US2492357A - Manufacture of quartz crystal assemblies - Google Patents

Manufacture of quartz crystal assemblies Download PDF

Info

Publication number
US2492357A
US2492357A US620819A US62081945A US2492357A US 2492357 A US2492357 A US 2492357A US 620819 A US620819 A US 620819A US 62081945 A US62081945 A US 62081945A US 2492357 A US2492357 A US 2492357A
Authority
US
United States
Prior art keywords
crystal
solder
manufacture
vessel
quartz crystal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US620819A
Inventor
Chatterjea Prafulla Kumar
Powers Stephen John
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
International Standard Electric Corp
Original Assignee
International Standard Electric Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by International Standard Electric Corp filed Critical International Standard Electric Corp
Application granted granted Critical
Publication of US2492357A publication Critical patent/US2492357A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • HELECTRICITY
    • H03ELECTRONIC CIRCUITRY
    • H03HIMPEDANCE NETWORKS, e.g. RESONANT CIRCUITS; RESONATORS
    • H03H9/00Networks comprising electromechanical or electro-acoustic elements; Electromechanical resonators
    • H03H9/02Details
    • H03H9/05Holders or supports
    • H03H9/10Mounting in enclosures
    • H03H9/1007Mounting in enclosures for bulk acoustic wave [BAW] devices
    • H03H9/1014Mounting in enclosures for bulk acoustic wave [BAW] devices the enclosure being defined by a frame built on a substrate and a cap, the frame having no mechanical contact with the BAW device
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/42Piezoelectric device making
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/4998Combined manufacture including applying or shaping of fluent material
    • Y10T29/49993Filling of opening

Definitions

  • This invention relates to the mounting of piezo-electric crystals such as quartz crystals used in telecommunication engineering.
  • crystals such as those used for controlling the frequency of a radio-frequency oscillation generator should be well shielded against the effects of varying atmospheric condition as well as bein protected against foreign bodies such as dust particles; and it is accordingly known to mount the crystal in a vacuum chamber.
  • the object of the present invention is to improve the process of mounting a crystal in a vacuum chamber so as to result in an assembly that is inexpensive, robust and accurate.
  • a crystal is mounted within a vessel having an aperture in its top wall which is sealed after evacuation of the vessel within a vacuum chamber.
  • an aperture in a top wall of a vessel containing a crystal is sealed after evacuation of the vessel within a vacuum chamber by solder melted by contact with an electric heating element within the chamber.
  • Fig. 1 shows a crystal mounted within a vessel during the evacuation process whilst Fig. 2 is a top view of the vessel containing the crystal.
  • the crystal l is mounted in any convenient manner upon a copper disc 2. and is then enclosed by an envelope 3 which may be of metal or may be of glass coated with metal. Electrical connections to the crystal I are provided by leads 4 passing through insulating and vacuum seals in the copper disc 2, such as glass beads. With the crystal I mounted in place upon the disc 2 and its electrical connections completed, the envelope 3 is fitted over and is sealed at its rim to the disc 2 as by soldering, thus providing a vacuum-tight joint.
  • the envelope 3 is preformed with a depression or recess 5 in its top wall, and with one or more small holes 6 in the recess.
  • the recess 5 is in the shape of a triangle preferably equilateral, as shown, and there are three holes 6 one at each apex of the triangle.
  • a ball of solder 1 is Placed a ball of solder 1, large enough to project above the top of the envelope 3 to the extent of about half its diameter.
  • the assembly is then put into a bell jar I, conveniently being stood upon a support 9 consisting of a cylinder of porcelain or any other convenient material.
  • connection to from the bell jar 8 to the exhaust pump is taken through an opening in the centre of the floor of the chamber, as shown, so that the porcelain (or other material) cylinder 9 surrounds this opening it, then the cylinder 9 must be perforated, as shown, to permit free flow of air.
  • a heating element is brought into position in proximity to the ball of solder.
  • This heating element consists of a strip of molybdenum ll carried between two copper terminal posts I! and bowed downwardly so as to contact the ball of solder I with a fair degree of pressure.
  • the heating strip it should not be in contact with the solder 1 when the strip is cold: in that case it may be arranged either by the use of a bimetallic strip or otherwise, that the heating strip II is out of contact with the solder I when cold and only makes contact when heated.
  • the copper disc 2 through which the leads 4 pass may be made in the form of a valve base with, any three, five, or seven pins to facilitate mounting the crystal in the equipment.
  • a wire can be left in the container 3 to help in checking the vacuum now and again during life, i. e. as a Pirani gauge, this wire being connected to two of the terminal pins in the base.
  • the container 3 can be made to have two spaced walls with a heating coil in between so that the temperature of the crystal may be kept constant.
  • a process of mounting a piezoelectric crystal which comprises mounting said crystal within a vessel having an aperture in a recess in the top wall thereof, sealing said vessel with the exception of said aperture, placing a piece of solder in said recess adjacent said aperture, placing said vessel within a vacuum chamber provided with an electric heating element within said chamber in position adjacent said solder, exhausting said chamber to the required degree, and locally heating said solder by connecting an electric current source to said heating element, thus melting the solder and sealing said aperture.
  • a process as claimed in claim 1 in which the step of placing the vessel within the vacuum chamber comprises pressing the piece of solder against a bowed strip of high resistance material heated by the passage 0! current therethrough.
  • step of placing the vessel within the vacuum chamber comprises placing the solder adjacent and spaced from a bimetallic strip, of high resistance materials heated by the passage of current therethrough, the heating of the bimetallic strip causin sa d strip to bend into contact with 15 Number said solder.

Landscapes

  • Physics & Mathematics (AREA)
  • Acoustics & Sound (AREA)
  • Piezo-Electric Or Mechanical Vibrators, Or Delay Or Filter Circuits (AREA)
  • Piezo-Electric Transducers For Audible Bands (AREA)

Description

1949 P. K. CHATTERJEA ET AL 2,492,357
MANUFACTURE OF QUARTZ CRYSTAL ASSEMBLIES Filed Oct. 6, 1945 Inventor Am my Patented Dec. 27, 1949 MANUFACTURE OF QUARTZ CRYSTAL ASSEMBLIES Praiulla Kumar Chatterjea and Stephen John Powers, London, England, assignors, by mesne assignments, to International Standard Electric Corporation, New York, N. Y., a corporation of Delaware Application October 6, 1945, Serial No. 620,819 In Great Britain September 1, 1944 Section 1, Public Law 690, August 8, 1946 Patent expires September 1, 1964 4 Claims. 3
This invention relates to the mounting of piezo-electric crystals such as quartz crystals used in telecommunication engineering.
It is known that crystals such as those used for controlling the frequency of a radio-frequency oscillation generator should be well shielded against the effects of varying atmospheric condition as well as bein protected against foreign bodies such as dust particles; and it is accordingly known to mount the crystal in a vacuum chamber.
The object of the present invention is to improve the process of mounting a crystal in a vacuum chamber so as to result in an assembly that is inexpensive, robust and accurate.
In accordance with one feature of the invention a crystal is mounted within a vessel having an aperture in its top wall which is sealed after evacuation of the vessel within a vacuum chamber.
In accordance with another feature of the invention an aperture in a top wall of a vessel containing a crystal is sealed after evacuation of the vessel within a vacuum chamber by solder melted by contact with an electric heating element within the chamber.
An embodiment of the invention will be described with reference to the accompanying drawings in which Fig. 1 shows a crystal mounted within a vessel during the evacuation process whilst Fig. 2 is a top view of the vessel containing the crystal.
Referring to the drawings the crystal l is mounted in any convenient manner upon a copper disc 2. and is then enclosed by an envelope 3 which may be of metal or may be of glass coated with metal. Electrical connections to the crystal I are provided by leads 4 passing through insulating and vacuum seals in the copper disc 2, such as glass beads. With the crystal I mounted in place upon the disc 2 and its electrical connections completed, the envelope 3 is fitted over and is sealed at its rim to the disc 2 as by soldering, thus providing a vacuum-tight joint.
The next question is that of evacuating the envelope 3 and finally sealing. To this the envelope 3 is preformed with a depression or recess 5 in its top wall, and with one or more small holes 6 in the recess. Conveniently the recess 5 is in the shape of a triangle preferably equilateral, as shown, and there are three holes 6 one at each apex of the triangle. In this recess 5 is Placed a ball of solder 1, large enough to project above the top of the envelope 3 to the extent of about half its diameter. The assembly is then put into a bell jar I, conveniently being stood upon a support 9 consisting of a cylinder of porcelain or any other convenient material. If the connection to from the bell jar 8 to the exhaust pump is taken through an opening in the centre of the floor of the chamber, as shown, so that the porcelain (or other material) cylinder 9 surrounds this opening it, then the cylinder 9 must be perforated, as shown, to permit free flow of air. With the assembly in place in the bell jar I, a heating element is brought into position in proximity to the ball of solder. This heating element consists of a strip of molybdenum ll carried between two copper terminal posts I! and bowed downwardly so as to contact the ball of solder I with a fair degree of pressure. The procedure then is, of course, simply to operate the exhaust pump until the bell Jar 8 is sumciently evacuated, and finally to pass a heating current through the molybdenum strip l l via terminal posts I! so that the solder 'l melts and fills up the recess 5 including the small holes 6 therein.
It may be desirable that the heating strip it should not be in contact with the solder 1 when the strip is cold: in that case it may be arranged either by the use of a bimetallic strip or otherwise, that the heating strip II is out of contact with the solder I when cold and only makes contact when heated.
The copper disc 2 through which the leads 4 pass may be made in the form of a valve base with, any three, five, or seven pins to facilitate mounting the crystal in the equipment.
A wire can be left in the container 3 to help in checking the vacuum now and again during life, i. e. as a Pirani gauge, this wire being connected to two of the terminal pins in the base.
The container 3 can be made to have two spaced walls with a heating coil in between so that the temperature of the crystal may be kept constant.
-What is claimed is:
1. A process of mounting a piezoelectric crystal which comprises mounting said crystal within a vessel having an aperture in a recess in the top wall thereof, sealing said vessel with the exception of said aperture, placing a piece of solder in said recess adjacent said aperture, placing said vessel within a vacuum chamber provided with an electric heating element within said chamber in position adjacent said solder, exhausting said chamber to the required degree, and locally heating said solder by connecting an electric current source to said heating element, thus melting the solder and sealing said aperture.
2. A process as claimed in claim 1 in which said electric heating element is a strip or high resistance material heated by the passage of current therethrough. v
3. A process as claimed in claim 1 in which the step of placing the vessel within the vacuum chamber comprises pressing the piece of solder against a bowed strip of high resistance material heated by the passage 0! current therethrough.
4. A process as claimed in claim 1 in which the step of placing the vessel within the vacuum chamber comprises placing the solder adjacent and spaced from a bimetallic strip, of high resistance materials heated by the passage of current therethrough, the heating of the bimetallic strip causin sa d strip to bend into contact with 15 Number said solder.
PRAFULLA KUMAR. CHA'I'I'ERJEA. STEPHEN JOHN POWERS.
REFERENCES CITED fThe iollowing references are of record in the file of this patent:
UNITED STATES PATENTS Number Name Date 1,820,553 Bethold et a1 Aug. 25, 1931 1,836,735 Tillyer Dec. 15, 1931 2,203,545 Peterson June 4, 1940 2,229,436 Beggs Jan. 21, 1941 2,260,707 Fair Oct. 28, 1941 FOREIGN PATENTS Country Date 154,262 Australia Sept. 10, 1938
US620819A 1944-09-01 1945-10-06 Manufacture of quartz crystal assemblies Expired - Lifetime US2492357A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB16726/44A GB581307A (en) 1944-09-01 1944-09-01 Improvements in or relating to the manufacture of piezo-electric crystal assemblies

Publications (1)

Publication Number Publication Date
US2492357A true US2492357A (en) 1949-12-27

Family

ID=10082543

Family Applications (1)

Application Number Title Priority Date Filing Date
US620819A Expired - Lifetime US2492357A (en) 1944-09-01 1945-10-06 Manufacture of quartz crystal assemblies

Country Status (3)

Country Link
US (1) US2492357A (en)
FR (1) FR931029A (en)
GB (1) GB581307A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2656473A (en) * 1950-05-24 1953-10-20 Bell Telephone Labor Inc Crystal unit for use at high temperatures
US2833942A (en) * 1953-02-05 1958-05-06 Leonard E Ravich Contaminant-proof electrical circuit components
US3017525A (en) * 1956-11-26 1962-01-16 John M Wolfskill Mounting support for piezoelectric crystal units
US3132239A (en) * 1962-04-25 1964-05-05 United Aircraft Corp Electron beam compression welding

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1820553A (en) * 1927-09-16 1931-08-25 Siemens Ag Device for cutting off vacuum vessels from the exhaust tubes of vacuum pumps
US1836735A (en) * 1924-07-16 1931-12-15 American Optical Corp Crystal oscillator
US2203545A (en) * 1938-06-18 1940-06-04 Gen Electric Piezoelectric device
US2229436A (en) * 1940-09-21 1941-01-21 Gen Electric Method of making metal-enclosed vacuum tubes
US2260707A (en) * 1939-06-20 1941-10-28 Bell Telephone Labor Inc Crystal controlled oscillator for ultra-high frequencies

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1836735A (en) * 1924-07-16 1931-12-15 American Optical Corp Crystal oscillator
US1820553A (en) * 1927-09-16 1931-08-25 Siemens Ag Device for cutting off vacuum vessels from the exhaust tubes of vacuum pumps
US2203545A (en) * 1938-06-18 1940-06-04 Gen Electric Piezoelectric device
US2260707A (en) * 1939-06-20 1941-10-28 Bell Telephone Labor Inc Crystal controlled oscillator for ultra-high frequencies
US2229436A (en) * 1940-09-21 1941-01-21 Gen Electric Method of making metal-enclosed vacuum tubes

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2656473A (en) * 1950-05-24 1953-10-20 Bell Telephone Labor Inc Crystal unit for use at high temperatures
US2833942A (en) * 1953-02-05 1958-05-06 Leonard E Ravich Contaminant-proof electrical circuit components
US3017525A (en) * 1956-11-26 1962-01-16 John M Wolfskill Mounting support for piezoelectric crystal units
US3132239A (en) * 1962-04-25 1964-05-05 United Aircraft Corp Electron beam compression welding

Also Published As

Publication number Publication date
GB581307A (en) 1946-10-08
FR931029A (en) 1948-02-11

Similar Documents

Publication Publication Date Title
US2125316A (en) Method of forming glass to metal seals
US2416565A (en) High-frequency electronic device
US2984759A (en) Photoconductive pick-up tube and method of manufacture
US2428610A (en) Method and apparatus for manufacturing electric discharge devices
US2792271A (en) Method of making electric discharge device
US2492357A (en) Manufacture of quartz crystal assemblies
US2877338A (en) Method of adjusting the operating frequency of sealed piezoelectric crystals
US1628982A (en) Electron-discharge device
US2191992A (en) Telephone transmitter
US2561520A (en) Vacuumtight seal for electrical apparatus and method of forming such seals
US2664180A (en) Quartz-to-metal seal
US2527587A (en) Electron discharge device
US2595037A (en) Piezoelectric crystal apparatus
US2859372A (en) Electron tube
US3947713A (en) Mercury capsule assembly for display panel
US2171226A (en) Electron discharge device
US2499197A (en) Metal envelope electric discharge device
US2522062A (en) Vacuum tube seal
US3007760A (en) Method of making electron tubes
US3408522A (en) Cup-shaped photoconductor tube
US2141387A (en) Electron discharge device
US2444158A (en) Thermionic device and getter elements therefor
US2078776A (en) Glass-to-metal seal
US2406827A (en) Electron discharge device
US2250183A (en) Electron discharge tube and method of manufacture