arc cathode 117 and the anode 127 are respectively connected to the negative and positive terminals of a suitable source of arc supply, the collimating electrode also being electrically connected to the anode 127 thus completing the electric network of the ion source unit 100.
Considering now the general principle of operation of the ion source unit 100 and more particularly the electron source 101, the current flowing through the filamentary cathode 121 is adjusted by means of the adjustable resistor 102a until the filamentary cathode 121 becomes electron emissive. The cathode supply circuit is thence completed so that electrons emitted by the filamentary cathode 121 are accelerated to and bombard the arc cathode 117, thereby raising the temperature of the arc cathode 117 to incandescence and to electron emission. Thereafter, the control electrode supply circuit is completed thus applying a bias to the control electrode 114. It will be understood that by varying the potential of the cathode supply the energy with which the electrons leaving the filamentary cathode 121 bombard the arc cathode 117 may be regulated. Further, by varying the potential of the control electrode supply and consequently the impressed bias on the control electrode 114 with respect to the filamentary cathode 121 the number of electrons which are emitted by the filamentary cathode 121 and bombard the arc cathode 117 may be space charge controlled. Inasmuch as the filamentary cathode 121 is so positioned that its projection along the magnetic field passes through the longitudinal slot 104 of the control electrode 114, and since the electrons traveling from the filamentary cathode 121 to the arc cathode 117 are confined to paths aligned with the magnetic field, the control electrode current will be small even though a large positive bias is applied thereto. This feature is of great advantage since the current density of the electron stream bombarding the arc cathode 117 may be simply adjusted with a minimum dissipation of current.
Consequently, the electron source arrangement 101 affords u a variable source of electrons for an arc discharge of the ion source unit which requires little additional apparatus of low current carrying capacity. Moreover, the electron emission of the arc cathode 117 may be also adjusted by varying the cathode supply voltage; but since the current output of the cathode supply is substantially high and the voltage swing necessary for a given change in the electron emission of the arc cathode 117 is greater than the voltage swing required on the control electrode 114, this method is not as facile as the method employing the control electrode. However either of these methods of control is easier than the previously used method of control by adjusting a large current in a directly heated cathode. Furthermore, inasmuch as the potential of the control electrode 114 relative to the arc cathode 117 is negative, the electrons emitted from the upper face of the arc cathode 117 will not bombard the control electrode 114.
The electrons emitted from the lower face of the arc cathode 117 are accelerated toward the collimating electrode 124, some of the electrons passing through the longitudinal slit 125 formed in the collimating electrode 124, which collimating slit defines the cross-section of the ionizing electron stream which is projected into the gaseous region between the collimating electrode 124 and the anode 127. The electrons thus projected into the gaseous region between the collimating electrode 124 and the anode 127 result in a discharge therethrough. This discharge through this region occurs between the arc cathode 117 and the anode 127 and is of the arc type, being characterized by a high current, a low voltage drop and a luminous plasma. Accordingly, there is defined a Zone of intense ionization having a cross-section of the same shape as the longitudinal slit 125, this zone constituting part of the arc discharge between the arc cathode 117 and the anode 127. It should be noted that the aforesaid zone of intense ionization has a ribbon-like configuration and is believed to be a plasma region with little variation in potential.
Referring now more particularly to Figs. 4 to 6, inclusive, of the drawings, there are illustrated the structural details of the source unit 100 which is arranged in the magnetic field between the pole pieces of the calutron in the manner previously explained, the source unit 100 comprising a charge receptacle 99 and an arc-block 102. The charge receptacle 99 comprises wall structure, including a removable cover 101a, defining an upstanding cylindrical cavity 103 therein, that is adapted to receive a removable cylindrical charge bottle 104a containing a charge 105 which is to be vaporized. The arc-block 102 comprises wall structure defining an upstanding vapor distributing chamber 106 and an upstanding arc chamber 107 therein, the cavity 103 communicating with the vapor distributing chamber 106 through a tubular member 108 supported by the wall structure of the charge receptacle 99 and the wall structure of the arc-block 102. The wall structure of the charge receptacle 99 carries an exteriorly arranged electric heater 109 of any suitable form, whereby the charge receptacle 99 and consequently the charge bottle 104a may be appropriately heated in order to vaporize the charge 105 contained in the charge bottle 104a. Similarly, the wall structure of the arc-block 102 carries an exteriorly arranged electric heater 110 of any suitable form, whereby the arc-block 102, and more particularly the vapor distributing chamber 106 therein, may be heated in order to prevent condensation of the contained vapor, as explained more fully hereinafter.
More particularly, the wall structure of the arc block 102 comprises a substantially inverted U-shaped frame member 111, supporting an upstanding baffie plate 112, the frame member 111 and the bafile plate 112 being formed of carbon or graphite. The frame member 111 is secured to the wall structure of the arc-block 102 by an arrangement comprising two upstanding strips 113, and comprises a top wall 128, two upstanding substantially parallel spaced-apart side walls 115 and a front wall 116, the front wall 116 having a centrally disposed longitudinal slot 117a formed therein and communicating with the arc chamber 107. The side edges of the baflle plate 112 are spaced a short distance from the side walls 115 of the frame member 111 in order to provide communication between the vapor distributing chamber 106 and the arc chamber 107, the baffle plate 112 defining the boundary between the chambers mentioned.
The wall structure of the charge receptacle 99 carries a standard 118 which supports cathode structure 119 in cooperating relationship with respect to the arc-block 102. More particularly, the cathode structure 119 comprises two terminals 120 supporting the opposite ends of the substantially U-shaped filamentary cathode 121, the
opposite ends of the filamentary cathode 121 being removably clamped in place by the respective terminals 120, and the two terminals being connected to the source of filament supply, as previously noted. The control electrode 114 is disposed immediately below the filamentary cathode 121 and is connected by way of the lead 115a to a terminal of the control electrode supply, the other terminal of the control electrode supply being connected to the filamentary cathode 121. Further, the arc cathode 117 is positioned below the control electrode 114 and the cathode supply is applied between the filamentary cathode 121 and the arc cathode 117 as has been heretofore described. It should be noted that insulating members 129 are inserted between the terminals of the filamentary cathode 121 and the control electrode 114, and between the terminals of the control electrode 114 and the arc cathode 117.
The central portion of the top wall 128 of the frame member 111 has a transversely extending slot 122 formed therethrough communicating with the arc chamber 107. The upper end of the transverse slot 122 is provided with a counterrecess 123 extending thereabout which receives the collimating electrode 124, the collimating electrode 124 having the transversely extending slot 125 formed therethrough, as previously noted, and communicating with the transverse slot 122 formed in the top wall 128 and consequently with the arc chamber 107, the length of the slot 125 being greater than the width of the slot 117a formed in the front wall 116. More particularly, the arc cathode 117 is spaced a short distance above the collimating electrode 124; the filamentary cathode 121, the
Considering now the detailed operation of the source unit 100, when the electric circuit for the heater 109 is completed, the charge receptacle 99 and consequently the charge bottle 104a are heated, whereby the charge 105 is vaporized, filling the cavity 103 in the charge receptacle 99. The vapor passes through the tubular member 108 into the vapor distributing chamber 106, whereby this chamber is filled with the vapor. The vapor is thoroughly diffused in the vapor distributing chamber 106 and passes around the side edges of the baffle plate 112 into the arc chamber 107, whereby this chamber is filled with the vapor. More particularly, the arc chamber 107 is thoroughly and uniformly filled with the vapor to be ionized, due to the arrangement of the vapor distributing chamber 106 and the baffle plate 112.
When the circuit for the filamentary cathode 121 is completed, the filamentary cathode 121 is heated and rendered electron emissive; and when the arc cathode circuit is completed between the filamentary cathode 121 and the arc cathode 117, electrons are projected from the filamentary cathode 121 through the slot 104 formed in the control electrode 114 and bombard the arc cathode 117 thus rendering the arc cathode 117 electron emissive. Further, the control electrode supply circuit is closed and by varying the potential applied to the control electrode 114 the number of electrons bombarding the arc cathode 117 and consequently the electron emission thereof may be adjusted. Thereafter the are supply circuit is closed and some of the electrons emitted by the arc cathode 117 are projected through the transverse slot 125 formed in the collimating electrode 124' into the arc chamber 107 and proceed toward the anode 127. Accordingly, the collimating electrode 124 causes a stream of electrons having a ribbon-like configuration to be projected through the are chamber 107, whereby the vapor in the are chamber 107 is ionized. Moreover, the width of the stream of electrons is greater than the width of the upstanding slot 117a formed in the front wall 116, whereby any vapor flowing through the arc chamber 107 and the slot 117a must traverse the electron stream and thus be subjected to its ionizing influence. The positive ions produced in the arc chamber 107 are drawn through the upstanding slot 117a formed in the front wall 116 of the frame member 111 by the associated ion accelerating structure, whereby a beam of positive ions having a substantially ribbon-like configuration is projected into the adjacent end of the associated liner and directed toward the cooperating collector block.
While there has been described what is at present considered to be the preferred embodiment of the invention, it will be understood that various modifications may be made therein and it is intended to cover in the appended claims all such modifications as fall within the true spirit and scope of the invention.
What is claimed is:
1. An ion source unit comprising means for establishing a magnetic field, a substantially U-shaped first cathode, a second cathode disposed transversely of said magnetic field with the discharge path between said cathodes aligned with said magnetic field, an anode mounted parallel to said second cathode with the path therebetween aligned with said magnetic field, a hollow arcblock defining a gaseous region therein positioned between said second cathode and said anode, means for rendering said first cathode electron emissive, means for applying a positive potential to said second cathode relative to said first cathode, whereby electrons emitted by said first cathode bombard said second cathode to raise said second cathode to an electron emissive temperature, a plate-shaped control electrode having an elongated slot with dimensions substantially equal to said first cathode disposed between said cathodes parallel to said first cathode, whereby the electron emission between said cathodes passes through the slot in said control electrode, means for applying a potential to said control electrode relative to said first cathode, whereby the electron emission between said cathodes may be controlled, means for applying a positive voltage to said anode with respect to said second cathode for establishing an arc,
therebetween, a plate-shaped collimating electrode having an elongated slot disposed transversely of said magnetic field between said second cathode and said anode, the slot of said collirnating electrode being positioned parallel to the slot in said control electrode for defining the cross section of said are, means for maintaining said collimating electrode at the potential of said anode, means for supplying gas to be ionized to said gaseous region, said arc-block having a slit in a wall thereof aligned with said magnetic field, and means for withdrawing a beam of ions from said gaseous region through said slit transversely of said magnetic field.
2. An electric discharge device comprising means for establishing a magnetic field, a substantially U-shaped filamentary cathode disposed in alignment with said magnetic field, a plate-shaped cathode disposed transversely of said magnetic field and spaced apart from said filamentary cathode with the path therebetween extending along said magnetic field, means for rendering said filamentary cathode electron emissive, a source of potential for rendering said plate-shaped cathode positive relative to said filamentary cathode, whereby electrons emitted by said filamentary cathode bombard said plate-shaped cathode to raise said plate-shaped cathode to an electron emissive temperature, a plate-shaped control electrode disposed transversely of said magnetic field between said cathode, said control electrode having an elongated slot extended parallel to and aligned with said filamentary cathode and having dimensions substantially equal to said filamentary cathode for defining the cross section of said electron emission between said cathodes, a source of potential connected between said filamentary cathode and said control electrode for controlling said electron emission between said cathodes, a plate-shaped anode disposed adjacent to and aligned with said plate-shaped cathode, a source of potential for rendering said anode positive relative to said plate-shaped cathode, whereby an arc discharge is established therebetween, and means for supplying a gas to be ionized between said plate-shaped cathode and said anode.
3. An electric discharge device comprising a vacuum envelope, a single gaseous region disposed therein, a filamentary cathode therein, and an anode therein, a second cathode therein disposed intermediate said filamentary cathode and said anode, means for rendering said filamentary cathode electron emissive, means for applying a positive potential to said second cathode relative to said filamentary cathode, whereby electrons emitted by said filamentary cathode create a nonplasma discharge that bombards said second cathode to raise said second cathode to an electron emissive temperature, a control electrode having an elongated slot formed therein positioned between said cathodes, said slot being disposed parallel to said filamentary cathode to limit the bombardment area of said second cathode, means for applying a potential to said control electrode relative to said filamentary cathode,
means for establishing a magnetic field along the discharge path between said cathodes, and means for producing an arc discharge in said gaseous region between said second cathode and said anode, said arc discharge being controlled by the potential of said control electrode.
4. In an ion source unit the combination comprising a hollow arc block defining a gaseous region and having an elongated exit slit in a front wall thereof, said slit being terminated at one end by an inwardly extended plate electrically conneted to said are block and at the other end by a top wall of said are block having a slot therein, said slot being disposed parallel to said front wall adjacent said slit and aligned with said plate, a substantially U- shaped first cathode disposed external of said are block and parallel to said slot, a plate-shaped second cathode disposed parallel to said slotted top wall and between said slotted top wall and said first cathode, a plate-shaped control electrode having an elongated aperture disposed parallel to said second cathode and between said cathodes,
first potential means connected between said cathodes for rendering said second cathode positive with respect to said first cathode, second potential means connected between said first cathode and said control electrode for controlling conduction therebetween, third potential means connected between said are block and said second cathode end by a top wall of said are block having a slot therein, said slot being disposed parallel to said front wall adjacent said slit and aligned with said plate, a substantially U-shaped first electron emissive cathode disposed external of said are block and parallel to said slot, a plateshaped electron emissive second cathode disposed parallel to said slotted top wall and between said slotted top wall and said first cathode, a plate-shaped control electrode having an elongated aperture disposed parallel to said second cathode and between said cathodes, first potential means connected between said cathodes for rendering said second cathode positive with respect to said first cathode, second potential means connected between said first cathode and said control electrode for controlling conduction therebetween, third potential means connected between said are block and said second cathode for establishing an arc the length of said exit slit and having a cross section similar to the shape of the slot in said top wall, means for establishing a magnetic field through said are block in the direction of said are, means for introducing a gas to be ionized into said gaseous region, and means for withdrawing ions through said slit.
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Priority Applications (1)
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US528818A US2717962A (en) | 1944-03-31 | 1944-03-31 | Electric discharge devices |
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US528818A US2717962A (en) | 1944-03-31 | 1944-03-31 | Electric discharge devices |
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US2717962A true US2717962A (en) | 1955-09-13 |
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US528818A Expired - Lifetime US2717962A (en) | 1944-03-31 | 1944-03-31 | Electric discharge devices |
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US2258149A (en) * | 1938-04-23 | 1941-10-07 | Fides Gmbh | Device for producing rapidly flying ions |
US2250511A (en) * | 1938-09-02 | 1941-07-29 | Univ Leland Stanford Junior | Oscillator stabilization system |
US2373151A (en) * | 1942-07-29 | 1945-04-10 | Cons Eng Corp | Analytical system |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2821662A (en) * | 1955-07-29 | 1958-01-28 | Jr William A Bell | Ion source |
US2908837A (en) * | 1956-08-22 | 1959-10-13 | Bendix Aviat Corp | Anode structure |
US3056740A (en) * | 1956-10-12 | 1962-10-02 | Edwards High Vacuum Ltd | Vapourisation of metals |
US4814612A (en) * | 1983-08-30 | 1989-03-21 | Research Corporation | Method and means for vaporizing liquids for detection or analysis |
US4861989A (en) * | 1983-08-30 | 1989-08-29 | Research Corporation Technologies, Inc. | Ion vapor source for mass spectrometry of liquids |
US4960992A (en) * | 1983-08-30 | 1990-10-02 | Research Corporation Technologies | Method and means for vaporizing liquids by means of heating a sample capillary tube for detection or analysis |
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