US2386529A - Salt bath furnace - Google Patents

Salt bath furnace Download PDF

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US2386529A
US2386529A US504688A US50468843A US2386529A US 2386529 A US2386529 A US 2386529A US 504688 A US504688 A US 504688A US 50468843 A US50468843 A US 50468843A US 2386529 A US2386529 A US 2386529A
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bath
electrodes
well
furnace
heating
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US504688A
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Wilson William
John J Brutvan
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Cleveland Twist Drill Co
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Cleveland Twist Drill Co
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/34Methods of heating
    • C21D1/44Methods of heating in heat-treatment baths
    • C21D1/46Salt baths

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  • This invention relates as indicated to salt bath furnaces or perhaps more accurately to furnaces of the-type which are commonly used in heat treating tools, forgings, machine parts, and the like and which are provided with a well adapted to contain an electrically heated fluid bath of' the type which is heated by its own internal electrical resistance. Into this bath, the work such as tools, forgings, or machine parts are suspended for a predetermined length of time in order to bring them to Ithe desired temperature.
  • the electrodes are closely spaced on one side of the well, a local hot spot may develop in spite of the stirring action of the bath. Or in all of the above cases, difficulty may be encountered with cold or frozen bottoms of the well which sometimes require a long time to melt and become fluid; or to be heated to the temperature of the body of the bath.
  • Baths which are excessively hot at the top surface result in non-uniform heating of the articles being processed and have the additional disadvantage of causing excessive erosion of the Attempts have been made in the prior art to overcome this tendency of internally heated fluid baths to become hotter a; the top than at the bottom.
  • One method has been to insert the electrodes into a bath which is much larger in crosssection at the top than at the bottom so that the electrodes slope towards each other at the bottom. This method, while producing a more uniform temperature distribution from top to bottom of the bath, entails certain other disadvantages because of the excessive amount of exposed bath surface.
  • FIG. 1 is a vertical transverse sectional view of one form of furnace embodying the principles of our invention.
  • Fig. 2 is a plan view of the same.
  • Fig. 3 is a plan view showing an alternative form of construction.
  • the furnace here illustrated comprises a metallic outer shell I encasing a thick layer of insulating material 2, and an inner metallic lining 3 to act as acontainer for any portion of the iiuld bath which might .leak through the inner refractory lining l.
  • the refractory lining 4 is commonly formed of a dense,- durable material which will withstand the action of the highly heated bath which is maintained in the well 5.
  • Our invention is concerned with the location, size, and arrangement of the electrodes such as 8 and 1- respectively which. in the preferred embodlment of our invention, hang into the well i -closely adjacent to'opposite sides thereof.
  • upper ⁇ terminals 8 and 9 of these electrodes are rebent to rest on the refractory upper portion of th'e furnace adjacent the well 5, and in this fashion, support the hanging portions of the serve both as enective electrical and thermal insulators.
  • the electrodes i and 1 are provided with rebent portions or toes Il and il respectively, which extend toward'each other in a plane slightly above the floor of the well.
  • the width of the well as viewed in Fig. 1 is about 1 0 inches.
  • the length of the toes ii and Il are such as to leave a space of about one inch therebetween. For best operation such space may vary from about V2 inch to abofutinchesr-v m v 'I'he toes Il and li are arranged at a distance .ofabout one inch above the door of 'the' well.
  • each electrode or series ofjelectrodes on one side. of the well as shown in Fig. 2 is. equal to at least well.
  • the effective distance between the vertical portions of the electrodes should be greater than the effective distance between the toes of the electrodes.
  • The' jeifective distance between the electrodesv in any area may be defined as the total distance minus the amount of such area which is normally occupied by work when the furnace is in use. It iswell known that the electrical resistancethrough the metallic work piece is generally less than through an equivalent volume of bath.
  • Each such pair is constructed, arranged and energized like the single -pair previously illustrated and described.
  • a furnace constructed in accordance with our invention may be conveniently started by vmerely heapingy enough salt on the floor of the Well so as to bridge the, ends ofthe electrodes.
  • a small rectangular steel bar may then be inserted between the ends of the electrodes. 'I'his loose connection strikes an varc generating locally an intense heat.
  • a 'small pool of the salt will be melted and then thesame serves as a resistance medium for the generation of sufficient ⁇ heat to progressively melt the additional quantities of the bath which may ,then be progressively added to the well.
  • the small steel bar should be When the electrodes are arranged in the manner illustrated and described, the major portion of the current owing between the electrodes will pass through that small section of the bath lying between the electrode toes I and l I. This highly heated portion of the bath will, by convection and electrical stirring, cause an even distribution of heat throughout the entire bath so that there are none of -the local hot areas which have characterized many of the prior art structures.
  • a still further and perhaps more important factor responsible for the successful operation of our furnace is the greatly reduced or almost total absence of current flow through that portion of the bath occupied by the metal articles undergoing treatment.
  • a structure in accordance with claim 3 which is further characterized in that said electrodes are at least 1/3 as wide as the well sides with which they are associated.
  • thermoelectric heating electrodes extending into said well at opposite sides thereof, hanging vertically and substantially parallel to each other from the top of the well to within a short distance of the bottom and extending horizontally toward each other near the bottom of the well, the distance between the portions thus extending toward each other beingv suillciently smaller than the distance between the vertical portions so that the major proportion of the heating current passing between the electrodes will be concentrated in the shorter horizontal path which accordingly has the lower electrical resistance.
  • the method of heating a heat-treating bath of the character which may be heated by its own internal electrical resistance, which comprises concentrating the major portion of the heating current horizontally in a local area in the center of the bottom of the bath.
  • An electric salt bath furnace comprising a plurality of electrodes for passing current through the bath and adapted to be connected to a source of current supply, said electrodes having. portions extending downwardly toward the bottom of the bath and having portions connected to said first portions and extending in a single plane substantially parallel to the bottom of the bath, said last named portions being positioned with their adjacentI edges relatively dose to generate large portions and extending in laterally spacedrelacurrents and produce vigorous thermal circulation relatively close to the bottom of the bath.
  • An electric salt bath furnace comprising a their adjacent edges relatively close as compared plurality of electrodes for passing current through 5 with the distance between said downwardly ex# lthe bath and adapted to be connected to a source tending portions.
  • said electrodes having portions WILLIAM WILSON. extending downwardly toward the bottom of the JOHN J. BRUTVAN.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Vertical, Hearth, Or Arc Furnaces (AREA)
  • Furnace Details (AREA)

Description

Oct@ @9 1945o w. wzLSON ETAL.,
SALT BATH FURNACE Filed '061. 2, 1945 IN VEN TORS WILLIAM WLLSON und JOHN J. BRUTVAN BY electrodes at the bath surface.
Patented Oct. 9, 1945 SALT BATH FURNACE William Wilson, Cleveland, and John J. Brutvan, Bedford, Ohio, assignors to The Cleveland Twist Drill Company, Cleveland, Ohio, a corporation of Ohio Application October 2, 1943, Serial No. 504,688
12 Claims.
This invention relates as indicated to salt bath furnaces or perhaps more accurately to furnaces of the-type which are commonly used in heat treating tools, forgings, machine parts, and the like and which are provided with a well adapted to contain an electrically heated fluid bath of' the type which is heated by its own internal electrical resistance. Into this bath, the work such as tools, forgings, or machine parts are suspended for a predetermined length of time in order to bring them to Ithe desired temperature.
In the design of furnaces of this character it has sometimes been the practice to have a metallic lining of the well constitute one electrode and to place another electrode at some location within the well. It has also sometimes been common practice to place two electrodes at opposite sides of a refractory lined well. These are sometimes vertical and sometimes sloping towards each other at the bottom. It has also been a well-known practice to place a closely spaced pair of electrodes on one sideof the well. All of these methods of the prior art have certain dilculties of operation. If the electrodes are so spaced that a major portion of the current fiows through the working space, tools in this space may short circuit the current causing them to be locally overheated. If the electrodes are closely spaced on one side of the well, a local hot spot may develop in spite of the stirring action of the bath. Or in all of the above cases, difficulty may be encountered with cold or frozen bottoms of the well which sometimes require a long time to melt and become fluid; or to be heated to the temperature of the body of the bath.
One of the most important requirements to be met by a fluid bath heated internally by the passage of electric current therethrough is that the temperature be uniform throughout the bath. The common practice of inserting two straight electrodes vertically in the bath and parallel to each other has the disadvantage of producing a higher temperature at the top of the bath than at the bottom. This undesirable condition develops from the fact that the hotter portions of the bath rise as they are heated, allowing the electrical current to pass mostly through the hotter upper portion which has a lower electrical resistance than does the colder bottom portion. Baths which are excessively hot at the top surface result in non-uniform heating of the articles being processed and have the additional disadvantage of causing excessive erosion of the Attempts have been made in the prior art to overcome this tendency of internally heated fluid baths to become hotter a; the top than at the bottom. One method has been to insert the electrodes into a bath which is much larger in crosssection at the top than at the bottom so that the electrodes slope towards each other at the bottom. This method, while producing a more uniform temperature distribution from top to bottom of the bath, entails certain other disadvantages because of the excessive amount of exposed bath surface. Some of such disadvantages are: (a) The excessive heat radiated from the larger bath surface causes severe discomfort to the furnace operator; (b) Excessive oxidation of electrodes at the bath surface; (c) Control instruments are subject to excessive temperatures if near enough to the furnace to be convenient for the operator; and (d) The useful working space in the bath is decreased because the walls of the Well slope towards each other at the bottom, so that there is danger of shorting long tools against the electrodes in the lower portionsof the bath.
All of the foregoing objections to the prior art are met in the present invention which has the advantages enumerated below.
It eliminates the hot top, cold bottom type of bath temperature distribution obtained with parallel vertical electrodes.
It eliminates the excessive surface heat losses associated with baths of the same work capacity which have a large cross-sectional area at the surface and taper to a smaller cross-sectional area at the bottom. In comparison with the latter type it allows more Work space in the bath so that there is less danger of shorting the work across the electrodes near the bottom.
When furnaces of this character are placed in operation, and this occurs at regular intervals during their normal use in industry, it becomes necessary to first melt a small amount of the salt between the electrodes in order that it may become a conductor and establish a path of current iiow between the electrodes. This pool of fluid salt then acts as a heating medium for the purpose of melting the remaining portions of the bath as they are added. When the elec- Lrodes are relatively widely spaced in the well, it becomes necessary in starting the bath to employ auxiliary resistance units such as for example -those illustrated in nlBellis Patent No. 1,864,885 or to employ other auxiliary heating means suchas an Oxy-acetylene name.
It is a principal object of our invention to provide a furnace of the character described in which the electrodes are soarranged as to obviate or improve all of the above mentioned diiliculties.
Other objects of our invention will appear as the description proceeds.
To the accomplishment of the foregoing and relatedv ends, said invention, then. consists of the means hereinafter fully described and particularly pointed out in theclaims, the following description and the annexed drawing .setting forth in detail certain means and one mode of carrying out the invention, such disclosed means and mode illustrating, however. but one of various ways in which' the principle of the invention may be used. l
' said annexed drawing:
greater than thedistance between the toes of the electrodes. The resistance in the bath between the vertical portions of the electrodes will then be greater than the resistance of the current g. 1 is a vertical transverse sectional view of one form of furnace embodying the principles of our invention; and
Fig. 2 is a plan view of the same; and
Fig. 3 is a plan view showing an alternative form of construction.
Referring now more specifically lto lthe drawing, the furnace here illustrated comprises a metallic outer shell I encasing a thick layer of insulating material 2, and an inner metallic lining 3 to act as acontainer for any portion of the iiuld bath which might .leak through the inner refractory lining l. The refractory lining 4 is commonly formed of a dense,- durable material which will withstand the action of the highly heated bath which is maintained in the well 5.
The construction of the furnace itself, that is, the bottom and side walls bywhich the well i is provided, are entirely conventional. and form-v no part of the present invention.
Our invention is concerned with the location, size, and arrangement of the electrodes such as 8 and 1- respectively which. in the preferred embodlment of our invention, hang into the well i -closely adjacent to'opposite sides thereof. The
upper` terminals 8 and 9 of these electrodes are rebent to rest on the refractory upper portion of th'e furnace adjacent the well 5, and in this fashion, support the hanging portions of the serve both as enective electrical and thermal insulators.
At their lower ends the electrodes i and 1 are provided with rebent portions or toes Il and il respectively, which extend toward'each other in a plane slightly above the floor of the well.
As illustrative of relative sizes and proportions of the variouspartait may be pointed out ithat in a v'commercial installation which has proven highly successful, the width of the well as viewed in Fig. 1 is about 1 0 inches. The length of the toes ii and Il are such as to leave a space of about one inch therebetween. For best operation such space may vary from about V2 inch to abofutinchesr-v m v 'I'he toes Il and li are arranged at a distance .ofabout one inch above the door of 'the' well.
In the previously identified commercial installation the width of each electrode or series ofjelectrodes on one side. of the well as shown in Fig. 2 is. equal to at least well.
The sizes and proportions given above are those which have been found to be desirable in a comniercial construction ofthe character and size above'identiiled.- As the size of .the furnace is changed, the illustrative sizes and proportions given above will also be changed. although not necessarily indirect proportiontothe changelin Vone-third the width of the path in the 'bath between the toes of the electrodes.. The major proportion of the current will consequently ow between the toes of the electrodes. There are several factors which enter into the final determination of these relative distances in any commercial construction. Such factors are the width of the bath, the depth to which the vertical portions of the electrodes extend into the bath, the surface area ofthe electrodes, and other' factors which will be apparent to those skilled in the art.
In general, the effective distance between the vertical portions of the electrodes should be greater than the effective distance between the toes of the electrodes. The' jeifective distance between the electrodesv in any area may be defined as the total distance minus the amount of such area which is normally occupied by work when the furnace is in use. It iswell known that the electrical resistancethrough the metallic work piece is generally less than through an equivalent volume of bath.
' At this point it will bej observed that one of the advantages of curi improved construction over prior art structures, in which the electrodes slope toward each other from the top to the bottom of the bath, is thatthe useful working space `electrodes in the well. The refractory materials in the bath is increased, and the danger of shortcirculting tools against the electrodes is decreased.
To the electrodes l and 8 there are connected j electrical power leads I2 and I3 respectively, the
same for convenience of illustration in the drawing being shown connected to a suitable source l of controllable electrical energy il.
In the embodiment of our invention shown in Figs. 1 and `2 of the drawing one pair of electrodes has been illustrated. Considerationsv of cost, size of furnace, and facility of manufacture may, however, make it more expedient to removed.A
employ a plurality of pairs of electrodes as illustrated in Fig. 3. Each such pair is constructed, arranged and energized like the single -pair previously illustrated and described.
A furnace constructed in accordance with our invention may be conveniently started by vmerely heapingy enough salt on the floor of the Well so as to bridge the, ends ofthe electrodes. A small rectangular steel bar may then be inserted between the ends of the electrodes. 'I'his loose connection strikes an varc generating locally an intense heat. Immediately a 'small pool of the salt will be melted and then thesame serves as a resistance medium for the generation of sufficient `heat to progressively melt the additional quantities of the bath which may ,then be progressively added to the well. After the poolbas been established, the small steel bar should be When the electrodes are arranged in the manner illustrated and described, the major portion of the current owing between the electrodes will pass through that small section of the bath lying between the electrode toes I and l I. This highly heated portion of the bath will, by convection and electrical stirring, cause an even distribution of heat throughout the entire bath so that there are none of -the local hot areas which have characterized many of the prior art structures.
A still further and perhaps more important factor responsible for the successful operation of our furnace is the greatly reduced or almost total absence of current flow through that portion of the bath occupied by the metal articles undergoing treatment.
Hence, there is no danger oi.' locally overheating the work by accidentally shorting it across the electrodes. Mostimportant of all, the ge'neration of most oi' the heat in the center of the bottom of the bath produces a uniform temperature distribution throughout the bath and tends to prevent warping and distortion of the work.
All of the foregoing advantages of our improved construction are secured by an arrangement of electrodes such that they may be removed or replaced without disturbing the remaining structure of the furnace, and accordingly when repairing, removing. or replacing the electrodes in our construction, it is neither necessary to cool the bath nor empty the bath. Because the electrodes do not pass through the wall of the furnace below the level of the bath, there is no possibility of leakage of the bath through the furnace wall around the electrodes.
We have accordingly provided an extremely simple structure which, as indicated, -obviates the dileuities of the prior art.
Other modes of applying the principle of our invention may be employed instead of the one explained, change being made as regards the means and the steps herein disclosed, provided those stated by any of the following claims or their equivalent be employed.
We therefore particularly point out and distinctly claim as our invention:
i. The combination with a heating furnace provided with a well adapted to contain a duid bath heated by its own internal electrical resistance, of heating electrodes so arranged in said well that the major proportion of the heating current passes horizontally therebetweenand is concentrated in an area of the bath closely overlying the bottom of the well.
2. The combination with a heating furnace provided with a well adapted to contain a fluid bath heated by its own internal electrical resistance, oi heating electrodes extending into. said well at opposite sides thereof, hanging vertically and parallel to each other from the top of the well to within a short distance of the bottom and extending horizontally toward each other near the bottom of the well whereby the major proportion of the heating current passing there.. between is concentrated in an area of the bath closely overlying the bottom of the well.
3. The combination with a heating furnace provided with a well adapted to contain a fluid bath heated by its own internal electrical resistance and inA which metallic articles to be heattreated may be suspended, of heating electrodes extending downwardly into said well closely adjacent opposite sides thereof to a plane below the area normally occupied by the work in said well and then horizontally toward each other tor a distance sumcient so that during normal operation of the bath substantially all of the heating current ilowing between said electrode passes horizontally through that area of the bath below the space occupied by the work.
4. A structure in accordance with claim 3 which is further characterized in that said electrodes are at least 1/3 as wide as the well sides with which they are associated.
5. The combination with a heating furnace provided with a well adapted to contain a uid bath heated by its own internal electrical resstance, of heating electrodes so arranged in said well that the major proportion of the current now horizontally through the bath is in an area in the center of and closely adjacent to the bottom oi' the well.
6. The combination with a heating furnace provided with a well adapted to contain a iluid bath heated by its own internal electrical resistance, of heating electrodes extending into said well at opposite sides thereof, hanging vertically and substantially parallel to each other from the top of the well to within a short distance of the bottom and extending horizontally toward each other near the bottom of the well, the distance between the portions thus extending toward each other beingv suillciently smaller than the distance between the vertical portions so that the major proportion of the heating current passing between the electrodes will be concentrated in the shorter horizontal path which accordingly has the lower electrical resistance.
7. The combination with a heating furnace provided with a well adapted to contain a iluid bath heated by its own internal electrical resistance, of heating electrodes so arranged in said well that the ends thereof approach each other across the bottom of the well to a horizontal distance within the limits of 1/2 inch to 6 inches.
8'. rhe combination with a heating furnace provided with a weli adapted to contain a fluid bain neared by its own internal electrical resistance, of heating electrodes so arranged in said well that the ends thereof approach each other across the bottom of the well to a horizontal distance of approximately 1 inch.
9. The combination with a heating furnace provided with a well adapted to contain a huid bath heated by ,its own internal electrical resistance, of a pair of heating electrodes respectively arranged to enter the bath at opposite sides of the surface, extend downwardly along the side walls of the well, then approach each other across the bottom of the well leaving a sap between the toes in the center of the bottom of the bath through which is concentrated the major portion of the current tlow through the molten bath.
i0. The method of heating a heat-treating bath of the character which may be heated by its own internal electrical resistance, which comprises concentrating the major portion of the heating current horizontally in a local area in the center of the bottom of the bath.
il. An electric salt bath furnace comprising a plurality of electrodes for passing current through the bath and adapted to be connected to a source of current supply, said electrodes having. portions extending downwardly toward the bottom of the bath and having portions connected to said first portions and extending in a single plane substantially parallel to the bottom of the bath, said last named portions being positioned with their adjacentI edges relatively dose to generate large portions and extending in laterally spacedrelacurrents and produce vigorous thermal circulation relatively close to the bottom of the bath.
jtion. A said last named portions being positioned with l2. An electric salt bath furnace comprising a their adjacent edges relatively close as compared plurality of electrodes for passing current through 5 with the distance between said downwardly ex# lthe bath and adapted to be connected to a source tending portions.
ofcurrent supply, said electrodes having portions WILLIAM WILSON. extending downwardly toward the bottom of the JOHN J. BRUTVAN.
bath and having portions connected to said ilrs't
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2570924A (en) * 1944-08-16 1951-10-09 Saint Gobain Method of producing phosphorus oxychloride

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2570924A (en) * 1944-08-16 1951-10-09 Saint Gobain Method of producing phosphorus oxychloride

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