US2677148A - Spinneret - Google Patents

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Publication number
US2677148A
US2677148A US165785A US16578550A US2677148A US 2677148 A US2677148 A US 2677148A US 165785 A US165785 A US 165785A US 16578550 A US16578550 A US 16578550A US 2677148 A US2677148 A US 2677148A
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Prior art keywords
spinneret
orifice
face
spinnerets
section
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Expired - Lifetime
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US165785A
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Wesley L Webb
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Akzo Nobel UK PLC
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American Viscose Corp
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Priority to US165785A priority Critical patent/US2677148A/en
Priority to US318157A priority patent/US2737831A/en
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Assigned to KELLOGG CREDIT CORPORATION A DE CORP. reassignment KELLOGG CREDIT CORPORATION A DE CORP. AGREEMENT WHEREBY SAID HELLER AND RAYONIER RELEASES ALL MORTGAGES AND SECURITY INTERESTS HELD BY AVTEX ON APRIL 28, 1978, AND JAN. 11, 1979, RESPECTIVELY AND ASSIGNS ITS ENTIRE INTEREST IN SAID MORT-AGAGE AGREEMENT TO ASSIGNEE (SEE RECORD FOR DETAILS) Assignors: AVTEX FIBERS INC., A NY CORP., ITT RAYONIER INCORPORATED, A DE CORP., WALTER E. HELLER & COMPANY, INC. A NY CORP.
Assigned to WALTER E. HELLER & COMPANY, INC., A CORP. OF DEL. reassignment WALTER E. HELLER & COMPANY, INC., A CORP. OF DEL. AGREEMENT WHEREBY AETNA RELEASES AVTEX FROM ALL MORTAGES AND SECURITY INTERESTS IN SAID INVENTIONS AS OF JANUARY 11,1979, AND ASSIGNS TO ASSIGNEE THE ENTIRE INTEREST IN SAID MORTAGE AGREEMENT TO ASSIGNEE (SEE RECORDS FOR DETAILS). Assignors: AETNA BUSINESS CREDIT, INC., A CORP. OF N.Y., AVTEX FIBERS, INC, A CORP. OF NY, KELLOGG CREDIT CORP., A CORP. OF DEL.
Expired - Lifetime legal-status Critical Current

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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D4/00Spinnerette packs; Cleaning thereof
    • D01D4/02Spinnerettes
    • D01D4/022Processes or materials for the preparation of spinnerettes

Definitions

  • This invention relates to the manufacture of artificial filaments, and in particular, to new and improved, spinnerets for the manufacture of artificial filaments and to a process for making the same.
  • the known and presently used spinnerets are the form of a cup formed from a non-corrosive metal, or non-corrosive non-metallic material such as glass, plastic, and the like, in the base of which are a number of extrusion orifices of the order to approximately 0.0015 to 0.0100 inch in diameter, through which the filament-forming material is extruded.
  • the orifice of a commonly used type has a conical or curved funnel shape at the top and a cylindrical shape at the bottom, that is, adjacent the face.
  • the cylindrical orifice is also 2 flow surfaces, with a decreased tendency to clog after long and continued use.
  • Another object of this invention is to produce a new and improved spinneret which overcomes the disadvantages and difliculties of the presently used spinnerets.
  • Figure 1 is a side elevation in section of a spinneret constructed in accordance with the invention
  • Figure 2 is a sectional view of an orifice and a tool illustrating one step in a method of making the spinneret extrusion orifice
  • Figure 3 is a fragmentary sectional view of the spinneret face and a tool illustrating a second step in forming the extrusion orifice shown in Figure 2,
  • Figure 4 is a fragmentary view in section of the extrusion orifice of the spinneret shown in Figure 1, and
  • Figure 5 is a fragmentary view in section of another embodiment of the extrusion orifice.
  • the spinneret of the invention may be formed of any non-corrosive metal such as nickel, platinum, silver, or alloys thereof, or non-metallic material such as plastic or glass; and the spinneret may be cup-shaped, conical, or plate type.
  • the orifice may be formed in accordance with the invention by any suitable means, e. g., by punching, grinding, drilling, or a combination of these methods. I'he invention is not to be limited by the following detailed description of one method of making the spinneret.
  • the base of the spinneret is operated upon by a suitable tool to form an opening or orifice having a conical upper part converging in the direction of flow and a substantial cylindrical remaining part adjacent the face of the jet.
  • the cylindrical portion of the orifice is enlarged and shaped so that it will be diverging in the direction of flow.
  • the resulting orifice has the configuration shown in Figure 4, in which the opening comprises two cones with their narrow parts adjacent resulting in a constricted area intermediate the open ends of the orifice, e. g., reverting to Figure 2 the spinneret base 4 is punched by means of a tool 6, the tool having a cylindrical section 6a and a conical section 62).
  • burr 1 is removed by suitable means such as grinding, cutting, polishing and the like.
  • a tool 9 having a uniform tapered portion 9a is inserted from the face of the jet into the cylindrical section II of the orifice, and the tool is worked upward in this section I l until this section is also given a conical shape such as the orifice portion I 2 seen in Figure 4.
  • the completed orifice comprises two cone shaped sections having their narrow ends adjacent, the constriction I 3 being located at a point intermediate the lower or outer face 5 and inner face 5a of the spinneret wall 4.
  • the taper of the conical section I2 of the orifice in Figure 4 is preferably between l%.
  • the upper portion l2a may be conical in shape or have curved sides.
  • the constriction l3 may be located exactly equidistant between the faces or approximately midway therebetween. However, it is preferable that any deviation from the equidistant location be belcw the centerline between the faces and the term midway is intended to include such deviation.
  • the percent taper is determined by taking the difference in the diameters between the top and the bottom of the cone and dividing this by the distance between the top and bottom of the cone and multiplying by 100.
  • the tapered surface 9 of the punch 8 presses evenly against the entire flow surface 12 of the lower cylindrical portion of the extrusion orifice (see Figure 4). Due to this even pressure over the entire fiow surface no one part or section of it can spring back. With some metals the tool 9 may produce an annular ripple [Be on the spinneret face 5 surrounding the extrusion orifice I2 (see Figure 5). This ripple will in no Way interfere with the filament forming operation and is not conducive to the formation of annular ring deposits.
  • spinnerets of the present invention show a decreased tendency to clog up due to the formation of annular deposits in the extrusion orifices.
  • spinnerets of the present invention show substantially less tendency to clog even though the conventional spinnerets are employed with a spinning bath and/or spinning solution containing an incrustation inhibitor or anti-clogging agent, while the spinnerets of the present invention can be employed without the aid of such assistants.
  • the spinnerets of the present invention are employed in connection with a spinnin solution and/or bath containing an anti-clogging agent, the results are much superior to conventional spinnerets.
  • both the present spinneret and the conventional spinneret were placed on the same spinning machine spinning viscose in a conventional viscose coagulating bath, which contained no spinning assistant or anti-clogging agent.
  • the results were as follows:
  • the above table shows that the present spinneret produced less than half as many abnormally small filaments and about half as many abnormally large filaments than the conventional cylindrical shaped jet orifice. It appears that the viscose solution streaming through the present jet is able to dislodge deposits from the orifice because the orifice diverges outwardly, Further, it was found that the present jets are easier to clean either by back washing or forward washing because of the diverting of the orifice adjacent each face. It is obvious that any material which passes the constricted area will certainly not clog or lodge at any point beyond this area in the present jet. Thus the process decreases the cost of production, and gives more uniformity to the product when making a multi-filament yarn.
  • a spinneret for forming multi-filament yarn comprising a base member of relatively thin metal having an outer face and an inner face thereon, walls defining a plurality of conical apertures tapering from the inner face toward the outer face and terminating in a plane midway between the inner and outer faces, walls defining a plurality of concentric conical apertures tapering from the outer face towards the inner face and terminating in said plane midway between the inner and outer faces and in alignment with the first mentioned walls to form a plurality of orifices in the base havin a circular constriction in each orifice substantially midway between the inner and outer faces, said walls having smooth uninterrupted surfaces and the difference between the diameter of the constriction and the diameter of the conical aperture in the outer face divided by the distance between the constriction and the outer face not exceeding 0.10.

Description

y 4, 1954 w. L. WEBB I 2,677,148
SPINNERET Filed June 2, 1950 (.Illlllllfl HIE Fig-.4
. INVEN WESLEY L. WE
ATTORNEi Patented May 4, 1954 STATES TENT OFFICE SPINNERET Application June 2, 1950, Serial N 0. 165,785
1 Claim. 1
This invention relates to the manufacture of artificial filaments, and in particular, to new and improved, spinnerets for the manufacture of artificial filaments and to a process for making the same.
In spinning artificial filaments, it is known that the quality of the filaments is closely connected with the nature, form and dimensions of the holes in the spinneret, no matter whether they are made by dry spinning or wet spinning.
The known and presently used spinnerets are the form of a cup formed from a non-corrosive metal, or non-corrosive non-metallic material such as glass, plastic, and the like, in the base of which are a number of extrusion orifices of the order to approximately 0.0015 to 0.0100 inch in diameter, through which the filament-forming material is extruded. The orifice of a commonly used type has a conical or curved funnel shape at the top and a cylindrical shape at the bottom, that is, adjacent the face.
The production of superior filaments requires the maintenance of a constant cross section of the extrusion orifices and of an extremely smooth and highly polished flow surface of definite configuration.
Spinnerets for making artificial filaments of types heretofore used are often characterized by having a small annular ridge or flashing of metal around the opening on the face of the jet wall. This flashing is extremely minute and can only be seen with a microscope. Because of its rou hness it forms an excellent place for the building of annular rings or deposits of materials such as sulfur, zinc salts, and sodium salts in the opening at the face of the jet. These deposits greatly constrict the diameter of the orifice and may ultimately close the orifice. These deposits result in greatly increasing the per cent of abnormally small filaments in multi-filament yarn spun with jets of the known type described.
Moreover, in jets of conventional type heretofore used, the orifice adjacent the face of the spinneret has conventionally been cylindrical in cross section, so that any deposit in this cylindrical capillary invariably resulted in the production small-sized filaments. This also resulted in an increase in the back pressure developed by the spinneret. very difficult to clean after such deposits have formed thereon.
It is an object of the present invention to produce a spinneret with orifices having smooth The cylindrical orifice is also 2 flow surfaces, with a decreased tendency to clog after long and continued use.
Another object of this invention is to produce a new and improved spinneret which overcomes the disadvantages and difliculties of the presently used spinnerets.
Other objects and advantages of the present invention will be obvious from the description thereof hereinafter.
Figure 1 is a side elevation in section of a spinneret constructed in accordance with the invention,
Figure 2 is a sectional view of an orifice and a tool illustrating one step in a method of making the spinneret extrusion orifice,
Figure 3 is a fragmentary sectional view of the spinneret face and a tool illustrating a second step in forming the extrusion orifice shown in Figure 2,
Figure 4 is a fragmentary view in section of the extrusion orifice of the spinneret shown in Figure 1, and
Figure 5 is a fragmentary view in section of another embodiment of the extrusion orifice.
The spinneret of the invention may be formed of any non-corrosive metal such as nickel, platinum, silver, or alloys thereof, or non-metallic material such as plastic or glass; and the spinneret may be cup-shaped, conical, or plate type. The orifice may be formed in accordance with the invention by any suitable means, e. g., by punching, grinding, drilling, or a combination of these methods. I'he invention is not to be limited by the following detailed description of one method of making the spinneret.
In the first step, the base of the spinneret is operated upon by a suitable tool to form an opening or orifice having a conical upper part converging in the direction of flow and a substantial cylindrical remaining part adjacent the face of the jet. In the second step, the cylindrical portion of the orifice is enlarged and shaped so that it will be diverging in the direction of flow. The resulting orifice has the configuration shown in Figure 4, in which the opening comprises two cones with their narrow parts adjacent resulting in a constricted area intermediate the open ends of the orifice, e. g., reverting to Figure 2 the spinneret base 4 is punched by means of a tool 6, the tool having a cylindrical section 6a and a conical section 62). This results in a hole having the same configuration, and also results in the production of a I small annular burr '1 around the opening on the face 5. In the next step the burr 1 is removed by suitable means such as grinding, cutting, polishing and the like. In the next step shown in Figure 3, a tool 9 having a uniform tapered portion 9a is inserted from the face of the jet into the cylindrical section II of the orifice, and the tool is worked upward in this section I l until this section is also given a conical shape such as the orifice portion I 2 seen in Figure 4.
Since the upper section I 2a of this orifice is already conical, the completed orifice comprises two cone shaped sections having their narrow ends adjacent, the constriction I 3 being located at a point intermediate the lower or outer face 5 and inner face 5a of the spinneret wall 4. The taper of the conical section I2 of the orifice in Figure 4 is preferably between l%. The upper portion l2a may be conical in shape or have curved sides. The constriction l3 may be located exactly equidistant between the faces or approximately midway therebetween. However, it is preferable that any deviation from the equidistant location be belcw the centerline between the faces and the term midway is intended to include such deviation. The percent taper is determined by taking the difference in the diameters between the top and the bottom of the cone and dividing this by the distance between the top and bottom of the cone and multiplying by 100.
The tapered surface 9 of the punch 8 presses evenly against the entire flow surface 12 of the lower cylindrical portion of the extrusion orifice (see Figure 4). Due to this even pressure over the entire fiow surface no one part or section of it can spring back. With some metals the tool 9 may produce an annular ripple [Be on the spinneret face 5 surrounding the extrusion orifice I2 (see Figure 5). This ripple will in no Way interfere with the filament forming operation and is not conducive to the formation of annular ring deposits.
Thus by means of the present invention there is produced a Venturi throat spinneret which can be used for much longer periods of time than conventional spinnerets without danger of the extrusion orifices becoming clogged.
By means of the present invention, there is produced a new and improved spinneret which shows a decreased tendency to clog up due to the formation of annular deposits in the extrusion orifices. When the spinnerets of the present invention are compared to conventional spin nerets they show substantially less tendency to clog even though the conventional spinnerets are employed with a spinning bath and/or spinning solution containing an incrustation inhibitor or anti-clogging agent, while the spinnerets of the present invention can be employed without the aid of such assistants. When, however, the spinnerets of the present invention are employed in connection with a spinnin solution and/or bath containing an anti-clogging agent, the results are much superior to conventional spinnerets.
To illustrate the superiority of the spinneret of the present invention, it was compared with a spinneret having a cylindrical orifice adjacent a face in the following test: both the present spinneret and the conventional spinneret were placed on the same spinning machine spinning viscose in a conventional viscose coagulating bath, which contained no spinning assistant or anti-clogging agent. The results were as follows:
The above table shows that the present spinneret produced less than half as many abnormally small filaments and about half as many abnormally large filaments than the conventional cylindrical shaped jet orifice. It appears that the viscose solution streaming through the present jet is able to dislodge deposits from the orifice because the orifice diverges outwardly, Further, it was found that the present jets are easier to clean either by back washing or forward washing because of the diverting of the orifice adjacent each face. It is obvious that any material which passes the constricted area will certainly not clog or lodge at any point beyond this area in the present jet. Thus the process decreases the cost of production, and gives more uniformity to the product when making a multi-filament yarn.
By use of the spinnerets of the present invention considerable saving in the cost of production is realized since spinneret cleaning is facilitated.
It is to be understood that changes and variations may be made without departing from the spirit and scope of the invention as defined in the appended claim.
I claim:
A spinneret for forming multi-filament yarn comprising a base member of relatively thin metal having an outer face and an inner face thereon, walls defining a plurality of conical apertures tapering from the inner face toward the outer face and terminating in a plane midway between the inner and outer faces, walls defining a plurality of concentric conical apertures tapering from the outer face towards the inner face and terminating in said plane midway between the inner and outer faces and in alignment with the first mentioned walls to form a plurality of orifices in the base havin a circular constriction in each orifice substantially midway between the inner and outer faces, said walls having smooth uninterrupted surfaces and the difference between the diameter of the constriction and the diameter of the conical aperture in the outer face divided by the distance between the constriction and the outer face not exceeding 0.10.
References Cited. in the file of this patent UNITED STATES PATENTS Number Name Date 749,725 Fehr Jan. 19, 1904 974,130 Kaufmann Nov. 1, 1910 1,492,594 Dreyfus et al. May 6, 1924 1,708,715 Akin Apr. 9, 1929 1,980,234 Taylor Nov. 13, 1934 1,999,072 Allen Apr. 23, 1935 FOREIGN PATENTS Number Country Date 472,409 France Aug. 4, 1914
US165785A 1950-06-02 1950-06-02 Spinneret Expired - Lifetime US2677148A (en)

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US318157A US2737831A (en) 1950-06-02 1952-11-01 Process for making a spinneret

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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2902715A (en) * 1956-07-02 1959-09-08 Norman Geoffrey Bertrand Extrusion-consolidation die
US2923969A (en) * 1960-02-09 Certificate of correction
US2959839A (en) * 1955-05-18 1960-11-15 Du Pont Linear condensation polymer fiber
US3056163A (en) * 1955-05-18 1962-10-02 American Viscose Corp Spinneret
US3084385A (en) * 1959-07-08 1963-04-09 Du Pont Extrusion apparatus
US3176342A (en) * 1962-06-25 1965-04-06 Monsanto Co Spinnerette
US3456292A (en) * 1967-03-30 1969-07-22 Du Pont Spinneret
FR2313990A1 (en) * 1975-06-13 1977-01-07 Owens Corning Fiberglass Corp METHOD AND APPARATUS FOR MAKING A CONTAINER FOR THE PRODUCTION OF MELT GLASS NETS
US4056597A (en) * 1975-04-03 1977-11-01 Phillips Petroleum Company Process and die for extrusion of a resinous material
US4316713A (en) * 1978-11-11 1982-02-23 Simon-Barron Limited Die for pelletizing machine
US20110215499A1 (en) * 2008-10-29 2011-09-08 Bayer Materialscience Ag Extrusion nozzle for polymers

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US749725A (en) * 1904-01-19 Method of producing heddles
US974130A (en) * 1908-07-23 1910-11-01 Steel Heddle Mfg Co Method of making heddles.
FR472409A (en) * 1914-05-16 1914-12-04 Andre Henri Morel Spinning die
US1492594A (en) * 1921-08-26 1924-05-06 American Cellulose & Chemical Spinning jet or nozzle for the manufacture of artificial silk, etc.
US1708715A (en) * 1927-03-01 1929-04-09 Robert M Akin Process of making dies
US1980234A (en) * 1932-06-02 1934-11-13 Celanese Corp Apparatus for the production of artificial threads of like products
US1999072A (en) * 1933-03-25 1935-04-23 Viscose Co Spinneret for the manufacture of rayon

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US749725A (en) * 1904-01-19 Method of producing heddles
US974130A (en) * 1908-07-23 1910-11-01 Steel Heddle Mfg Co Method of making heddles.
FR472409A (en) * 1914-05-16 1914-12-04 Andre Henri Morel Spinning die
US1492594A (en) * 1921-08-26 1924-05-06 American Cellulose & Chemical Spinning jet or nozzle for the manufacture of artificial silk, etc.
US1708715A (en) * 1927-03-01 1929-04-09 Robert M Akin Process of making dies
US1980234A (en) * 1932-06-02 1934-11-13 Celanese Corp Apparatus for the production of artificial threads of like products
US1999072A (en) * 1933-03-25 1935-04-23 Viscose Co Spinneret for the manufacture of rayon

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2923969A (en) * 1960-02-09 Certificate of correction
US2959839A (en) * 1955-05-18 1960-11-15 Du Pont Linear condensation polymer fiber
US3056163A (en) * 1955-05-18 1962-10-02 American Viscose Corp Spinneret
US2902715A (en) * 1956-07-02 1959-09-08 Norman Geoffrey Bertrand Extrusion-consolidation die
US3084385A (en) * 1959-07-08 1963-04-09 Du Pont Extrusion apparatus
US3176342A (en) * 1962-06-25 1965-04-06 Monsanto Co Spinnerette
US3456292A (en) * 1967-03-30 1969-07-22 Du Pont Spinneret
US4056597A (en) * 1975-04-03 1977-11-01 Phillips Petroleum Company Process and die for extrusion of a resinous material
FR2313990A1 (en) * 1975-06-13 1977-01-07 Owens Corning Fiberglass Corp METHOD AND APPARATUS FOR MAKING A CONTAINER FOR THE PRODUCTION OF MELT GLASS NETS
US4316713A (en) * 1978-11-11 1982-02-23 Simon-Barron Limited Die for pelletizing machine
US20110215499A1 (en) * 2008-10-29 2011-09-08 Bayer Materialscience Ag Extrusion nozzle for polymers

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AS Assignment

Owner name: WALTER E. HELLER & COMPANY, INC., A CORP. OF DEL.

Free format text: AGREEMENT WHEREBY AETNA RELEASES AVTEX FROM ALL MORTAGES AND SECURITY INTERESTS IN SAID INVENTIONS AS OF JANUARY 11,1979, AND ASSIGNS TO ASSIGNEE THE ENTIRE INTEREST IN SAID MORTAGE AGREEMENT TO ASSIGNEE;ASSIGNORS:AETNA BUSINESS CREDIT, INC., A CORP. OF N.Y.;AVTEX FIBERS, INC, A CORP. OF NY;KELLOGG CREDIT CORP., A CORP. OF DEL.;REEL/FRAME:003959/0250

Effective date: 19800326

Owner name: KELLOGG CREDIT CORPORATION A DE CORP.

Free format text: AGREEMENT WHEREBY SAID HELLER AND RAYONIER RELEASES ALL MORTGAGES AND SECURITY INTERESTS HELD BY AVTEX ON APRIL 28, 1978, AND JAN. 11, 1979, RESPECTIVELY AND ASSIGNS ITS ENTIRE INTEREST IN SAID MORT-AGAGE AGREEMENT TO ASSIGNEE;ASSIGNORS:WALTER E. HELLER & COMPANY, INC. A NY CORP.;ITT RAYONIER INCORPORATED, A DE CORP.;AVTEX FIBERS INC., A NY CORP.;REEL/FRAME:003959/0350

Effective date: 19800326