US2167028A - Condenser - Google Patents

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US2167028A
US2167028A US39263A US3926335A US2167028A US 2167028 A US2167028 A US 2167028A US 39263 A US39263 A US 39263A US 3926335 A US3926335 A US 3926335A US 2167028 A US2167028 A US 2167028A
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condenser
section
column
vapors
tubes
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Expired - Lifetime
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US39263A
Inventor
Frank J Mcgovern
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CB&I Technology Inc
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Lummus Co
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033Other features
    • B01D5/0045Vacuum condensation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0003Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
    • B01D5/0009Horizontal tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033Other features
    • B01D5/0048Barometric condensation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • B01D5/0063Reflux condensation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0078Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
    • B01D5/0093Removing and treatment of non condensable gases
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T74/00Machine element or mechanism
    • Y10T74/19Gearing
    • Y10T74/19642Directly cooperating gears
    • Y10T74/19698Spiral
    • Y10T74/19828Worm

Definitions

  • the present invention relates to condensers and more particularly to condensers for condensing oil vapors distilled under vacuum.
  • the principal objects of the present invention are to provide a condenser associated with a vacuum distilling column and requiring a minimum of structural support, to provide a condenser opposing a minimum of resistance between the distilling column and the evacuating system, to provide for eifective separation and collection of entrainment in steam distillation, and also to provide means for simple and effective cleaning of the condenser tubes.
  • the present invention comprises the apparatus hereinafter described and particularly defined in the claims.
  • Fig. 1 is a sectional elevation of one form of the present invention
  • Fig. 2 is a sectional elevation on line 2-2 of Fig. 1
  • Fig. 2a' is a section on line 2a.2a of Fig. 2, showing the arrangement of the shell and partitions, the condenser section being removed
  • Fig. 3 is a sectional elevation of a modified form of the invention.
  • the apparatus shown in Figs. 1 and 2 comprises ashell 6 having boiling cap decks of any suitable form.
  • reflux liquid is introduced on the top deck by a pipe 8.
  • the shell is provided with rectangular openings to receive the tubes of the condenser sections l0 and I2.
  • the condenser sections are enclosed between vertical partitions l4 and Hi, a space l8 being provided between the sections for access to the tubes.
  • the space I8 is enclosed by removable cover. plates 20.
  • Angles 22 and 24 extending across the column serve as supports for the condenser sections during insertion or removal.
  • the partition l6 is formed at the bottom with a semi-circular collecting pan which is covered with any suitable insulating material 26.
  • the condenser tubes of the section H) are connected with headers 28 and 30, the former having connections 32 for circulating the cooling fluid.
  • the tubes of the section 2 are similarly connected into headers 34 and 36', of which the former has the cooling liquid connections 38.
  • Thepartition walls l4 and I6 together with parts of the shell 6 form bifurcated vapor conduits 39 around the condenser section so that vapors of steam and oil rising from above the boiling cap decks pass around the condenser section as indicated by the arrows in Figure '1.
  • the vapors then combine in the vapor collecting section Go from which the vapors pass downward through the opening into the condenser section across the tube bundles.
  • the condensing action is particularly eificient because of the uniform cross-section presented to the vapor flow, whereby maximum contact of vapors with previously condensed liquid is effected.
  • the condensate collects in the semi-circular. portion of the partition l6 and is withdrawn by a pipe 40.
  • vapors comprising primarily steam with some oil pass under a semi-cylindrical baflie 42 which is supported by brackets 44 depending from the angles 24.
  • the baffle 42 is formed along its sides with upwardly facing channels 46 serving to catch some of the entrained drops of oil which would otherwise pass under the baflle. Since the baflle is inclined, as shown in Fig. 2, the entrainment flows into the semi-circular pan.
  • the vapors continue, as indicated by the arrow in Fig. 2, into a cylindrical outlet 48 which is disposed within the baille 42.
  • the outlet 48 is partially closed at the end by a baflle plate 50 and is provided with an opening part-way along the top, as indicated at 52.
  • the tortuous course of the vapors in passing from the condenser tubes around the end and bottom of the bafiie 42 and over the bafiie plate 50 into the outlet pipe 48 serves to prevent passage of a considerable part of the entrainment with the steam.
  • the outlet pipe 48 leads into a final entrainment separator 54 consisting of a vertical cage with vertical baflie plates 56 of any suitable form.
  • the baflle plates serve to separate any remnant of entrained oil, which is withdrawn from the bottom of the cage by a pipe 58.
  • the outlet pipe then leads into the usual barometric condenser 60 and vacuum jet system 6
  • the present invention contemplates a simple method of cleaning the condenser tubes.
  • valves in the draw-off lines 40, 58, etc. are closed. and a cleaning solution is introduced around the tubes by means of a pipe 66. If hot cleaning solution is required, steam" is introduced in.-
  • the cleaning solution may be brought' to the boiling point.
  • the solution may be removed from the system by opening the valve in the draw-01f line 40.
  • the apparatus shown in Fig. 3 is similar to that previously described;
  • the condenser tube bundles I0 and I2 are supported in the shell.
  • the uncondensed upper tube bundle I0 is enclosed between partitions H but the lower tube bundle is enclosed between a short partition 10 on one side and an angle partition I2 on the other side, the latter extending to a point considerably below the tube bundle and having a horizontal pan 14 extending into the shell.
  • the column 6 is similarly bifurcated with the vapor conduit passages 38 and 39a formed by the wall 12 and the shell on one side, and the partitions I4 and 10 and the shell on the other side.
  • the vapors pass from the boiling cap section upwardly through the conduit 39 at the left of the condensers, into the vapor collecting chamber 6a, thence downwardly through the condensers, and upwardly through the other bifurcated vapor space 39a at the right of the condensers, and finally out through an outlet pipe 18.
  • the condensate drops on the partition 14 which serves as a collecting pan and is withdrawn by a pipe 80.
  • entrainment catching ballles 82 are provided, these being formed with hooked edges to free the steam vapors of withdrawn oil.
  • the bailles 82 are preferably inclined to direct the entrainment into the pan.
  • the outlet 18 leads into the barometric condenser 82 and vacuum jet equipment 84, as in the previously described construction.
  • the external apparatus is mounted on a bracket 86 identical with that shown in Fig. 2.
  • Cleaning of the'tubes may be effected by introducing cleaning fluid through the pipe 66, as in the construction of Figs. 1 and 2.
  • the present invention provides a condensing and evacuating system, of which the major portion of the weight is supported centrally of the column itself.
  • the rectangular cross-section of The invention having been thus described, wha
  • the horizontal pan l4 and the vertical partitions at the left side of the con- 3. The combination with a column having a distilling section, of a condenser having tubes in the upper part ofthe column, a partition forming a. vapor. space leading from the distilling section to the top of the condenser, a condensate pan below the condenser, a bailie between the condenser and the pan, and an outlet ,below the baflie.
  • a condenser comprising a bundle of horizontal tubes extending across the upper part of the column, fixed partitions extending completely across the column alongside the tube bundle and forming vapor spaces between the tube bundle and the column wall whereby vapors from the distilling section are directed to the top of the condenser, a condensate pan below the condenser and connected with at least one of the partitions, headers for the tube bundle, and means for removablysupporting the tube bundle and headers independently of the partitions and condensate pan.
  • a condenser comprising a bundle of horizontal tubes of generally rectangular cross-section extending across the upper part of the column, fixed vertical partitions extending completely across the column alongside the tube bundle and forming vapor spaces between the tube bundle and the column wall whereby vapors from the distilling section are directed to the top of the condenser, a condensate pan below the condenser and connected with at least one -of the partitions, headers for the tube bundle,
  • a column having. a distilling section, a bifurcated vapor section, and a vapor collecting section in communication with the distilling sec-' tion through a part of said bifurcated vapor section, means to close off another part of the bifurcated vapor section from direct communication with the distilling section, a condenser chamber between the walls of. the bifurcated vapor section with walls in common, said condenser chamber receiving vapors from said vapor collecting section, means to condense vapors in the condenser chamber and means to remove uncondensed vapors through another part of said bifurcated vapor section.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

July 25, 1939. F. J. McGOVERN CONDENSER Original Filed Sept. 5, 1935 2 Sheets-Sheet 1 o o o o o F 0 0 0 0 0 0 o o o o I 0 0 0 0 0 0 0 0 0 0 MM 1 v o o o d u 0 0 0 0 1 L o o o o o l o o o o 0 0 0 0 0 0 0 o o o o n i/ifneau MW July 25, 1939. F. J. MQGOVERN 2,167,028
' CONDENSER Original Filed Sept. 5, 1955 2 Sheets-Sheet 2 I o o o o o o o o o z o o o o Patented July 25, 1939 PATENT OFFICE.
f 2,167,028 CONDENSER.
Frank J. McGovern, Forest Hills, N. Y., assignor to The Lummus Company, New York, N. Y., a corporation of Delaware Application September 5, 1935, Serial No. 39,263 Renewed May 14, 1938 8 Claims.
The present invention relates to condensers and more particularly to condensers for condensing oil vapors distilled under vacuum.
The principal objects of the present invention are to provide a condenser associated with a vacuum distilling column and requiring a minimum of structural support, to provide a condenser opposing a minimum of resistance between the distilling column and the evacuating system, to provide for eifective separation and collection of entrainment in steam distillation, and also to provide means for simple and effective cleaning of the condenser tubes.
With these and other objects in view, as. will hereinafter appear, the present invention comprises the apparatus hereinafter described and particularly defined in the claims.
In the accompanying drawings, Fig. 1 is a sectional elevation of one form of the present invention; Fig. 2 is a sectional elevation on line 2-2 of Fig. 1; Fig. 2a'is a section on line 2a.2a of Fig. 2, showing the arrangement of the shell and partitions, the condenser section being removed; and Fig. 3 is a sectional elevation of a modified form of the invention.
The apparatus shown in Figs. 1 and 2 comprises ashell 6 having boiling cap decks of any suitable form. For fractionation of the vapors, reflux liquid is introduced on the top deck by a pipe 8. In the upper part of the column, the shell is provided with rectangular openings to receive the tubes of the condenser sections l0 and I2. The condenser sections are enclosed between vertical partitions l4 and Hi, a space l8 being provided between the sections for access to the tubes. The space I8 is enclosed by removable cover. plates 20. Angles 22 and 24 extending across the column serve as supports for the condenser sections during insertion or removal.
As shown in Fig. 1, the partition l6is formed at the bottom with a semi-circular collecting pan which is covered with any suitable insulating material 26.
The condenser tubes of the section H) are connected with headers 28 and 30, the former having connections 32 for circulating the cooling fluid.
The tubes of the section 2 are similarly connected into headers 34 and 36', of which the former has the cooling liquid connections 38.
Thepartition walls l4 and I6 together with parts of the shell 6 form bifurcated vapor conduits 39 around the condenser section so that vapors of steam and oil rising from above the boiling cap decks pass around the condenser section as indicated by the arrows in Figure '1.
and braced by an inclined strut 64.
Above the condenser section, the vapors then combine in the vapor collecting section Go from which the vapors pass downward through the opening into the condenser section across the tube bundles. The condensing action is particularly eificient because of the uniform cross-section presented to the vapor flow, whereby maximum contact of vapors with previously condensed liquid is effected. The condensate collects in the semi-circular. portion of the partition l6 and is withdrawn by a pipe 40. vapors comprising primarily steam with some oil pass under a semi-cylindrical baflie 42 which is supported by brackets 44 depending from the angles 24. The baffle 42 is formed along its sides with upwardly facing channels 46 serving to catch some of the entrained drops of oil which would otherwise pass under the baflle. Since the baflle is inclined, as shown in Fig. 2, the entrainment flows into the semi-circular pan.
The vapors continue, as indicated by the arrow in Fig. 2, into a cylindrical outlet 48 which is disposed within the baille 42. The outlet 48 is partially closed at the end by a baflle plate 50 and is provided with an opening part-way along the top, as indicated at 52. The tortuous course of the vapors in passing from the condenser tubes around the end and bottom of the bafiie 42 and over the bafiie plate 50 into the outlet pipe 48 serves to prevent passage of a considerable part of the entrainment with the steam.
Outside the column, the outlet pipe 48 leads into a final entrainment separator 54 consisting of a vertical cage with vertical baflie plates 56 of any suitable form. The baflle plates serve to separate any remnant of entrained oil, which is withdrawn from the bottom of the cage by a pipe 58. The outlet pipe then leads into the usual barometric condenser 60 and vacuum jet system 6| which are mounted on a bracket 62 extending from the shell The present invention contemplates a simple method of cleaning the condenser tubes. The
valves in the draw-off lines 40, 58, etc., are closed. and a cleaning solution is introduced around the tubes by means of a pipe 66. If hot cleaning solution is required, steam" is introduced in.-
ternally of the tubes by the steam lines 68. By
this means, the cleaning solution may be brought' to the boiling point. After "the cleaning operation, the solution may be removed from the system by opening the valve in the draw-01f line 40.
The apparatus shown in Fig. 3 is similar to that previously described; The condenser tube bundles I0 and I2 are supported in the shell. The
The uncondensed upper tube bundle I0 is enclosed between partitions H but the lower tube bundle is enclosed between a short partition 10 on one side and an angle partition I2 on the other side, the latter extending to a point considerably below the tube bundle and having a horizontal pan 14 extending into the shell.
denser bundles are covered with insulating material I6; 1
As in the prior construction the column 6 is similarly bifurcated with the vapor conduit passages 38 and 39a formed by the wall 12 and the shell on one side, and the partitions I4 and 10 and the shell on the other side. In this construction however, the vapors pass from the boiling cap section upwardly through the conduit 39 at the left of the condensers, into the vapor collecting chamber 6a, thence downwardly through the condensers, and upwardly through the other bifurcated vapor space 39a at the right of the condensers, and finally out through an outlet pipe 18. The condensate drops on the partition 14 which serves as a collecting pan and is withdrawn by a pipe 80.
In the vertical space leading to the outlet 18, entrainment catching ballles 82 are provided, these being formed with hooked edges to free the steam vapors of withdrawn oil. The bailles 82 are preferably inclined to direct the entrainment into the pan.
The outlet 18 leads into the barometric condenser 82 and vacuum jet equipment 84, as in the previously described construction. The external apparatus is mounted on a bracket 86 identical with that shown in Fig. 2.
Cleaning of the'tubes may be effected by introducing cleaning fluid through the pipe 66, as in the construction of Figs. 1 and 2.
The present invention provides a condensing and evacuating system, of which the major portion of the weight is supported centrally of the column itself. The rectangular cross-section of The invention having been thus described, wha
is claimed is:
1. The combination with a column having a distilling section, of a condenser having tubes in the upper part of-the column, a partition forming a vapor space leading from the distilling section to the top of the condenser, an outlet for uncondensed vapors, evacuating equipment con-' nected with said outlet, and means for supporting the evacuating equipment from the side of the column.
2. The combination with a column having a distilling section, of a condenser having tubes in the upper part of the column, a partition forming a vaporspace leading from the distilling section to the top of the condenser, a condensate pan below the condenser, an inlet for cleaning fluid above the condenser to permit filling of the space above the pan, and means for passing heating fluid through the tubes to heat the cleaning fluid.
The horizontal pan l4 and the vertical partitions at the left side of the con- 3. The combination with a column having a distilling section, of a condenser having tubes in the upper part ofthe column, a partition forming a. vapor. space leading from the distilling section to the top of the condenser, a condensate pan below the condenser, a bailie between the condenser and the pan, and an outlet ,below the baflie.
4. The combination with ,a column having a across-the upper part of the column to define a L rectangular condenser space between them and to provide vapor spaces between the partitions and the column wall, a condenser section having tubes in a bundle of rectangular,cross-section enclosed within the partitions, and a condensate pan extending from the bottom of one partition below the other partition to the column wall.
'6. The combination with a column having a distilling section, of a condenser comprising a bundle of horizontal tubes extending across the upper part of the column, fixed partitions extending completely across the column alongside the tube bundle and forming vapor spaces between the tube bundle and the column wall whereby vapors from the distilling section are directed to the top of the condenser, a condensate pan below the condenser and connected with at least one of the partitions, headers for the tube bundle, and means for removablysupporting the tube bundle and headers independently of the partitions and condensate pan.
'7. The combination with a column having a distilling section, of a condenser comprising a bundle of horizontal tubes of generally rectangular cross-section extending across the upper part of the column, fixed vertical partitions extending completely across the column alongside the tube bundle and forming vapor spaces between the tube bundle and the column wall whereby vapors from the distilling section are directed to the top of the condenser, a condensate pan below the condenser and connected with at least one -of the partitions, headers for the tube bundle,
and means for removably supporting the tube bundle arid headers independently of the partitions and condensate pan. u
8. A columnhaving. a distilling section, a bifurcated vapor section, and a vapor collecting section in communication with the distilling sec-' tion through a part of said bifurcated vapor section, means to close off another part of the bifurcated vapor section from direct communication with the distilling section, a condenser chamber between the walls of. the bifurcated vapor section with walls in common, said condenser chamber receiving vapors from said vapor collecting section, means to condense vapors in the condenser chamber and means to remove uncondensed vapors through another part of said bifurcated vapor section.
- FRANK J. MCGOVERN.
US39263A 1935-09-05 1935-09-05 Condenser Expired - Lifetime US2167028A (en)

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2584211A (en) * 1949-09-01 1952-02-05 Lummus Co Vacuum control system
US2662850A (en) * 1950-09-07 1953-12-15 Lummus Co Condensing system for distillation column
US2776938A (en) * 1951-12-29 1957-01-08 Foster Wheeler Corp Distilling apparatus
US3165455A (en) * 1959-05-21 1965-01-12 Gea Luftkuhler Ges M B H Distilling arrangement
US3175960A (en) * 1960-08-16 1965-03-30 Gea Luftkuehler Happel Gmbh Air cooled condenser for distilling apparatus
US3362891A (en) * 1965-05-12 1968-01-09 Combustion Eng Process and apparatus for separating acidic gas such as hydrogen sulfide and carbon dioxide from gaseous mixtures
US4134450A (en) * 1976-03-30 1979-01-16 Ecolaire Incorporated Surface condenser with vertically separated tube bundles
US4579629A (en) * 1983-02-23 1986-04-01 Shell Oil Company Apparatus for fractional distillation under vacuum
US4584061A (en) * 1985-01-02 1986-04-22 Shelton Robert E Vacuum desalinization device
US20100276122A1 (en) * 2009-04-30 2010-11-04 Daly Phillip F Re-direction of vapor flow across tubular condensers
CN102706185A (en) * 2012-01-12 2012-10-03 无锡湖光工业炉有限公司 Tubular intercooler
US20170307300A1 (en) * 2009-04-30 2017-10-26 Uop Llc Re-direction of vapor flow across tubular condensers
US10039998B2 (en) * 2010-10-14 2018-08-07 Nanjing University Anti-thermosensitization rectification tower and the rectification process thereof for separating thermosensitive natural substances

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2584211A (en) * 1949-09-01 1952-02-05 Lummus Co Vacuum control system
US2662850A (en) * 1950-09-07 1953-12-15 Lummus Co Condensing system for distillation column
US2776938A (en) * 1951-12-29 1957-01-08 Foster Wheeler Corp Distilling apparatus
US3165455A (en) * 1959-05-21 1965-01-12 Gea Luftkuhler Ges M B H Distilling arrangement
US3175960A (en) * 1960-08-16 1965-03-30 Gea Luftkuehler Happel Gmbh Air cooled condenser for distilling apparatus
US3362891A (en) * 1965-05-12 1968-01-09 Combustion Eng Process and apparatus for separating acidic gas such as hydrogen sulfide and carbon dioxide from gaseous mixtures
US4134450A (en) * 1976-03-30 1979-01-16 Ecolaire Incorporated Surface condenser with vertically separated tube bundles
US4579629A (en) * 1983-02-23 1986-04-01 Shell Oil Company Apparatus for fractional distillation under vacuum
US4584061A (en) * 1985-01-02 1986-04-22 Shelton Robert E Vacuum desalinization device
US20100276122A1 (en) * 2009-04-30 2010-11-04 Daly Phillip F Re-direction of vapor flow across tubular condensers
US8910702B2 (en) * 2009-04-30 2014-12-16 Uop Llc Re-direction of vapor flow across tubular condensers
US9671173B2 (en) 2009-04-30 2017-06-06 Uop Llc Re-direction of vapor flow across tubular condensers
US20170307300A1 (en) * 2009-04-30 2017-10-26 Uop Llc Re-direction of vapor flow across tubular condensers
US10039998B2 (en) * 2010-10-14 2018-08-07 Nanjing University Anti-thermosensitization rectification tower and the rectification process thereof for separating thermosensitive natural substances
CN102706185A (en) * 2012-01-12 2012-10-03 无锡湖光工业炉有限公司 Tubular intercooler

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