US2159899A - Utilization of the heat content of hot residual liquors - Google Patents
Utilization of the heat content of hot residual liquors Download PDFInfo
- Publication number
- US2159899A US2159899A US105093A US10509336A US2159899A US 2159899 A US2159899 A US 2159899A US 105093 A US105093 A US 105093A US 10509336 A US10509336 A US 10509336A US 2159899 A US2159899 A US 2159899A
- Authority
- US
- United States
- Prior art keywords
- utilization
- heat content
- heat
- pressure release
- hot residual
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/11—Batch distillation
Definitions
- This invention relates to the utilization of the heat content of residual liquors. It has already been proposed to utilize the residual liquor for preheating mash, for instance by passing it though a preheater, through the tube system of which the mash flows. The heat is thus used again indirectly.
- the sucked-off and compressed vapours resulting from the pressure release were then introduced separate from the live steam into the distillation vessel.
- This mode of operation is particularly simple 45 as regards the method and the apparatus employed. This ensures a completely satisfactory and reliable control and furthermore there isa more complete utilization of the heat content of the residual liquor, as, owing to the more simple 50 construction of the apparatus, heat losses connot 5'5 from the following.
- the saving in steam effected by the mode of operation according to the invention is considerable in certain circumstances. It is greater, the higher the pressure of the live steam employed. Whilst, for instance, with a live steam pressure of 2 atmospheres the saving in steain amounts as a rule to lessthan 10%, with a pressure of 6 atmospheres the saving in steam will be about
- the accompanying drawing illustrates one constructional example of the invention.
- heating stea is fed through: the pipes I andZ.
- an injector B the suction branch of which is in communication through the -pipe.3 with the pressure release vessel C, preferably with the upper part thereof, whereby a partial vacuum is produced in C.
- the vapour resulting from the pressure release develops in the vessel C in accordance with the reduction in temperature accompanying this partial vac-- uum and the consequent giving ofl of heat by the residual liquor which flows through the pipe 4 out of the distillation apparatus A to the pressure release vessel C.
- the residual liquor relieved of pressure is then conveyed into the open.
- vapour resulting from from the fractionator removing a bottom stream consisting practically exclusively of heavy material for the fractinnatnr intrnducinl the bottom ing efiected by live steam but without any supply of additional heat to the bottom stream in the pressure release zone, and using the live steam I together with the evacuated vapours for heating the material to be distilled.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Description
May 23, 1939. R Z 2,159,899
UTILIZATION OF THE HEAT CONTENT OF HOT RESIDUAL LIQUORS Filed Oct. 10, 1936 lm/en for UNITED STATES PATENT OFFICE UTILIZATION OF THE HEAT CONTENT OF HOT RESIDUAL LIQUOR-S Bertold Mannheim-Waldhof, Germany,
assignor of one-half to Zellstofliabrik Waldhof, Mannheim-Waldhof, Germany Application October 10, 1936, Serial No. 105,093 a In Germany November 28, 1935 1 Claim. (01. 202-49) This invention relates to the utilization of the heat content of residual liquors. It has already been proposed to utilize the residual liquor for preheating mash, for instance by passing it though a preheater, through the tube system of which the mash flows. The heat is thus used again indirectly.
It has also already been proposed to utilize the heat content of the residual liquor directly in the distillation apparatus, by withdrawing by suction the vapours which develop from the residue, when expanding in a separate pressure release vessel by means of a separate suction device, for instance by means of a compressor, out ofthe I pressure release vessel 'and, after compression,
conveying them to the distillation apparatus.
has also been proposed to arrange a plurality of such pressure release vessels in series and to provide a corresponding .number of compressors.
The sucked-off and compressed vapours resulting from the pressure release were then introduced separate from the live steam into the distillation vessel.
It has been found, however, that in this way it is not possible to recover the waste heat of the liquor in a manner which satisfies both economical and technical requirements. Owing to the complicated constructionof the apparatus there is the possibility of the occurrence of heat losses, which may in certain circumstances be considerable, and of disturbances in the operation of the apparatus.
These disadvantages may be avoided and a completely satisfactory utilization of the heat content of the residual liquorobtained, by driving the heat pump, by means of which the vapour, formed in the pressure release vessel are withdrawn,-with the live steam for heating the distillation apparatus and by conveying the said live steam to the distillation apparatus together with the withdrawn vapours. As the heat pump, an injector, a compressor of a known type or the like may be used.
This mode of operation is particularly simple 45 as regards the method and the apparatus employed. This ensures a completely satisfactory and reliable control and furthermore there isa more complete utilization of the heat content of the residual liquor, as, owing to the more simple 50 construction of the apparatus, heat losses connot 5'5 from the following. Whereas in the hitherto The considerable simknown methods of conveying the vapours withdrawn by suction from the pressure release vessel into the distillation apparatus in addition to the supply of live steam a separate source of power is required, in the new method the increased consumption of energy for the double supply and also the cause of many sources of trouble are removed by only a single source of power being used, since both the supplying of the live steam and the withdrawal by suction of the vapours resulting from the pressure release and their conveyance to the distillation vessel are efiected by the heat pump.
The saving in steam effected by the mode of operation according to the invention is considerable in certain circumstances. It is greater, the higher the pressure of the live steam employed. Whilst, for instance, with a live steam pressure of 2 atmospheres the saving in steain amounts as a rule to lessthan 10%, with a pressure of 6 atmospheres the saving in steam will be about The accompanying drawing illustrates one constructional example of the invention.
' To the distillation apparatus A heating stea is fed through: the pipes I andZ. In these supply pipes is interposed an injector B, the suction branch of which is in communication through the -pipe.3 with the pressure release vessel C, preferably with the upper part thereof, whereby a partial vacuum is produced in C. The vapour resulting from the pressure release develops in the vessel C in accordance with the reduction in temperature accompanying this partial vac-- uum and the consequent giving ofl of heat by the residual liquor which flows through the pipe 4 out of the distillation apparatus A to the pressure release vessel C. Through the pipe 5 the residual liquor relieved of pressure is then conveyed into the open. The vapour resulting from from the fractionator, removing a bottom stream consisting practically exclusively of heavy material for the fractinnatnr intrnducinl the bottom ing efiected by live steam but without any supply of additional heat to the bottom stream in the pressure release zone, and using the live steam I together with the evacuated vapours for heating the material to be distilled.
IBERTOLD KRANZ.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2159899X | 1935-11-28 |
Publications (1)
Publication Number | Publication Date |
---|---|
US2159899A true US2159899A (en) | 1939-05-23 |
Family
ID=7987867
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US105093A Expired - Lifetime US2159899A (en) | 1935-11-28 | 1936-10-10 | Utilization of the heat content of hot residual liquors |
Country Status (1)
Country | Link |
---|---|
US (1) | US2159899A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2943026A (en) * | 1953-12-14 | 1960-06-28 | Phillips Petroleum Co | Removal of salt from solutions |
US3476823A (en) * | 1966-02-03 | 1969-11-04 | Phillips Petroleum Co | Separation of products of ethylene polymerization |
DE2507209A1 (en) * | 1974-02-22 | 1975-08-28 | Sasakura Eng Co Ltd | CONTINUOUS PROCESS OF EVAPORATION AND MULTI-STAGE EVAPORATOR FOR THIS |
-
1936
- 1936-10-10 US US105093A patent/US2159899A/en not_active Expired - Lifetime
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2943026A (en) * | 1953-12-14 | 1960-06-28 | Phillips Petroleum Co | Removal of salt from solutions |
US3476823A (en) * | 1966-02-03 | 1969-11-04 | Phillips Petroleum Co | Separation of products of ethylene polymerization |
DE2507209A1 (en) * | 1974-02-22 | 1975-08-28 | Sasakura Eng Co Ltd | CONTINUOUS PROCESS OF EVAPORATION AND MULTI-STAGE EVAPORATOR FOR THIS |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US3585104A (en) | Organosolv pulping and recovery process | |
US2159899A (en) | Utilization of the heat content of hot residual liquors | |
CN109355083A (en) | The technique and system of tri-mixed fractions are adopted in a kind of tar vacuum distillation | |
CA1135100A (en) | Method of cooking cellulose material | |
US2979443A (en) | Multi-stage flash evaporator | |
GB1443554A (en) | Apparatus for distilling natural water | |
GB1043460A (en) | Improvements in continuous aqueous prehydrolysis of wood chips | |
US2675311A (en) | Paper pulp process and apparatus | |
US3745063A (en) | Process for simultaneous turpentine recovery and odor control | |
US2320294A (en) | Sulphite process | |
US3428107A (en) | Method in evaporation of waste liquor discharged from continuously operating cellulose digester or boiler | |
US5382321A (en) | Process for the concentration of spent liquors | |
US2282982A (en) | Process of steam fractionation | |
US3816239A (en) | Recovery of terpenes | |
US2025891A (en) | Reclaiming by-products | |
US1972157A (en) | Vacuum distillation | |
JPS6021994A (en) | Pretreatment method and apparatus of lignocellulose materialin continuous digestion thereof to cellulose pulp | |
US3764482A (en) | Method for recovering gas generated in a coke oven when charging coal | |
US2008635A (en) | Process of and apparatus for producing pulp | |
US2824800A (en) | Method of cooking sulphite pulp | |
US3783095A (en) | Process for recovering turpentine and heat in connection with the evaporation of black lye | |
US2038780A (en) | Method of and apparatus for cooking pulp | |
US2074689A (en) | Combined inert gas recirculation and tar heater operation | |
GB1300472A (en) | Improvements in or relating to evaporation plant | |
US1597718A (en) | Apparatus for recovering heat from coke, slags, ashes, and other solid substances |