US2483710A - Apparatus for bleaching fatty substances - Google Patents

Apparatus for bleaching fatty substances Download PDF

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US2483710A
US2483710A US549921A US54992144A US2483710A US 2483710 A US2483710 A US 2483710A US 549921 A US549921 A US 549921A US 54992144 A US54992144 A US 54992144A US 2483710 A US2483710 A US 2483710A
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bleaching
mixture
stream
temperature
oleaginous material
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US549921A
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Adrian A Robinson
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Standard Brands Inc
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Standard Brands Inc
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption

Definitions

  • the object of my invention is to provide improved means by which oils or fats in a continuous stream may be effectively bleached at low cost.
  • oleaginous material is used throughout the present specification ⁇ and claims as a generic term including both oils and fats.
  • Ill indicates a supply reservoir for the liquid material to be bleached, and II a pump capable of delivering a continuous stream therefrom to and through a mixer I2.
  • a pump I3 supplied from a mixing tank I4 equipped with a mechanical agitator I5.
  • Tank I4 contains a supply of bleaching materia', such as fullers earth, preferably as a slurry, with a convenient amount of the liquid to be bleached.
  • the eluent from mixer I2 is delivered as a spray from a nozzle I6 in a vacuum chamber Il, the spray forming a thin stream on baffles I8 and passing into a sump I9 whence it is discharged by pump 20.
  • a relatively high vacuum is maintained in chamber I1 by well known means, not shown, so that occluded air in the mixture under treatment is extracted in order that the result of the bleaching action may be more stable.
  • the material to be treated is at a relatively low temperature but sufiiciently high to render it adequately uid, and little, if any, bleaching action occurs prior to arrival beyond pump 20.
  • heating chamber passes into one end of a tube 21 jacketed by heat insulation 28 and provided with inwardly projecting pins 29 with which are interdigitated beaters 30 carried by rotary shaft 3I.
  • any desired relation between heating time and bleaching time may be definitely established.
  • the effluent from tube 21 passes to filters 32, 32 which, by alternateuse in conjunction with valves 33, 33', will permit continuity of bleaching for an indefinite period.
  • Thepumps II, I3 and 20 may be driven by any wellknovvn means preferably including speedvarying means so that rates of oW and local pressures may be established as desired.
  • tube 22 is 46 long, 4 in diameter, shaft 23 diameter 31/2", tube 2'I length 46", diameter 15", and shaft 3I diameter 2", there will be provided .a heating period of approximately 2.5 seconds and a bleaching period of 1.57 minutes at anormal pressure established by pump 20.
  • Apparatus for accomplishing bleaching of a flowable oleaginous material comprising a source of supply of such material, a source of supply of a bleaching agent, and converging conduit means for establishing a flowing stream composed of a mixtureof such material with such bleaching agent, means for subjecting a section of said stream to subatmospheric pressure substantially at atmospheric temperature, whereby occluded and means for subjecting a section of the stream beyond said first-named section of said air-freed mixture to heat sucient to result in bleaching of the oleaginous material.
  • a -means to define a restricted section of said mixture stream means in advance of said restricting means for raising the pressure upon said stream, means for heating said restricted stream section to bleaching temperature within a few seconds, and subsequent means for defining a less restricted section of said stream and maintaining it at bleaching temperature.
  • Apparatus for accomplishing bleaching of a iiowable oleaginous material comprising means for establishing a flowing stream composed of a mixture of such material with a comminuted bleaching agent, means for subjecting a section of such stream to sub-atmospheric pressure, means for increasing the pressure upon a second section of said stream beyond said first section, and means for heating a third section of said stream beyond said second section to a temperature sufiicient to bleach the oleaginous material.
  • Apparatus for accomplishing bleaching -of af flowable oleaginous material comprising means providing a passage, means for mixing such material with a bleaching agent. means for causing the mixture to flow in a continuous stream through said passage, means for subjecting successive portions of said stream to sub-atmospheric pressure at substantially atmospheric temperature, whereby occluded air therein will be extracted therefrom, subsequent means for returning the pressure upon said stream at least to atmospheric value, means beyond said last-named 'means to define a restricted section of said mixture stream, means for heating said restricted stream section to bleaching temperature within a few seconds, subsequent means for defining a less restricted section of said stream and maintaining it at bleaching temperature, and means within said last-mentioned means for mechanically mixing the mixture stream therein.
  • Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means providing a passage, means for causing a stream of definitely proportioned successive quantities of oleaginous material and a bleaching agent to ilow through said passage, means for subsequently extracting occluded air from the mixture substantially at atmospheric temperature, means acting on such mixture after such extraction for raising the temperature of successive portions, within a period of a few seconds, of said mixture to bleaching temperature, and means for subsequently maintaining successive portions of said mixture at bleaching temperature until desired bleaching has been attained.
  • Apparatus for accomplishing bleaching of a owable oleaginous material comprising means providing a passage, means for establishing through said passage a flowing stream of definitely proportioned successive quantities of oleaginous material and a slurry of such oleaginous material and a bleaching agent, means for subsequently extracting occluded air from the mixture substantially at atmospheric temperature, means acting on such mixture after such extraction for raising the temperature of successive portions,
  • Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means for establishing a continuously flowing stream of definitely proportioned successive quantities of ⁇ oleaginous material and a bleaching agent, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restricting the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, and a bleaching chamber arranged to receive the effluent from said cylinder and having a capacity sufiicient to cause a decreased velocity of fiow therethrough affording adequate bleaching time.
  • Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means for establishing a flowing 'stream of definitely proportioned successive quantities of oleaginous material and a bleaching agent, means for subsequently extracting occluded airfrom the mixture, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinderl and restricting the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, a bleaching chamber arranged to receive the effluent from said cylinder and having a capacity sufiicient to cause a decreased velocity of flow therethrough affording adequate bleaching time, agitating means within said bleaching chamber, and means for driving said beater and said agitating means.
  • Apparatus for accomplishing bleaching of a flowable oleaginous material comprising means for establishing a flowing stream of definitely proportioned successive quantities of oleaginous material and a slurry of such oleaginous material, and a bleaching agent, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restricting the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperatures, a bleaching chamber arranged to receive the efiuent from said cylinder and having a capacity sufficient to cause a decreased velocity of now therethrough affording adequate bleaching time, and agitating means within said bleaching chamber.
  • Apparatus for accomplishing bleaching of a iiowable oleaginous material comprising means for establishing a flowing stream of definitely .i proportioned successive quantities of oleaginous material and a slurry of such oleaginous material and a bleaching agent, means for subsequently extracting occluded air from the mixture, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restricting the effective volume thereof to an annulus of relatively small radial extent, means for driving said beaten, means associated with said cylinder for.
  • a bleaching chamber arranged to receive the effluent from said cylinder and having a capacity sufiicient to cause a decreased velocity of flow therethrough affording adequate bleaching time.
  • Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means for establishing a fiowing stream of definitely proportioned successive quantities of oleaginous material and a slurry of such oleaginous material and a bleaching agent, means for subsequently extracting occluded air from the mixture, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restrict ⁇ ing the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, a bleaching chamber arranged to receive the eiilu- Number ent from said cylinder and having a capacity sufficient to cause a decreased Velocityof ow therethrough affording adequate bleaching time, agitating means within said bleaching chamber, and means for driving said beater and said agitating means.

Description

4, N4." A. A. ROBANSON 2,483,71
PPRTUS FOR BLEACHING FTTY SUBSTNCES Filed Aug. 17, 1944 i A INVENTOR. inw/,w /Z ,QM/N5 a@ Patented oct. 4, 1949 APPARATUS FOR BLEACHING FATTY SUBSTAN CES Adrian A. Robinson, Indianapolis, Ind., assigner,
by mesne assignments, to Standard Brands Inoorporated, New York, N. Y., a corporation of Delaware Applicationaugust 17, 1944, serial No. 549,921
11 Claims.
The object of my invention is to provide improved means by which oils or fats in a continuous stream may be effectively bleached at low cost. The term oleaginous material is used throughout the present specification `and claims as a generic term including both oils and fats.
The accompanying drawing illustrates, diagrammatically, an embodiment of my invention.
In the drawing Ill indicates a supply reservoir for the liquid material to be bleached, and II a pump capable of delivering a continuous stream therefrom to and through a mixer I2. Also delivering to mixer I2 is a pump I3 supplied from a mixing tank I4 equipped with a mechanical agitator I5. Tank I4 contains a supply of bleaching materia', such as fullers earth, preferably as a slurry, with a convenient amount of the liquid to be bleached. The eluent from mixer I2 is delivered as a spray from a nozzle I6 in a vacuum chamber Il, the spray forming a thin stream on baffles I8 and passing into a sump I9 whence it is discharged by pump 20. A relatively high vacuum is maintained in chamber I1 by well known means, not shown, so that occluded air in the mixture under treatment is extracted in order that the result of the bleaching action may be more stable.
Up to this point, the material to be treated is at a relatively low temperature but sufiiciently high to render it adequately uid, and little, if any, bleaching action occurs prior to arrival beyond pump 20.
It is well known that bleaching occurs best at a temperature in the neighborhood of 240 F. and within a relatively short time. I believe it to be advantageous that each particle of oleaginous material and its accompanying particle of bleacher be brought to bleaching temperature as promptly as possible and that that temperature be maintained only long enough for the bleaching action to be accomplished. To this end, the eflluent from pump 20 is to be delivered to one end of a relatively thin annular heating chamber 2l formed between tube 22, and a rotary beater shaft '23 provided on its periphery with beaters 24 which will scrape tube 22. Tube 22 is jacketed by heating means 25 which, in turn, is jacketed by heat insulation 26, the arrangement being such that the mixture under treatment is brought to proper temperature Within a short period of 1 to 10 seconds.
Under proper conditions of uniform heating and thorough mixture of oleaginous material and bleacher, bleaching will be accomplished within a few minutes and therefore the eflluent from the air therein will be extracted therefrom,
2 heating chamber passes into one end of a tube 21 jacketed by heat insulation 28 and provided with inwardly projecting pins 29 with which are interdigitated beaters 30 carried by rotary shaft 3I.
By properly proportioning the effective capacities of the heating chamber and the mixer 2li-29, any desired relation between heating time and bleaching time may be definitely established.
The effluent from tube 21 passes to filters 32, 32 which, by alternateuse in conjunction with valves 33, 33', will permit continuity of bleaching for an indefinite period.
Thepumps II, I3 and 20 may be driven by any wellknovvn means preferably including speedvarying means so that rates of oW and local pressures may be established as desired.
Merely as illustrative, it may be noted that if tube 22 is 46 long, 4 in diameter, shaft 23 diameter 31/2", tube 2'I length 46", diameter 15", and shaft 3I diameter 2", there will be provided .a heating period of approximately 2.5 seconds and a bleaching period of 1.57 minutes at anormal pressure established by pump 20.
I claim as my invention:
l. Apparatus for accomplishing bleaching of a flowable oleaginous material comprising a source of supply of such material, a source of supply of a bleaching agent, and converging conduit means for establishing a flowing stream composed of a mixtureof such material with such bleaching agent, means for subjecting a section of said stream to subatmospheric pressure substantially at atmospheric temperature, whereby occluded and means for subjecting a section of the stream beyond said first-named section of said air-freed mixture to heat sucient to result in bleaching of the oleaginous material.
2. 'Apparatus for accomplishing bleaching of a lowable oleaginous material comprising means for mixing such material with a bleaching agent and for causing such mixture to flow in a continuous stream, means for subjecting a section of said stream to subatmospheric pressure substantially at atmospheric temperature, whereby occluded air therein will be extracted therefrom,
A -means to define a restricted section of said mixture stream, means in advance of said restricting means for raising the pressure upon said stream, means for heating said restricted stream section to bleaching temperature within a few seconds, and subsequent means for defining a less restricted section of said stream and maintaining it at bleaching temperature.
3. Apparatus for accomplishing bleaching of a iiowable oleaginous material, comprising means for establishing a flowing stream composed of a mixture of such material with a comminuted bleaching agent, means for subjecting a section of such stream to sub-atmospheric pressure, means for increasing the pressure upon a second section of said stream beyond said first section, and means for heating a third section of said stream beyond said second section to a temperature sufiicient to bleach the oleaginous material.
4. Apparatus for accomplishing bleaching -of af flowable oleaginous material comprising means providing a passage, means for mixing such material with a bleaching agent. means for causing the mixture to flow in a continuous stream through said passage, means for subjecting successive portions of said stream to sub-atmospheric pressure at substantially atmospheric temperature, whereby occluded air therein will be extracted therefrom, subsequent means for returning the pressure upon said stream at least to atmospheric value, means beyond said last-named 'means to define a restricted section of said mixture stream, means for heating said restricted stream section to bleaching temperature within a few seconds, subsequent means for defining a less restricted section of said stream and maintaining it at bleaching temperature, and means within said last-mentioned means for mechanically mixing the mixture stream therein.
5. Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means providing a passage, means for causing a stream of definitely proportioned successive quantities of oleaginous material and a bleaching agent to ilow through said passage, means for subsequently extracting occluded air from the mixture substantially at atmospheric temperature, means acting on such mixture after such extraction for raising the temperature of successive portions, within a period of a few seconds, of said mixture to bleaching temperature, and means for subsequently maintaining successive portions of said mixture at bleaching temperature until desired bleaching has been attained. V
6. Apparatus for accomplishing bleaching of a owable oleaginous material comprising means providing a passage, means for establishing through said passage a flowing stream of definitely proportioned successive quantities of oleaginous material and a slurry of such oleaginous material and a bleaching agent, means for subsequently extracting occluded air from the mixture substantially at atmospheric temperature, means acting on such mixture after such extraction for raising the temperature of successive portions,
within a period of a few seconds, of said mixture to bleaching temperature, and means for subsequently maintaining successive portions of said mixture at bleaching temperature until desired bleaching has been attained.
7. Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means for establishing a continuously flowing stream of definitely proportioned successive quantities of` oleaginous material and a bleaching agent, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restricting the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, and a bleaching chamber arranged to receive the effluent from said cylinder and having a capacity sufiicient to cause a decreased velocity of fiow therethrough affording adequate bleaching time.
8. Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means for establishing a flowing 'stream of definitely proportioned successive quantities of oleaginous material and a bleaching agent, means for subsequently extracting occluded airfrom the mixture, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinderl and restricting the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, a bleaching chamber arranged to receive the effluent from said cylinder and having a capacity sufiicient to cause a decreased velocity of flow therethrough affording adequate bleaching time, agitating means within said bleaching chamber, and means for driving said beater and said agitating means.
9. Apparatus for accomplishing bleaching of a flowable oleaginous material comprising means for establishing a flowing stream of definitely proportioned successive quantities of oleaginous material and a slurry of such oleaginous material, and a bleaching agent, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restricting the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperatures, a bleaching chamber arranged to receive the efiuent from said cylinder and having a capacity sufficient to cause a decreased velocity of now therethrough affording adequate bleaching time, and agitating means within said bleaching chamber.
10. Apparatus for accomplishing bleaching of a iiowable oleaginous material comprising means for establishing a flowing stream of definitely .i proportioned successive quantities of oleaginous material and a slurry of such oleaginous material and a bleaching agent, means for subsequently extracting occluded air from the mixture, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restricting the effective volume thereof to an annulus of relatively small radial extent, means for driving said beaten, means associated with said cylinder for. rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, and a bleaching chamber arranged to receive the effluent from said cylinder and having a capacity sufiicient to cause a decreased velocity of flow therethrough affording adequate bleaching time.
1l. Apparatus for accomplishing bleaching of a fiowable oleaginous material comprising means for establishing a fiowing stream of definitely proportioned successive quantities of oleaginous material and a slurry of such oleaginous material and a bleaching agent, means for subsequently extracting occluded air from the mixture, a cylinder receiving said mixture, a rotary beater extending lengthwise in said cylinder and restrict` ing the effective volume thereof to an annulus of relatively small radial extent, means associated with said cylinder for rapidly raising the temperature of successive portions of mixture flowing through said annulus to bleaching temperature, a bleaching chamber arranged to receive the eiilu- Number ent from said cylinder and having a capacity sufficient to cause a decreased Velocityof ow therethrough affording adequate bleaching time, agitating means within said bleaching chamber, and means for driving said beater and said agitating means.
ADRIAN A. ROBINSON.
REFERENCES CITED The following references are of record in the 111e of this patent:
UNITED STATES vPATENTS Name Date 1,067,513 Feldmeier et a1 July 15, 1913 1,818,452 Bayiis Aug. 11, 1931 Number `15 Number
US549921A 1944-08-17 1944-08-17 Apparatus for bleaching fatty substances Expired - Lifetime US2483710A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2768747A (en) * 1951-07-21 1956-10-30 Pintsch Bamag Ag Apparatus for bleaching fatty materials

Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1067513A (en) * 1913-07-15 Burrell D H & Co Apparatus for pasteurizing milk.
US1818452A (en) * 1926-01-18 1931-08-11 Filtrol Company Of California Process of purifying vegetable oil
AU1079633A (en) * 1933-11-29 1933-12-07 The Merrill Company Amendment
US1987175A (en) * 1932-07-26 1935-01-08 Victor C Benjamin Apparatus for clay-treating oils
US2047157A (en) * 1928-08-14 1936-07-07 Rodman Process for purifying oils
US2090586A (en) * 1937-08-17 Apparatus fob bodying tung oil
US2116344A (en) * 1935-03-30 1938-05-03 Buckeye Lab Inc Purification of oil
US2150733A (en) * 1937-07-02 1939-03-14 Refining Inc Process for refining glyceridetype oils
US2210906A (en) * 1938-01-03 1940-08-13 Harry F Langlois Oil reclaiming apparatus
US2216104A (en) * 1939-01-06 1940-10-01 Refining Inc Method for purifying refined oils
US2248177A (en) * 1936-05-11 1941-07-08 Karlstrom Adolf Magnus Rupert Apparatus for purifying water
US2254390A (en) * 1939-07-08 1941-09-02 Charles A Olcott Temperature conditioning of sugar bearing material
US2268567A (en) * 1932-08-30 1942-01-06 Refining Inc Process of refining oils containing free fatty acids
US2360811A (en) * 1941-09-18 1944-10-17 Dorr Co Inc Purification of liquids

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2090586A (en) * 1937-08-17 Apparatus fob bodying tung oil
US1067513A (en) * 1913-07-15 Burrell D H & Co Apparatus for pasteurizing milk.
US1818452A (en) * 1926-01-18 1931-08-11 Filtrol Company Of California Process of purifying vegetable oil
US2047157A (en) * 1928-08-14 1936-07-07 Rodman Process for purifying oils
US1987175A (en) * 1932-07-26 1935-01-08 Victor C Benjamin Apparatus for clay-treating oils
US2268567A (en) * 1932-08-30 1942-01-06 Refining Inc Process of refining oils containing free fatty acids
AU1079633A (en) * 1933-11-29 1933-12-07 The Merrill Company Amendment
US2116344A (en) * 1935-03-30 1938-05-03 Buckeye Lab Inc Purification of oil
US2248177A (en) * 1936-05-11 1941-07-08 Karlstrom Adolf Magnus Rupert Apparatus for purifying water
US2150733A (en) * 1937-07-02 1939-03-14 Refining Inc Process for refining glyceridetype oils
US2210906A (en) * 1938-01-03 1940-08-13 Harry F Langlois Oil reclaiming apparatus
US2216104A (en) * 1939-01-06 1940-10-01 Refining Inc Method for purifying refined oils
US2254390A (en) * 1939-07-08 1941-09-02 Charles A Olcott Temperature conditioning of sugar bearing material
US2360811A (en) * 1941-09-18 1944-10-17 Dorr Co Inc Purification of liquids

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2768747A (en) * 1951-07-21 1956-10-30 Pintsch Bamag Ag Apparatus for bleaching fatty materials

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