US22590A - Improvement in defecating and clarifying cane-juice - Google Patents

Improvement in defecating and clarifying cane-juice Download PDF

Info

Publication number
US22590A
US22590A US22590DA US22590A US 22590 A US22590 A US 22590A US 22590D A US22590D A US 22590DA US 22590 A US22590 A US 22590A
Authority
US
United States
Prior art keywords
juice
improvement
defecating
cane
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
Publication date
Application granted granted Critical
Publication of US22590A publication Critical patent/US22590A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C13SUGAR INDUSTRY
    • C13BPRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00Purification of sugar juices
    • C13B20/02Purification of sugar juices using alkaline earth metal compounds
    • C13B20/04Purification of sugar juices using alkaline earth metal compounds followed by saturation
    • C13B20/06Purification of sugar juices using alkaline earth metal compounds followed by saturation with carbon dioxide or sulfur dioxide

Definitions

  • I fab-6732f wg fl /ZMM N. PETERS. Phowumn m hu. Washin uh.
  • My invention or improvement consists in passing or disseminating in any convenient manner throughout the saccharine matter sulphurous acid or gas produced by a slow con1- bustion, in a nearly closed retort, of sulphur or common roll brimstone.
  • This cylinder may be lined partially or wholly with any substance upon which the burning sulphur will not act. At one end of this retort there is an opening to admit the sulphur, having a door or stopper and a small perforation, asay one inch diameter-capable of adjustment for the slow admission of air. At the other end there is an opening-say four inches diameter-communicating with a pipe, I, of similar diameter, the other extremity of the pipe P communicating with an air-tight vessel of water, XV, and its end may dip downward into the water a short distance; and, if thought desirable, there may be another similar vessel of water connected with the first by a pipe of similar diameter opening into each above the water-line.
  • Thescwater-vessels may bethesize of a common barrel. From the water-vessels there is a pipe, P about four inches diameter, extending to the upper end of a vertical air-tight cylinder,V, which I term the vacuum-cylinder, about ten feet high by three feet diameter, and this vacuum-cylinder communicating at its lower end with the top of the steam-boilers B by a pipe, P say two inches diameter-and with the receiver of the cane-juice by another pipe, P, at its upper end.
  • the tubes in the bottom of said receiver have small perforations on their upper sides,
  • the operation is as follows, viz: The brin1- stone pulverized I spread from end to end along the bottom of the retort a, and ignite it at the end nearest the pipe P.
  • the admission of air being very slow, sulphurous gas or acid is constantly produced, with, perhaps, a small quantity of sulphuric acid, all of which remains in the retort until allowed to pass forward.
  • lVhen it is allowed to pass forward to the vacuum-cylinder, it passes first through the water-vessel ⁇ V, when any sulphuric acid which may have been formed in the retort will be principally absorbed.
  • the juice-receiver is filled with cane-juice.
  • the stop-cocks c and c are opened, whereby the steam passes into the vacuum-cylinder, expelling the air there from.
  • the cocks c and c are then closed, and the condensation of the steam in the vacuumcylinder produces a partial vacuum therein.
  • the stop-cock c is then opened, and the sulphurous gas passes forward to fill the vacuum-cylinder.
  • the stop-cock c is then closed and c and c are opened, when the steam rushes into the vacuum-cylinder, forces the sulphur ous gas therein through the pipe P and perforated pipes throughout the cane-j nice in the receiver.
  • jets of cold water may be used in the vacuumchamher.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Treating Waste Gases (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Description

R. A. STEWART.
Defecating and Clarifying Saccharine vLiquids. No. 22,590. Patented Jan. 11, I859.
I fab-6732f: wg fl /ZMM N. PETERS. Phowumn m hu. Washin uh.
NiTnn STATES PATENT @rrrcn.
RICHARD A. STEWVART, OF ST. BERNARD PARISH, LOUISIANA.
IMPROVEMENT IN DEFECATING AND CLARlFYING CANE-JUICE.
Specificationforming part of Letters Patent No. 5225590, dated January 11, 1839.
T0 at whom it may concern.-
Be it known that I, RICHARD A. STEWART, of the parish of St. Bernard and State of Louisiana, have invented a new and useful improvement in the defecation and clarification of cane-juice, sirup, molasses, and saccharine matter generally, when in a liquid. or semiliqnid state, of which the following is a speciiication.
My invention or improvement consists in passing or disseminating in any convenient manner throughout the saccharine matter sulphurous acid or gas produced by a slow con1- bustion, in a nearly closed retort, of sulphur or common roll brimstone. There are obviously various modes of producing this gas and of disseminating it through thesaceharine liquid, all of which are useful and will involve the principle or character of my invention, and I leave to all the adoption of such of the obvious modes of effecting the object as may be preferred; but the means I have assayed and found to produce the most satisfactory results, defecating and clarifying the saccharine liquid as perfectly and more economically than I have ever before seen it in the manufacture of sugar, is as follows: I use a horizontal air-tight cylindrical retort, rsay twelve feet long and three feet diameter-made of iron, references being had to the drawing hereto annexed, and making a part hereof. This cylinder may be lined partially or wholly with any substance upon which the burning sulphur will not act. At one end of this retort there is an opening to admit the sulphur, having a door or stopper and a small perforation, asay one inch diameter-capable of adjustment for the slow admission of air. At the other end there is an opening-say four inches diameter-communicating with a pipe, I, of similar diameter, the other extremity of the pipe P communicating with an air-tight vessel of water, XV, and its end may dip downward into the water a short distance; and, if thought desirable, there may be another similar vessel of water connected with the first by a pipe of similar diameter opening into each above the water-line. Thescwater-vesselsmay bethesize of a common barrel. From the water-vessels there is a pipe, P about four inches diameter, extending to the upper end of a vertical air-tight cylinder,V, which I term the vacuum-cylinder, about ten feet high by three feet diameter, and this vacuum-cylinder communicating at its lower end with the top of the steam-boilers B by a pipe, P say two inches diameter-and with the receiver of the cane-juice by another pipe, P, at its upper end. The tubes in the bottom of said receiver have small perforations on their upper sides,
and such perforations being numerous to dis tribute the discharge from the pipe uniformly throughout the juice. The pipe from the top of the vacuum-cylinder, leading to the perforated tubes in the bottom of the juice-receiver, should rise above the receiver and lead downward.
The operation is as follows, viz: The brin1- stone pulverized I spread from end to end along the bottom of the retort a, and ignite it at the end nearest the pipe P. The admission of air being very slow, sulphurous gas or acid is constantly produced, with, perhaps, a small quantity of sulphuric acid, all of which remains in the retort until allowed to pass forward. lVhen it is allowed to pass forward to the vacuum-cylinder, it passes first through the water-vessel \V, when any sulphuric acid which may have been formed in the retort will be principally absorbed. The juice-receiver is filled with cane-juice. The stop-cocks c and c are opened, whereby the steam passes into the vacuum-cylinder, expelling the air there from. The cocks c and c are then closed, and the condensation of the steam in the vacuumcylinder produces a partial vacuum therein. The stop-cock c is then opened, and the sulphurous gas passes forward to fill the vacuum-cylinder. The stop-cock c is then closed and c and c are opened, when the steam rushes into the vacuum-cylinder, forces the sulphur ous gas therein through the pipe P and perforated pipes throughout the cane-j nice in the receiver. I prefer to pass the sulphurousgas through the cane-juice; but it may be beneficially introduced in more advanced stages of the process of making sugar. I sometimes pass two or three successive charges of the gas through the saccharine liquid, which is accomplished in a few minutes and at an expense of but few cents to the hogshead of sugar.
To render the vacuum more perfect, jets of cold water may be used in the vacuumchamher.
My improvement entirely dispenses with the necessity of using either bone-black or bisulwhat I claim as new in the defecation and phate of lime in the process of clarifying and clarification of cane-juice and other liquid or defecating. semi-liquid forms of saccharine matter, is
The apparatus I have described is suffieient Disseminating throughout the same sulphurfor the largest sugar-house. ous gas or sulphurous-acid gas, for the pur I Having fully madeknown the nature of my poses herein set forth. improvement and the manner in which I have reduced the same to practice, I do not claim, W'itnesses: broadly, the use of sulphurous gas or sulphur- C. II. DAVIS, ous-aeid gas in the manufacture of sugar; but I OHS. G. ALLEN,
RICHARD A. STEWART.
US22590D Improvement in defecating and clarifying cane-juice Expired - Lifetime US22590A (en)

Publications (1)

Publication Number Publication Date
US22590A true US22590A (en) 1859-01-11

Family

ID=2089257

Family Applications (1)

Application Number Title Priority Date Filing Date
US22590D Expired - Lifetime US22590A (en) Improvement in defecating and clarifying cane-juice

Country Status (1)

Country Link
US (1) US22590A (en)

Similar Documents

Publication Publication Date Title
US26401A (en) Improved mode of
US22590A (en) Improvement in defecating and clarifying cane-juice
CN101660007A (en) Low-carbon and low-sulphur syrup clarifying method
Spencer A handbook for cane-sugar manufacturers and their chemists
US963275A (en) Manufacture of alcohol and by-products and apparatus therefor.
US66377A (en) Theodtjle moiullon and uesin naqtjin
US135014A (en) Improvement in treating sugar with sulphurous acid in the vacuum-pan
US66370A (en) Fbanz
US33086A (en) Improvement in apparatus for treating cane-juice with sulphurous-acid gas
US41999A (en) Improved apparatus for preventing the loss of sugar during evaporation
US880629A (en) Method of crystallizing sugar.
Maxwell Sulphitation in white sugar manufacture
US264A (en) Apparatus ob machinery employed in the manufacture of carbonate of
US107158A (en) Improvement in the manufacture of albumen
US250824A (en) Mode of making sugar
US3256A (en) Improvement in disti lling alcohol
US95958A (en) Improved apparatus for evaporating- liquids to obtain sugar
AT159139B (en) Device for continuous or interrupted saturation of sugar juices.
US6626A (en) Gas apparatus
US4108A (en) Improvement in making sugar
US62715A (en) Improved apparatus for making vinegar
TEWODROS OPTIMIZATION OF CHEMICALS ON JUICE CLARIFICATION TO REDUCE SUCROSE LOSSES AND SCALE FORMATION: THE CASE OF METEHARA SUGAR FACTORY
SU105542A1 (en) The method of controlling the alkalinity of beet juice being grated and the device for its implementation
TESFAYE OPTIMIZATION OF CHEMICALS ON JUICE CLARIFICATION TO REDUCE SUCROSE LOSSES AND SCALE FORMATION
US108514A (en) Improvement in the manufacture of sugar