US2656885A - Concentrating apparatus - Google Patents

Concentrating apparatus Download PDF

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US2656885A
US2656885A US76730A US7673049A US2656885A US 2656885 A US2656885 A US 2656885A US 76730 A US76730 A US 76730A US 7673049 A US7673049 A US 7673049A US 2656885 A US2656885 A US 2656885A
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cylinder
vapor
steam
passage
shaft
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US76730A
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Burton S Hughes
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ZAREMBA CO
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ZAREMBA CO
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/22Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • B01D1/222In rotating vessels; vessels with movable parts
    • B01D1/228In rotating vessels; vessels with movable parts horizontally placed cylindrical container or drum
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/08Concentrating or drying of juices
    • A23L2/10Concentrating or drying of juices by heating or contact with dry gases
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S159/00Concentrating evaporators
    • Y10S159/41Removable units

Definitions

  • This invention relates generally to certain new and useful improvements in concentrators, but more particularly to a concentrating apparatus for evaporating water from fruit juices and like solutions which cause the coating of the heating surfaces with a slimy or gelatinous layer and interfere with the heat transfer unless continuously removed.
  • Another object is to provide a concentrating apparatus which will effect concentration of the material in one pass therethrough and thereby prevent loss of valuable properties, particularlyin sensitive materials, due to the short time the material is in contact with the heating surfaces.
  • a further object of the invention is to provide a concentrator whose interior parts are so designed and arranged as to enable their ready withdrawal for cleaning.
  • Figure 1 is a side elevation of the concentrating apparatus embodying my invention.
  • Figure 2 is an enlarged fragmentary central longitudinal section thereof.
  • Figure 3 is an end view of the same, viewing the left hand end of Figure 1.
  • Figures 4 and 5 are cross sections taken substantially on the correspondingly numbered lines in Figure 2.
  • Figure 6 is a longitudinal section taken on line 6-45, Figure 5.
  • Figure 7 is an enlarged fragmentary cross section taken on line 'l-1, Figure 2, showing one of the scrapers for cleaning the inside surface of the steam jacket cylinder.
  • Figure 8 is a fragmentary longitudinal section taken on line 8--8, Figure 7.
  • the invention comprises an outer stationary heating unit or steam jacketed cylinder I! supported on suitable pedestals II, II, and an inner, slowly rotating cylinder 12 of substantially frusto-conical shape disposed therein and between the annular surfaces of which cylinders. the liquid to be concentrated is introduced and passed.
  • an outer stationary heating unit or steam jacketed cylinder I! supported on suitable pedestals II, II, and an inner, slowly rotating cylinder 12 of substantially frusto-conical shape disposed therein and between the annular surfaces of which cylinders. the liquid to be concentrated is introduced and passed.
  • the steam jacketed cylinder I0 consists of an outer shell l3 and a concentrically-spaced inner shell I4 having helically-disposed ribs l5 therebetween providing a helical or spiral passage l6, closed at its ends, for the circulation of the steam which is introduced thereto through an inlet l1 located adjacent one end of such cylinder.
  • This helical steam passage is gradually decreased in cross-sectional area from. its intake end in such proportion as to maintain a fairly uniform velocity of the steam.
  • this cylinder In its outer shell i3 this cylinder has a plurality of condensate drains I8, and in its top it has a vent I 9 for non-condensibles.
  • the inner rotatable cylinder [2 is tapered from the vent end of the stationary cylinder to its steam intake end and provided on its outer surface are helices or spiral ribs 26 which form a helical or spiral passage 2! for vapor between this rotating cylinder and the inner shell 14 of the companion cylinder.
  • the ends of this passage are closed by walls 22, 23 and the wall 22 has a plurality of small intake ports 24 therein for the liquid to be concentrated while the opposite wall 23 has a plurality of larger outlet ports 25 therein.
  • the ends of the rotating cylinder are closed by dished heads 23 having collars Z1 thereon and these collars are attached to a hollow shaft 28 extending axially through the cylinder and supported at its ends in suitable adjustable bearings 29 attached to heads 30, 3
  • the head 30 is detachably connected to an end closure flange 33 applied to the some sponding end of the cylinder in while the companion head 3i may be fixed by welding or the like.
  • a drive sprocket 34 is fixed on one end of this shaft for connection to a suitable source of power to impart a slow rotation to the inner cylinder 12.
  • the inner shell IA of the stationary or steamjacketed cylinder Ill is extended at one end beyond the tapered end of the rotating cylinder l2 to provide a vapor chamber 35 havmg a discharge passage 36 adapted for connection to a condenser.
  • This chamber has a transverse partition or annular member 31 substantially centrally thereof to divide it into two parts and to prevent any of the concentrate discharged from the spiral passage 2
  • the extended portion of this cylinder has a discharge opening 38 for the concentrate and at the opposite. or outer side thereof it has a drain 39 for removing the water while washing the interior of the apparatus.
  • a scraping blade 42 Disposed between and mounted on each pair of helices 2c is a scraping blade 42 in contact with the inner surface of the shell l4 ofthe steam jacket cylinder It to keep such surface clean of foreign matter during the rotation of the cylinder I2 and maintain the heat transfer into the spiral passage 2
  • a light, substantially U-shaped spring 43 adjacent each end of the blade maintains it against the inner shell-surface, and the ends of the blade fit into a shallow notch 44 provided in the edges of adjoining helices with a milled slot 45 into which the edge of the scraper is inserted for holding it in place.
  • a beam 46 Extending through and beyond either end of the hollow shaft 28 is a beam 46, which may be of I-beam cross section, as shown in Figure 5, and which is supported at its opposite ends on vertically-adjustable pads 41 applied to companion jack-screws 43 mounted on frames 49.
  • Trolleys 5e are arranged adjacent the ends of this hollow shaft, each including four wheels 5
  • This apparatus is particularly useful in the evaporation of such products as fruit juices and the like which coat the heating surfaces with a slimy or gelatinous-like layer, and due to its structural arangement of parts and the high velocity of the steam and the vapor, the rates of heat transfer are high and a minimum of heating surface is required for a given amount of evaporation, all of which makes possible the concentration of the juice or solution in one pass through the concentrator without loss of valuable properties because of the short time it is in contact with the heating surfaces.
  • This apparatus because of the ready removability of its interior parts for thorough cleaning, is also adaptable for evaporating water from milk or other solutions which must be concentrated under completely sanitary conditions.
  • the inner cylinder l2 can be stationary and need not be revolved.
  • An apparatus of the character described comprising an outer steam jacketed cylinder including helices therein. to define a spiral-like pausage for the steam and having end heads containing axial bearings, an inner tapered rotatable cylinder disposed axially of and in spaced relation to said outer cylinder for removal therefrom and to provide a forwardly-diverging annular passage adapted for communication at its converging intake end with the solution to be concentrated, said inner cylinder having helices on the exterior thereof extending through said annular passage from end to end thereof, and a hollow shaft extending axially of the inner cylinder and journaled at its ends in the head bearings of the outer cylinder and constituting a support for said cylinders, the outer cylinder having a chambered portion extending beyond the converging end of the inner cylinder and in communication with the diverging end of said passage and having a vapor ou let and a concentrate discharge therein, and an annular transverse partitionin said chamber separating said discharge from said vapor outlet.
  • An apparatus of the character described comprising an outer cylinder having end heads one of which is removable, bearings applied axially of said heads, an inner revolvable cylinder disposed axially of and in spaced relation to said outer cylinder for removal therefrom, a hollow shaft extending axially of said inne cylinder and journaled at its end in the outer cylinder bearings, a beam extending through said shaft and adapted to be supported beyond the ends of the same, and trolley devices in said shaft including wheels in longitudinal guiding contact with said beam and rollers for contact with the inner surface of said shaft.
  • An apparatus of the character described comprising an outer cylinder having end heads provided with bearings, one of said heads being removably mounted on such cylinder, a revolving cylinder removably arranged within said outer cylinder and including a hollow shaft extending at its ends through said end heads and journaled in the bearings thereof, a beam extending freely through said hollow shaft, vertically-adjustable supports for the ends of said beam, and trolley means disposed between the beam and the interior of said shaft and having wheels thereon for rolling contact with said beam and rollers normally out of contact with said shaft but adapted to contact the inner Wall thereof in an elevated position of the beam when removing the revolving cylinder from the outer cylinder.
  • a concentrating apparatus comprising a horizontally-disposed cylindrical heating unit including inner and outer spaced shells having means in the annular space therebetween for circulating a heating medium therethrough in a helical path with the cross-sectional area of such path decreasing from one end thereof to the other to maintain a substantially uniform velocity of the heating medium, the outer shell having a plurality of openings therein for the continuous removal of the condensed heating medium, a

Description

Oct. 27, 1953 Filed Feb. 16. 1949 B. S. HUGHES CONCENTRATING APPARATUS 2 Sheets-Sheet l M: Q -MJM ZSnven-l'or (Ittomeg Oct. 27, 1953 s. s. HUGHES CONCENTRATING APPARATUS 2 Sheets-Shoot Filed Feb. 16. 1949 Patented Oct. 27, 1953 2,656,885 CONOENTRATING APPARATUS Burton S. Hughes, Bufialo, N. Y., assignor to Zaremba Company, tion of New York Buffalo, N. Y., a corpora- Application February 16, 1949, Serial No. 76,730
4 Claims. 1
This invention relates generally to certain new and useful improvements in concentrators, but more particularly to a concentrating apparatus for evaporating water from fruit juices and like solutions which cause the coating of the heating surfaces with a slimy or gelatinous layer and interfere with the heat transfer unless continuously removed.
It is one of the objects of this invention to provide a concentrator of this character which is so designed and constructed as to provide for a high velocity of steam and vapor therethrough with a high rate of heat transfer and with less heating surface required for a given amount of evaporation.
Another object is to provide a concentrating apparatus which will effect concentration of the material in one pass therethrough and thereby prevent loss of valuable properties, particularlyin sensitive materials, due to the short time the material is in contact with the heating surfaces.
A further object of the invention is to provide a concentrator whose interior parts are so designed and arranged as to enable their ready withdrawal for cleaning.
Other features of the invention reside inthe construction and arrangement of parts hereinafter described and particularly pointed out in the appended claims.
In the accompanying drawings:
Figure 1 is a side elevation of the concentrating apparatus embodying my invention. Figure 2 is an enlarged fragmentary central longitudinal section thereof. Figure 3 is an end view of the same, viewing the left hand end of Figure 1. Figures 4 and 5 are cross sections taken substantially on the correspondingly numbered lines in Figure 2. Figure 6 is a longitudinal section taken on line 6-45, Figure 5. Figure 7 is an enlarged fragmentary cross section taken on line 'l-1, Figure 2, showing one of the scrapers for cleaning the inside surface of the steam jacket cylinder. Figure 8 is a fragmentary longitudinal section taken on line 8--8, Figure 7.
Similar characters of reference indicate corresponding parts throughout the several views.
In the preferred embodiment of the invention shown in the drawings, it comprises an outer stationary heating unit or steam jacketed cylinder I!) supported on suitable pedestals II, II, and an inner, slowly rotating cylinder 12 of substantially frusto-conical shape disposed therein and between the annular surfaces of which cylinders. the liquid to be concentrated is introduced and passed.
The steam jacketed cylinder I0 consists of an outer shell l3 and a concentrically-spaced inner shell I4 having helically-disposed ribs l5 therebetween providing a helical or spiral passage l6, closed at its ends, for the circulation of the steam which is introduced thereto through an inlet l1 located adjacent one end of such cylinder. This helical steam passage is gradually decreased in cross-sectional area from. its intake end in such proportion as to maintain a fairly uniform velocity of the steam. In its outer shell i3 this cylinder has a plurality of condensate drains I8, and in its top it has a vent I 9 for non-condensibles.
The inner rotatable cylinder [2 is tapered from the vent end of the stationary cylinder to its steam intake end and provided on its outer surface are helices or spiral ribs 26 which form a helical or spiral passage 2! for vapor between this rotating cylinder and the inner shell 14 of the companion cylinder. The ends of this passage are closed by walls 22, 23 and the wall 22 has a plurality of small intake ports 24 therein for the liquid to be concentrated while the opposite wall 23 has a plurality of larger outlet ports 25 therein. The ends of the rotating cylinder are closed by dished heads 23 having collars Z1 thereon and these collars are attached to a hollow shaft 28 extending axially through the cylinder and supported at its ends in suitable adjustable bearings 29 attached to heads 30, 3| applied to the extended end portions of the stationary cylinder I 0 and having stuifing boxes 32 disposed between the shaft and such heads. The head 30 is detachably connected to an end closure flange 33 applied to the some sponding end of the cylinder in while the companion head 3i may be fixed by welding or the like. A drive sprocket 34 is fixed on one end of this shaft for connection to a suitable source of power to impart a slow rotation to the inner cylinder 12.
The inner shell IA of the stationary or steamjacketed cylinder Ill is extended at one end beyond the tapered end of the rotating cylinder l2 to provide a vapor chamber 35 havmg a discharge passage 36 adapted for connection to a condenser. This chamber has a transverse partition or annular member 31 substantially centrally thereof to divide it into two parts and to prevent any of the concentrate discharged from the spiral passage 2| being carried out by the vapor. At the inner side of this partition the extended portion of this cylinder has a discharge opening 38 for the concentrate and at the opposite. or outer side thereof it has a drain 39 for removing the water while washing the interior of the apparatus. Between the opposing heads 26 and 30 there is provided a chamber into which the liquid to be concentrated is introduced through an inlet 4! formed in the head 30 and from which chamber the liquid is discharged through the ports 24 into the spiral passage 2| between the companion cylinders I!) and I2.
Disposed between and mounted on each pair of helices 2c is a scraping blade 42 in contact with the inner surface of the shell l4 ofthe steam jacket cylinder It to keep such surface clean of foreign matter during the rotation of the cylinder I2 and maintain the heat transfer into the spiral passage 2| at a maximum at all times. A light, substantially U-shaped spring 43 adjacent each end of the blade maintains it against the inner shell-surface, and the ends of the blade fit into a shallow notch 44 provided in the edges of adjoining helices with a milled slot 45 into which the edge of the scraper is inserted for holding it in place.
Extending through and beyond either end of the hollow shaft 28 is a beam 46, which may be of I-beam cross section, as shown in Figure 5, and which is supported at its opposite ends on vertically-adjustable pads 41 applied to companion jack-screws 43 mounted on frames 49. Trolleys 5e are arranged adjacent the ends of this hollow shaft, each including four wheels 5| in rolling contact with the base-flanges of the beam and two rollers 52 having their axes parallel with the axis of the shaft and adapted for contact with the inside of such shaft when the beam 46 is elevated. In the normal position of the parts shown in the drawings, with the beam lowered, the rollers 52 are free from contact with the hollow shaft 28 and it can turn freely. However, when the beam is raised by the jack-screws 43, these rollers contact the inner surface of the shaft and the inner assembly l2 of the concentrator and its associated parts can be removed from the outer assembly it for cleaning, as shown by dot-dash lines in Figure 1. The inner assembly can be rotated on the trolley-rollers 52 for convenience in washing and scrubbing the parts.
This apparatus is particularly useful in the evaporation of such products as fruit juices and the like which coat the heating surfaces with a slimy or gelatinous-like layer, and due to its structural arangement of parts and the high velocity of the steam and the vapor, the rates of heat transfer are high and a minimum of heating surface is required for a given amount of evaporation, all of which makes possible the concentration of the juice or solution in one pass through the concentrator without loss of valuable properties because of the short time it is in contact with the heating surfaces.
This apparatus, because of the ready removability of its interior parts for thorough cleaning, is also adaptable for evaporating water from milk or other solutions which must be concentrated under completely sanitary conditions. For such use the inner cylinder l2 can be stationary and need not be revolved.
I claim as my invention:
1. An apparatus of the character described, comprising an outer steam jacketed cylinder including helices therein. to define a spiral-like pausage for the steam and having end heads containing axial bearings, an inner tapered rotatable cylinder disposed axially of and in spaced relation to said outer cylinder for removal therefrom and to provide a forwardly-diverging annular passage adapted for communication at its converging intake end with the solution to be concentrated, said inner cylinder having helices on the exterior thereof extending through said annular passage from end to end thereof, and a hollow shaft extending axially of the inner cylinder and journaled at its ends in the head bearings of the outer cylinder and constituting a support for said cylinders, the outer cylinder having a chambered portion extending beyond the converging end of the inner cylinder and in communication with the diverging end of said passage and having a vapor ou let and a concentrate discharge therein, and an annular transverse partitionin said chamber separating said discharge from said vapor outlet.
2. An apparatus of the character described, comprising an outer cylinder having end heads one of which is removable, bearings applied axially of said heads, an inner revolvable cylinder disposed axially of and in spaced relation to said outer cylinder for removal therefrom, a hollow shaft extending axially of said inne cylinder and journaled at its end in the outer cylinder bearings, a beam extending through said shaft and adapted to be supported beyond the ends of the same, and trolley devices in said shaft including wheels in longitudinal guiding contact with said beam and rollers for contact with the inner surface of said shaft.
3. An apparatus of the character described, comprising an outer cylinder having end heads provided with bearings, one of said heads being removably mounted on such cylinder, a revolving cylinder removably arranged within said outer cylinder and including a hollow shaft extending at its ends through said end heads and journaled in the bearings thereof, a beam extending freely through said hollow shaft, vertically-adjustable supports for the ends of said beam, and trolley means disposed between the beam and the interior of said shaft and having wheels thereon for rolling contact with said beam and rollers normally out of contact with said shaft but adapted to contact the inner Wall thereof in an elevated position of the beam when removing the revolving cylinder from the outer cylinder.
4. A concentrating apparatus, comprising a horizontally-disposed cylindrical heating unit including inner and outer spaced shells having means in the annular space therebetween for circulating a heating medium therethrough in a helical path with the cross-sectional area of such path decreasing from one end thereof to the other to maintain a substantially uniform velocity of the heating medium, the outer shell having a plurality of openings therein for the continuous removal of the condensed heating medium, a
cylinder of substantially frusto-conical shape,
and closed at its ends, disposed axially within said heating unit in spaced relation thereto and having helices on its exterior surface defining a helical passage for the vaporizing of the solution to be concentrated, the helical pas-sage being closed at its ends and having intake ports at one end for the liquid to be concentrated and outlet ports at its opposite end and the cross sectional area of such passage increasing from its intake to its discharge end, the inner shell of said heatmg unit extending beyond the reduced end of the frusto-conical cylinder to provide a communicating vapor chamber having a concentrate discharge in its lower side and a vapor discharge in its upper side, and an annular partition disposed in said vapor chamber in a plane between the concentrate and vapor discharges to prevent the concentrated material being carried out by the vapor.
BURTON S. HUGHES.
References Cited in the file of this patent UNITED STATES PATENTS 10 Number Name Date Miller May 9, 1922 Mellott Mar. 16, 1926 Pezold Apr. 13, 1926 Rugh Oct. 8, 1929 Mortensen Apr. 19, 1932 Zorn et a1. Mar. 6, 1936 FOREIGN PATENTS Country Date Great Britain Feb. 5, 1894 Norway May 28, 1906
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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3253643A (en) * 1963-03-18 1966-05-31 Arne R Gudheim Horizontally axised evaporator of the rotary wiped thin film type
US3261391A (en) * 1964-05-20 1966-07-19 Arne R Gudheim Thin-film processing apparatus
US3292683A (en) * 1962-10-14 1966-12-20 Buchi Walter Wiped falling film evaporator
US3357477A (en) * 1966-12-23 1967-12-12 Artisan Ind Thin film processing apparatus
US3372095A (en) * 1964-11-05 1968-03-05 Nester And Faust Mfg Corp Separator
US5085410A (en) * 1989-12-14 1992-02-04 Jersey Nuclear-Avco Isotopes, Inc. Modular processing system
US5185757A (en) * 1989-12-14 1993-02-09 Jersey Nuclear-Avco Isotopes, Inc. Modularized replaceable vaporizer and extractor apparatus
EP2100649A1 (en) * 2008-03-13 2009-09-16 Buss-SMS-Canzler GmbH Thin-film vaporiser

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB189402498A (en) * 1894-02-05 1894-04-28 Hugo Kohl Improvements in Means for Heating by Steam Feed Water and other Liquids.
US942407A (en) * 1908-12-17 1909-12-07 Charles Ordway Evaporating apparatus.
US1164413A (en) * 1915-03-16 1915-12-14 Edward Shaw Apparatus for evaporating or concentrating liquids.
US1355702A (en) * 1919-05-05 1920-10-12 Shaw Edward Apparatus for evaporating or concentrating liquids
US1415255A (en) * 1918-05-10 1922-05-09 Evaporating And Drying Machine Evaporator
US1576838A (en) * 1921-02-04 1926-03-16 Howard S Mellott Concentrator
US1580164A (en) * 1922-01-28 1926-04-13 George J Pezold Drying apparatus
US1730902A (en) * 1925-07-25 1929-10-08 American Cyanamid Co Method of and means for drying
US1854619A (en) * 1930-08-28 1932-04-19 Mortensen Cornelius Milk treating apparatus
US2032785A (en) * 1932-06-20 1936-03-03 Low Temperature Proc Company Method of and apparatus for disassociating the components of solutions and mixtures

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB189402498A (en) * 1894-02-05 1894-04-28 Hugo Kohl Improvements in Means for Heating by Steam Feed Water and other Liquids.
US942407A (en) * 1908-12-17 1909-12-07 Charles Ordway Evaporating apparatus.
US1164413A (en) * 1915-03-16 1915-12-14 Edward Shaw Apparatus for evaporating or concentrating liquids.
US1415255A (en) * 1918-05-10 1922-05-09 Evaporating And Drying Machine Evaporator
US1355702A (en) * 1919-05-05 1920-10-12 Shaw Edward Apparatus for evaporating or concentrating liquids
US1576838A (en) * 1921-02-04 1926-03-16 Howard S Mellott Concentrator
US1580164A (en) * 1922-01-28 1926-04-13 George J Pezold Drying apparatus
US1730902A (en) * 1925-07-25 1929-10-08 American Cyanamid Co Method of and means for drying
US1854619A (en) * 1930-08-28 1932-04-19 Mortensen Cornelius Milk treating apparatus
US2032785A (en) * 1932-06-20 1936-03-03 Low Temperature Proc Company Method of and apparatus for disassociating the components of solutions and mixtures

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3292683A (en) * 1962-10-14 1966-12-20 Buchi Walter Wiped falling film evaporator
US3253643A (en) * 1963-03-18 1966-05-31 Arne R Gudheim Horizontally axised evaporator of the rotary wiped thin film type
US3261391A (en) * 1964-05-20 1966-07-19 Arne R Gudheim Thin-film processing apparatus
US3372095A (en) * 1964-11-05 1968-03-05 Nester And Faust Mfg Corp Separator
US3357477A (en) * 1966-12-23 1967-12-12 Artisan Ind Thin film processing apparatus
US5085410A (en) * 1989-12-14 1992-02-04 Jersey Nuclear-Avco Isotopes, Inc. Modular processing system
US5185757A (en) * 1989-12-14 1993-02-09 Jersey Nuclear-Avco Isotopes, Inc. Modularized replaceable vaporizer and extractor apparatus
EP2100649A1 (en) * 2008-03-13 2009-09-16 Buss-SMS-Canzler GmbH Thin-film vaporiser

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