US2475857A - Sampling device - Google Patents

Sampling device Download PDF

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Publication number
US2475857A
US2475857A US729138A US72913847A US2475857A US 2475857 A US2475857 A US 2475857A US 729138 A US729138 A US 729138A US 72913847 A US72913847 A US 72913847A US 2475857 A US2475857 A US 2475857A
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Prior art keywords
condenser
vapors
conduit
flowing stream
mouth
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US729138A
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Armin E Reinert
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
    • G01N1/2035Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
    • G01N2001/2064Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping using a by-pass loop
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
    • G01N1/2035Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
    • G01N2001/2071Removable sample bottle

Definitions

  • This invention relates to improvements in sampling devices for collecting samples of condensed vapors.
  • the device may be attached to single or multiple effect evaporators to determine entrainment losses by condensing a small portion of the vapors goingto the condenser or from one effect to another.
  • suitable adjustments can be made on the evaporator to reduce the losses to a minimum.
  • Fig. 1 is a View partly in vertical section of a sampling device embodying the invention.
  • Fig. 2 is an end view in the device shown in Fig. 1.
  • Condenser 2 represents in its entirety an elongated tubular condenser.
  • Condenser 2 as shown of the surface type, has been found adequate for most purposes, that is, where the room temperature is 20 degrees F. or more below the temperature in the vapor line. However, where the room temperature is not at least 26 degrees F. below the temperature in the vapor line any suitable and well known system of tubes and cooling water, not illustrated, may form a part of the condenser.
  • Condenser 2 at opposite end portions thereof, is provided with shanks ii and 6 threaded for coupling engagement with inlet and return tubes 8 and iii, respectively.
  • the projecting ends of tubes 8 and ID are fashioned similarly to each other by a diagonal out forming pyramidal tip portions which project into the vapor line.
  • Such a vapor line in the form of a conduit or duct for 2 a flowing stream of vapors is represented at A and the direction of the flow is indicated by the arrows.
  • the tubes 8 and it) may be secured to the wall of conduit A in any well known manner.
  • the mouth ll of inlet tube 8 faces upstream and is preferably so positioned with respect to the conduit that the base portion Id thereof is disposed at the outer rim of the flowing stream and the apex portion is thereof is disposed at the center of theflowing stream. In this manner, the flow pressure will positively force a portion of the flowing stream of vapors adequate for ordinarysampling purposes into the condenser 2.
  • the mouth I2 of outer or return tube it faces downstream of the flowing stream of vapors.
  • the mouth it of the inlet tube return mouth [2 is so positioned with respect to the conduit A that the base portion I l thereof is at the outer rim of the flowing stream and the apex portion l3 thereof is disposed at the center of the flowing stream.
  • a vacuum is produced which draws the uncondensed vapors from the condenser back into the vapor line.
  • the novel construction of the mouths It and i2 permits a minimum of interference with the flow through conduit A and at the same time eiiects a positive and adequate intake and discharge, respectively, of vapors regardless the force or volume of the flow in the conduit.
  • the device shown in Fig. 1 is adapted for continuous operation and ordinarily a portion of the flowing stream of vapors constantly passes through condenser 2.
  • the invention contemplates that the inlet tube 3 be rotatable so that by turning the mouth H in either direction away from the vapor stream the portion of entering vapors may be reduced or, by rotating the tube 8 so that the mouth I! thereof faces downstream in the manner of mouth 52, flow through condenser 2 may be cut off entirely.
  • any accumulation of non-fluid material may conveniently be cleaned from condenser 2 by removing end plate 16 suitably secured such as by bolts to annular flange It provided at the outlet end of condenser 2.
  • any suitable container such as a bottle 2c is provided.
  • condenser 2 is provided with a depending drain or outlet tube 22 having intermediate the ends thereof an annular flange is against which the mouth of container 28 may bear, preferably through the 3 medium of a gasket 26, as shown.
  • the projecting end of drain tube 22 extends interiorly of container 20 to tend against leakage.
  • a plurality of coil springs 28 are provided having the ends thereof detachably connected through apertures in the flange 2B and the plate 30 provided as a support for the bottom of the container.
  • a vapor sampling device comprising a con denser, an inlet tube adapted for connection with a flowing stream of vapors and having an elongated mouth extending transversely of and substantially from the center to the outer rim of the flowing stream for conductin a sample of the vapors to said condenser, a return tube adapted for connection, with said flowing stream. of vapors for returning uncondensed vapors to said' flowing stream, and means for collecting condensate for said condenser.
  • a vapor sampling system comprising, a conduit for a flowing stream of vapors, a condenser, an inlet tube connecting said condenser with said conduit and having an elongated mouth extending transversely of the, flowing stream and open substantially from the center to the inner wall of said.- conduit for conducting a sample of the vapors to said condenser, a return tube for returning uncondensed vapors to said conduit, and means for collecting the condensate from said condenser.
  • a vapor line sampling system comprising, a conduit for a flowing streamof vapors, a condenser, an inlet tube connecting said condenser with said conduit for conducting a portion of the vapors from the said flowing stream to said condenser, the mouth of said inlet tube being dis posed diagonally to form a pyramidal tip for said tube and said tube bein connected with said conduit in such a manner that the base of said tip is positioned at the outer rim of the vapor stream and the apex of said tip is positioned at the center of the vapor stream, a return tube connecting said condenser with said conduit for returning uncondensed vapors, and means for collecting the condensate from said condenser.
  • a vapor line sampling system comprising, a conduit for a flowing stream of vapors, a condenser, an inlet tube connecting said condenser with said conduit for conducting a portion of the vapors from the said flowing stream to said condenser, a return tube connecting said condenser with said conduit for returnin uncondensed vapors, the mouths of said inlet and return tubes being disposed diagonally to form pyramidal tips for said tubes and said tubes being connected with said conduit in such a manner that the bases of said tips are positioned at the outer rim of the vapor stream and the apexes of said tips are positioned at the center of the vapor stream, and means for collecting the condensate from said condenser.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Sampling And Sample Adjustment (AREA)

Description

y 1949. A. EJREINERT 2,75,57
SAMPLING DEVICE Filed Feb. 1'7, 1947 grwwwkov;
Arm/n E. Remerf Patented July 12, 1949 UNITED STATES E A'E'ENT OFFICE SAMPLING DEVICE Armin E. lReinert, Shawano, Wis. Application February 17, 1947, Serial No. 729,138
4 Claims.
This invention relates to improvements in sampling devices for collecting samples of condensed vapors. In a particular adaptation of the invention, the device may be attached to single or multiple effect evaporators to determine entrainment losses by condensing a small portion of the vapors goingto the condenser or from one effect to another. When such entrainment losses are determined from the sample of condensed vapors suitable adjustments can be made on the evaporator to reduce the losses to a minimum.
It is an object of the invention to provide a sampling device which may be readily attached to a conduit for a flowing stream of vapors to extract therefrom a portion for sampling purposes.
It is another object of the invention to provide such a device which may be operated continuously returning any uncondensed vapors to the vapor conduit.
It is a further object of the invention to provide a sampling device which is simple in construction and positive and eificient in operation.
Other and further objects and advantages of the invention will be apparent from the follow ing detailed explanation taken in conjunction with the accompanying drawings wherein a preferred embodiment of the principles of the invention have been selected for exemplification.
In the drawings:
Fig. 1 is a View partly in vertical section of a sampling device embodying the invention, and
Fig. 2 is an end view in the device shown in Fig. 1.
Referring more particularly to the drawings, wherein like numerals refer to like parts, 2 represents in its entirety an elongated tubular condenser. Condenser 2, as shown of the surface type, has been found adequate for most purposes, that is, where the room temperature is 20 degrees F. or more below the temperature in the vapor line. However, where the room temperature is not at least 26 degrees F. below the temperature in the vapor line any suitable and well known system of tubes and cooling water, not illustrated, may form a part of the condenser.
Condenser 2, at opposite end portions thereof, is provided with shanks ii and 6 threaded for coupling engagement with inlet and return tubes 8 and iii, respectively. The projecting ends of tubes 8 and ID are fashioned similarly to each other by a diagonal out forming pyramidal tip portions which project into the vapor line. Such a vapor line, in the form of a conduit or duct for 2 a flowing stream of vapors is represented at A and the direction of the flow is indicated by the arrows. The tubes 8 and it) may be secured to the wall of conduit A in any well known manner.
As shown, the mouth ll of inlet tube 8 faces upstream and is preferably so positioned with respect to the conduit that the base portion Id thereof is disposed at the outer rim of the flowing stream and the apex portion is thereof is disposed at the center of theflowing stream. In this manner, the flow pressure will positively force a portion of the flowing stream of vapors adequate for ordinarysampling purposes into the condenser 2.
The mouth I2 of outer or return tube it, as shown, faces downstream of the flowing stream of vapors. Similarly to the mouth it of the inlet tube return mouth [2 is so positioned with respect to the conduit A that the base portion I l thereof is at the outer rim of the flowing stream and the apex portion l3 thereof is disposed at the center of the flowing stream. In this manher, as the vapors in conduit A pass the mouth 52, a vacuum is produced which draws the uncondensed vapors from the condenser back into the vapor line. The novel construction of the mouths It and i2 permits a minimum of interference with the flow through conduit A and at the same time eiiects a positive and adequate intake and discharge, respectively, of vapors regardless the force or volume of the flow in the conduit.
The device shown in Fig. 1 is adapted for continuous operation and ordinarily a portion of the flowing stream of vapors constantly passes through condenser 2. The invention, however, contemplates that the inlet tube 3 be rotatable so that by turning the mouth H in either direction away from the vapor stream the portion of entering vapors may be reduced or, by rotating the tube 8 so that the mouth I! thereof faces downstream in the manner of mouth 52, flow through condenser 2 may be cut off entirely.
Any accumulation of non-fluid material may conveniently be cleaned from condenser 2 by removing end plate 16 suitably secured such as by bolts to annular flange It provided at the outlet end of condenser 2.
For collecting the condensate from condenser- 2, any suitable container such as a bottle 2c is provided. For positioning container 2%, condenser 2 is provided with a depending drain or outlet tube 22 having intermediate the ends thereof an annular flange is against which the mouth of container 28 may bear, preferably through the 3 medium of a gasket 26, as shown. The projecting end of drain tube 22 extends interiorly of container 20 to tend against leakage. To urge container 29 into airtight engagement with the drain tube 22, a plurality of coil springs 28 are provided having the ends thereof detachably connected through apertures in the flange 2B and the plate 30 provided as a support for the bottom of the container.
The operation of the. device herein described and illustrated will be readily apparent. As a portion of the flowing stream of vapors in conduit A is by-passed through condenser 2, any condensate will find its way to container 20, Container 20 may be removed merely by detaching springs 28 from either the flange 24 or the supporting plate 30 and an empty container quickly substituted.
It will be understood that the particular con struction herein illustrated and described is eX- emplary only of the principles of the invention which embrace such modified constructions fall within the scope of the following claims.
I claim:
1. A vapor sampling device comprising a con denser, an inlet tube adapted for connection with a flowing stream of vapors and having an elongated mouth extending transversely of and substantially from the center to the outer rim of the flowing stream for conductin a sample of the vapors to said condenser, a return tube adapted for connection, with said flowing stream. of vapors for returning uncondensed vapors to said' flowing stream, and means for collecting condensate for said condenser.
2. A vapor sampling system comprising, a conduit for a flowing stream of vapors, a condenser, an inlet tube connecting said condenser with said conduit and having an elongated mouth extending transversely of the, flowing stream and open substantially from the center to the inner wall of said.- conduit for conducting a sample of the vapors to said condenser, a return tube for returning uncondensed vapors to said conduit, and means for collecting the condensate from said condenser.
3. A vapor line sampling system comprising, a conduit for a flowing streamof vapors, a condenser, an inlet tube connecting said condenser with said conduit for conducting a portion of the vapors from the said flowing stream to said condenser, the mouth of said inlet tube being dis posed diagonally to form a pyramidal tip for said tube and said tube bein connected with said conduit in such a manner that the base of said tip is positioned at the outer rim of the vapor stream and the apex of said tip is positioned at the center of the vapor stream, a return tube connecting said condenser with said conduit for returning uncondensed vapors, and means for collecting the condensate from said condenser.
4. A vapor line sampling system comprising, a conduit for a flowing stream of vapors, a condenser, an inlet tube connecting said condenser with said conduit for conducting a portion of the vapors from the said flowing stream to said condenser, a return tube connecting said condenser with said conduit for returnin uncondensed vapors, the mouths of said inlet and return tubes being disposed diagonally to form pyramidal tips for said tubes and said tubes being connected with said conduit in such a manner that the bases of said tips are positioned at the outer rim of the vapor stream and the apexes of said tips are positioned at the center of the vapor stream, and means for collecting the condensate from said condenser.
ARMIN E. REINERT.
REFERENCES CITED The following references are of record in the file of this patent:
UNITED STATES PATENTS Number Name Date 961,419 Muchka June 14, 1910 1,601,383 Todd Sept. 28, 1926 1,697,432 Martin Jan. 1, 1929 1,837,853 Grace Dec. 22, 1931 1,845,247 Davidson Feb. 16, 1932 2,030,682 Campbell Feb. 11,. 1936 2,146,072 Howard Feb. 7, 1939 2,301,815 Robison Nov. 10, 1942 2,322,018 Huber June 15, 1943 2,425,669 Brock Aug. 12, 1947 2,446,587 Henry Aug, 10, 1948
US729138A 1947-02-17 1947-02-17 Sampling device Expired - Lifetime US2475857A (en)

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Cited By (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2688980A (en) * 1949-01-13 1954-09-14 Edward Valves Inc Valve equalizer
US2720788A (en) * 1952-05-28 1955-10-18 American Cyanamid Co Continuous vapor sampler
US3177706A (en) * 1963-01-24 1965-04-13 Hughes Aircraft Co Fluid inspection device
US3260120A (en) * 1964-02-17 1966-07-12 Rexall Drug Chemical Sampling device
US3400575A (en) * 1966-01-28 1968-09-10 Cox Instr Contaminant sampling apparatus and method
US3595087A (en) * 1969-10-20 1971-07-27 Phillips Petroleum Co Sampling apparatus
US4131011A (en) * 1977-02-28 1978-12-26 Abbott Laboratories Method and device for determining the end point for drying
US4150574A (en) * 1977-12-28 1979-04-24 Harry Wolf Fluid sampling system
US4791821A (en) * 1985-04-05 1988-12-20 Spencer R Wilson Sample injection means
US4800761A (en) * 1987-05-29 1989-01-31 Spencer R Wilson Sample extraction system
US4986138A (en) * 1985-04-05 1991-01-22 Spencer R Wilson Sample injection means
US5003830A (en) * 1987-05-29 1991-04-02 Spencer R Wilson Sample extraction system
US5127258A (en) * 1991-01-30 1992-07-07 The United States Of America As Represented By The United States Department Of Energy Duplex sampling apparatus and method
US5301560A (en) * 1991-11-22 1994-04-12 Texas Sampling, Inc. Closed loop liquid sampler and sampling system
US5390553A (en) * 1992-12-22 1995-02-21 Lynn; Lewis G. Liquid sampling apparatus and method
US5431067A (en) * 1991-11-22 1995-07-11 Texas Sampling, Inc. Closed loop liquid sampler and sampling system
US5460054A (en) * 1993-09-28 1995-10-24 Tran; Sa C. Apparatus for choke-free sampling of fluids and slurries
US5625156A (en) * 1996-04-29 1997-04-29 General Motors Corporation Apparatus for sensing exhaust gas
US5844148A (en) * 1997-07-30 1998-12-01 Pittway Corporation Detector with adjustable sampling tubes
US6593146B1 (en) * 1999-02-16 2003-07-15 Brand Gmbh & Co. Kg Fabrik Fur Laborgerate Metering device and method for operating a metering device
US20070240490A1 (en) * 2005-12-20 2007-10-18 Desrochers Eric M Duct probe assembly system for multipoint air sampling
US20160139008A1 (en) * 2010-09-10 2016-05-19 Xtralis Technologies Ltd. Duct detector

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US961419A (en) * 1908-05-28 1910-06-14 Josef Muchka Testing device.
US1601383A (en) * 1925-06-23 1926-09-28 Emery W Todd Liquid-testing apparatus
US1697432A (en) * 1925-08-06 1929-01-01 Charles A Martin Control system
US1837853A (en) * 1927-10-19 1931-12-22 Florez Luis De Pyrometric device
US1845247A (en) * 1927-03-07 1932-02-16 Standard Oil Co Gas testing device
US2030682A (en) * 1930-09-30 1936-02-11 Eugene G Campbell Apparatus for treating or sampling substances
US2146072A (en) * 1935-08-02 1939-02-07 Pneumatic Scale Corp Receptacle filling machine
US2301815A (en) * 1940-11-08 1942-11-10 Sidney J Robison Pulverized material sampler
US2322018A (en) * 1941-01-16 1943-06-15 Standard Oil Dev Co Sampling and metering device
US2425669A (en) * 1943-08-26 1947-08-12 Townson & Mercer Ltd Condenser
US2446587A (en) * 1946-06-11 1948-08-10 Robert S Henry Sludge trap

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US961419A (en) * 1908-05-28 1910-06-14 Josef Muchka Testing device.
US1601383A (en) * 1925-06-23 1926-09-28 Emery W Todd Liquid-testing apparatus
US1697432A (en) * 1925-08-06 1929-01-01 Charles A Martin Control system
US1845247A (en) * 1927-03-07 1932-02-16 Standard Oil Co Gas testing device
US1837853A (en) * 1927-10-19 1931-12-22 Florez Luis De Pyrometric device
US2030682A (en) * 1930-09-30 1936-02-11 Eugene G Campbell Apparatus for treating or sampling substances
US2146072A (en) * 1935-08-02 1939-02-07 Pneumatic Scale Corp Receptacle filling machine
US2301815A (en) * 1940-11-08 1942-11-10 Sidney J Robison Pulverized material sampler
US2322018A (en) * 1941-01-16 1943-06-15 Standard Oil Dev Co Sampling and metering device
US2425669A (en) * 1943-08-26 1947-08-12 Townson & Mercer Ltd Condenser
US2446587A (en) * 1946-06-11 1948-08-10 Robert S Henry Sludge trap

Cited By (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2688980A (en) * 1949-01-13 1954-09-14 Edward Valves Inc Valve equalizer
US2720788A (en) * 1952-05-28 1955-10-18 American Cyanamid Co Continuous vapor sampler
US3177706A (en) * 1963-01-24 1965-04-13 Hughes Aircraft Co Fluid inspection device
US3260120A (en) * 1964-02-17 1966-07-12 Rexall Drug Chemical Sampling device
US3400575A (en) * 1966-01-28 1968-09-10 Cox Instr Contaminant sampling apparatus and method
US3595087A (en) * 1969-10-20 1971-07-27 Phillips Petroleum Co Sampling apparatus
US4131011A (en) * 1977-02-28 1978-12-26 Abbott Laboratories Method and device for determining the end point for drying
US4150574A (en) * 1977-12-28 1979-04-24 Harry Wolf Fluid sampling system
US4791821A (en) * 1985-04-05 1988-12-20 Spencer R Wilson Sample injection means
US4986138A (en) * 1985-04-05 1991-01-22 Spencer R Wilson Sample injection means
US4800761A (en) * 1987-05-29 1989-01-31 Spencer R Wilson Sample extraction system
US5003830A (en) * 1987-05-29 1991-04-02 Spencer R Wilson Sample extraction system
US5127258A (en) * 1991-01-30 1992-07-07 The United States Of America As Represented By The United States Department Of Energy Duplex sampling apparatus and method
US5301560A (en) * 1991-11-22 1994-04-12 Texas Sampling, Inc. Closed loop liquid sampler and sampling system
US5431067A (en) * 1991-11-22 1995-07-11 Texas Sampling, Inc. Closed loop liquid sampler and sampling system
US5604320A (en) * 1991-11-22 1997-02-18 Texas Sampling, Inc. Shroud with removable insert for a closed loop liquid sampler
US5390553A (en) * 1992-12-22 1995-02-21 Lynn; Lewis G. Liquid sampling apparatus and method
US5460054A (en) * 1993-09-28 1995-10-24 Tran; Sa C. Apparatus for choke-free sampling of fluids and slurries
US5625156A (en) * 1996-04-29 1997-04-29 General Motors Corporation Apparatus for sensing exhaust gas
US5844148A (en) * 1997-07-30 1998-12-01 Pittway Corporation Detector with adjustable sampling tubes
US6593146B1 (en) * 1999-02-16 2003-07-15 Brand Gmbh & Co. Kg Fabrik Fur Laborgerate Metering device and method for operating a metering device
US20070240490A1 (en) * 2005-12-20 2007-10-18 Desrochers Eric M Duct probe assembly system for multipoint air sampling
US7415901B2 (en) * 2005-12-20 2008-08-26 Aircuity, Inc. Duct probe assembly system for multipoint air sampling
US20160139008A1 (en) * 2010-09-10 2016-05-19 Xtralis Technologies Ltd. Duct detector
US10267711B2 (en) * 2010-09-10 2019-04-23 Garrett Thermal Systems Limited Duct detector

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