US2218586A - Manufacture of a basis for face powder - Google Patents

Manufacture of a basis for face powder Download PDF

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Publication number
US2218586A
US2218586A US221360A US22136038A US2218586A US 2218586 A US2218586 A US 2218586A US 221360 A US221360 A US 221360A US 22136038 A US22136038 A US 22136038A US 2218586 A US2218586 A US 2218586A
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US
United States
Prior art keywords
basis
talc
zinc
face powder
manufacture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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US221360A
Inventor
Quaedvlieg Matthias
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Winthrop Chemical Co Inc
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Winthrop Chemical Co Inc
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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/27Zinc; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing

Definitions

  • This invention relates to the manufacture of bases for face powder by treating talc and similar earthy materials with a suitable fatty acid salt in molten or dissolved state. It has been found that in this manner the outstanding properties of the aforesaid fatty acid salts may be imparted to talc, kaolin, china clay or the like when the zinc, strontium and magnesium salts of higher fatty acids are used.
  • a soluble metal salt for instance zinc chloride, magnesium sulfate or the like.
  • a better basis for face powder is obtained by treating 30 tale with zinc stearate or strontium undecanate in a suitable organic solvent, for instance, carbon tetrachloride, xylene, chlorobenzene or the like, if desired at a raised temperature.
  • a suitable organic solvent for instance, carbon tetrachloride, xylene, chlorobenzene or the like.
  • Example 1 Into a solution of 20 parts of zinc stearate in 100 parts by weight of xylene are introdnced at 120 C. 100 parts of talc, and the whole is allowed to cool while stirring, then fil- 45 tered and the solid matter dried.
  • the process for improving the covering power of talc powder when used as a basis for face powder which comprises treating the tale with a fatty acid metal saltv of the group consisting of zinc-, strontium-, and aluminium salts of fatty acids containing at least 10 carbon atoms said fatty acid metalsalt being in the liquid phase.
  • the process for improving the covering power of' talc powder when used as a basis for face powder which comprises treating the tale powder with a solution of a fatty acid metal salt of the group consisting of zinc-, strontium-, and aluminium salts of fatty acids containing at least 10 carbon atoms, and evaporating the solvent.
  • the process for improving the covering power 40 of talc powder when used as a basis for face powder which comprises treating'the talc powder with a melt of a fatty acid metal salt of the group consisting of zinc-, strontium-, and aluminium salts of fatty acids containing at least 10 carbon atoms.

Description

' Patented Oct. 22, 1940 UNITED," STATES MANUFACTURE or A BASIS FOB FACE rownsn 'Mattl iias Quaedvlieg, Dessau in Anhalt, Germany,
assignor to.
Winthrop Chemical Company, Inc.,
New York, N. Y., a corporation of New York No Drawing. Application July 26, 1938, Serial No. 221,360. In Germany August 26, 1937 sciaims. (01. 167-92) As a basis for-face powder there have been used the zinc, strontium and aluminium salts of fatty acids of high molecular weight, for instance stearic acid and undecanic acid, also the fatty acid salts described in U. S. A. specification No. 1,995,663.- They have a good covering power, are strongly adherent and can be well rubbed in. As an extender for these-highly valuable materials talc and like earthy materials have long been used; these, however, possess in very low degree the good properties of the aforesaid fatty Y acid salts, apart from their capacity for being rubbed in.
This invention relates to the manufacture of bases for face powder by treating talc and similar earthy materials with a suitable fatty acid salt in molten or dissolved state. It has been found that in this manner the outstanding properties of the aforesaid fatty acid salts may be imparted to talc, kaolin, china clay or the like when the zinc, strontium and magnesium salts of higher fatty acids are used. When an aqueous solution is used, the talc, for example, is suspended in the 25 aqueous alkali soap solution and the insoluble metal salt is precipitated on the talc by adding a soluble metal salt, for instance zinc chloride, magnesium sulfate or the like. However, a better basis for face powder is obtained by treating 30 tale with zinc stearate or strontium undecanate in a suitable organic solvent, for instance, carbon tetrachloride, xylene, chlorobenzene or the like, if desired at a raised temperature. Talc thus treated has animproved covering power, a re-' 35 markable adherence and far excels a mechani cally made mixture of talc with zinc stearate for instance.
The following examples illustrate the invention: 1
40 Example 1.Into a solution of 20 parts of zinc stearate in 100 parts by weight of xylene are introdnced at 120 C. 100 parts of talc, and the whole is allowed to cool while stirring, then fil- 45 tered and the solid matter dried.
. mixed:
For making a high class powder there are Parts Talc treated as above '70 Titanium dioxide 3 Zinc oxide 20 Calcium carbonate 2 5 Magnesium carbonate 5 Example 2.-100 parts of talc are thoroughly stirred into a solution of 20 parts of sodium undecanate and 0.5 part of a preparation which is a condensation product of hydroxy-alkyl amine m with a higher organic'acid made as described in Canadian Patent No. 313,993 which corresponds with U. S. A. application Serial No. 340,015, filed February 14, 1929, by Ulrich and Nuesslein.
There is then run in gradually at 90 C. a solution of 6.6 parts of zinc chloride in.15o parts of water, the whole is stirred for a short time, filtered and the solid matter washed and dried.
In theforegoing examples use is made of zinc stearate and zinc undecanate. In the same manner the corresponding strontium or aluminium salts'of the said acids or the zinc, strontium or aluminium salts of any fatty acid having at least 10 carbon atoms in its molecule, may be used.
What I claim is:
1. The process for improving the covering power of talc powder when used as a basis for face powder which comprises treating the tale with a fatty acid metal saltv of the group consisting of zinc-, strontium-, and aluminium salts of fatty acids containing at least 10 carbon atoms said fatty acid metalsalt being in the liquid phase.
2. The process for improving the covering power of' talc powder when used as a basis for face powder which comprises treating the tale powder with a solution of a fatty acid metal salt of the group consisting of zinc-, strontium-, and aluminium salts of fatty acids containing at least 10 carbon atoms, and evaporating the solvent.
3. The process for improving the covering power 40 of talc powder when used as a basis for face powder which comprises treating'the talc powder with a melt of a fatty acid metal salt of the group consisting of zinc-, strontium-, and aluminium salts of fatty acids containing at least 10 carbon atoms.
, MATIHIAS QUAEDVHEG.
US221360A 1937-08-26 1938-07-26 Manufacture of a basis for face powder Expired - Lifetime US2218586A (en)

Applications Claiming Priority (1)

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DE2218586X 1937-08-26

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3033692A (en) * 1959-10-08 1962-05-08 Robert F Herrling Composition for providing an effective water-vapor barrier on postage stamps and other adhesive surfaces
FR2423216A1 (en) * 1978-04-19 1979-11-16 Ducam Gilbert Hand drying compsn. - comprising resinous sawdust, colophony and magnesium carbonate
US4605553A (en) * 1983-01-31 1986-08-12 Peter Passalacqua Dry pressed powder stick composition and vehicle therefor

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3033692A (en) * 1959-10-08 1962-05-08 Robert F Herrling Composition for providing an effective water-vapor barrier on postage stamps and other adhesive surfaces
FR2423216A1 (en) * 1978-04-19 1979-11-16 Ducam Gilbert Hand drying compsn. - comprising resinous sawdust, colophony and magnesium carbonate
US4605553A (en) * 1983-01-31 1986-08-12 Peter Passalacqua Dry pressed powder stick composition and vehicle therefor

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