US2311389A - Method and apparatus for handling asphalt - Google Patents
Method and apparatus for handling asphalt Download PDFInfo
- Publication number
- US2311389A US2311389A US404812A US40481241A US2311389A US 2311389 A US2311389 A US 2311389A US 404812 A US404812 A US 404812A US 40481241 A US40481241 A US 40481241A US 2311389 A US2311389 A US 2311389A
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- Prior art keywords
- asphalt
- water
- flume
- rod
- temperature
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Links
- 239000010426 asphalt Substances 0.000 title description 60
- 238000000034 method Methods 0.000 title description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 36
- 238000002844 melting Methods 0.000 description 7
- 230000008018 melting Effects 0.000 description 7
- 239000012530 fluid Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 4
- 241000272184 Falconiformes Species 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 241000612703 Augusta Species 0.000 description 1
- 230000001609 comparable effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000012809 cooling fluid Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
- C10C3/00—Working-up pitch, asphalt, bitumen
- C10C3/14—Solidifying, Disintegrating, e.g. granulating
- C10C3/16—Solidifying, Disintegrating, e.g. granulating by direct contact with liquids
Definitions
- This invention has for its object the provision of a method whereby high soft point asphalts may be processed into a finished product form of small dimensions, generallyfree from fines, ca-
- the invention is based upon the discovery that if hard asphalt, melted, but below a certain temperature limit, be fed in small streams upon a, rapidly but quietly flowing stream of water, that smooth walled rods of small dimension may be formed, and that these rods may be broken readily into short pieces, to give a small size asphalt product ready for final crushing and substantially free from fines.
- Figure 1 shows in diagrammatic section a side view of the apparatus used, in its simplest form. It consists of a sloping flume l0, some sixty or eighty feet long and aboutsix feet in width, at the upper end of which there is a water distributing chamber H into which water is discharged by pipe l2, with weir board l3 and flash board It serving to distribute th'at water into a rapidly flowing even sheet l5, passing down the flume at a rather rapid rate, but with a substantially undisturbed surface, i. e., with'out ripples of substantial size.
- the flash board I4 is preferably adjustable in order that flow of water may be controlled by regulating the clearance between the lower edge of the board and the bottom of the flume to compensate for other operating variables or adjust conditions to a particular operation.
- This asphalt distribution box is supplied with hot asphalt by insulatedpipe l8 and is provided upon its downstream side with a plurality of orifices l9, each about in diameter, from each of which a stream of asphalt 20 is deposited upon the flowing sheet .of water l5.
- Each asphalt stream so deposited forms a ribbon 2
- the e flume I'll is of sufiicient length that by the time the asphalt ribbon has arrived at its downstream end the heat of the asphalt is so reduced that asphalt particles in a pile, without further cooling, will not again melt” together. At this temperature, the rods are quite brittle, and, in falling with the water from the end of the flume, are broken into short rods 22.
- the general dimension of the asphalt pieces produced by this method, using the equipment shown, are about as follows: Section, oval; thickness about A,"; width, about A"; length about 1-2 inches; surface, smoothexcept for a few shrinkage wrinkles upon upper surface. Such a particle is shown, approximatelyfull size, in Figure 2.
- the asphalt pieces may conveniently be allowed to collect in a pile 23 in a drainage pit below the flume end, from which pile they may be removed from time to time, as by a power breakage of the rods, the downstream end of the flume may be somewhat constricted, to give a turbulence at this point, which may be seen clearly at 24 in Figure 3, which is a plan view (If the simple form of the device.
- This conveyor discharges to a loader 2B which places the finished material within a freight car 21.
- the flume should be so designed as to give a rapidly and quietly flowing sheet of water from about one to four inches in depth. In practice a fall of about one inch per foot has been found except as by such difiiculties as may be had in getting a uniform sheet of water and keeping it uniformly flowing until such time as the rods of asphalt may have hardened sufficiently so as not to cohere upon contact.
- the lineal velocity of the water sheet thus gotten will be from about 1 to about 2 feet per second. Distribution of the water may be gotten readily in flumes of usual width by the arrangement of overflow dam and inverted weir or fiashboard shown. Without the inverted weir or fiashboard, the water sheetwill tend to form a central ripple or wave longitudinal of the flume.
- the length of the flume is that necessary to cool the asphalt to such a point that the broken rods will not re-cohere when'piled together. This will depend somewhat, of course, upon the temperature of the asphalt and of the water. In general, with 70 water and about 400 asphalt, sixty or seventy feet of flume will be sufiicient. The length of -the flume depends to a large 'extent on the temperature of the water available.
- the asphalt handling equipment consists merely of a distributing box to which hot asphalt is discharged.
- This box may be steam jacketed or steam bottomed, to prevent cooling and deposition of asphalt therein. It must be placed close to the surface of the water sheet so that the falling streams of asphalt are not broken up.
- the streams of asphalt are produced by holes in the downstream side of the box.
- the streams should be large enough to not break up upon hitting the water, and sufliciently small to give a quickly cooled rod. I We have found diameter holes to be suitable. They should be closely spaced for space and water conservation, but far enough apart to prevent their streams from colliding after hitting the water. found 1 centers tobe convenient.
- the temperature of the asphalt should be of major im ortance in operating after this method. It should be heated sufficiently to be fluid, but should be below about 400 F. since at temperatures of the range and above it is hot enough to vaporize water on contact disrupting' the rod or at best giving a porous prod- The width is not-limited I We have not which cannot be dried effectively. With 240 F. soft point asphalt we have found a temperature of asphalt of about 375 F. to be satisfactory. This temperature, while always below 400 R, will vary somewhat for best operation, depending upon the hardness of the asphalt. With increase of temperature above the melting point, the rods tend to become smaller in cross section, due to decrease in fluid viscosity. This should be avoided by keeping temperature fairly low.
- Quantity tons/hour 10 Witnthis operation as above outlined, rodform asphalt, as described, may be continuously produced at a high commercial rate. With this operation only. a very minor loss in fines .is experienced, far less than in any crushing or bulk handling operation known to use. Due to the smooth skin of the rod-like fragment, very little difliculty is had with dewatering and drying, and the product is readily reduced below 3% total moisture.
- Apparatus for reducing molten asphalt to small pieces comprising means defining an elongated sloping fiuid channel sharply constricted transversely at the lower end thereof, fluid supply means to supply a smooth stream of cooling fiuid to the upper end of said channel, asphalt supply means below said fluid supply means to discharge upon said stream a plurality of horizontally spaced streams of molten asphalt, said channel being of suflicient length below said asphalt supply means to permit the molten asphalt to become brittle by cooling through heat exchange with said cooling fluid before the same reaches the constricted portion of the channel.
- the method of reducing fluid asphalt of high melting point to the form of small pieces comprising flowing the asphalt at a temperature above its melting point and below about 400 F. in a stream upon the surface of a smooth- 15 ly flowing stream of water to cool the asphalt and form a rod-like moving band of asphalt. continuing such flow of water with the asphalt on the surfacethereof as a rod to cool the rod to brittleness,-maintaining concurrent fiow of asphalt and water below the point at which the rod becomes brittle while sharply restricting the stream of water to thereby induce turbulence therein and break the rod intoshort lengths While retaining said asphalt on the surface of the water stream and separating water from the short rod-like pieces of asphaltafter such breaking.
Description
Feb. 16, 1943-. R. c. HAWKS ETAL 2,311,389
METHOD AND APPARATUS FOR HANDLING ASPHALT Filed July 31, .1941 2 Sheets-Sheet 1 Feb 16, 1943. 4 R. C. HAW KS ETAL. Y 2,311,389
METHOD AND APPARATUS FOR HANDLiNG ASPHALT Filed July 31, 1941 2 SheetsSheet 2 CON V5701? Patented Feb. 16, 1943 UNITED STATES PATENT OFFICE APPARATUS FbR HANDLING ASPHALT METHOD AND Robert O. Hawks and Emory M. Skinner, Augusta,
Kans., assignors to Socony-Vacuum Oil Company, Incorporated, New York, N. Y., a corporation of New York Application July 31, 1941, Serial No. 404,812
3 Claims. (01. 83-91) I of heavy paper containers into which the hot asphalt is poured has largely replaced this older practice. The paper containers must still be broken from the asphalt and disposed of, and many of the objections to the older form of package still obtain. Most users of high melting point asphalts pulverize the asphalt or at least reduce it to small sizes before melting down for use. The oldest method, that of allowing the asphalt to solidify in an open pit, or pitch-bay,.
breaking it into lumps, and shipping thoselumps still prevails, but is open to many objections. Partially crushing those lumps, for example to pass a 1%" grizzly, gives a product more nearly in the form desired by the usual purchaser, but due to the brittle nature of the asphalt, this crushing gives rise to a large percentage of fines, usually not acceptable to the purchaser, and the handling of the product is a dirty, inconvenient, and costly job.
This invention has for its object the provision of a method whereby high soft point asphalts may be processed into a finished product form of small dimensions, generallyfree from fines, ca-
pable of convenient handling in bulk form without undue further breakage.
The invention is based upon the discovery that if hard asphalt, melted, but below a certain temperature limit, be fed in small streams upon a, rapidly but quietly flowing stream of water, that smooth walled rods of small dimension may be formed, and that these rods may be broken readily into short pieces, to give a small size asphalt product ready for final crushing and substantially free from fines.
In order to understand this invention, reference is now made to the drawings attached hereto.
In the drawings, Figure 1 shows in diagrammatic section a side view of the apparatus used, in its simplest form. It consists of a sloping flume l0, some sixty or eighty feet long and aboutsix feet in width, at the upper end of which there is a water distributing chamber H into which water is discharged by pipe l2, with weir board l3 and flash board It serving to distribute th'at water into a rapidly flowing even sheet l5, passing down the flume at a rather rapid rate, but with a substantially undisturbed surface, i. e., with'out ripples of substantial size. The flash board I4 is preferably adjustable in order that flow of water may be controlled by regulating the clearance between the lower edge of the board and the bottom of the flume to compensate for other operating variables or adjust conditions to a particular operation. Downstream from the water box I I there is an asphalt distributor box l6, having a double bottom H, which serves as a steam chest for heat control purposes. This asphalt distribution box is supplied with hot asphalt by insulatedpipe l8 and is provided upon its downstream side with a plurality of orifices l9, each about in diameter, from each of which a stream of asphalt 20 is deposited upon the flowing sheet .of water l5.
Each asphalt stream so deposited forms a ribbon 2| upon the surface of the water, and as it moves forward is chilled thereby, first forming a smooth outer skin and then solidifying internally. The e flume I'll is of sufiicient length that by the time the asphalt ribbon has arrived at its downstream end the heat of the asphalt is so reduced that asphalt particles in a pile, without further cooling, will not again melt" together. At this temperature, the rods are quite brittle, and, in falling with the water from the end of the flume, are broken into short rods 22. The general dimension of the asphalt pieces produced by this method, using the equipment shown, are about as follows: Section, oval; thickness about A,"; width, about A"; length about 1-2 inches; surface, smoothexcept for a few shrinkage wrinkles upon upper surface. Such a particle is shown, approximatelyfull size, in Figure 2. Returning to Figure 1, at the downstream end of the flume I 0, the asphalt pieces may conveniently be allowed to collect in a pile 23 in a drainage pit below the flume end, from which pile they may be removed from time to time, as by a power breakage of the rods, the downstream end of the flume may be somewhat constricted, to give a turbulence at this point, which may be seen clearly at 24 in Figure 3, which is a plan view (If the simple form of the device.
In commercial practice, this development perto be quite acceptacle.
if desired, with air blasts near its discharge end to completely dry the product. This conveyor discharges to a loader 2B which places the finished material within a freight car 21.
Certain limitations prevail in the design of the apparatus and in its operation to accomplish the method.
The flume, should be so designed as to give a rapidly and quietly flowing sheet of water from about one to four inches in depth. In practice a fall of about one inch per foot has been found except as by such difiiculties as may be had in getting a uniform sheet of water and keeping it uniformly flowing until such time as the rods of asphalt may have hardened sufficiently so as not to cohere upon contact. The lineal velocity of the water sheet thus gotten will be from about 1 to about 2 feet per second. Distribution of the water may be gotten readily in flumes of usual width by the arrangement of overflow dam and inverted weir or fiashboard shown. Without the inverted weir or fiashboard, the water sheetwill tend to form a central ripple or wave longitudinal of the flume. width, having a grade of one inch per foot, handling 500 gallons per minute of water; is found to provide a satisfactory watesrwsheet. The length of the flume is that necessary to cool the asphalt to such a point that the broken rods will not re-cohere when'piled together. This will depend somewhat, of course, upon the temperature of the asphalt and of the water. In general, with 70 water and about 400 asphalt, sixty or seventy feet of flume will be sufiicient. The length of -the flume depends to a large 'extent on the temperature of the water available.
Thus comparable effects may be obtained with warmer water by using a longer flume. The constriction at the end of the flume is optional but advisable. A six foot flume may be conveniently constricted to four feet of width.
The asphalt handling equipment consists merely of a distributing box to which hot asphalt is discharged. This box may be steam jacketed or steam bottomed, to prevent cooling and deposition of asphalt therein. It must be placed close to the surface of the water sheet so that the falling streams of asphalt are not broken up. The streams of asphalt are produced by holes in the downstream side of the box. The streams should be large enough to not break up upon hitting the water, and sufliciently small to give a quickly cooled rod. I We have found diameter holes to be suitable. They should be closely spaced for space and water conservation, but far enough apart to prevent their streams from colliding after hitting the water. found 1 centers tobe convenient.
We have found the temperature of the asphalt to be of major im ortance in operating after this method. It should be heated sufficiently to be fluid, but should be below about 400 F. since at temperatures of the range and above it is hot enough to vaporize water on contact disrupting' the rod or at best giving a porous prod- The width is not-limited I We have not which cannot be dried effectively. With 240 F. soft point asphalt we have found a temperature of asphalt of about 375 F. to be satisfactory. This temperature, while always below 400 R, will vary somewhat for best operation, depending upon the hardness of the asphalt. With increase of temperature above the melting point, the rods tend to become smaller in cross section, due to decrease in fluid viscosity. This should be avoided by keeping temperature fairly low.
Conditions: i. e. asphalt inlet temperature, water temperature, and flume length; should be so controlled as to give an asphalt sufficiently cooled so that the pieces will not re-cohere from softening due to internal heat after discharge. This will also vary somewhat with the hardness of the asphalt, with a final asphalt temperature of about 125-150 F. for 240 F. soft point asphalt being sufiicient. From this standpoint the use of the dewatering conveyor in a set up such as Figure 4 is preferable to the piling of A flume-six feet in pieces shown in Figure 1, for the asphalt pieces can be further cooled completely on such conveyor.
Operating and construction details upon a commercial equipment are of interest.
Flume:
Width 6'0" Length 60'0" Width at constricted end 4'-0" Grade l" per 12" Water:
Quantity 500 g. p, m. Temperture-in F. Temperatureout 83 F.
Lineal velocity ft. 'second 1.1 to 1.6 Asphalt:
Grade 240 F. soft point (R. & B.) Temperaturein 378 F.
Quantity tons/hour 10 Witnthis operation, as above outlined, rodform asphalt, as described, may be continuously produced at a high commercial rate. With this operation only. a very minor loss in fines .is experienced, far less than in any crushing or bulk handling operation known to use. Due to the smooth skin of the rod-like fragment, very little difliculty is had with dewatering and drying, and the product is readily reduced below 3% total moisture.
We claim:
1. Apparatus for reducing molten asphalt to small pieces comprising means defining an elongated sloping fiuid channel sharply constricted transversely at the lower end thereof, fluid supply means to supply a smooth stream of cooling fiuid to the upper end of said channel, asphalt supply means below said fluid supply means to discharge upon said stream a plurality of horizontally spaced streams of molten asphalt, said channel being of suflicient length below said asphalt supply means to permit the molten asphalt to become brittle by cooling through heat exchange with said cooling fluid before the same reaches the constricted portion of the channel.
2. The method of reducing fluid asphalt of high melting point to the form of small pieces comprising flowing the asphalt at a temperature above its melting point and below about 400 F.
form a rod-like moving band of asphalt, ,continuing such flow of water with the asphalt on the surface thereof as a rod to cool the rod ,to brittleness, inducing turbulent flow of the stream of water below the point at which the rod becomes brittle to thereby break the rod. into short lengths while retaining said asphalt on the surface of the water stream and separating water from the short rod-like pieces of asphalt after such breaking.
3. The method of reducing fluid asphalt of high melting point to the form of small pieces comprising flowing the asphalt at a temperature above its melting point and below about 400 F. in a stream upon the surface of a smooth- 15 ly flowing stream of water to cool the asphalt and form a rod-like moving band of asphalt. continuing such flow of water with the asphalt on the surfacethereof as a rod to cool the rod to brittleness,-maintaining concurrent fiow of asphalt and water below the point at which the rod becomes brittle while sharply restricting the stream of water to thereby induce turbulence therein and break the rod intoshort lengths While retaining said asphalt on the surface of the water stream and separating water from the short rod-like pieces of asphaltafter such breaking.
ROBERT C. HAWKS.
EMORY M. SKINNER.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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US404812A US2311389A (en) | 1941-07-31 | 1941-07-31 | Method and apparatus for handling asphalt |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US404812A US2311389A (en) | 1941-07-31 | 1941-07-31 | Method and apparatus for handling asphalt |
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US2311389A true US2311389A (en) | 1943-02-16 |
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US404812A Expired - Lifetime US2311389A (en) | 1941-07-31 | 1941-07-31 | Method and apparatus for handling asphalt |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2543069A (en) * | 1946-12-21 | 1951-02-27 | Houdry Process Corp | Art of preparing gel |
US2550838A (en) * | 1944-08-03 | 1951-05-01 | Union Chimique Belge Sa | Process for making granulated pitch |
US2562149A (en) * | 1947-04-17 | 1951-07-24 | Gilman B Mollring | Asphalt pelletizer |
US2634098A (en) * | 1948-02-28 | 1953-04-07 | Arthur L Armentrout | Means and method of recovering lost circulation in drilling wells |
US3046606A (en) * | 1959-07-29 | 1962-07-31 | Eastman Kodak Co | Process for producing solid non-porous pellets from polyolefins and pellets produced thereby |
US3988085A (en) * | 1975-11-24 | 1976-10-26 | Krchma Ludwig C | Apparatus for forming uniform shaped particles of thermoplastic material |
FR2549847A1 (en) * | 1983-07-29 | 1985-02-01 | Elf France | Process and device for the manufacture of granulates from at least one liquefied solid |
US6592350B1 (en) * | 1999-03-23 | 2003-07-15 | Berstorff Gmbh | Underwater pelletizer with separator |
-
1941
- 1941-07-31 US US404812A patent/US2311389A/en not_active Expired - Lifetime
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2550838A (en) * | 1944-08-03 | 1951-05-01 | Union Chimique Belge Sa | Process for making granulated pitch |
US2543069A (en) * | 1946-12-21 | 1951-02-27 | Houdry Process Corp | Art of preparing gel |
US2562149A (en) * | 1947-04-17 | 1951-07-24 | Gilman B Mollring | Asphalt pelletizer |
US2634098A (en) * | 1948-02-28 | 1953-04-07 | Arthur L Armentrout | Means and method of recovering lost circulation in drilling wells |
US3046606A (en) * | 1959-07-29 | 1962-07-31 | Eastman Kodak Co | Process for producing solid non-porous pellets from polyolefins and pellets produced thereby |
US3988085A (en) * | 1975-11-24 | 1976-10-26 | Krchma Ludwig C | Apparatus for forming uniform shaped particles of thermoplastic material |
FR2549847A1 (en) * | 1983-07-29 | 1985-02-01 | Elf France | Process and device for the manufacture of granulates from at least one liquefied solid |
US6592350B1 (en) * | 1999-03-23 | 2003-07-15 | Berstorff Gmbh | Underwater pelletizer with separator |
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