US2679570A - Formation of electrode tip by electric current heating - Google Patents

Formation of electrode tip by electric current heating Download PDF

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US2679570A
US2679570A US242565A US24256551A US2679570A US 2679570 A US2679570 A US 2679570A US 242565 A US242565 A US 242565A US 24256551 A US24256551 A US 24256551A US 2679570 A US2679570 A US 2679570A
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wire
point
heating
spherical
formation
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US242565A
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Luther E Cisne
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AT&T Corp
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Bell Telephone Laboratories Inc
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21FWORKING OR PROCESSING OF METAL WIRE
    • B21F5/00Upsetting wire or pressing operations affecting the wire cross-section
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S228/00Metal fusion bonding
    • Y10S228/904Wire bonding

Definitions

  • This invention is concerned with the shaping of the ends of wires or filaments and more particularly to making spherical terminations on such wires or filaments, which are to be used, for example, as electrodes. Wires thus terminated are suitable for use as the contact wires in crystal rectifiers of the point contact type and for similar devices.
  • the spring section may take various shapes, e. g., helical, C-shape, S-shape, etc.
  • the S-shape is commonly used and may conveniently form the basis for a description of some of the details of this invention.
  • the area of contact between the wire tip or point and the crystal surface may be considered as a function of several. factors, one of which is point shape. With the usual sharp point, a considerable force is expanded.
  • An object of this invention is to enable the ready fabrication of an electrode or contact wire having a spherical point, free from surface irregularities and composed of fine grain homogeneous material.
  • a feature of this invention resides in controllably melting a small portion of a wire by Joulean heat, whereby a spherical. surface of relatively fine grain material is formed.
  • a further feature of this invention pertains to cooling portions of a wire adjacent to the heated portion to confine the melting to the desired zone and to aid in controlling the shape of the point made.
  • Another feature of this invention resides in 2 controlling the speed of heating to aid in determining the size and configuration of the spherical portion of the wire.
  • Fig. 1 is a perspective view of an apparatus suitable for carrying out the method of this invention, the heating circuit being of the directcurrent type;
  • Fig. 2 is a plan view of like apparatus with an alternating-current circuit illustrated
  • Figs. 3 to 6, inclusive show various point configurations obtainable with this method.
  • '7 is an elevational view of the apparatus provided with a cover to confine the heating zone to a desired ambient atmosphere.
  • a wire it of tungsten, Phosphor bronze, platinum or other suitable material may serve as the basis for making two spherical points.
  • the wire is, in this embodiment of the invention, clamped between two pairs of conductive blocks i ill-l lb and 2a-- lib by clamps i3 and H5, respectively.
  • An important function of the pairs of blocks ila-i lb and l2a-l2b is to serve as heat sinks or storage means to aid in confining the heating, later to be described, to a limited zone of the wire it intermediate these two heat sinks,
  • the heat sinks may for convenience be designated respectively as I! and it.
  • the clamp i3 is secured by the fas ening means E5 to the base it.
  • a weight ll secured by a cord 13 to the clamp Hi passes over pulley is to apply tension to the wire.
  • the size of the weight ll may be chosen to give a de sired tension on wire it or if different values of tension are needed a plurality of graded weights may be used.
  • Other means such as a spring of suitable proportions, motor means, etc, may be employed instead of the weight ii to apply the proper tension to the wire ill.
  • Electric power for heating the wire it may be introduced by various means such as the binding posts 20 and ti secured respectivelyto the heat sinks ll and I2. Either direct or alternating current may be used.
  • a direct current may be obtained from a battery 22 connected through a switch 23 and an adjustable resistor 24 for limiting the current to a suitable value, as illustrated in Fig. 1.
  • a suitable value as illustrated in Fig. 1.
  • means comprising a transformer 25, a switch 26,. and an adjustable impedance 2'! may be connected between the binding posts 202l and an alternatingcurrent power line, as illustrated in Fig. 2.
  • Other suitable current supply means may obviously be used, one such being a means for applying a condenser discharge to the Wire.
  • an enclosure may be provided. This may take various forms one of which may be a glass or like cover 35 as illustrated in Fig. 7. If a nonoxidizing lighter-than-air gas, such as hydrogen, is to be used, the cover may simply rest on the base E5. The hydrogen may be introduced through the opening that accommodates cord 18 or by any other convenient means. If another gas requiring a tighter enclosure or if pressure higher or lower than atmospheric is used, the enclosure may be by any convenient e2 pedient.
  • a nonoxidizing lighter-than-air gas such as hydrogen
  • points on the wire IE3 is accomplished by passing suflicient current through the wire to heat its intermediate portion to the melting point, whereby the wire is severed and spherical ends formed thereon due to the effect of surface tension forces in the wire.
  • Figs. 3 to 6, inclusive illustrate some point configurations which may be obtained.
  • the points of Fig. 3 are of substantially the same radius as the wire. This illustrates what may be called an intermediate situation. That is, with a given size of wire-and spacing of heat sinks, the point radius is a function of the speed of heating. A moderate speed will give a point as in Fig. 3. If the heating speed is higher, less material is melted and a large radius, relatively flat point as at Fig. l, is formed. At a relatively low heating speed more material is melted and the point takes the appearance of Fig. 5 with a radius greater than that of the wire and a ball point. In other words, the points of Fig. 3 are minimum radius points. The variations in point contour thus far described assume substantially no deformation of the wire due to the tension thereon.
  • a point of less radius than that of the wire may be obtained by relatively slow speed heating and relatively high tension. Under these conditions the wire, while in a plastic condition prior to melting, may be reduced or necked by the tension and may break before melting.
  • the tension on the wire should be relatively small along with a moderate heating rate as previously noted. It has been found that an optimum heating rate for producing the Fig. 3 type of point may be found for a fair range of tensions. For example, tensions of from three pounds to less than onehalf pound were used successfully with tungsten wire .005 inch in diameter.
  • Spherical points may be made with substantially no tension on the wire, although low tension appears to be somewhat more advantageous. It is possible to make spherical points by clamping separate wires in the two heat sinks, bringing their ends together, applying direct current to the joined wires and then pulling the wires apart to draw an are which melts the wire ends.
  • the blocks [Ia and lib may be provided with mating grooves of proper configuration to locate the wire so that the point will be formed at the proper place. Grooves of this type may also be provided in blocks H0. and i212 so that two contact wires of given configuration may be pointed at the same time.
  • the heat sinks may be of copper, brass or other material of relatively high thermal conductivity. With .005 inch diameter wire, blocks of brass or of copper .625 inch square and .250 inch thick have been used giving a heat sink .625 inch by .625 inch by .500 inch. Heat sinks about the volume of the foregoing are also satisfactory. The spacing between the heat sinks for a .005 inch diameter wire may be from .075 to .150 inch, the greater separation giving larger balls at the end of the wire. With both heat sinks of about the same heat absorbing ability, the wire is severed at a point substantially equidistant from each sink.
  • the size of the balls on the wire ends may be controlled by the pressure of the ambient atmosphere, being large for a vacuum, medium for atmospheric pressure, and small for pressures above atmospheric.
  • the effect of this environmental control is correlated with the other heat controlling factors to secure a desired over-all effect.
  • the fine drawn wires of tungsten and other suitable materials used for the point contacts in rectifiers and like devices usually have a grain structure that is coarse relative to their diameters. As a consequence of this grain structure it is necessary when making points by etching or grinding, to be extremely careful to avoid a rough surface.
  • the melting of the present invention fines the grain of the metal and makes for a very j smooth as well as a spherical point or tip.
  • spherical denotes a surface that is a portion of a sphere and is not intended to cover a complete sphere.
  • Apparatus for making spherical termination a wire filament by the operation of heat and surface tension comprising a base, spaced U-shaped clamps supported by said base with their open ends relation, means for anchoring one of cl maps to said base, means for applying a measured force to the other of clamps to eve aid clamp away from the anchored clamp. a of removable massive heat absorbing blocks secured in each of said clamps for gripping spaced portions of the filament, and a regulatable source of electric power connected across said blocks for heating the portion of the filament intermediate said blocks.

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Wire Processing (AREA)

Description

May 25, 1954 L. E CISNE FORMATION OF ELECTRODE TIP BY ELECTRIC CURRENT HEATING Filed Aug. 18, 1951 I I I4 lNl ENTOR L. E. c/s/vE; 6 WM A T TOR/VE Y Patented May 25, 1954 FORMATION OF ELECTRODE TIP BY ELECTRIC CURRENT HEATING Luther E. Cisne, Glen Ellyn, Ill., assignor to Bell Telephone Laboratories,
Incorporated, New
York, N. Y., a corporation of New York Application August 18, 1951, Serial No. 242,565
1 Claim.
This invention is concerned with the shaping of the ends of wires or filaments and more particularly to making spherical terminations on such wires or filaments, which are to be used, for example, as electrodes. Wires thus terminated are suitable for use as the contact wires in crystal rectifiers of the point contact type and for similar devices.
It is desirable in the manufacture of point contact wires for crystal rectifiers and like devices to closely control the area of contact between the wire and the crystal surface. For example, in point contact devices of this type, which are to be used at very high frequencies, an optimum contact area capable of. exhibiting at the same time suitable resistance and capacitance characteristics is of considerable importance. 1
Contact wires falling in the category under discussion are usually made with a spring section, the function of which is to apply a suitable contact pressure. The spring section may take various shapes, e. g., helical, C-shape, S-shape, etc. The S-shape is commonly used and may conveniently form the basis for a description of some of the details of this invention.
The area of contact between the wire tip or point and the crystal surface, for example, may be considered as a function of several. factors, one of which is point shape. With the usual sharp point, a considerable force is expanded.
in the inelastic deformation of the point to produce a suitable area of contact. A spherical point on the other hand would have a greater and a more predictable range of elastic deforms.
tion. Such a point would allow the realization of a contact area of suitable proportions with a much smaller total force than that required with sharper points. This would result among other things, in a lower unit contact pressure and consequently less strain at or near the surface of the crystal.
The foregoing and other desirable features may be realized by making spherical points or termi nations in accordance with the method of this invention.
An object of this invention is to enable the ready fabrication of an electrode or contact wire having a spherical point, free from surface irregularities and composed of fine grain homogeneous material.
A feature of this invention resides in controllably melting a small portion of a wire by Joulean heat, whereby a spherical. surface of relatively fine grain material is formed.
A further feature of this invention pertains to cooling portions of a wire adjacent to the heated portion to confine the melting to the desired zone and to aid in controlling the shape of the point made.
Another feature of this invention resides in 2 controlling the speed of heating to aid in determining the size and configuration of the spherical portion of the wire.
Other and further objects and features of this invention will appear more fully and clearly from the following description of exemplary embodiments thereof taken in connection with the appended drawings in which:
Fig. 1 is a perspective view of an apparatus suitable for carrying out the method of this invention, the heating circuit being of the directcurrent type;
Fig. 2 is a plan view of like apparatus with an alternating-current circuit illustrated;
Figs. 3 to 6, inclusive, show various point configurations obtainable with this method, and
'7 is an elevational view of the apparatus provided with a cover to confine the heating zone to a desired ambient atmosphere.
As illustrated in Figs. 1, 2 and 7, a wire it of tungsten, Phosphor bronze, platinum or other suitable material, may serve as the basis for making two spherical points. The wire is, in this embodiment of the invention, clamped between two pairs of conductive blocks i ill-l lb and 2a-- lib by clamps i3 and H5, respectively.
An important function of the pairs of blocks ila-i lb and l2a-l2b is to serve as heat sinks or storage means to aid in confining the heating, later to be described, to a limited zone of the wire it intermediate these two heat sinks, The heat sinks may for convenience be designated respectively as I! and it.
In order that tension may be applied to the wire iii, the clamp i3 is secured by the fas ening means E5 to the base it. A weight ll secured by a cord 13 to the clamp Hi passes over pulley is to apply tension to the wire. The size of the weight ll may be chosen to give a de sired tension on wire it or if different values of tension are needed a plurality of graded weights may be used. Other means such as a spring of suitable proportions, motor means, etc, may be employed instead of the weight ii to apply the proper tension to the wire ill.
Electric power for heating the wire it may be introduced by various means such as the binding posts 20 and ti secured respectivelyto the heat sinks ll and I2. Either direct or alternating current may be used.
A direct current may be obtained from a battery 22 connected through a switch 23 and an adjustable resistor 24 for limiting the current to a suitable value, as illustrated in Fig. 1. If an alternating current is to be used, means comprising a transformer 25, a switch 26,. and an adjustable impedance 2'! may be connected between the binding posts 202l and an alternatingcurrent power line, as illustrated in Fig. 2. Other suitable current supply means may obviously be used, one such being a means for applying a condenser discharge to the Wire.
In those cases where it is desirable to exclude oxygen from the wire to avoid oxidation thereof during heating, or to control the pressure, or other characteristics of the ambient atmosphere, an enclosure may be provided. This may take various forms one of which may be a glass or like cover 35 as illustrated in Fig. 7. If a nonoxidizing lighter-than-air gas, such as hydrogen, is to be used, the cover may simply rest on the base E5. The hydrogen may be introduced through the opening that accommodates cord 18 or by any other convenient means. If another gas requiring a tighter enclosure or if pressure higher or lower than atmospheric is used, the enclosure may be by any convenient e2 pedient.
The formation of points on the wire IE3 is accomplished by passing suflicient current through the wire to heat its intermediate portion to the melting point, whereby the wire is severed and spherical ends formed thereon due to the effect of surface tension forces in the wire.
Figs. 3 to 6, inclusive, illustrate some point configurations which may be obtained. The points of Fig. 3 are of substantially the same radius as the wire. This illustrates what may be called an intermediate situation. That is, with a given size of wire-and spacing of heat sinks, the point radius is a function of the speed of heating. A moderate speed will give a point as in Fig. 3. If the heating speed is higher, less material is melted and a large radius, relatively flat point as at Fig. l, is formed. At a relatively low heating speed more material is melted and the point takes the appearance of Fig. 5 with a radius greater than that of the wire and a ball point. In other words, the points of Fig. 3 are minimum radius points. The variations in point contour thus far described assume substantially no deformation of the wire due to the tension thereon.
If a point of less radius than that of the wire is desired, it may be obtained by relatively slow speed heating and relatively high tension. Under these conditions the wire, while in a plastic condition prior to melting, may be reduced or necked by the tension and may break before melting. In
this case the arc across the break will melt the ends of the wire and produce spherical surfaces of smaller radius than that of the wire as illustrated in Fig. 6. In order to have the arc of sufficient duration to melt the wire ends, a directcurrent source should be used, since an alternatingwurrent arc would extinguish too quickly to accomplish the purpose.
If the minimum radius required is that of the wire, as illustrated in Fig. 3, the tension on the wire should be relatively small along with a moderate heating rate as previously noted. It has been found that an optimum heating rate for producing the Fig. 3 type of point may be found for a fair range of tensions. For example, tensions of from three pounds to less than onehalf pound were used successfully with tungsten wire .005 inch in diameter.
Spherical points may be made with substantially no tension on the wire, although low tension appears to be somewhat more advantageous. It is possible to make spherical points by clamping separate wires in the two heat sinks, bringing their ends together, applying direct current to the joined wires and then pulling the wires apart to draw an are which melts the wire ends.
This is somewhat like what is done in forming the points of Fig. 6 without the initial reduction in diameter and parting of the wire during the plastic stage.
If rectifier contact wires having an e-shaped or other convoluted portion are to be pointed by this method, the blocks [Ia and lib may be provided with mating grooves of proper configuration to locate the wire so that the point will be formed at the proper place. Grooves of this type may also be provided in blocks H0. and i212 so that two contact wires of given configuration may be pointed at the same time.
The heat sinks may be of copper, brass or other material of relatively high thermal conductivity. With .005 inch diameter wire, blocks of brass or of copper .625 inch square and .250 inch thick have been used giving a heat sink .625 inch by .625 inch by .500 inch. Heat sinks about the volume of the foregoing are also satisfactory. The spacing between the heat sinks for a .005 inch diameter wire may be from .075 to .150 inch, the greater separation giving larger balls at the end of the wire. With both heat sinks of about the same heat absorbing ability, the wire is severed at a point substantially equidistant from each sink.
The size of the balls on the wire ends may be controlled by the pressure of the ambient atmosphere, being large for a vacuum, medium for atmospheric pressure, and small for pressures above atmospheric. The effect of this environmental control is correlated with the other heat controlling factors to secure a desired over-all effect.
The fine drawn wires of tungsten and other suitable materials used for the point contacts in rectifiers and like devices usually have a grain structure that is coarse relative to their diameters. As a consequence of this grain structure it is necessary when making points by etching or grinding, to be extremely careful to avoid a rough surface. The melting of the present invention fines the grain of the metal and makes for a very j smooth as well as a spherical point or tip.
The term spherical as herein employed denotes a surface that is a portion of a sphere and is not intended to cover a complete sphere.
Although this invention been described by means of illustrative embodiments thereof it is not intended that these be taken as limiting the scope of the invention.
What is claimed is:
Apparatus for making spherical termination a wire filament by the operation of heat and surface tension. fcrces therein, that comprises a base, spaced U-shaped clamps supported by said base with their open ends relation, means for anchoring one of cl maps to said base, means for applying a measured force to the other of clamps to eve aid clamp away from the anchored clamp. a of removable massive heat absorbing blocks secured in each of said clamps for gripping spaced portions of the filament, and a regulatable source of electric power connected across said blocks for heating the portion of the filament intermediate said blocks.
References Cited in the file of this patent UNITED STATES PATENTS Number Name Date 363,550 Sedgwick May 24, 1887 396,014 Thomson Jan. 8, 1889 2,399,466 Carlson Apr. 30, 1946
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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2770753A (en) * 1951-11-23 1956-11-13 Hartford Nat Bank & Trust Co Tightening member for filaments
US2867715A (en) * 1954-08-13 1959-01-06 Gen Motors Corp Method for making lamp bulb
US2979600A (en) * 1956-08-31 1961-04-11 Plessey Co Ltd Electrode systems for electronic valves
US3401723A (en) * 1966-08-08 1968-09-17 Fabri Tek Inc Needle making method and apparatus
US3870852A (en) * 1969-12-01 1975-03-11 Semperit Ag Process and apparatus for cutting rubberised stranded wire
US3934108A (en) * 1974-09-16 1976-01-20 Uthe Technology, Inc. Lead bonding method and apparatus
US3941969A (en) * 1973-08-09 1976-03-02 E. I. Du Pont De Nemours And Co. Apparatus and process for applying contact dots
US3945698A (en) * 1973-10-05 1976-03-23 Hitachi, Ltd. Method of stabilizing emitted electron beam in field emission electron gun
US3950631A (en) * 1970-06-19 1976-04-13 U.S. Philips Corporation Device for welding a wire by means of thermo-compression bonding
US4014199A (en) * 1976-01-26 1977-03-29 Gte Sylvania Incorporated Apparatus and method for providing an electrical contact with a tip portion substantially free of burrs
US4098447A (en) * 1975-05-15 1978-07-04 The Welding Institute Bonding method and apparatus
FR2443933A1 (en) * 1978-12-15 1980-07-11 Dataproducts Corp BALL NEEDLE FOR PRINTING HEAD AND METHOD AND DEVICE FOR MANUFACTURING SAID NEEDLE
EP0042036A1 (en) * 1980-06-13 1981-12-23 Olympia Werke Ag Method and apparatus for making tubular pieces with a closed, shaped end portion
US4323759A (en) * 1977-07-26 1982-04-06 The Welding Institute Electrical inter-connection method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US363550A (en) * 1887-05-24 Manufacture of watch-mainsprings
US396014A (en) * 1889-01-08 Electric metal workjng
US2399466A (en) * 1942-01-08 1946-04-30 Rca Corp Metalworking

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US363550A (en) * 1887-05-24 Manufacture of watch-mainsprings
US396014A (en) * 1889-01-08 Electric metal workjng
US2399466A (en) * 1942-01-08 1946-04-30 Rca Corp Metalworking

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2770753A (en) * 1951-11-23 1956-11-13 Hartford Nat Bank & Trust Co Tightening member for filaments
US2867715A (en) * 1954-08-13 1959-01-06 Gen Motors Corp Method for making lamp bulb
US2979600A (en) * 1956-08-31 1961-04-11 Plessey Co Ltd Electrode systems for electronic valves
US3401723A (en) * 1966-08-08 1968-09-17 Fabri Tek Inc Needle making method and apparatus
US3870852A (en) * 1969-12-01 1975-03-11 Semperit Ag Process and apparatus for cutting rubberised stranded wire
US3950631A (en) * 1970-06-19 1976-04-13 U.S. Philips Corporation Device for welding a wire by means of thermo-compression bonding
US3941969A (en) * 1973-08-09 1976-03-02 E. I. Du Pont De Nemours And Co. Apparatus and process for applying contact dots
US3945698A (en) * 1973-10-05 1976-03-23 Hitachi, Ltd. Method of stabilizing emitted electron beam in field emission electron gun
US3934108A (en) * 1974-09-16 1976-01-20 Uthe Technology, Inc. Lead bonding method and apparatus
US4098447A (en) * 1975-05-15 1978-07-04 The Welding Institute Bonding method and apparatus
US4014199A (en) * 1976-01-26 1977-03-29 Gte Sylvania Incorporated Apparatus and method for providing an electrical contact with a tip portion substantially free of burrs
US4323759A (en) * 1977-07-26 1982-04-06 The Welding Institute Electrical inter-connection method
FR2443933A1 (en) * 1978-12-15 1980-07-11 Dataproducts Corp BALL NEEDLE FOR PRINTING HEAD AND METHOD AND DEVICE FOR MANUFACTURING SAID NEEDLE
EP0042036A1 (en) * 1980-06-13 1981-12-23 Olympia Werke Ag Method and apparatus for making tubular pieces with a closed, shaped end portion

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