US2622779A - Method of and apparatus for pressurizing and sealing thermostat tubes - Google Patents

Method of and apparatus for pressurizing and sealing thermostat tubes Download PDF

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US2622779A
US2622779A US146364A US14636450A US2622779A US 2622779 A US2622779 A US 2622779A US 146364 A US146364 A US 146364A US 14636450 A US14636450 A US 14636450A US 2622779 A US2622779 A US 2622779A
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tube
chamber
pressure
sealed
gas
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US146364A
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William M Smith
Don A Brosseau
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Vapor Heating Corp
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Vapor Heating Corp
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K5/00Measuring temperature based on the expansion or contraction of a material
    • G01K5/02Measuring temperature based on the expansion or contraction of a material the material being a liquid
    • G01K5/025Manufacturing of this particular type of thermometer
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S53/00Package making
    • Y10S53/03Sealing electron tubes

Definitions

  • thermometers or thermostatis of the tube type emple'yingan expansible column of mercury or mercury alley-it has been customary practice to remove the atmosphere from above '--the mercury column and introduce a non-corrosive gas therein preliminary to the "final sealing of-the tube; This is done to avoidpossible corrosion of the mercury in the thermostat, since any trace of oxygen in the tube will cause -objectional-corrosion of r the mercury contained-in the tube.
  • thermometer tube containing a: column .of .expansible liq'uidyandthereafter ;resealing the tube in the" presence: of
  • thermometer tube containing the desired quantity of mercury
  • a chamberfilled with hydrogen. or. other pressure producing gas containing the desired quantity of mercury
  • an'inertgas such. as nitrogen.
  • the 'tube is supported 'ata location above "the "hotplastic area of the tube. Therefore'the weight'of the thermometer tube. and the pressure from the inert-gas is utilized to cause the tube to neck in atxthe point of rescaling.
  • the apparatus-herein illustrated for performing the several steps of the method includes the provision of a gas chamber having an opening therein to receive the closed end of a thermostat tube within the said gas chamber.
  • A' means in the form of a compressible ring surrounds the thermostat tube for sealing the opening in the gas chamber and for clamping the tube inposition to be pressurized and thereafter rescaled.
  • the said resilient ring is interposed between the said gas chamber and a fixed part of the apparatus.
  • a pivoted yoke type of clamp is positioned to move into and out of clamping engagement with the upper end of the housing defining said gas chamber to hold-the housing in position and to simultaneously compress the resilient ring into clamping engagementwith the thermometer tube.
  • thermometer tube extending into the gas chamberis manually operable to knock off thetip of the thermometer tube to permit the pressurizing gas to enter and fill that portion of the thermometer tube which extends above the column of mercury contained in'the tube.
  • Another gas chamber preferably containing nitrogen underpressure, surrounds the portion of the tube which extends below theresilient clamping ring.
  • the housing defining this chamber is preferably composed of two par-tsa fixed portion and-a removable lower portion.
  • the lower portion of this housing is removably clampedto the fixedportion by means of a second pivotedyoke formof clamp, which clamp may be quickly released and *moved out of its clamping position when it is desired to remove a pressurized-tube and thereafter insert another tube in'theapparatus.
  • An' ele'ctrical heater is positioned in the nitrogen chamber at alocation where it is de-- sired to sever and reseal the thermometertube.
  • Fig. 1 is an elevational view of a thermometer tube containing a column of expansion liquid with an evacuated space above the said column and adapted to be acted upon according to the process and apparatus of the present invention
  • Fig. 2 is a perspective view of an apparatus according to the present invention for sealing and pressurizing a thermometer shown in Fig. 1;
  • Fig. 3 is an enlarged vertical section taken through a portion of the apparatus of Fig. 2 showing the thermometer of Fig. 1 in position to be acted upon by the apparatus of Fig. 2;
  • Fig. 4 is a view similar to Fig. 3 but showing the thermometer of Fig. 2 after being subjected to pressurizing of the liquid column and partially rescaled; and Fig. 5 isan elevational view of a thermometer which has been scaled under pressure according to the process and apparatus of Figs. 2, 3 and 4.
  • a thermostat tube I9 which includes a reservoir I I for mercury or other expansible liquid having the property of conducting electricity.
  • the tube I has a capillary I2 therein, which communicates with the reservoir II, and which is sealed generally under vacuum, as at I3, at the end remote from the reservoir I I.
  • the tube I0 is provided with circuit closing contacts I4 having fine platinum wire (not shown) sealed in the wall of the tube and intersecting the bore of the capillary I2, so that when the column of mercury is subjected to changing temperature conditions, circuits which include the thermostat III will be made or broken.
  • the apparatus shown represents certain preferred embodiments and is constructed to subject the capillary I2 of the thermostat tube It! to an internal pressure of preferably 110 pounds. It also facilitates rescaling the tube I9 at a desired point above the column of mercury therein while the capillary I2 is under said pressure.
  • the apparatus I5 consists generally of a base support I6 having extending therefrom vertical standards IT.
  • the standards I! support a generally rectangular housing I8 divided by a wall I9 into a pair of chambers 2
  • the housing I 8 is formed with a flange 26 which bears against a sealing gasket 2'! and a closure member 28, the
  • the housing I8 is formed with a cylindrical recess 32 and an axial opening 33, the wall I9 forming a seat for a resilient clamping member which is adapted to have pressure exerted thereon by a nipple-like extension 31, having a central bore 38 of an annular cup shaped housing 39 defining a gas chamber 49.
  • the upper end of said housing is closed by a screw plug M.
  • the said gas chamber housing 49 is held clamped in its normal operative position by means of a pivoted yoke type of clamp 42 including a thrust or clamping screw 43.
  • the yoke type of pivoted clamp is pivoted at 44 to the housing I8 so that the clamp can be readily swung into and out of clamping position.
  • the screw 43 seats in a socket 45 formed in the plug. It will be seen, therefore, that when thescrew 43 is thrust against the plug 4
  • Means are provided for subjecting the sealed end I3 of the tube ID to gaseous pressure, the seal I3 being broken in the presence of the gaseous pressure to fillthe capillary with gas at approxi-' mately pounds pressure per square inch and expose the liquid in the capillary I2 to such pressure.
  • the chamber 49 is first connected with a suction device (not shown) to withdraw the atmosphere from the chamber. It is thereafter filled with gas under pressure before the sealed end- I3 of the thermometer tube I0 is broken.
  • a conduit 46 leads from the chamber 49 to a main pipe '41 (Fig.
  • the vacuum within the chamber 40 has a value of 29 inches of mercury.
  • the means for breaking the sealed end I3 of tube I0 comprises a plunger 52 supported in a tubular guide 53, the plunger to move in a bore 54 leading through a wall of chamber 49.
  • a resilient packing 55 is compressed between a portion 56 ofthe housing 39 and a guide wall 51 which prevents the escape of gas from the chamber 40.
  • a disk form of collar 58 is secured to the plunger. 54. The said disk fits loosely in a chamber 59 and provides a movable abutment for a spring 60 which encircles the plunger 52, and abuts an end wall 6
  • the position of the sealed end I3 of the tube I0 within the chamber 40 may be observedby means of a window 62-62 formed in the opposite walls of the housing 39.
  • the pivoted arms of the clamp member 42 are likewise formed with holes 63--63 which, when the clamp member 42 is in the position shown in Figs. 2, 3 and 4, provide sight openings in alignment with the windows 62-62.
  • the sealed end l3 of the tube Ill may be broken by moving the plunger 5A to the rightagainst the force of thespring '86 and then releasing the plunger 52 to cause the end thereof to strike the sealed tip i3 smartly and break same.
  • the capillary I2 is then subject to the pressure maintained within the chamber 40.
  • the chamber 22 encloses the lower portion of the thermometer tube H] and isadapted to contain an inert. gas, for example, nitrogen at a pressure higher than the internal pressure of the capillary, whereby the difie'rentialin the internal and external pressure will aid in collapsing the tube when a portion of it is heated to a plastic state in the lower chamber.
  • the gas pressures herein specified for the chambers 40 and 22 are not critical and may be varied. However, it is desirable, in the present invention, to maintain the hydrogen in the tube If] at 110 pounds pressure. Consequently, the gas pressure in the chamber 22 surrounding the lower portion of the tube is maintained at 120 pounds pressure so as to providea convenient differential between the internal and external pressure exerted against the walls of the tube.
  • the connections for introducing nitrogen into chamber 22 includes a tube 65 branching from a supply pipe 66 provided with a pressure adjusting valve Bl and a pressure measuring gauge 68. It will be seen that the portionof the tube 10 extending below the clamping member 34 is thus subjected to pressure from the gas within the chamber 22.
  • a T-fitting and valve 69 connect into the supply pipe 66 and in a branch suction pipe 10 leading to the vacuum pump (not shown).
  • Means are provided for subjecting the portion of the tube Ill extending below the clamping member 34 and within the chamber 22 to localized heat sufficient to cause a portion of the glass tube 10 to become plastic, whereupon the weight of the mercury in the tube causes the heated portion of the glass tube to stretch, during downward movement of the mercury loaded end of the tube.
  • This downward movement of the tube together with the fact that external nitrogen pressure is greater than the internal hydrogen pressure causes the heated portion of the tu'beto neck in as shown at T l and thereby effect thorough sealing of the central bore l2 of the tube it).
  • the said tube is heated by means of an electrical heater l2 and is mounted in the upper end of a gland element 13 threaded through an opening in the closure member 28 associated with the fixed housing H! of gas chamber 22.
  • the lower portion of gas chamber 22 is defined by a cylindrical housing 14 which is removably clamped to the lower portion of gland 13 by means of a pivoted yoke type of clamp which includes a thrust screw '55 adapted to exert clamping pressure against the bottom of said cylindrical housing M and thereby clamp the open upper end of housing 74 against said gland 13.
  • the housing section 14 is preferably provided with oppositely disposed windows 16-16 so that the operator of the pressurizing apparatus can see when the lower portion of the thermometer 6 tube It! has moved downwardly to the position shown in Fig.4. In this position the lower end of the tube rests on a resilient pad Tl.
  • thermometer tube I8 In operation, the pressure exerted by the thrust screw 15'is released and the cylindrical housing 14 is removed. The end l3 of a thermometer tube I8 is thrust past the resilient support 34 into the chamber 46, the proper position of the tube being observed through the windows 62.
  • a hinged gauge support 78 provided with an adjustable screw 19 to support the tube Ill in position swings inwardly beneath the tube so as to support it until the thrust screw 43 is tightened to compress the resilient ring 34 and thereby hold the tube W in its proper position. After'the ring 32 is compressed sufficiently tohold the tube 19, the gauge support 18 is swung outwardly to its inoperative position, as shown in Figs.
  • valves 49 and 61 are opened and the suction pump (not shown) functions to withdraw the atmosphere from the chambers it and 22.
  • the valves 49 and '81] are closed and the valves 59 and 61 are opened to fill the said chambers 40 and 22 with gas, preferably hydrogen for chamber 43 and nitrogen for chamber 22.
  • the hydrogen in chamber 69' is maintained at a gauge pressure of pounds and the nitrogen inchamber 22 is maintainedat a gauge pressure of pounds.
  • the valves 50 and 61 are closed and plunger 52 is operated to knock ofi the sealed end l3.
  • a localized portion of the glass tube ID is then heated to a plastic state. This is performed by energizing the electrical heater #2 of the apparatus.
  • the pressure chambers 22 and 4t may be relieved by partially opening the valves 80 and 49, respectively.
  • the thrust screw '55 may be released and the cylindrical housing removed whereupon the entire tube EU may be removed from the apparatus by releasing the thrust screw G3 so as to relieve the compression and consequently the tube clamping action of the resilient ring '34.
  • thermometers with the liquid column under pressure
  • sealing being characterized by employing a differential of the internal and external gaseous pressure to facilitate the resealing process
  • process and apparatus being also characterized by freedom from danger of explosion or fire in the event an explosive gas is employed to pressurize the liquid column.
  • apparatus of the class described for pressurizing a column of liquid within a sealed tube means for supporting said tube at a point intermediate its ends, means defining a chamber exposed to a source of gas under pressure into which a sealed end of said tube extends, means for breaking the sealed end of said tube within said chamber to expose said column of liquid to said pressure, means defining a second chamber intermediate the point of support of said tube and the opposite end thereof for subjecting the exterior of said sealed tube to an atmosphere of inert gas, means surrounding said sealed tube to an atmosphere of inert gas, means surrounding said sealed tube within said last named chamber for heating a localized area of said tube to a plastic condition in the presence of said inert gas for resealing and severing said tube within the column therein subject to gaseous pressure, and a chamber interposed between both of said chambers for providing circulation of a coolant for localizing the heating of said tube.
  • said support means defining a seal between said chambers for preventing movement of gas from either of said chambers to the other, means surrounding said sealed tube within said last named chamber for localized heating of said tube to a plastic condition in the presence of said inert gas for resealing said tube while the liquid column therein is subjected to gaseous pressure, and a chamber interposed between both of said chambers for providing circulation of a coolant.
  • thermometer tube containing a liquid column therein comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber enclosing the portion of the tube containing the liquid colunm and a portion contiguous thereto and intermediate the said liquid column and the sealed end of the tube, compressible means interposed between said chambers for sealing said connecting passages and for supporting said tube, means for delivering gas under pressure into said upper chamber, means for delivering gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube, and means located within the lower chamber for plasticizing a portion of said contiguous portion of said tube, whereby the gaseous pressure in said lower chamber compresses the plasticized portion of the tube to seal the same.
  • An apparatus for pressurizing and rescaling a glass thermometer tube containing a liquid column therein comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and intermediate the said liquid column and the sealed end of the tubeycompressibl'e. means interposed. between said chambers.
  • An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and intermediate the liquid column and the sealed end of the tube, compressible means interposed between said chambers for sealing said connecting passages and for supporting said tube, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube comprising a manually actuated spring pressed plunger extending into said chamber at one side thereof,
  • An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and intermediate the liquid column and the sealed endof the tube, compressible means interposed between said chambers for sealing said connecting pas-- sages and for supporting said tube, clamping means for maintaining the upper chamber in position and for exerting compressive force on said compressible means, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube comprising a manually actuated spring pressed plunger extending into said chamber at one side thereof, and means located within the lower chamber for heating a portion of said con
  • An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid. column therein comprising housing means defining upper and lower chambers having connect- 1'0 ing, passages and together enclosing a sealed thermometer tube extending through said passages, the upperchamber enclosing a sealed end of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and'intermediate the liquid column and the sealedend of the tube, compressible means interposed between said chambers for sealing said connecting passages and for supporting said tube, clamping means for maintaining the upper chamber in position and for exerting compressive force" on said: compressible means comprising a pivoted yoke movable into and out of position above the upper chamber housing and a screw carriedby the yoke for exerting downward pressure on the top portion of said upper chamber housing, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher
  • An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermostat tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber comprising separable housing sections which together enclose the portion of the tube containing the liquid column and a portion contiguous thereto intermediate said liquid column and the sealed end of the tube, means for clamping the separable housing sections together comprising a pivoted yoke and a thrust screw carried thereby for releasably clamping the separable sections oi the lower chamber housing together, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a pressure higher than that maintained in the upper chamber, manually operable means for rupturing the sealed end of the tube, and means located within the lower chamber for heating a portion of said contiguous portion of said tube to a
  • An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermostat tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber comprising separable housing sections which together enclose the portion of the tube containing the liquid column and a portion contiguous thereto intermediate said liquid column and the sealed end of the tube, means for clamping the separable housing sections together, a swingable support for adjustably positioning the tube in position pre-- liminary to the application of the removable section of the lower chamber housing so that the 11 lower end of the tubeis supported in spaced relation to the bottom of said removable housing section, means for delivering gas under pressure into said upper chamber, means for delivering gas into said lower chamber at a pressure higher than thatmaintained in the upper chamber, means for rupturing the sealed end of said tube, an electrical heating means located within the lower chamber for heating a portion

Description

Dec. 23, 1952 w. M. SMITH ET AL 2,622,779
METHOD OF AND APPARATUS FOR PRESSURIZING AND SEALING THERMOSTAT TUBES Filed Feb. 25, 1950 2 SHEETS-SHEET 1 O 0 V 7a V --7AZ 75 A T i @J? INVENT0R$. if 12 F%%%ZZ? BY I 1/ 42. W
Dec. 23, 1952 2,622,779
W. M. SMITH ET AL METHOD OF AND APPARATUS FOR PRESSURIZING AND SEALING THERMOSTAT TUBES Filed Feb. 25, 1950 2 SHEETS-SHEET 2 Patented Dec. 23, ,1952
METHODuOF AND APPARATUS FOR. PRES-. SURIZING AN D SEALING THERMOSTAT TUBES William'-M. Smith, Glen Ellyn, and Don-A.'Brosseam-Chicago, Ill., *assignors to Vaporv Heating Corporation, Chicago, Ill.,-- a a corporation of Delaware Application February 25, 1950', Serial No'.146',364 13 Claims. (Cl;226-20-) This invention-- relates generallyto the ar-tcrof manufacturing liquid column-thermostats and particularly to the sealing of a thermometer tube containing an expansible'liquid column "subjected to gaseous pressure.
In the manufacture of thermometers or thermostatis of the tube type emple'yingan expansible column of mercury or mercury alley-it has been customary practice to remove the atmosphere from above '--the mercury column and introduce a non-corrosive gas therein preliminary to the "final sealing of-the tube; This is done to avoidpossible corrosion of the mercury in the thermostat, since any trace of oxygen in the tube will cause -objectional-corrosion of r the mercury contained-in the tube.-
It is also desirable to subjectthe column of mercury to gaseous pressure so that the expansible column will not'separate from the main body of mercury upon alternate heating and cooling thereof. Hydrogen is anexample of a non-corrosive =gasawhichis suitable for use in-mercury column thermostats, since itwi ll apply the desired pressure on the mercury -co'lumn-without combining or reacting with the-mercury.
In:.the. manufacture ot-suchthermometersfthe capillary tubes are first; sealed undervacuum and the sealeat the end of the-tube; remote. fromjthe main reservoir oimereury, is brokento introduce the pressure producing gas into the tube andthe tube is thereafter sealed. Since hydrogenis Fan explosive gas, it is difficult to reseal the tube without the attendant danger otexplosion and fire.
Withtherioregoing considerations in mind it isian object ofthis inventionto providea process and apparatus for introducing and-sealing abody oigasinian end-portion of the thermometer tube containing a: column .of .expansible liq'uidyandthereafter ;resealing the tube in the" presence: of
an inert. ga'swith the pressureprod-ucinggas held; within the tube during the process of-:'reseal-i ng andiiat the. conclusiomof .the resealing process.
The several steps. of the. improvedprocess-may be-described briefly as follows: The sealed end-bf a thermometer tube containing the desired quantity of mercury is enclosed :in a chamberfilled with hydrogen. or. other pressure producing gas- Thesealed'end of the-tube is opened in the presence of such gas and the-tubeis thereafter of an'inertgas, such. as nitrogen. The 'tube is supported 'ata location above "the "hotplastic area of the tube. Therefore'the weight'of the thermometer tube. and the pressure from the inert-gas is utilized to cause the tube to neck in atxthe point of rescaling. This'facilitates resealing the tube at a-location above the mercury column so that a quantity of hydrogenis contained in the sealed tube in the space above the mercury column. The introduction of the hydro-- gen gas into the tube and the rescaling thereof is characterized by complete freedom from any possibility of explosionor fire hazard.
The apparatus-herein illustrated for performing the several steps of the method includes the provision of a gas chamber having an opening therein to receive the closed end of a thermostat tube within the said gas chamber. A' means in the form of a compressible ring surrounds the thermostat tube for sealing the opening in the gas chamber and for clamping the tube inposition to be pressurized and thereafter rescaled.
The said resilient ring is interposed between the said gas chamber and a fixed part of the apparatus. A pivoted yoke type of clamp is positioned to move into and out of clamping engagement with the upper end of the housing defining said gas chamber to hold-the housing in position and to simultaneously compress the resilient ring into clamping engagementwith the thermometer tube.
'Aeplunger extending into the gas chamberis manually operable to knock off thetip of the thermometer tube to permit the pressurizing gas to enter and fill that portion of the thermometer tube which extends above the column of mercury contained in'the tube.
Another gas chamber, preferably containing nitrogen underpressure, surrounds the portion of the tube which extends below theresilient clamping ring. The housing defining this chamber is preferably composed of two par-tsa fixed portion and-a removable lower portion. The lower portion of this housing is removably clampedto the fixedportion by means of a second pivotedyoke formof clamp, which clamp may be quickly released and *moved out of its clamping position when it is desired to remove a pressurized-tube and thereafter insert another tube in'theapparatus.- An' ele'ctrical heater is positioned in the nitrogen chamber at alocation where it is de-- sired to sever and reseal the thermometertube.
When'the glass wallsof thetube areheated'to a plastic state the weight of the ---tube and the mercury contained therein stretchesthe molten area'oi' glass; Also the external pressureoi the nitrogen gas against the plastic portion' of the tube'a-ids in sealing'the tube. The releasable v 3 yoke type of clamp permits the lower portion of the nitrogen chamber housing to be readily separated. In this way the upper and lower portions of the glass tube which ordinarily remain connected until they are removed, may be withdrawnfrom the apparatus and another tube inserted therein.
It is a principal object of the invention to provide an improved process as hereinabove briefly described for pressurizing thermometer tubes and to also provide an improved apparatus constructed as hereinabove described for carrying out the several steps of the process. Still other objects of the invention, which are more or less ancillary to those above recited, will appear from the following description of the embodiment of the invention shown in the accompanying drawings. It is to be understood, however, that the embodiment shown is intended as an illustration and not as a limitation.
. In the drawings:
Fig. 1 is an elevational view of a thermometer tube containing a column of expansion liquid with an evacuated space above the said column and adapted to be acted upon according to the process and apparatus of the present invention;
Fig. 2 is a perspective view of an apparatus according to the present invention for sealing and pressurizing a thermometer shown in Fig. 1; Fig. 3 is an enlarged vertical section taken through a portion of the apparatus of Fig. 2 showing the thermometer of Fig. 1 in position to be acted upon by the apparatus of Fig. 2;
Fig. 4 is a view similar to Fig. 3 but showing the thermometer of Fig. 2 after being subjected to pressurizing of the liquid column and partially rescaled; and Fig. 5 isan elevational view of a thermometer which has been scaled under pressure according to the process and apparatus of Figs. 2, 3 and 4. Referring now to Fig. l of the drawings, there isshown a thermostat tube I9 which includes a reservoir I I for mercury or other expansible liquid having the property of conducting electricity. The tube I has a capillary I2 therein, which communicates with the reservoir II, and which is sealed generally under vacuum, as at I3, at the end remote from the reservoir I I. The tube I0 is provided with circuit closing contacts I4 having fine platinum wire (not shown) sealed in the wall of the tube and intersecting the bore of the capillary I2, so that when the column of mercury is subjected to changing temperature conditions, circuits which include the thermostat III will be made or broken.
Referring now particularly to Figs. 2 and 3 of the drawings wherein an apparatus constructed according'to the present invention is indicated generally by the reference numeral I: The apparatus shown represents certain preferred embodiments and is constructed to subject the capillary I2 of the thermostat tube It! to an internal pressure of preferably 110 pounds. It also facilitates rescaling the tube I9 at a desired point above the column of mercury therein while the capillary I2 is under said pressure. The apparatus I5 consists generally of a base support I6 having extending therefrom vertical standards IT. The standards I! support a generally rectangular housing I8 divided by a wall I9 into a pair of chambers 2| and 22, chamber 2| having pipes 23 and 24 connected thereto for circulating a supply of liquid coolant such as water. The housing I 8 is formed with a flange 26 which bears against a sealing gasket 2'! and a closure member 28, the
4 assembly of the housing I8, the gasket 2! and the closure member 28 being bolted to laterally bent end portions 29 of the standards I! by means of attaching bolts and nuts at 39 and 3|. The housing I8 is formed with a cylindrical recess 32 and an axial opening 33, the wall I9 forming a seat for a resilient clamping member which is adapted to have pressure exerted thereon by a nipple-like extension 31, having a central bore 38 of an annular cup shaped housing 39 defining a gas chamber 49. The upper end of said housing is closed by a screw plug M. The said gas chamber housing 49 is held clamped in its normal operative position by means of a pivoted yoke type of clamp 42 including a thrust or clamping screw 43. The yoke type of pivoted clamp is pivoted at 44 to the housing I8 so that the clamp can be readily swung into and out of clamping position. The screw 43 seats in a socket 45 formed in the plug. It will be seen, therefore, that when thescrew 43 is thrust against the plug 4| of housing 39, the housing exerts pressure on the resillient clamping member 34 so as to compress the same and thereby seat the axial opening 38 leading into chamber 40 and also cause the member to grip tightly the outer surface of the thermometer tube l0.
Means are provided for subjecting the sealed end I3 of the tube ID to gaseous pressure, the seal I3 being broken in the presence of the gaseous pressure to fillthe capillary with gas at approxi-' mately pounds pressure per square inch and expose the liquid in the capillary I2 to such pressure. To this end, referring particularly to Fig. 3, the chamber 49 is first connected with a suction device (not shown) to withdraw the atmosphere from the chamber. It is thereafter filled with gas under pressure before the sealed end- I3 of the thermometer tube I0 is broken. For the purpose of evacuating the atmosphere from the said chamber 49, a conduit 46 leads from the chamber 49 to a main pipe '41 (Fig. 2) and a branch 48, the latter of which leads through a valve 49 to a vacuum pump (not shown). The conduit 46 and pipe 4'! also lead through a valve 50 to a source of hydrogen under pressure (not shown). Consequently, when the valve 50 is closed and the valve 49 is open, the atmosphere is withdrawn from the chamber 49. .Preferably the vacuum within the chamber 40 has a value of 29 inches of mercury.
. After the chamber 40 is sufiiciently cleared of atmosphere, the valve 49 is closed and the valve 59 is slowly opened to admit hydrogen gas into the chamber 40 until a gauge pressure of 110 pounds is obtained; the measuring gauge being designated 5|. The sealed end I3 of the tube I0 is then broken, to subject the capillary I2 thereof to pressure within the chamber 49. The means for breaking the sealed end I3 of tube I0 comprises a plunger 52 supported in a tubular guide 53, the plunger to move in a bore 54 leading through a wall of chamber 49. A resilient packing 55 is compressed between a portion 56 ofthe housing 39 and a guide wall 51 which prevents the escape of gas from the chamber 40. A disk form of collar 58 is secured to the plunger. 54. The said disk fits loosely in a chamber 59 and provides a movable abutment for a spring 60 which encircles the plunger 52, and abuts an end wall 6| of the plunger guide 53.
The position of the sealed end I3 of the tube I0 within the chamber 40 may be observedby means of a window 62-62 formed in the opposite walls of the housing 39. The pivoted arms of the clamp member 42 are likewise formed with holes 63--63 which, when the clamp member 42 is in the position shown in Figs. 2, 3 and 4, provide sight openings in alignment with the windows 62-62. It will be apparent that the sealed end l3 of the tube Ill may be broken by moving the plunger 5A to the rightagainst the force of thespring '86 and then releasing the plunger 52 to cause the end thereof to strike the sealed tip i3 smartly and break same. The capillary I2 is then subject to the pressure maintained within the chamber 40.
The chamber 22 encloses the lower portion of the thermometer tube H] and isadapted to contain an inert. gas, for example, nitrogen at a pressure higher than the internal pressure of the capillary, whereby the difie'rentialin the internal and external pressure will aid in collapsing the tube when a portion of it is heated to a plastic state in the lower chamber. The gas pressures herein specified for the chambers 40 and 22 are not critical and may be varied. However, it is desirable, in the present invention, to maintain the hydrogen in the tube If] at 110 pounds pressure. Consequently, the gas pressure in the chamber 22 surrounding the lower portion of the tube is maintained at 120 pounds pressure so as to providea convenient differential between the internal and external pressure exerted against the walls of the tube.
The connections for introducing nitrogen into chamber 22 includes a tube 65 branching from a supply pipe 66 provided with a pressure adjusting valve Bl and a pressure measuring gauge 68. It will be seen that the portionof the tube 10 extending below the clamping member 34 is thus subjected to pressure from the gas within the chamber 22. For the purpose of withdrawing the nitrogen from the chamber 22, a T-fitting and valve 69 connect into the supply pipe 66 and in a branch suction pipe 10 leading to the vacuum pump (not shown).
Means are provided for subjecting the portion of the tube Ill extending below the clamping member 34 and within the chamber 22 to localized heat sufficient to cause a portion of the glass tube 10 to become plastic, whereupon the weight of the mercury in the tube causes the heated portion of the glass tube to stretch, during downward movement of the mercury loaded end of the tube. This downward movement of the tube together with the fact that external nitrogen pressure is greater than the internal hydrogen pressure causes the heated portion of the tu'beto neck in as shown at T l and thereby effect thorough sealing of the central bore l2 of the tube it).
The said tube is heated by means of an electrical heater l2 and is mounted in the upper end of a gland element 13 threaded through an opening in the closure member 28 associated with the fixed housing H! of gas chamber 22. The lower portion of gas chamber 22 is defined by a cylindrical housing 14 which is removably clamped to the lower portion of gland 13 by means of a pivoted yoke type of clamp which includes a thrust screw '55 adapted to exert clamping pressure against the bottom of said cylindrical housing M and thereby clamp the open upper end of housing 74 against said gland 13.
The housing section 14 is preferably provided with oppositely disposed windows 16-16 so that the operator of the pressurizing apparatus can see when the lower portion of the thermometer 6 tube It! has moved downwardly to the position shown in Fig.4. In this position the lower end of the tube rests on a resilient pad Tl.
In operation, the pressure exerted by the thrust screw 15'is released and the cylindrical housing 14 is removed. The end l3 of a thermometer tube I8 is thrust past the resilient support 34 into the chamber 46, the proper position of the tube being observed through the windows 62. However,.in order to insure'that all tubes of a predetermined length shallbe located in like positions, a hinged gauge support 78 provided with an adjustable screw 19 to support the tube Ill in position swings inwardly beneath the tube so as to support it until the thrust screw 43 is tightened to compress the resilient ring 34 and thereby hold the tube W in its proper position. After'the ring 32 is compressed sufficiently tohold the tube 19, the gauge support 18 is swung outwardly to its inoperative position, as shown in Figs. 2 and 4, and the cylindrical housing M is inserted over the lower end of the tube and clamped firmly against the gland '13. The valves 49 and are opened and the suction pump (not shown) functions to withdraw the atmosphere from the chambers it and 22. When a vacuum equivalent to 29 inches of mercury is drawn on saidjchambers 4E] and 22, the valves 49 and '81] are closed and the valves 59 and 61 are opened to fill the said chambers 40 and 22 with gas, preferably hydrogen for chamber 43 and nitrogen for chamber 22. The hydrogen in chamber 69' is maintained at a gauge pressure of pounds and the nitrogen inchamber 22 is maintainedat a gauge pressure of pounds. The valves 50 and 61 are closed and plunger 52 is operated to knock ofi the sealed end l3. A localized portion of the glass tube ID is then heated to a plastic state. This is performed by energizing the electrical heater #2 of the apparatus. When the glass tube is heated sufficiently to permit it to move downwardly to the position shown in Fig. 4, as may be observed through the window 16, the pressure chambers 22 and 4t may be relieved by partially opening the valves 80 and 49, respectively. The thrust screw '55 may be released and the cylindrical housing removed whereupon the entire tube EU may be removed from the apparatus by releasing the thrust screw G3 so as to relieve the compression and consequently the tube clamping action of the resilient ring '34.
After'removing the entire tube from the apparatus, it may be broken at the necked in seal 1 I. The sealed end of the portion containing the mercury is then heated and the sealed end rounded substantially as shown in Fig. 5.
According to the present invention there has been provided a novel and simple apparatus and process for rescaling thermometers with the liquid column under pressure, the sealing being characterized by employing a differential of the internal and external gaseous pressure to facilitate the resealing process, the process and apparatus being also characterized by freedom from danger of explosion or fire in the event an explosive gas is employed to pressurize the liquid column.
While the invention has been described in terms of an embodiment which it may assume in prac-- tice its scope is not intended to be limited in terms of the embodiment shown nor otherwise than by the appended claims.
We claim:
1. The process of pressurizing a column of liquid within a sealed tube which comprises subjecting a sealed end of the tube to gaseous pressure, breaking the sealed end in the presence of said gaseous pressure to admit the gas under pressure into the interior of the tube above said liquid column, subjecting an external portion of said tube at a point remote from said sealed end to an inert gas at a pressure higher than the interior pressure of the tube, and heating said external portion of said tube locally to a plastic condition in the presence of said inert gas, whereby the higher external gaseous pressure forces the plastic glass inwardly toward the center of the tube to seal the same.
. 2. The process of pressurizing a column of liquid within a sealed tube which comprises freely supporting said tube at a point intermediate its ends, subjecting a sealed end thereof to gaseous pressure, breaking the sealed end in the presence of said gaseous pressure, subjecting an external portion of said tube at a point remote from said sealed end to inert gaseous pressure substantially higher than the pressure inside the tube, and heating a portion of said tube to a plastic condition at a location intermediate said sealed end and said column of liquid in the presence of said inert gas to reseal said tube under gaseous pressure, and employing the weight of the free end of said tube and the pressure from said inert gas to effect necking in of said tube at the point of local heating thereof during the rescaling thereof.
3. In apparatus of the class described for pressurizing a column of liquid within a sealed tube, means for supporting said tube at a point intermediate its ends, means defining a chamber exposed to a source of gas under pressure into which a sealed end of said tube extends, means for breaking the sealed end of said tube within said chamber to expose said column of liquid to said pressure, means defining a second chamber intermediate the point of support of said tube and the opposite end thereof for subjecting the exterior of said sealed tube to an atmosphere of inert gas under pressure substantially higher than the internal pressure in the tube, and means surrounding said tube within said last named chamber for applying localized heat to said tube to produce localized plasticity thereof in the presence of said inert gas, whereby the external pressure on the tube forces the plastic glass in a direction to seal the bore of the tube.
4. In apparatus of the class described for pressurizing a column of liquid within a sealed tube, means for supporting said tube at a point intermediate its ends, means defining a chamber exposed to a source of gas under pressure into which a sealed end of said tube extends, means for breaking the sealed end of said tube within said chamber to expose said column of liquid to said pressure, means defining a second chamber intermediate the point of support of said tube and the opposite end thereof for subjecting the exterior of said sealed tube to an atmosphere of inert gas, said support means defining a seal between said chambers for preventing movement of gas from either of said chambers to the other and means surrounding said sealed tube within said last named chamber for heating an area of said tube to a plastic condition in the presence of said inert gas, whereby the external pressure forces the plastic glass inwardly to reseal the tube at a location above the said liquid column.
5. In apparatus of the class described for pressurizing a column of liquid within a sealed tube, means for supporting said tube at a point intermediate its ends, means defining a chamber exposed to a source of gas under pressure into which a sealed end of said tube extends, means for breaking the sealed end of said tube within said chamber to expose said column of liquid to said pressure, means defining a second chamber intermediate the point of support of said tube and the opposite end thereof for subjecting the exterior of said sealed tube to an atmosphere of inert gas, means surrounding said sealed tube to an atmosphere of inert gas, means surrounding said sealed tube within said last named chamber for heating a localized area of said tube to a plastic condition in the presence of said inert gas for resealing and severing said tube within the column therein subject to gaseous pressure, and a chamber interposed between both of said chambers for providing circulation of a coolant for localizing the heating of said tube.
6. In apparatus of the class described for pressurizing a column of liquid within a sealed tube, means for supporting said tube at a point intermediate its ends, means defining a chamber exposed to a source of gas under pressure into which a sealed end of said tube extends, means for breaking the sealed end of said tube within said chamber to expose said column of liquid to said pressure, means defining a second chamber intermediate the point of support of said tube and the opposite end thereof for subjecting the exterior of said sealed tube to an atmosphere of inert gas,
said support means defining a seal between said chambers for preventing movement of gas from either of said chambers to the other, means surrounding said sealed tube within said last named chamber for localized heating of said tube to a plastic condition in the presence of said inert gas for resealing said tube while the liquid column therein is subjected to gaseous pressure, and a chamber interposed between both of said chambers for providing circulation of a coolant.
7. An apparatus for pressurizing and rescaling a thermometer tube containing a liquid column therein, comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber enclosing the portion of the tube containing the liquid colunm and a portion contiguous thereto and intermediate the said liquid column and the sealed end of the tube, compressible means interposed between said chambers for sealing said connecting passages and for supporting said tube, means for delivering gas under pressure into said upper chamber, means for delivering gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube, and means located within the lower chamber for plasticizing a portion of said contiguous portion of said tube, whereby the gaseous pressure in said lower chamber compresses the plasticized portion of the tube to seal the same.
8. An apparatus for pressurizing and rescaling a glass thermometer tube containing a liquid column therein, comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and intermediate the said liquid column and the sealed end of the tubeycompressibl'e. means interposed. between said chambers. for sealing said connecting passages and for supporting said tube, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means forrupturing the sealed end of the tube, and means located'within the lower chamber for heating a portion of said contiguous portion of said tube to a plastic condition, whereby the gaseous pressure in said lower chamber compresses the plasticized portion of the tube to seal the same.
9. An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein, comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and intermediate the liquid column and the sealed end of the tube, compressible means interposed between said chambers for sealing said connecting passages and for supporting said tube, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube comprising a manually actuated spring pressed plunger extending into said chamber at one side thereof,
and means located within the lower chamber for heating a portion of said contiguous portion of said tube to a plastic condition, whereby the gaseous pressure in said lower chamber compresses the pressurized portion of the tube to seal the same.
10. An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein, comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermometer tube extending through said passages, the upper chamber enclosing a sealed end of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and intermediate the liquid column and the sealed endof the tube, compressible means interposed between said chambers for sealing said connecting pas-- sages and for supporting said tube, clamping means for maintaining the upper chamber in position and for exerting compressive force on said compressible means, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube comprising a manually actuated spring pressed plunger extending into said chamber at one side thereof, and means located within the lower chamber for heating a portion of said contiguous portion of said tube to a plastic condition, whereby the gaseous pressure in said lower chamber compresses the pressurized portion of the tube to seal the same.
11. An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid. column therein, comprising housing means defining upper and lower chambers having connect- 1'0 ing, passages and together enclosing a sealed thermometer tube extending through said passages, the upperchamber enclosing a sealed end of the tube and the lower chamber enclosing the portion of the tube containing the liquid column and a portion contiguous thereto and'intermediate the liquid column and the sealedend of the tube, compressible means interposed between said chambers for sealing said connecting passages and for supporting said tube, clamping means for maintaining the upper chamber in position and for exerting compressive force" on said: compressible means comprising a pivoted yoke movable into and out of position above the upper chamber housing and a screw carriedby the yoke for exerting downward pressure on the top portion of said upper chamber housing, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a higher pressure than that maintained in the upper chamber, means for rupturing the sealed end of the tube comprising a manually actuated spring pressed plunger extending into said chamber at one side thereof, and means located within the lower chamber for heating a portion of said contiguous portion of said tube to a plastic condition, whereby the gaseous pressure in said lower chamber compresses the pressurized portion of the tube to seal the same.
12. An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein, comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermostat tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber comprising separable housing sections which together enclose the portion of the tube containing the liquid column and a portion contiguous thereto intermediate said liquid column and the sealed end of the tube, means for clamping the separable housing sections together comprising a pivoted yoke and a thrust screw carried thereby for releasably clamping the separable sections oi the lower chamber housing together, means for delivering gas under pressure into said upper chamber, means for delivering an inert gas into said lower chamber at a pressure higher than that maintained in the upper chamber, manually operable means for rupturing the sealed end of the tube, and means located within the lower chamber for heating a portion of said contiguous portion of said tube to a plastic condition. whereby the gaseous pressure in said lower chamber compresses the plastic portion of the tube to seal the central bore therein.'
13. An apparatus for pressurizing and resealing a glass thermometer tube containing a liquid column therein, comprising housing means defining upper and lower chambers having connecting passages and together enclosing a sealed thermostat tube extending through said passages, the upper chamber enclosing a sealed end portion of the tube and the lower chamber comprising separable housing sections which together enclose the portion of the tube containing the liquid column and a portion contiguous thereto intermediate said liquid column and the sealed end of the tube, means for clamping the separable housing sections together, a swingable support for adjustably positioning the tube in position pre-- liminary to the application of the removable section of the lower chamber housing so that the 11 lower end of the tubeis supported in spaced relation to the bottom of said removable housing section, means for delivering gas under pressure into said upper chamber, means for delivering gas into said lower chamber at a pressure higher than thatmaintained in the upper chamber, means for rupturing the sealed end of said tube, an electrical heating means located within the lower chamber for heating a portion of said contiguous portion of the tube to a plastic condition, whereby downward movement of the lower portion of the tube, by action of gravity, stretches the plastic portion of the tube and the external gaseous pressure against said plastic portion causes a necking in of the tube to seal the central bore thereof.
WILLIAM M. SMITH.
DON A. BROSSEAU.
REFERENCES CITED The following references are of record in the file of this patent:
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2793480A (en) * 1955-11-29 1957-05-28 Owens Illinois Glass Co Method of and apparatus for producing thermometers
US3032941A (en) * 1959-08-07 1962-05-08 Texas Instruments Inc Differential sealing of glass components
US3055084A (en) * 1958-03-07 1962-09-25 Seci Method of making covered electrical resistors
US3254980A (en) * 1960-02-08 1966-06-07 Maricq Eugene-Paul Electrothermic machine for welding glass containers, chiefly pharmaceutic phials
US3355273A (en) * 1962-11-19 1967-11-28 Warner Lambert Pharmaceutical Method for making bubble free fiber optical image-transfer devices
US3490886A (en) * 1966-06-16 1970-01-20 Milton Stoll Method and apparatus for producing glass to metal seals using two sealing gas pressures
US3893837A (en) * 1972-12-22 1975-07-08 Pratiga S R L Equipment for welding glass capillary tubes for biological analyses

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR507307A (en) * 1919-03-04 1920-09-10 Andre Jousset Apparatus for charging with pressurized gas and soldering ampoules for hypodermic injections and others
US2215100A (en) * 1937-05-22 1940-09-17 Westinghouse Electric & Mfg Co Method and machine for sealing vitreous vessels
US2278500A (en) * 1941-01-31 1942-04-07 Rca Corp Vacuum tube seal-off
US2361413A (en) * 1940-06-28 1944-10-31 Font Juan Luis Pujoly Method and apparatus for making ampoules containing compressed gas
US2381764A (en) * 1943-05-18 1945-08-07 Gen Electric Apparatus for charging and sealing tubular containers

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR507307A (en) * 1919-03-04 1920-09-10 Andre Jousset Apparatus for charging with pressurized gas and soldering ampoules for hypodermic injections and others
US2215100A (en) * 1937-05-22 1940-09-17 Westinghouse Electric & Mfg Co Method and machine for sealing vitreous vessels
US2361413A (en) * 1940-06-28 1944-10-31 Font Juan Luis Pujoly Method and apparatus for making ampoules containing compressed gas
US2278500A (en) * 1941-01-31 1942-04-07 Rca Corp Vacuum tube seal-off
US2381764A (en) * 1943-05-18 1945-08-07 Gen Electric Apparatus for charging and sealing tubular containers

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2793480A (en) * 1955-11-29 1957-05-28 Owens Illinois Glass Co Method of and apparatus for producing thermometers
US3055084A (en) * 1958-03-07 1962-09-25 Seci Method of making covered electrical resistors
US3032941A (en) * 1959-08-07 1962-05-08 Texas Instruments Inc Differential sealing of glass components
US3254980A (en) * 1960-02-08 1966-06-07 Maricq Eugene-Paul Electrothermic machine for welding glass containers, chiefly pharmaceutic phials
US3355273A (en) * 1962-11-19 1967-11-28 Warner Lambert Pharmaceutical Method for making bubble free fiber optical image-transfer devices
US3490886A (en) * 1966-06-16 1970-01-20 Milton Stoll Method and apparatus for producing glass to metal seals using two sealing gas pressures
US3893837A (en) * 1972-12-22 1975-07-08 Pratiga S R L Equipment for welding glass capillary tubes for biological analyses

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