US2448930A - Porous filter - Google Patents

Porous filter Download PDF

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Publication number
US2448930A
US2448930A US563236A US56323644A US2448930A US 2448930 A US2448930 A US 2448930A US 563236 A US563236 A US 563236A US 56323644 A US56323644 A US 56323644A US 2448930 A US2448930 A US 2448930A
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Prior art keywords
spacing layer
disc
ceramic
plastic
layers
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Expired - Lifetime
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US563236A
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Stokes Edward Arthur
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Vokes Ltd
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Vokes Ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/063Preparing or treating the raw materials individually or as batches
    • C04B38/0635Compounding ingredients
    • C04B38/0645Burnable, meltable, sublimable materials
    • C04B38/065Burnable, meltable, sublimable materials characterised by physical aspects, e.g. shape, size or porosity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/39Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with hollow discs side by side on, or around, one or more tubes, e.g. of the leaf type
    • B01D29/41Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with hollow discs side by side on, or around, one or more tubes, e.g. of the leaf type mounted transversely on the tube
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00793Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms

Definitions

  • the unit includes a main porous filtering wall of deeply re-entrant form whereof the hollows or some of the hollows are filled or reinforced with the same material (including a material of sufficiently similar properties) in skeleton form and integral with the main porous wall.
  • skeleton is meant that the mass affords a large number of free ⁇ pas-- sages, as will be understood from the specific example to be described later.
  • the invention arose from the idea that the ideal from the point of view of mechanical strength and making satisfactory joints in a pack of ceramic discs forming a hollow fined construction would be to have the hollows in the fins filled with a ceramic of coarse grain moulded integrally with the fine-grained filtering wall. In practice this is not easy, because ceramics f different porosity have different coefficients of expansion during processing and cracking of the fine wall is likely to result.
  • This difficulty can be avoided by a method which forms an important part of the invention namely inserting a suitable foramlnated spacing layer between two layers of ceramic material in plastic state, moulding the element with the spacing layer in position so as to produce a filling of the interstices in the spacing layer of the plastic ceramic material integral with that of the two layers and removing the filling layer .by heat.
  • moulding is used in a wide sense to include forming by the use of moulds, or the like of any appropriate form.
  • a cellulosic mesh material such as cotton gauze, with intermeshed threads of suitable sizeprobably not less than 22 and perhaps preferably 16 gauge with a mesh of 6 or 8 threads per inch -would be suitable for a wall 1A inch thick.
  • a gauze or perforated sheet of low melting point metal or plastic could be used.
  • the cellulosic material would be carbonised to remove it; and the metal or plastic would be melted out and the material could be recovered.
  • the preferred material of those tried up to the present is thick perforatd filter paper or blotting paper which will eventually leave a skeleton filling or reinforcement in the form of a series of pillars or ribs of any desired shape and arrangement.
  • Felts and the like suit-ably foraminated could also be used: in fact a great variety of materials combustible 4below the processing temperatures of the ceramic or otherwise readily removable or capable of leaving sufficiently free passage in due course.
  • Flg. 1 is a perspective view of a disc or 1in partly broken away.
  • Fig. 2 shows a foraminated spacing layer in the form of a disc of blotting paper
  • Fig. 3 is a central section of the disc of Fig. 1 in process of manufacture
  • Fig. 4 is a central section showing how completed discs are assembled as fins of a filter unit.
  • 'I'he disc illustrated comprises an annulus with a central hole l and upper, lower and outer walls 2, I and 4.
  • the material for the lower half in its plastic state is first placed in the mould, the rather smaller perforated disc 5 laid on it, the material for the upper half placed on top and suiiicient moulding pressure applied to integrate the two halves of the outer wall 4 and form the integral skeleton reinforcement in the form of pillars i in the perforations of the disc 5, to produce the complete disc in its plastic state (Fig. 3).
  • the processing of the disc then proceeds conventionally according to the particular ceramic employed and during the kilning the temperature is sufficient to cause the material of the disc 5 to decompose and leave the space 1 traversed by the pillars 6. It will be observed that the space 1 can be a mere fraction of the thickness of the walls, economising space and making an extremely compact, simple and convenient component. It is desirable, as is shown, to ensure that there is sufficient reinforcement where the assembly pressure is to be applied-in this case near the inner periphery of the annulus-at the same time allowing ample passage space for the filtered liquid.
  • Figure 4 illustrates a typical assembly of the discs which are threaded on to a perforated tube 8 between packing rings 9 which also serve to set the spacing of the hollow iins thus formed.
  • the number of iins can be readily varied to provide units of diiferent capacity and .the assembly completed by suitable end pieces Il, Il and clamping means shown as a central assembly rod I2 attached to a spider il formed in the end piece I Il and provided with a tightening nut I4 and lock nut I5.
  • the component shown is intended for nltration from outside to in. the dirty liquid being fed to a conventional surrounding casing and the clean liquid delivered through the end piece Il.
  • a method of forming a hollow filtering ele--- ment which includes inserting a suitable foraminated spacing layer between two layers ofceramic material in plastic state, moulding the element with the spacing layer in position so as to produce a filling of the interstices in the spacing layer of the plastic ceramic material integral with that of the two layers and removing the filling layer by heat.
  • a method of forming a hollow filtering element which includes inserting between two layers oi' ceramic material in plastic state a foraminated spacing layer of material carbonizing at a temperature not greater than is later employed for kilning the ceramic material, moulding 'the element with the spacing layer in position so as to produce a filling of the interstices in the spacing layer of the plastic ceramic material integral with that of" the two layers and removing the filling layer by heat.
  • a method of forming a hollow ltering element which includes inserting between two layers of ceramic material in plastic state a foraminated layer of spacing material having a melting point below that which can be withstood without damage by the ceramic material, moulding the element with the spacing layer in position so as to produce a lling of the interstices in the spacing layer of the plastic ceramic material integral with that of the two layers and removing the filling layer by heat.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtering Materials (AREA)

Description

Sept. 7, 1948. E. A. sToKr-:s 2,448,930
POROUS FILTER Filed Nov. 15, 1944 lla 4/ l E L 76 y 4 idf/,975i
Patented Sept. 7, 1948 POBOUS FILTER Edward Arthur Stokes, Guildford, England, as-
signor to Volles Limited, Guildford, England Application November 13, 1944, Serial No. 563,236 In Great Britain December 15, 1943 Various iilter units are given a large surface relatively to space occupied by the employment of deeply re-entrant forms of filtering screen, including screens formed with pockets, pleats, corrugations and so forth. The use of ceramic discs to make up a filter unit of hollow finned construction is quite well known. It is suggested in a copending specification Number 500,872, that the hollows in the fins or the spaces between fins or both could be filled with coarser material. This would limit the strain movement when a pack is compressed and so improve mechanical strength.
According to the present invention the unit includes a main porous filtering wall of deeply re-entrant form whereof the hollows or some of the hollows are filled or reinforced with the same material (including a material of sufficiently similar properties) in skeleton form and integral with the main porous wall. By skeleton is meant that the mass affords a large number of free `pas-- sages, as will be understood from the specific example to be described later.
The invention arose from the idea that the ideal from the point of view of mechanical strength and making satisfactory joints in a pack of ceramic discs forming a hollow fined construction would be to have the hollows in the fins filled with a ceramic of coarse grain moulded integrally with the fine-grained filtering wall. In practice this is not easy, because ceramics f different porosity have different coefficients of expansion during processing and cracking of the fine wall is likely to result.
This difficulty can be avoided by a method which forms an important part of the invention namely inserting a suitable foramlnated spacing layer between two layers of ceramic material in plastic state, moulding the element with the spacing layer in position so as to produce a filling of the interstices in the spacing layer of the plastic ceramic material integral with that of the two layers and removing the filling layer .by heat. The word moulding is used in a wide sense to include forming by the use of moulds, or the like of any appropriate form. Once the underlying idea of the method is understood it ls clear that it will lend itself to the use of a variety of materials a'nd forms for the spacing layer. For example, a cellulosic mesh material such as cotton gauze, with intermeshed threads of suitable sizeprobably not less than 22 and perhaps preferably 16 gauge with a mesh of 6 or 8 threads per inch -would be suitable for a wall 1A inch thick. Or a gauze or perforated sheet of low melting point metal or plastic could be used. The cellulosic material would be carbonised to remove it; and the metal or plastic would be melted out and the material could be recovered. The preferred material of those tried up to the present is thick perforatd filter paper or blotting paper which will eventually leave a skeleton filling or reinforcement in the form of a series of pillars or ribs of any desired shape and arrangement. Felts and the like suit-ably foraminated could also be used: in fact a great variety of materials combustible 4below the processing temperatures of the ceramic or otherwise readily removable or capable of leaving sufficiently free passage in due course.
The parts of the invention for which a monopoly is desired are those delimited by the claims.
A typical form of the invention is illustrated by the accompanying drawings in which- Flg. 1 is a perspective view of a disc or 1in partly broken away.
Fig. 2 shows a foraminated spacing layer in the form of a disc of blotting paper,
Fig. 3 is a central section of the disc of Fig. 1 in process of manufacture, and
Fig. 4 is a central section showing how completed discs are assembled as fins of a filter unit.
'I'he disc illustrated comprises an annulus with a central hole l and upper, lower and outer walls 2, I and 4. The material for the lower half in its plastic state is first placed in the mould, the rather smaller perforated disc 5 laid on it, the material for the upper half placed on top and suiiicient moulding pressure applied to integrate the two halves of the outer wall 4 and form the integral skeleton reinforcement in the form of pillars i in the perforations of the disc 5, to produce the complete disc in its plastic state (Fig. 3).
The processing of the disc then proceeds conventionally according to the particular ceramic employed and during the kilning the temperature is sufficient to cause the material of the disc 5 to decompose and leave the space 1 traversed by the pillars 6. It will be observed that the space 1 can be a mere fraction of the thickness of the walls, economising space and making an extremely compact, simple and convenient component. It is desirable, as is shown, to ensure that there is sufficient reinforcement where the assembly pressure is to be applied-in this case near the inner periphery of the annulus-at the same time allowing ample passage space for the filtered liquid.
Figure 4 illustrates a typical assembly of the discs which are threaded on to a perforated tube 8 between packing rings 9 which also serve to set the spacing of the hollow iins thus formed. The number of iins can be readily varied to provide units of diiferent capacity and .the assembly completed by suitable end pieces Il, Il and clamping means shown as a central assembly rod I2 attached to a spider il formed in the end piece I Il and provided with a tightening nut I4 and lock nut I5. The component shown is intended for nltration from outside to in. the dirty liquid being fed to a conventional surrounding casing and the clean liquid delivered through the end piece Il. Flow from inside to out can equally readily be arranged for by having an inner wall to the annulus and access from the space 1 to the outer periphery, near which the clamping would then take place with the discs preferably spaced and assembled in an external perforated tube. as will be apparent to skilled persons without further illustration. The ideas underlying the invention can also be applied to more complicated components when found desirable, or to plates or discs of various fiat or curved forms 'according to the assembly required, as will be apparent.
I claim:
1. A method of forming a hollow filtering ele-- ment which includes inserting a suitable foraminated spacing layer between two layers ofceramic material in plastic state, moulding the element with the spacing layer in position so as to produce a filling of the interstices in the spacing layer of the plastic ceramic material integral with that of the two layers and removing the filling layer by heat.
2. A method of forming a hollow filtering element which includes inserting between two layers oi' ceramic material in plastic state a foraminated spacing layer of material carbonizing at a temperature not greater than is later employed for kilning the ceramic material, moulding 'the element with the spacing layer in position so as to produce a filling of the interstices in the spacing layer of the plastic ceramic material integral with that of" the two layers and removing the filling layer by heat.
3. A method of forming a hollow ltering element which includes inserting between two layers of ceramic material in plastic state a foraminated layer of spacing material having a melting point below that which can be withstood without damage by the ceramic material, moulding the element with the spacing layer in position so as to produce a lling of the interstices in the spacing layer of the plastic ceramic material integral with that of the two layers and removing the filling layer by heat.
EDWARD ARTHUR STORES.
REFERENCES CITED The following references are of record in the
US563236A 1943-12-15 1944-11-13 Porous filter Expired - Lifetime US2448930A (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2598322A (en) * 1945-12-03 1952-05-27 Vokes Ltd Porous filter
US3891735A (en) * 1971-12-29 1975-06-24 Atomic Energy Authority Uk Sintered artefacts and the like
US4196027A (en) * 1976-03-26 1980-04-01 Process Scientific Innovations Ltd. Method of making filter elements for gas or liquid
US4902420A (en) * 1987-03-27 1990-02-20 Pall Corporation Segmented filter disc with slotted support and drainage plate and support spacer
US5100551A (en) * 1987-03-27 1992-03-31 Pall Corporation Segmented filter disc with slotted support and drainage plate
US5385700A (en) * 1991-05-03 1995-01-31 Programme 3 Patent Holdings Method of making a holder of ceramic material
US5628901A (en) * 1993-04-30 1997-05-13 Castrol Industrial North America Inc. Vessel for treating liquids
US20030150794A1 (en) * 2000-05-12 2003-08-14 Dieter Blase Discoid filtration body
US20220347603A1 (en) * 2021-04-30 2022-11-03 Pall Corporation Filter disk segments

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US366726A (en) * 1887-07-19 Agitating filter-diaphragms with abrading material for cleansing their surfaces
US509441A (en) * 1893-11-28 Santueto
US622562A (en) * 1899-04-04 Siphon-filter
US741090A (en) * 1902-09-27 1903-10-13 John F Ziegler Filter.
FR473187A (en) * 1913-09-10 1915-01-05 Emmanuel Simoneton Improvements to plate filters

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US366726A (en) * 1887-07-19 Agitating filter-diaphragms with abrading material for cleansing their surfaces
US509441A (en) * 1893-11-28 Santueto
US622562A (en) * 1899-04-04 Siphon-filter
US741090A (en) * 1902-09-27 1903-10-13 John F Ziegler Filter.
FR473187A (en) * 1913-09-10 1915-01-05 Emmanuel Simoneton Improvements to plate filters

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2598322A (en) * 1945-12-03 1952-05-27 Vokes Ltd Porous filter
US3891735A (en) * 1971-12-29 1975-06-24 Atomic Energy Authority Uk Sintered artefacts and the like
US4196027A (en) * 1976-03-26 1980-04-01 Process Scientific Innovations Ltd. Method of making filter elements for gas or liquid
US4902420A (en) * 1987-03-27 1990-02-20 Pall Corporation Segmented filter disc with slotted support and drainage plate and support spacer
US5100551A (en) * 1987-03-27 1992-03-31 Pall Corporation Segmented filter disc with slotted support and drainage plate
US5385700A (en) * 1991-05-03 1995-01-31 Programme 3 Patent Holdings Method of making a holder of ceramic material
US5628901A (en) * 1993-04-30 1997-05-13 Castrol Industrial North America Inc. Vessel for treating liquids
US20030150794A1 (en) * 2000-05-12 2003-08-14 Dieter Blase Discoid filtration body
US20220347603A1 (en) * 2021-04-30 2022-11-03 Pall Corporation Filter disk segments

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